Using An Energy Beam Or Field, A Particle Beam Or Field, Or A Plasma (e.g., Ionization, Pecvd, Cbe, Mombe, Rf Induction, Laser) Patents (Class 117/92)
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Patent number: 7399357Abstract: A method for the controlled growth of thin films by atomic layer deposition by making use of multilayers and using energetic radicals to facilitate the process is described in this invention. In this method, a first reactant is admitted into the reaction chamber volume, where there is a substrate to be coated. This first reactant then adsorbs, in a self-limiting process, onto the substrate to be coated. After removing this first reactant from the reaction chamber volume, leaving a layer coating the substrate, a second reactant is then admitted into the reaction chamber volume, which adsorbs onto this initial layer in a self-limiting process. The second reactant is then also removed from the reaction chamber volume. Following this procedure a self-limited multilayer of unreacted species remains adsorbed on the substrate to be coated. If additional chemical species are desirable, these exposures and removals could be continued. Next this multilayer is exposed to a flux of radicals.Type: GrantFiled: May 8, 2003Date of Patent: July 15, 2008Inventor: Arthur Sherman
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Patent number: 7396409Abstract: By uniformly forming an indefinite number of microscopic acicular crystals on a surface of a silicon substrate so as to be perpendicular to the surface of the substrate by plasma CVD method using a catalyst, it is possible to reliably, homogeneously and massively form an ultramicroscopic acicular silicon crystal having a substantial cone shape tapered so as to have a radius of curvature of not less than 1 nm to no more than 20 nm at its tip end and having a diameter of bottom surface of not less than 10 nm, and a height equivalent to or more than the diameter of bottom surface, at a desired location.Type: GrantFiled: September 4, 2003Date of Patent: July 8, 2008Assignees: Covalent Materials Corporation, Techno Network Shikoku Co., Ltd.Inventors: Akitmitsu Hatta, Hiroaki Yoshimura, Keiichi Ishimoto, Hiroaki Kanakusa, Shinichi Kawagoe
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Patent number: 7387678Abstract: A GaN substrate comprises a GaN single crystal substrate, an AlxGa1-xN intermediate layer (0<x?1) epitaxially grown on the substrate, and an GaN epitaxial layer grown on the intermediate layer. The intermediate layer is made of AlGaN and this AlGaN grows over the entire surface of the substrate with contaminants thereon and high dislocation regions therein. Thus, the intermediate layer is normally grown on the substrate, and a growth surface of the intermediate layer can be made flat. Since the growth surface is flat, a growth surface of the GaN epitaxial layer epitaxially grown on the intermediate layer is also flat.Type: GrantFiled: June 25, 2004Date of Patent: June 17, 2008Assignee: Sumitomo Electric Industries, Ltd.Inventors: Katsushi Akita, Eiryo Takasuka, Masahiro Nakayama, Masaki Ueno, Kouhei Miura, Takashi Kyono
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Patent number: 7374617Abstract: The invention includes atomic layer deposition methods and chemical vapor deposition methods. In a particular aspect of the invention, a source of microwave radiation is provided proximate a reaction chamber. At least a fragment of a precursor material is chemisorbed on a substrate within the reaction chamber while not exposing the precursor material to microwave radiation from the source. Excess precursor material is removed from the chamber, and the chemisorbed material is subsequently exposed to microwave radiation from the source within the reaction chamber.Type: GrantFiled: April 25, 2002Date of Patent: May 20, 2008Assignee: Micron Technology, Inc.Inventor: Brian A. Vaartstra
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Patent number: 7361221Abstract: A light irradiation apparatus includes a light modulation element which has a phase modulation area having at least one basic pattern for modulating a light beam, an illumination system which illuminates the phase modulation area of the light modulation element with a light beam, and an image formation optical system which causes a light beam on an irradiation target surface a light intensity distribution having an inverse-peak-shaped pattern formed based on the light beam phase-modulated by the phase modulation element to fall on an irradiation target object. Dimensions of the basic pattern are not greater than a point spread function range of the image formation optical system converted in terms of the light modulation element. The phase modulation area is configured in such a manner that a phase distribution in a light complex amplitude distribution on the irradiation target surface becomes a saw-tooth-like distribution along a line segment in a lateral direction.Type: GrantFiled: August 25, 2005Date of Patent: April 22, 2008Assignee: Advanced LCD Technologies Development Center Co., Ltd.Inventors: Masakiyo Matsumura, Yukio Taniguchi
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Patent number: 7341628Abstract: Gallium Nitride layers grown as single crystals by epitaxy such as Hydride Vapor Phase Epitaxy (HVPE) contain large numbers of crystal defects such as hexagonal pits, which limit the yield and performance of opto- and electronic devices. In this method, the Gallium Nitride layer is first coated with an Aluminum layer of approximate thickness of 0.1 microns. Next, Nitrogen is ion implanted through the Aluminum layer so as to occupy mostly the top 0.1 to 0.5 microns of the Gallium Nitride layer. Finally, through a pulsed directed energy beam such as electron or photons, with a fluence of approximately 1 Joule/cm2 the top approximately 0.5 microns are converted to a single crystal with reduced defect density.Type: GrantFiled: December 16, 2004Date of Patent: March 11, 2008Inventor: Andreas A. Melas
