Abstract: A method of manufacturing corrosion resistant tubing from seam welded stock of a titanium or titanium alloy metallic material having a hexagonal close-packed crystal structure. The method includes cold pilgering a seam welded tube hollow having a weld area along the seam in a single pass to a final sized tube. The cold pilgering effects a reduction in cross sectional area of the tube hollow of at least 50% and a reduction of wall thickness of at least 50% thereby orienting the crystals in a radial direction. The method also includes annealing the final sized tubing at a temperature and for a time sufficient to effect complete recrystallization and reform grains in the weld area into smaller, homogeneous radially oriented grains. After the recrystallization annealing step, the tubing exhibits enhanced corrosion resistance which is similar to seamless tubing.

Abstract: The present invention relates to a low cost process for providing equivalent or superior ballistic resistance performance compared to standard Ti-6Al-4V alloys. The present inventions process involves increasing the oxygen content of Ti-6Al-4V beyond the conventional limit of 0.20% maximum reported for prior art compounds and subsequently thereafter heating the oxygen rich titanium alloy at temperatures within the beta phase field for further processing.Additionally, the present invention provides a novel Ti-6Al-4V alloy composition which exhibits improved tensile and yield strength properties. Titanium compositions of the present invention exhibit improved ballistic properties compared to titanium compositions previously disclosed in the art. The novel Ti-6Al-4V composition of the present invention is obtained by modifying the alloy composition limits to 5.5 to 6.75% Al, 3.5 to 4.5% V, 0.20 to 0.30% O.sub.2, <0.50% Fe and 0.

Abstract: The specification describes novel zirconium-based hydrogen storage materials useful as negative electrodes for rechargeable batteries. The materials according to the present invention are represented by the following empirical formula:Zr-based metal hydrides+Mx (I)wherein M is a light rare earth metal selected from the group consisting of La, Nd, and Mm; 0<x<0.1; and the Zr-base metal hydrides means mainly that the metal hydrides are mainly in Zr-based Laves phase such as ZrCrNi, Zr (V.sub.0.33 Ni.sub.0.67).sub.2.4. Another group of the materials is represented by the following formula:ZrCr.sub.1+y Ni.sub.1+z (II)wherein, 0.ltoreq.y.ltoreq.0.2, and 0.ltoreq.z.ltoreq.0.2, provided that y and z cannot denote 0 concurrently. The negative electrodes made of these alloys need only a small number of activation cycles and thus, exhibit an improved activation behavior without any pretreatments for the activation.

Abstract: A new ternary sulfide alloy exhibits a metal-semiconductor phase transition with hysteresis as a function of temperature. One embodiment of the bistable material includes barium, cobalt, nickel and sulfur in amounts in accordance with the formula Ba(Co.sub.1-x Ni.sub.x)S.sub.2-y, and x is between 0 and 1 and y varies from 0 to 2.

Abstract: A process for producing a crack-free, laser nitride-hardened layer on a titanium substrate, the process including preheating the substrate, melting a small area of substrate with a laser, and shrouding the melted area with a gas mixture having a maximum critical amount of nitrogen not greater than 85%. A crack-free pump shaft so hardened to Rockwell 52 C is produced.

Abstract: The present invention relates to novel compounds that exhibit unusually low electrical resistivity at room temperature. More specifically, it has been discovered that the incorporation of at least 1 to 15 atomic percent of gallium and/or at least 1 to 15 atomic percent gold into stoichiometric copper germanide (Cu.sub.3 Ge) compound results in a room temperature resistivity comparable to elemental copper, but with superior chemical and electronic stability upon exposure to air or oxygen at high temperatures. Furthermore, the compounds of the present invention have none of the problems associated with the diffusion of copper into elemental and compound semiconductors which oftentimes lead to the degradation of the semiconductor device characteristics. Additionally, the present invention relates to a method of preparing the novel compounds mentioned previously hereinabove.

Abstract: A method for hot forging coarse grain materials to enhance hot workability and to refine microstructure is described which comprises the steps of imposing minimum initial deformation at low strain rate to effect initial dynamic recrystallization and grain refinement without fracture, and thereafter increasing the deformation rate to recrystallize the material and further refine grain structure. Depending on the deformation required to achieve full recrystallization at a given rate, deformation rate can be increased a number of times to further refine grain structure.

Abstract: Process for the manufacture of components from untreated steel, comprising a series of heat treatment and forming operations, characterised by heating the steel to a temperature above the transition point (austenizing), isothermal quenching in a fluidized bed bath immediately after the austenizing heating giving the steel a bainitic structure and then forming the components under mild conditions.

Abstract: A TiAl composition is prepared to have high strength, high oxidation resistance and to have acceptable ductility by altering the atomic ratio of the titanium and aluminum to have what has been found to be a highly desirable effective aluminum concentration and by addition of chromium and tantalum and boron ingredients according to the approximate formula Ti-Al.sub.46-50 Cr.sub.2 Ta.sub.2-4 B.sub.0.05-0.2. Homogenization of the composition above the alpha transus temperature is used in combination with the boron doping to achieve higher ductility without sacrifice of strength.

Abstract: An autogenous superconducting joint metallurgically bonding a pair of shaped superconducting pieces. Each of the pieces is formed by combining the metallic elements of a superconducting oxide in substantially the stoichiometric proportions needed to form the superconducting oxide, and then forming the combined metallic elements into a shaped piece. The microstructure of the joint is substantially the same as that of the portions of the pieces adjacent the joint.

