One A Neutralizer For Another Patents (Class 134/27)
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Patent number: 11034921Abstract: Methods, compositions, and kit(s) for removing corrosion or scale from a metal or a non-metal article are disclosed. In a first stage of the method, an article exhibiting corrosion can be exposed to an acid wash composition including a first acid component having one or more of HCl, Phosphoric Acid, Oxalic Acid, a second acid inhibitor/surfactant component including ethoxylated alkyl mercaptan, and a third thixotropic gelling agent component including Talc or Fumed silica, sufficient to cause gelling of the acid wash composition. In a second stage of the method performed subsequent to the first stage, the article can be exposed to an acid neutralizing composition comprising bicarbonate, borax, isopropyl alcohol and water.Type: GrantFiled: May 15, 2019Date of Patent: June 15, 2021Inventor: Adam Mason Prince
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Patent number: 10828679Abstract: A method of treating a sensor array including a plurality of sensors and an isolation structure, where a sensor of the plurality of sensors has a sensor pad exposed at a surface of the sensor array and the isolation structure is disposed between the sensor pad and sensor pads of other sensors of the plurality of sensors, comprises exposing the sensor pad and the isolation structure to a non-aqueous organo-silicon solution including an organo-silicon compound and a first non-aqueous carrier; applying an acid solution including an organic acid and a second non-aqueous carrier to the sensor pad; and rinsing the acid solution from the sensor pad and the isolation structure.Type: GrantFiled: October 24, 2019Date of Patent: November 10, 2020Assignee: Life Technologies CorporationInventors: James A. Ball, Phil Waggoner, Scott Parker
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Patent number: 10816505Abstract: A sensor array includes a plurality of sensors. A sensor of the plurality of sensors has a sensor pad exposed at a surface of the sensor array. A method of treating the sensor array includes exposing at least the sensor pad to a wash solution including sulfonic acid and an organic solvent and rinsing the wash solution from the sensor pad.Type: GrantFiled: November 18, 2019Date of Patent: October 27, 2020Assignee: Life Technologies CorporationInventors: James A. Ball, Brian Reed
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Patent number: 10428279Abstract: The invention is directed to a germicidal treatment fluid comprising electrolyzed water and an amine, and methods for producing and using same to kill microorganisms which produce hydrogen sulphide or sulfate-reducing bacteria.Type: GrantFiled: December 15, 2017Date of Patent: October 1, 2019Inventors: William Dale Storey, Norman L. Arrison, Dale R. Schadeck
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Patent number: 10226409Abstract: This invention describes pyruvate and related ?-ketocarboxylates as novel adjuvants in the treatment of acute post-tooth-whitening pain and sensitivity; the key feature is the cytoprotective efficacy of pyruvate on oral soft tissue, especially after topical application of high and therefore cytotoxic concentrations of H2O2, currently used in tooth whitening procedures.Type: GrantFiled: September 22, 2017Date of Patent: March 12, 2019Inventors: Zoltan Rusznak, Rolf Bunger
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Patent number: 10182977Abstract: Pyruvate may be used to stabilize hyaluronic acid compositions. For example, these compositions may have improved heat and/or storage stability.Type: GrantFiled: August 4, 2016Date of Patent: January 22, 2019Assignee: Allergan Industrie, S.A.S.Inventor: Sebastien Pierre
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Patent number: 9963802Abstract: A method of delinting cotton seeds with an alkanesulfonic acid comprises the steps of applying the alkanesulfonic acid to surfaces of linted cotton seeds, optionally heating the linted cotton seeds, and applying mechanical force to the surfaces of the linted cotton seeds. A composition for delinting cotton seeds comprises an alkanesulfonic acid (e.g. methanesulfonic acid (MSA)), a surfactant, and water.Type: GrantFiled: March 3, 2015Date of Patent: May 8, 2018Assignee: BASF SEInventors: Joseph P. Borst, Kenneth L. Zack
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Patent number: 9950279Abstract: The present invention discloses methods of neutralizing apatite surfaces, for example after a flow-through collection of a target and prior to cleaning the chromatography solid support.Type: GrantFiled: July 19, 2017Date of Patent: April 24, 2018Assignee: Bio-Rad Laboratories, Inc.Inventor: Larry J. Cummings
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Patent number: 9873838Abstract: The invention is directed to a treatment fluid comprising electrolyzed water and an amine, and methods for producing and using same in the treatment of a gas or liquid containing a contaminant such as an acid gas or a sulphur compound.Type: GrantFiled: April 4, 2016Date of Patent: January 23, 2018Inventors: William Dale Storey, Norman L. Arrison, Dale R. Schadeck