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Patent number: 7338582Abstract: It is an object of the present invention to provide an oxygen reduction electrode having excellent oxygen reduction catalysis ability. In a method of manufacturing a manganese oxide nanostructure having excellent oxygen reduction catalysis ability and composed of secondary particles which are aggregations of primary particles of manganese oxide, a target plate made of manganese oxide is irradiated with laser light to desorb the component substance of the target plate, and the desorbed substance is deposited on a substrate facing substantially parallel to the aforementioned target plate.Type: GrantFiled: August 16, 2005Date of Patent: March 4, 2008Assignee: Matsushita Electric Industrial Co., Ltd.Inventors: Nobuyasu Suzuki, Yasunori Morinaga, Hidehiro Sasaki, Yuka Yamada
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Patent number: 7332030Abstract: Process for the treatment of a component, at least one zone to be treated of which located in the depth of this component at a certain distance from the surface thereof, has at least one property that can be modified when this zone is subjected to a thermal energy density above a specified treatment level, comprises: placing the component to be treated at a thermal energy level below the specified level; and subjecting, through its aforementioned surface, for a specified time and in the form of at least one pulse, the component to a power flux generated by a particle emission unit, this emission unit being regulated so as to produce a thermal energy density that is concentrated on or has a localized maximum in the zone to be treated and reaching, in at least part of this zone, a level above the specified treatment level.Type: GrantFiled: January 15, 2003Date of Patent: February 19, 2008Inventor: Michel Bruel
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Publication number: 20080029021Abstract: A method for forming a silicon nitride film in a PECVD batch type chamber is provided. In the PECVD silicon nitride film deposition method, as the number of batches of processed wafers increases, a silicon nitride deposition time is gradually adjusted to be longer as each batch of wafers is processed. Therefore a uniform thickness of the silicon nitride film is maintained despite variations in deposition rates resulting from an RF plasma cleaning process.Type: ApplicationFiled: July 31, 2007Publication date: February 7, 2008Applicant: DONGBU HITEK CO., LTD.Inventor: Gwang Su KIM
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Publication number: 20070289526Abstract: A unibody, multi-piece crucible for use in for use in elemental purification, compounding, and growth of semi-conductor crystals, e.g., in the process of molecular beam epitaxy (MBE) for melting silicon and the like at high temperature. The crucible has an outer coating layer that fixedly joins the multi pieces making up the crucible. The invention also provides a method for making a unibody containing structure comprising pyrolytic boron nitride having a negative draft, which method obviates the need of complicated overhang structure of graphite mandrels or the removal of the graphite mandrels by burning at high temperatures.Type: ApplicationFiled: October 30, 2006Publication date: December 20, 2007Applicant: General Electric CompanyInventors: Yuji Morikawa, Kazuo Kawasaki, Sun-joong Hwang, Marc Schaepkens
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Publication number: 20070266932Abstract: In an aspect of the present invention, a vapor phase growth apparatus may include a chamber, a gas supply provided in the chamber, configured to supply a raw material gas from a central region outwardly, a susceptor provided above the gas supply in the chamber, being capable of revolve around the axis, and configured to mount a substrate facing downward, the substrate being inclined toward the axis, and a heater provided above the holder in the chamber.Type: ApplicationFiled: May 18, 2007Publication date: November 22, 2007Applicant: KABUSHIKI KAISHA TOSHIBAInventor: Shoji Hiramatsu
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Patent number: 7291218Abstract: A method of fabricating an orientation film for a liquid crystal display device is provided. An orientation film is formed on a substrate. An ion-beam irradiation apparatus having an ion generation element is provided. The substrate is placed on a stage in a vacuum chamber. The angle of the substrate is controlled such that the orientation film has a predetermined angle with respect to an ion beam of the ion-beam irradiation apparatus. An ion beam from the ion-beam irradiation apparatus irradiates a surface of the orientation film. The ion beam has an energy intensity of about 300 eV to about 800 eV and a predetermined dose.Type: GrantFiled: April 25, 2005Date of Patent: November 6, 2007Assignee: LG. Philips LCD Co., Ltd.Inventor: Yong-Sung Ham
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Publication number: 20070251445Abstract: Embodiments of an apparatus and methods for forming a tantalum containing film using plasma enhanced atomic layer deposition are generally described herein. Other embodiments may be described and claimed.Type: ApplicationFiled: May 7, 2007Publication date: November 1, 2007Applicant: Tokyo Electron LimitedInventor: Tadahiro Ishizaka