Abstract: Objects of titanium or titanium alloys having the surface converted to a hard and wear-resistant nitride layer with good adhesion, which is distributed uniformly and also provides internal capillaries. The objects are produced by being treated in a vacuum furnace with an atmosphere of pure nitrogen gas at a temperature of 650.degree.-1000.degree. C. and at a pressure below atmospheric pressure. The thickness of the nitride layer can be controlled by controlling the treatment time and temperature.

Abstract: There is provided a composite copper alloy having a copper alloy core and a modified surface layer containing a nitride or carbide film. Alternatively, the modified surface layer may contain a carbo-nitride film. The alloy is formed by reacting a copper alloy with nitrogen, carbon or a nitrogen/carbon mixture at elevated temperatures. The resultant surface layer improves the tribological and mechanical properties of the alloy while maintaining useful electrical conductivity.

Abstract: Magnesium base metal alloy sheet is produced by rolling the rolling stock extruded or forged from a billet at a temperature ranging from 200.degree. C. to 300.degree. C. The billet is consolidated from rapidly solidified magnesium based alloy powder that consists essentially of the formula Mg.sub.bal Al.sub.a Zn.sub.b X.sub.c, wherein X is at least one element selected from the group consisting of manganese, cerium, neodymium, praseodymium, and yttrium, "a" ranges from about 0 to 15 atom percent, "b" ranges from about 0 to 4 atom percent, "c" ranges from about 0.2 to 3 atom percent, the balance being magnesium and incidental impurities, with the proviso that the sum of aluminum and zinc present ranges from about 2 to 15 atom percent. The alloy has a uniform microstructure comprised of fine grain size ranging from 0.2-1.0 .mu.m together with precipitates of magnesium and aluminum containing intermetallic phases of a size less than 0.1 .mu.m.

Abstract: A corrosion resistant Ti based alloy comprising:Cr: 0.005-2.0 wt %, and furthercomprising one or more of elements selected from:______________________________________ Ni: 0.005-2.0 wt %, Pd: 0.005-2.0 wt %, Ru: 0.005-2.0 wt %, Pt: 0.005-2.0 wt %, Os: 0.005-2.0 wt %, Ir: 0.005-2.0 wt %, Rh: 0.005-2.0 wt %, and ______________________________________the balance of Ti and inevitable impurities.Cr may be replaced with one or more of 0.005-1.5 wt % of Cu and 0.005-1.5 wt % of Si, or 0.005-2.0 wt % of Al. The corrosion resistant Ti based alloy has excellent corrosion resistance also in a non-oxidative atmosphere and also has an excellent crevice corrosion resistance.

Abstract: A method and apparatus for heat-treating nickel base superalloy articles to provide different properties in different regions of the article. An initially fine grain microstructure is heated such that a portion of the article is held above the .gamma.' solvus temperature long enough to provide a coarse grain microstructure while the remainder of the article remains below the .gamma.' solvus temperature and retains the fine grain microstructure. The coarse grain microstructure provides a reduced rate of fatigue crack growth rate while the fine grain microstructure retains good tensile properties. The invention is particularly applicable to the fabrication of turbine disks for gas turbine engines.

Abstract: The invention relates to a process for the preparation of finely divided microcrystalline-to-amorphous metal and/or alloy powders and of metals and/or alloys in the form of colloidal solutions in organic solvents, which is process is characterized in that in inert organic solvents metal salts individually or in admixture are reacted with alkaline metal or alkaline earth metal hydrides which are maintained in solution by means of organoboron or organogallium complexing agents, or with tetraalkylammonium triorgano-borohydrate, respectively.

Abstract: A method of surface hardening cobalt-chromium based orthopedic implant devices, and a cobalt-chromium orthopedic implant device prepared by the disclosed method. An orthopedic implant device made of a cobalt-chromium or cobalt-chromium-molybdenum alloy, such as ASTM F-75 or ASTM F-799 is exposed to molecular nitrogen gas or ionized nitrogen at a process temperature and for a process time duration sufficient to enhance surface hardness and wear resistance properties, without the formation of a measurable nitrogen layer that tends to increase surface roughness and brittleness and diminish wear resistance properties. The process temperature is in the range of 500.degree. F. to 2400.degree. F., preferably about 1400.degree. F., and the process time duration at the preferred process temperature is approximately 48 hours.

Abstract: A tungsten based heavy alloy having a W--Ni--Fe based composition containing traces of lanthanum or calcium, thereby capable of exhibiting high toughness, irrespective of the content of impurities such as phosphorous and sulfur contained therein, the cooling rate after the sintering treatment and the re-heating treatment. The present invention provides a method for making the high toughness tungsten based heavy alloy. The tungsten based heavy alloy of the present invention is useful to manufacture warheads for breaking armor plates, which require high toughness.

Abstract: The present invention relates to a process for improving the fatigue crack growth resistance of .alpha.-.beta. titanium alloys and the like alloys/metals which comprises in making a single laser trail on the sheet or component of alloy/metal with the a selected power and scan speed and with the focal spot being upto 200 .mu.m above or below the treating surface. The width of the trail is measured so as to adjust a job manupulator to cause successive scans with an overlap of 5 to 50%. The component is covered by successive scanning under an inert gas at a pressure of 20-48 PSI.

Abstract: A titanium alloy part having a structure comprising ex-beta acicular grains and with equi-axial alpha phases gathered in a plurality of rows at boundaries of the grains. The alloy comprises, by weight, 2 to 5% Mo, 3.5 to 6.5% Al, 1.5 to 2.5% Sn, 1.5 to 4.8% Zr, Fe.ltoreq.1.5%, 4 to 12% Mo+V+Cr, and the balance, titanium and impurities.