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Patent number: 9845447Abstract: The invention is directed to methods of generating carbonate in situ in a use solution under an enriched CO2 atmosphere. In another aspect, the invention is directed to methods of cleaning food processing surfaces under an enriched CO2 atmosphere comprising contacting a food processing surface with a cleaning composition comprised of an alkalinity source, a surfactant, and water, monitoring the pH during the wash cycle and adjusting the pH by recirculating a use solution, adding a secondary alkalinity source, or both recirculating a use solution and adding a secondary alkalinity source, to generate carbonate in situ in the use solution. In a particular embodiment of the invention the alkalinity source is an alkali metal carbonate and the secondary alkalinity source is an alkali metal hydroxide.Type: GrantFiled: November 5, 2015Date of Patent: December 19, 2017Assignee: Ecolab USA Inc.Inventors: Anthony W. Erickson, Peter J. Fernholz
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Patent number: 9833536Abstract: A contact lens storage system that includes sterilized solution, at least one contract lens, a buffering agent, and a container. The sterilized solution and contact lens are physically separated from the buffering agent. Also described herein are related methods for neutralizing a sterilized contact lens solution, methods of inserting a contact lens onto an eye, and methods of disinfecting and neutralizing a contact lens.Type: GrantFiled: February 3, 2016Date of Patent: December 5, 2017Assignee: Medivators Inc.Inventors: John J. Matta, Jon Olson, Matt Conlon
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Patent number: 9637677Abstract: An aqueous cleaning composition for removing paraffin, asphaltene, and scale deposits or plugs from a hydrocarbon system. The aqueous cleaning composition is formed of a cleaning composition and an aqueous liquid. The cleaning composition contains about 21-33% of a silicate, about 20-35% of a peroxygen, about 3-15% of a phosphate, about 15-40% of a carbonate or bicarbonate, about 1-10% of a chelating agent, about 1-5.5% of a surfactant combination. In one embodiment, the surfactant combination includes a surfactant polymer mixture containing a block polymer and a reverse polymer, and a wetting agent containing a sulfonated material or an ethoxylated alcohol.Type: GrantFiled: September 4, 2014Date of Patent: May 2, 2017Assignee: IDEAL ENERGY SOLUTIONS IP CONTROL, LLCInventor: Charles Bullick Talley
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Patent number: 9580831Abstract: A pickling process designed for pickling a metal strip such as a stainless steel strip reduces the amount of HF and/or HNO3. The strip is immersed in at least one first pickling tub that contains a mixture of an acid such as H2SO4, an excess of at least one oxidizing agent, and includes electrodes that may apply a current to the strip that runs through the mixture.Type: GrantFiled: September 26, 2012Date of Patent: February 28, 2017Assignee: AK Steel Properties, Inc.Inventors: Amanda R. Glass, Ronald D. Rodabaugh, David M. Price
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Patent number: 9551162Abstract: A method for treating a swimming pool, including introducing Mg2+ to a level from 60 ppm to 300 ppm to the swimming pool by addition of a soluble magnesium compound to the swimming pool, or Mg2+ to a level from 60 ppm to 1000 ppm by addition of a magnesium halide in addition to a further soluble magnesium compound.Type: GrantFiled: April 29, 2011Date of Patent: January 24, 2017Assignee: ZODIAC GROUP AUSTRALIA PTY LTD.Inventors: Ross Leslie Palmer, Stuart Bruce Anderson
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Publication number: 20150144160Abstract: The present invention provides an etchant which is a reaction product of sulfuric acid and ammonium persulfate, wherein the concentration of the ammonium persulfate is 1˜25%, the concentration of the sulfuric acid is 98%. The etchant is produced by adding the ammonium persulfate into the sulfuric acid at a temperature of 100 to 200 degree Celsius. According to the present invention, the ammonium persulfate substitute the conventional oxidizing agent of hydrogen peroxide. Since the ammonium persulfate is in a powder form, the operation becomes more convenient. Furthermore, since sulfuric acid is formed as a by-product instead of water, the etchant will not be diluted after being used for many times, which reduces the production cost.Type: ApplicationFiled: March 27, 2013Publication date: May 28, 2015Inventors: Sally Ann Henry, Jintao Huang, Jia Ma, Yi Wu, Yujia Su
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Patent number: 8961699Abstract: A method for operating a water-conducting domestic appliance, including a domestic dishwasher, wherein the water-conducting domestic appliance includes a program controller for performing a plurality of sequential program steps and the program controller operatively interacts with at least a detergent-dosing system, the method including the step of adding at least one cleaning substance having a function during at least one program step.Type: GrantFiled: August 29, 2007Date of Patent: February 24, 2015Assignee: BSH Bosch und Siemens Hausgeraete GmbHInventors: Egbert Classen, Michael Fauth, Caroline Heiligenmann, Helmut Jerg, Kai Paintner
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Patent number: 8956464Abstract: Methods for cleaning polymeric microfiltration or ultrafiltration membranes. The membrane may be contacted with a first cleaning solution including at least one oxidising agent. A second cleaning solution including at least one reducing agent may then be introduced to the membrane and first cleaning solution. The oxidising and reducing agents may undergo a neutralisation reaction to form an oxidation-neutral mixed cleaning solution. The membrane may be simultaneously cleaned during the neutralisation reaction.Type: GrantFiled: June 11, 2010Date of Patent: February 17, 2015Assignee: Evoqua Water Technologies LLCInventors: Peter Zauner, Fufang Zha