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Patent number: 7288153Abstract: A method of fabricating an orientation film for a liquid crystal display device is provided. The orientation film is formed on a substrate. An ion-beam irradiation apparatus having an ion generator and a vacuum chamber having a stage on which the substrate is disposed are provided. The chamber is evacuated and an angle of the substrate having the orientation film is controlled such that the orientation film has a predetermined angle with respect to an ion beam of the ion-beam irradiation apparatus using the ion generator or the stage. The surface of the orientation film is irradiated by the ion beam. The ion beam has a predetermined intensity and dose. The substrate is subsequently heated at a predetermined temperature and time sufficient to harden a thermal polymerization functional group of the orientation layer.Type: GrantFiled: April 25, 2005Date of Patent: October 30, 2007Assignee: LG. Philips LCD Co., Ltd.Inventor: Yong-Sung Ham
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Publication number: 20070215037Abstract: A light irradiation apparatus irradiates a target plane with light having a predetermined light intensity distribution. The apparatus includes a light modulation element having a light modulation pattern of a periodic structure represented by a primitive translation vector (a1, a2), an illumination system for illuminating the modulation element with the light, and an image forming optical system for forming the predetermined light intensity distribution obtained by the modulation pattern on the target plane. A shape of an exit pupil of the illumination system is similar to the Wigner-Seitz cell of a primitive reciprocal lattice vector (b1, b2) obtained from the primitive translation vector (a1, a2) by the following equations: b1=2?(a2×a3)/(a1·(a2×a3)) and b2=2?(a3×a1)/(a1·(a2×a3)) in which a3 is a vector having an arbitrary size in a normal direction of a flat surface of the modulation pattern of the modulation element, “·” is an inner product of the vector, and “×” is an outer product of the vector.Type: ApplicationFiled: March 16, 2007Publication date: September 20, 2007Inventor: Yukio TANIGUCHI
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Patent number: 7255746Abstract: MBE nitrogen sources of dimethylhydrazine, tertiarybutlyhydrazine, nitrogentrifloride, and NHx radicals. Those nitrogen sources are beneficial in forming nitrogen-containing materials on crystalline subtrates using MBE. Semiconductor lasers in general, and VCSEL in particular, that have nitrogen-containing layers can be formed using such nitrogen sources.Type: GrantFiled: September 4, 2002Date of Patent: August 14, 2007Assignee: Finisar CorporationInventors: Ralph H. Johnson, Jin K. Kim, James K. Guenter
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Publication number: 20070163489Abstract: A method of forming a layer, including forming an insulation layer having an opening on a single crystalline substrate, the opening partially exposing an upper face of the substrate, forming a first seed layer in the opening, converting an upper portion of the first seed layer to a first amorphous layer, converting the first amorphous layer to a second seed layer, forming a second amorphous layer on the second seed layer, and converting the second amorphous layer to a single crystalline layer.Type: ApplicationFiled: January 12, 2007Publication date: July 19, 2007Inventors: Yong-Hoon Son, Jong-Wook Lee
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Patent number: 7238232Abstract: A synthesis route to grow textured thin film of gallium nitride on amorphous quartz substrates and on single crystalline substrates such as c-sapphire and polycrystalline substrates such as pyrolytic boron nitride (PBN), alumina and quartz using the dissolution of atomic nitrogen rather than molecular nitrogen to allow for growth at subatmospheric pressure.Type: GrantFiled: April 30, 2003Date of Patent: July 3, 2007Assignee: University of LouisvilleInventors: Mahendra Kumar Sunkara, Hari Chandrasekaran, Hongwei Li
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Patent number: 7235130Abstract: An apparatus for producing diamond in a deposition chamber including a heat-sinking holder for holding a diamond and for making thermal contact with a side surface of the diamond adjacent to an edge of a growth surface of the diamond, a noncontact temperature measurement device positioned to measure temperature of the diamond across the growth surface of the diamond and a main process controller for receiving a temperature measurement from the noncontact temperature measurement device and controlling temperature of the growth surface such that all temperature gradients across the growth surface are less than 20° C.Type: GrantFiled: January 27, 2005Date of Patent: June 26, 2007Assignees: Carnegie Institution of Washington, The UAB Research FoundationInventors: Russell J. Hemley, Ho-kwang Mao, Chih-shiue Yan, Yogesh K. Vohra
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Patent number: 7235131Abstract: A method for forming a single crystalline film including the steps of forming an amorphous film on a single crystalline substrate, forming an opening in the amorphous film and thereby exposing a part of a surface of the substrate, and introducing atomic beams, molecular beams or chemical beams onto the surface of the substrate at their incident angle of not more than 40 degrees with respect to the substrate surface under a reduced atmosphere and thereby selectively and epitaxially growing a single crystalline film on the exposed surface of the substrate and then in a lateral direction parallel to the surface of the substrate on the amorphous film.Type: GrantFiled: February 23, 2000Date of Patent: June 26, 2007Assignee: The University of TokyoInventor: Tatau Nishinaga