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Patent number: 8936686Abstract: A method of selecting a mercury-contaminated solid surface followed by heating a cleaning solution to a temperature less than 100° C. The cleaning solution can contain hydrocarbon oil and one or more organic sulfur compounds. Afterwards, the heated cleaning solution is contacted with the mercury-contaminated solid surface to remove the mercury contamination.Type: GrantFiled: September 8, 2011Date of Patent: January 20, 2015Assignee: ConocoPhillips CompanyInventors: Charles John Lord, III, Lars Torsten Lambertsson, Erik Lennart Bjorn, Wolfgang Frech
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Publication number: 20150007859Abstract: The present invention concerns methods for removing sulfur from yarn comprising the steps of: a) contacting never-dried polymeric yarn with an aqueous base, the polymer comprising imidazole groups and said polymer comprising sulfur atoms characterized as being in the form of sulfate anions; b) contacting the yarn with an aqueous acid solution of pH 5 or lower; and c) rinsing the yarn.Type: ApplicationFiled: January 11, 2012Publication date: January 8, 2015Applicant: E I DU PONT DE NEMOURS AND COMPANYInventors: Steven R. Allen, Vlodek Gabara, Joseph Lenning Lowery, Christopher William Newton, David J. Rodini, Andrew J. Sitter
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Publication number: 20150000704Abstract: A method of cleaning a substrate such as semiconductor substrate for IC fabrication is described that includes cleaning the semiconductor substrate with a first mixture of ozone and one of an acid and a base, followed by a second mixture of ozone and the other one of the acid and the base. The cleaning mixtures may further include de-ionized water. In an embodiment, the mixture is sprayed onto a heated substrate surface. The acid may be HF; the base may be NH4OH.Type: ApplicationFiled: September 18, 2014Publication date: January 1, 2015Inventors: Ming-Hsi Yeh, Sung-Hsun Wu, Chao-Cheng Chen, Syun-Ming Jang, Bo-Wei Chou
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Publication number: 20150000701Abstract: An apparatus and method for removing accumulated ash and soot from DPFs which uses a combination of ultrasonic energy coupled via a liquid cleaning solution to the internal and external surfaces of the DPF to dislodge and remove the accumulated materials, and a system of directing clean solution for rinsing of the filter elements by continuous filtration of the rinse solution, and a means of drawing residual material-laden cleaning solution from the filter to complete the cleaning process.Type: ApplicationFiled: October 22, 2012Publication date: January 1, 2015Inventors: Mark TEVELEY, Byron KIESER
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Publication number: 20140366917Abstract: A cleaning system configured to use a hydrogen peroxide solution to clean contact lenses. The cleaning system includes a reservoir to hold the cleaning solution and a complex base coupled to the reservoir to insure a hermetically closed reservoir environment. The complex base is separated into at least a first and a second segment. A lens holder assembly holds the lenses within the solution and is coupled to the complex base in the first segment. A motor is located in the second segment of the complex base to selectively introduce a catalyst to the cleaning solution. The cleaning system has additional features that permit the system to allow for the storage of the contact lenses by converting a neutralized cleaning solution into a storage solution to prevent recontamination.Type: ApplicationFiled: October 12, 2012Publication date: December 18, 2014Inventor: Yoseph YAACOBI
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Patent number: 8876983Abstract: A method for in-line cleaning of ultrasonic welding tools is described. The method includes applying cleaning solution onto a work surface of a welding tool to be cleaned using an application device. Then the method involves removing residue dissolved in the cleaning solution from the work surface using a cleaning device. Next, the work surface is neutralized and rinsed using purified water and polished with a cleaning cloth. Finally, the work surface is rinsed using cleaning alcohol and blow-dried with compressed air.Type: GrantFiled: September 1, 2011Date of Patent: November 4, 2014Assignee: Ford Global Technologies, LLCInventor: Humi Widhalm
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Patent number: 8864915Abstract: A method of processing a substrate having a transparent conductive oxide disposed thereon, including: exposing the substrate to a first cleaning solution comprising hydrogen peroxide and ammonium citrate; exposing the substrate to a second cleaning solution having a pH within a range from about 6 to about 7, the second cleaning solution different than the first cleaning solution; agitating the second cleaning solution; and depositing a silicon-containing film on the transparent conductive oxide.Type: GrantFiled: August 3, 2011Date of Patent: October 21, 2014Assignee: Applied Materials, Inc.Inventors: Renhe Jia, Adam Brand, Liming Zhang, Dapeng Wang, Tzay-Fa Su, Vijay Parihar