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Patent number: 7229501Abstract: The present invention provides a silicon epitaxial wafer having an excellent IG capability all over the radial direction thereof and a process for manufacturing the same. The present invention is directed to a silicon epitaxial wafer having an excellent gettering capability all over the radial direction thereof, wherein density of oxide precipitates detectable in the interior of a silicon single crystal substrate after epitaxial growth is 1×109/cm3 or higher at any position in the radial direction.Type: GrantFiled: January 17, 2003Date of Patent: June 12, 2007Assignee: Shin-Etsu Handotai Co., Ltd.Inventor: Hiroshi Takeno
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Patent number: 7229500Abstract: Crystallization Photoresist (PR) apparatus and methods which allow for fast screening and determination of protein crystallization conditions with small protein quantities and rapid crystallization. The apparatus comprise a first region comprising a first nucleation catalyst material and a second region comprising a second nucleation catalyst material, with the first and second regions positioned adjacent to each other and configured to support at least one crystal, and with the first region having a variation in a nucleation property of the first nucleation catalyst material in the first region. The crystal may be supported at an interface of the adjacent regions.Type: GrantFiled: November 20, 2001Date of Patent: June 12, 2007Assignee: Parallel Synthesis Technologies, Inc.Inventors: Robert C. Haushalter, Xiao-Dong Sun
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Patent number: 7223306Abstract: It is an object to provide a laser apparatus, a laser irradiating method and a manufacturing method of a semiconductor device that can perform uniform a process with a laser beam to an object uniformly. The present invention provides a laser apparatus comprising an optical system for sampling a part of a laser beam emitted from an oscillator, a sensor for generating an electric signal including fluctuation in energy of the laser beam as a data from the part of the laser beam, a means for performing signal processing to the electrical signal to grasp a state of the fluctuation in energy of the laser beam, and controlling a relative speed of an beam spot of the laser beam to an object in order to change in phase with the fluctuation in energy of the laser beam.Type: GrantFiled: September 17, 2003Date of Patent: May 29, 2007Assignee: Semiconductor Energy Laboratory Co., Ltd.Inventors: Hidekazu Miyairi, Akihisa Shimomura, Tamae Takano, Masaki Koyama
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Patent number: 7217324Abstract: The invention relates to a method for producing an X-ray detector for imaging. By increasing the epitaxial layers, a GaAs material (1) is placed on a substrate n<+> (or p<+>) (2). p<+> (or n<+>)< >ions are then implanted on the external face (11) of the material (1) in order to form a p<+>/i/n<+> structure after annealing. Ohmic contacts (12) are subsequently disposed on the two faces and individual detectors (pixels) (13) are produced over the entire surface using means of dry or chemical masking and pickling. The epitaxial material (1) has a thickness d? that is sufficient to absorb effectively the X photons and means can be used to reduce the residual doping of said material (1). The material obtained in this way is suitable for medical (mammography, dental, etc.) and industrial imaging.Type: GrantFiled: January 30, 2002Date of Patent: May 15, 2007Assignee: Universite Pierre et Marie CurieInventor: Jacques Bourgoin
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Patent number: 7215456Abstract: A method for patterning self-assembled colloidal photonic crystals and a method for fabricating three-dimensional photonic crystal waveguides having an inverted-opal structure using the patterning method. The patterning method includes depositing first and second conductive films separate from each other, on an area corresponding to a pattern of the self-assembled colloidal photonic crystals that are to be formed on a substrate and on another area except for the area corresponding to the pattern, respectively, and growing the photonic crystals on the substrate on which the first and second conductive films are deposited by dip-coating in a fluid containing colloidal particles while applying a DC voltage to the respective first and second conductive films. Various types of colloidal photonic crystals can be fabricated depending on the electrode pattern defined on the substrate.Type: GrantFiled: February 14, 2005Date of Patent: May 8, 2007Assignee: Samsung Electronics Co., Ltd.Inventors: Il-kwon Moon, Jong-ho Kim, Sang-hoon Shin, Suk-han Lee
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Patent number: 7194801Abstract: A method and system for fabricating solid-state energy-storage devices including fabrication films for devices without an anneal step. A film of an energy-storage device is fabricated by depositing a first material layer to a location on a substrate. Energy is supplied directly to the material forming the film. The energy can be in the form of energized ions of a second material. Supplying energy directly to the material and/or the film being deposited assists in controlling the growth and stoichiometry of the film. The method allows for the fabrication of ultrathin films such as electrolyte films and dielectric films.Type: GrantFiled: March 23, 2001Date of Patent: March 27, 2007Assignee: Cymbet CorporationInventors: Mark Lynn Jenson, Victor Henry Weiss
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Patent number: 7189287Abstract: Formation of a layer of material on a surface by atomic layer deposition methods and systems includes using electron bombardment of the chemisorbed precursor.Type: GrantFiled: June 29, 2004Date of Patent: March 13, 2007Assignee: Micron Technology, Inc.Inventor: Neal R. Rueger
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Patent number: 7182811Abstract: A semiconductor light emitting device comprises: a substrate; an n-type layer provided on the substrate and made of a nitride semiconductor material; a multiple quantum well structure active layer including a plurality of well layers each made of InxGa(1-x-y)AlyN (0?x, 0?y, x+y<1) and a plurality of barrier layers each made of InaGa(1-a-t)AltN (0?s, 0?t, s+t<1), the multiple quantum well structure active layer being provided on the n-type layer; and a p-type layer provided on the multiple quantum well structure active layer and made of a nitride semiconductor material. The p-type layer contains hydrogen, and the hydrogen concentration of the p-type layer is greater than or equal to about 1×1016 atoms/cm3 and less than or equal to about 1×1019 atoms/cm3.Type: GrantFiled: February 23, 2004Date of Patent: February 27, 2007Assignee: Sharp Kabushiki KaishaInventor: Masaya Ishida
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Patent number: 7150789Abstract: An atomic layer deposition method includes positioning a semiconductor substrate within an atomic layer deposition chamber. A first precursor gas is flowed to the substrate within the atomic layer deposition chamber effective to form a first monolayer on the substrate. After forming the first monolayer, a reactive intermediate gas is flowed to the substrate within the deposition chamber. The reactive intermediate gas is capable of reaction with an intermediate reaction by-product from the first precursor flowing under conditions of the reactive intermediate gas flowing. After flowing the reactive intermediate gas, a second precursor gas is flowed to the substrate within the deposition chamber effective to form a second monolayer on the first monolayer. Other aspects and implementations are contemplated.Type: GrantFiled: July 29, 2002Date of Patent: December 19, 2006Assignee: Micron Technology, Inc.Inventors: Paul J. Castovillo, Cem Basceri, Garo J. Derderian, Gurtej S. Sandhu
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Patent number: 7141116Abstract: Provided are improved methods for forming silicon films, particularly single-crystal silicon films from amorphous silicon films in which a single-crystal silicon substrate is prepared by removing any native oxide, typically using an aqueous HF solution, and placed in a reaction chamber. The substrate is then heated from about 350° C. to a first deposition temperature under a first ambient to induce single-crystal epitaxial silicon deposition primarily on exposed silicon surfaces. The substrate is then heated to a second deposition temperature under a second ambient that will maintain the single-crystal epitaxial silicon deposition on exposed single-crystal silicon while inducing amorphous epitaxial silicon deposition on insulating surfaces. The amorphous epitaxial silicon can then be converted to single-crystal silicon using a solid phase epitaxy process to form a thin, high quality silicon layer.Type: GrantFiled: April 1, 2005Date of Patent: November 28, 2006Assignee: Samsung Electronics Co., Ltd.Inventors: Yong Hoon Son, Jae Young Park, Cha Dong Yeo, Jong Wook Lee, Yu Gyun Shin
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Patent number: 7141115Abstract: A method of fabricating a high-quality relaxed SiGe-on-insulator substrate material is provided in which a prefabricated silicon-on-insulator substrate is first exposed to an unstrained Ge-containing source and then heated (annealed/oxidized) to cause Ge diffusion and thermal mixing of Ge within a single-crystal Si-containing layer of the prefabricated silicon-on-insulator substrate. The unstrained Ge-containing source can comprise a solid Ge-containing source, a gaseous Ge-containing source, or ions of Ge.Type: GrantFiled: September 2, 2004Date of Patent: November 28, 2006Assignee: International Business Machines CorporationInventors: Stephen W. Bedell, Keith E. Fogel, Devendra K. Sadana
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Patent number: 7135071Abstract: A fractal structure is formed to have a plurality of regions different in fractal dimension characterizing the self-similarity. The fractal structure is grown from one or more origins under growth conditions providing a first fractal dimension in a first portion of the growth process from the start point of time to a first point of time, and under growth conditions providing a second fractal dimension lower than the first fractal dimension in another portion of the growth process from the first point of time to a second point of time. By adjusting the timing for changing the growth conditions, the fractal structure is controlled in nature of phase transition, such as critical temperature for ferromagnetic phase transition, which occurs in the fractal structure. For enhancing the controllability, the first fractal dimension is preferably larger than 2.7 and the second fractal dimension is preferably smaller than 2.3.Type: GrantFiled: August 24, 2001Date of Patent: November 14, 2006Assignee: Sony CorporationInventor: Ryuichi Ugajin
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Patent number: 7128787Abstract: An atomic layer deposition method includes positioning a semiconductor substrate within an atomic layer deposition chamber. A first precursor gas is flowed to the substrate within the atomic layer deposition chamber effective to form a first monolayer on the substrate. After forming the first monolayer, a reactive intermediate gas is flowed to the substrate within the deposition chamber. The reactive intermediate gas is capable of reaction with an intermediate reaction by-product from the first precursor flowing under conditions of the reactive intermediate gas flowing. After flowing the reactive intermediate gas, a second precursor gas is flowed to the substrate within the deposition chamber effective to form a second monolayer on the first monolayer. Other aspects and implementations are contemplated.Type: GrantFiled: September 30, 2004Date of Patent: October 31, 2006Assignee: Micron Technology, Inc.Inventors: Paul J. Castovillo, Cem Basceri, Garo J. Derderian, Gurtej S. Sandhu
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Patent number: 7101434Abstract: A fractal structure is formed to have a plurality of regions different in fractal dimension characterizing the self-similarity. Especially in a stellar fractal structure, a region with a low fractal dimension is formed around a core with a high fractal dimension. By adjusting the ratios in volume of these regions relative to the entire fractal structure, the nature of phase transition occurring in the fractal structure, such as a magnetization curve of Mott transition or ferromagnetic phase transition, quantum chaos in the electron state, or the like. For enhancing the controllability, the fractal dimension of the core is preferably larger than 2.7 and the fractal dimension of the region around the core is preferably smaller than 2.3.Type: GrantFiled: May 22, 2001Date of Patent: September 5, 2006Assignee: Sony CorporationInventor: Ryuichi Ugajin
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Patent number: 7094289Abstract: A method for manufacturing a highly-crystallized oxide powder, wherein an oxide powder is produced by ejecting a starting material powder containing at least one metal element and/or semimetal element, which will become a constituent component of the oxide, into a reaction vessel together with a carrier gas through a nozzle; and heating the starting material powder at a temperature higher than the decomposition temperature or reaction temperature thereof and not lower than (Tm/2)° C., where Tm° C. stands for a melting point of the oxide, in a state in which the starting material powder is dispersed in a gas phase at a concentration of not higher than 10 g/L. In the above method, the starting material powder may be mixed and dispersed in the carrier gas by using a dispersing machine prior to being ejected into the reaction vessel through a nozzle.Type: GrantFiled: July 30, 2003Date of Patent: August 22, 2006Assignee: Shoei Chemical Inc.Inventors: Yuji Akimoto, Masami Nakamura, Kazuro Nagashima
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Patent number: 7090723Abstract: High temperature composites and thermal barrier coatings, and related methods, using anisotropic ceramic materials, such materials as can be modified to reduce substrate thermal mismatch.Type: GrantFiled: January 20, 2004Date of Patent: August 15, 2006Assignee: Applied Thin Films, Inc.Inventors: Sankar Sambasivan, Kimberly Steiner
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Patent number: 7074272Abstract: Device quality, single crystal film of cubic zinc-blende aluminum nitride (AlN) is deposited on a cubic substrate, such as a silicon (100) wafer by plasma source molecular beam epitaxy (PSMBE). The metastable zinc-blende form of AlN is deposited on the substrate at a low temperature by a low energy plasma beam of high-energy activated aluminum ions and nitrogen ion species produced in a molecular beam epitaxy system by applying a pulsed d.c. power to a hollow cathode source. In this manner, films having a thickness of at least 800 ? were produced. The lattice parameter of as-deposited films was calculated to be approximately 4.373 ? which corresponds closely to the theoretical calculation (4.38 ?) for cubic zinc-blende AlN. An interfacial layer of silicon carbide, specifically the cubic 3C—SiC polytype, interposed between the epitaxial film of zinc-blende AlN and the Si(100) wafer provides a template for growth and a good lattice match.Type: GrantFiled: February 10, 2003Date of Patent: July 11, 2006Assignee: Wayne State UniversityInventors: Margarita P. Thompson, Gregory W. Auner
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Patent number: 7063742Abstract: A substrate is polished and made an inclined substrate, which is exposed to a hydrogen plasma and is thereby smoothened. The substrate is then heated controlledly until it surface temperature reaches 830° C. Meanwhile, a gas mixture of 1% methane, 50 ppm hydrogen sulfide and hydrogen is introduced in a tubular reaction vessel to flow therethrough at 200 ml/min, where microwave plasma is excited to cause n-type semiconductor diamond to epitaxially grow on the substrate. An ion doped n-type semiconductor is thus formed that has a single donor level of an activation energy at 0.38 eV and is high in mobility and of high quality.Type: GrantFiled: March 27, 2000Date of Patent: June 20, 2006Assignee: Japan Science and Technology AgencyInventors: Toshihiro Ando, Yoichiro Sato, Eiji Yasu, Mika Gamo, Isao Sakaguchi
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Patent number: 7060131Abstract: The present invention relates a method for epitaxial growth of a second group III-V crystal having a second lattice constant over a first group III-V crystal having a first lattice constant, wherein strain relaxation associated with lattice-mismatched epitaxy is suppressed and thus dislocation defects do not form. In the first step, the surface of the first group III-V crystal (substrate) is cleansed by desorption of surface oxides. In the second step, a layer of condensed group-V species is condensed on the surface of the first group III-V crystal. In the third step, a mono-layer of constituent group-III atoms is deposited over the layer of condensed group-V species in order for the layer of constituent group-III atoms to retain the condensed group-V layer. Subsequently, the mono-layer of group-III atoms is annealed at a higher temperature.Type: GrantFiled: May 9, 2001Date of Patent: June 13, 2006Assignee: HRL Laboratories, LLCInventor: Binqiang Shi
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Patent number: 7060130Abstract: A process for growing by chemical vapor deposition a heteroepitaxial single crystal diamond is disclosed. The process provides a substrate which enables the growth of single crystal diamond which is vapor coated on an iridium film. An intermediate process for producing a composite composition with diamond nuclei is also described. Further described are composite compositions of metal oxide, iridium and single crystal diamond films or diamond nuclei. Single crystal diamond is useful in a variety of electronics and acoustics fields.Type: GrantFiled: August 5, 2003Date of Patent: June 13, 2006Assignee: Board of Trustees of Michigan State UniversityInventors: Brage Golding, Connie Bednarski-Meinke, Zhong-ning Dai
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Patent number: 7033434Abstract: A method of crystallizing amorphous silicon is used for manufacturing an array substrate having thin film transistors, pixel electrodes and an alignment key. The method includes forming an amorphous silicon layer over a substrate, forming an alignment key in the amorphous silicon layer, preparing a mask including pattern portions and an alignment key pattern, disposing the mask over the substrate having the amorphous silicon layer, wherein the alignment key pattern is aligned with the alignment key, and applying a first shot of a laser beam to in the amorphous silicon layer to form first polycrystalline silicon areas corresponding to the pattern portions of the mask.Type: GrantFiled: December 29, 2003Date of Patent: April 25, 2006Assignee: LG. Philips LCD Co., Ltd.Inventor: Young-Joo Kim
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Patent number: 7022183Abstract: To improve the laser annealing process for polycrystallizing amorphous silicon to form silicon thin films having large crystal particle diameters at a high throughput, the present invention is directed to a process of crystallization by irradiation of a semiconductor thin film formed on a substrate with pulsed laser light. The process comprises having a means to shape laser light into a linear beam and a means to periodically and spatially modulate the intensity of pulsed laser in the direction of the long axis of the linear beam by passing through a phase-shifting stripy pattern perpendicular to the long axis, and collectively forming for each shot a polycrystalline film composed of crystals which have grown in a certain direction over the entire region irradiated with the linear beam.Type: GrantFiled: June 17, 2003Date of Patent: April 4, 2006Assignee: Hiatchi, Ltd.Inventors: Kazuo Takeda, Jun Gotou, Masakazu Saito, Makoto Ohkura, Takeshi Satou, Hiroshi Fukuda, Takeo Shiba
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Patent number: 7018469Abstract: A substrate is positioned within a deposition chamber. Trimethylsilane is flowed to the chamber and a first inert gas is flowed to the chamber under conditions effective to chemisorb a first species monolayer comprising silicon onto the substrate. The first inert gas is flowed at a first rate. After forming the first species monolayer, an oxidant is flowed to the chamber and a second inert gas is flowed to the chamber under conditions effective to react the oxidant with the chemisorbed first species and form a monolayer comprising silicon dioxide on the substrate. The second inert gas flowing is at a second rate which is less than the first rate. The a) trimethylsilane and first inert gas flowing and the b) oxidant and second inert gas flowing are successively repeated effective to form a silicon dioxide comprising layer on the substrate. Other implementations and aspects are contemplated.Type: GrantFiled: September 23, 2003Date of Patent: March 28, 2006Assignee: Micron Technology, Inc.Inventors: Li Li, Weimin Li, Gurtej S. Sandhu
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Patent number: 7014710Abstract: A method of growing single crystal Gallium Nitride on silicon substrate is disclosed including: removing oxide layer of silicon substrate, growing buffer layer of Silicon Carbon Nitride (SiCN), and growing single crystalline Gallium Nitride thin film, characterized in that a buffer layer of SiCN is grown to avoid lattice mismatch which appears when Gallium Nitride is grown directly on silicon substrate, and that Rapid Thermal Chemical Vapor Deposition is adopted to grow SiCN buffer layer, and that Metalorganic Chemical Vapor Deposition is adopted to grow single crystalline GaN thin film.Type: GrantFiled: July 8, 2003Date of Patent: March 21, 2006Assignee: National Cheng-Kung UniversityInventors: Yean Kuen Fang, Wen Rong Chang, Shyh Fann Ting, Hon Kuan, Cheng Nan Chang
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Patent number: 7014708Abstract: An amorphous silicon pattern is formed first. A first region, a second region, at least one first pointed region adjacent to the second region and having a second height, at least one fourth region between the first region and each first pointed region are included in the amorphous silicon pattern. Each fourth region has a fourth height smaller than the second height. A laser crystallization process is performed to form a first single crystal silicon grain in each fourth region.Type: GrantFiled: June 10, 2004Date of Patent: March 21, 2006Assignee: Toppoly Optoelectronics Corp.Inventor: Ching-Wei Lin
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Patent number: 7001459Abstract: A method of making a spinel-structured metal oxide on a substrate by molecular beam epitaxy, comprising the step of supplying activated oxygen, a first metal atom flux, and at least one other metal atom flux to the surface of the substrate, wherein the metal atom fluxes are individually controlled at the substrate so as to grow the spinel-structured metal oxide on the substrate and the metal oxide is substantially in a thermodynamically stable state during the growth of the metal oxide. A particular embodiment of the present invention encompasses a method of making a spinel-structured binary ferrite, including Co ferrite, without the need of a post-growth anneal to obtain the desired equilibrium state.Type: GrantFiled: August 29, 2003Date of Patent: February 21, 2006Assignee: Battelle Memorial InstituteInventor: Scott A. Chambers
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Patent number: 6994751Abstract: A nitride-based semiconductor element having superior mass productivity and excellent element characteristics is obtained. This nitride-based semiconductor element comprises a substrate comprising a surface having projection portions, a mask layer formed to be in contact with only the projection portions of the surface of the substrate, a first nitride-based semiconductor layer formed on recess portions of the substrate and the mask layer and a nitride-based semiconductor element layer, formed on the first nitride-based semiconductor layer, having an element region. Thus, the first nitride-based semiconductor layer having low dislocation density is readily formed on the projection portions of the substrate and the mask layer through the mask layer serving for selective growth.Type: GrantFiled: February 25, 2002Date of Patent: February 7, 2006Assignee: Sanyo Electric Co., Ltd.Inventors: Masayuki Hata, Tatsuya Kunisato, Nobuhiko Hayashi
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Patent number: 6962613Abstract: A method and system for fabricating solid-state energy-storage devices including fabrication films for devices without an anneal step, especially a cathode anneal of thin-film batteries. A film of an energy-storage device is fabricated by depositing a first material layer to a location on a substrate. Energy is supplied directly to the material forming the film. The energy can be in the form of energized ions of a second material. Supplying energy directly to the material and/or the film being deposited assists the growth of the crystalline structure of film. For lithium-ion energy-storage devices, the first material is an intercalation material, which releasably stores lithium ions therein. Supercapacitors and energy-conversion devices are also fabricated according the methods.Type: GrantFiled: March 23, 2001Date of Patent: November 8, 2005Assignee: Cymbet CorporationInventor: Mark L. Jenson
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Patent number: 6958094Abstract: The present invention provides a method for slicing a single crystal, wherein the single crystal is sliced by irradiating a portion to be sliced with an ultra short pulse laser beam while supplying a gas containing gaseous molecules or radicals that react with atoms constituting the single crystal to become stable gaseous molecules in the vicinity of the portion under slicing. Thus, there is provided a method for slicing a single crystal by using a laser processing, in which a single crystal is processed while obtaining a good sliced surface and markedly reducing a slicing loss.Type: GrantFiled: July 6, 2001Date of Patent: October 25, 2005Assignee: Shin-Etsu Handotai Co., Ltd.Inventors: Tadahiro Ohmi, Shigetoshi Sugawa, Toshikuni Shinohara, Tatsuo Ito, Koichi Kanaya
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Patent number: 6929695Abstract: The present invention is an tri-phase epitaxy method for preparing a single crystal oxide thin film, comprising the steps of depositing on a substrate an oxide thin film serving as a seed layer and having the same composition as that of an oxide thin film to be formed, depositing on the seed layer a thin film comprising a substance capable of being melted and liquidized by heat from the substrate and dissolving the oxide to be subsequent by deposited onto the seed layer, heating the substrate to form a liquid layer, and depositing an oxide on the seed layer through the liquid layer by use of a vapor-phase epitaxy method to form the single crystal oxide thin film. In this method, the oxygen partial pressure on the liquid layer is set in the range of 1.0 to 760 Torr during the film-forming step.Type: GrantFiled: August 31, 2001Date of Patent: August 16, 2005Assignee: Japan Science and Technology AgencyInventors: Hideomi Koinuma, Masashi Kawasaki, Yuji Matsumoto