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Patent number: 8834643Abstract: A method for cleaning objects made of organic or inorganic materials, wherein the relevant material is brought into contact with a composition in the form of a fluid nanophase system, comprising a) at least one water-insoluble substance having a water solubility of less than 4 grams per liter, b) at least one amphiphilic substance (NP-MCA) which has no surfactant structure, is not structure-forming on its own, the solubility of which in water or oil ranges between 4 g and 1000 g per liter and which does not preferably accumulate at the oil-water interface, c) at least one anionic, cationic, amphoteric and/or non-ionic surfactant, d) at least one polar protic solvent, in particular having hydroxy functionality, e) if necessary one or more auxiliary substance.Type: GrantFiled: March 22, 2010Date of Patent: September 16, 2014Assignee: Bubbles and Beyond GmbHInventors: Dirk Schumann, Rainer Surkow
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Patent number: 8801867Abstract: A method for cleaning process apparatus used for production of liquids, especially for cleaning filters, for example membrane filters. The apparatus is contacted with a solution of periodate. It is especially preferred that the cleaning process is carried out at a temperature between 15 and 95° C.Type: GrantFiled: January 26, 2010Date of Patent: August 12, 2014Assignee: X-Flow B.V.Inventors: Arie Cornelis Besemer, Elmar Van Mastrigt, André Mepschen
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Patent number: 8758520Abstract: Methods of acidic warewashing are disclosed. The compositions can include other materials including surfactants and chelating agents, and are preferably phosphorous free. Methods of using the acidic compositions are also disclosed. Exemplary methods include using the acidic compositions together with other compositions, including alkaline compositions and rinse aids employed in an alternating alkaline/acid/alkaline manner. The methods also include acidic compositions that serve multiple roles.Type: GrantFiled: May 18, 2012Date of Patent: June 24, 2014Assignee: Ecolab USA Inc.Inventors: Lee J. Monsrud, Michael S. Rischmiller, Daniel Osterberg, John Mansergh
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Patent number: 8747567Abstract: A hard floor surface care process comprising a process of identifying, cleaning, polishing, and protecting manmade and natural stone hard floor surfaces having a single surface or multi-surface quality. The hard floor surface care process comprising an acid reactive or nonreactive hard floor surface identifying process; an emulsifying solution, agitating, and toweling cleaning process; a polishing process utilizing a lubricating solution with a polishing chemistry or pad, and a protecting process utilizing a protecting chemistry selected as a function of the identifying process.Type: GrantFiled: September 30, 2013Date of Patent: June 10, 2014Inventor: Steven D. Azevedo
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Patent number: 8741070Abstract: Disclosed are a liquid processing method, a liquid processing apparatus, and a recording medium that can prevent convex portions of a target substrate from collapsing when a rinsing liquid is dried. A base surface of a target substrate is hydrophilized and the surfaces of convex portions become water-repellent by surface-processing the target substrate which includes a main body, a plurality of convex portions protruding from the main body, and a base surface formed between the convex portions on the substrate main body. Next, a rinsing liquid is supplied to the target substrate which has been subjected to the surface processing. Thereafter, the rinsing liquid is removed from the target substrate.Type: GrantFiled: December 16, 2011Date of Patent: June 3, 2014Assignee: Tokyo Electron LimitedInventors: Nobutaka Mizutani, Tsutae Omori, Takehiko Orii, Akira Fujita
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Patent number: 8728334Abstract: A protective chuck is disposed on a substrate with a gas layer between the bottom surface of the protective chuck and the substrate surface. The gas layer protects a surface region against a fluid layer covering the substrate surface. In some embodiments, the pressure fluctuation at the gas layers is monitored, and through the dynamic feedback, the gas flow rate can be adjusted to achieve a desired operation regime. The dynamic control of operation regime setting can also be applied to high productivity combinatorial systems having an array of protective chucks.Type: GrantFiled: November 29, 2011Date of Patent: May 20, 2014Assignee: Intermolecular, Inc.Inventor: Rajesh Kelekar
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Patent number: 8709167Abstract: A method of warewashing for the removal of starch is described herein. The method includes applying an alkaline composition to a dish, then applying an acidic composition to a dish, and then applying a second alkaline composition to the dish. The method may include additional steps. Compositions for using with the method are also disclosed. Finally, dish machines that may be used in accordance with the method are disclosed.Type: GrantFiled: May 20, 2011Date of Patent: April 29, 2014Assignee: Ecolab USA Inc.Inventors: Werner Strothoff, Winfried Troll, Helmut Maier, John P. Furber, Bryan A. Maser, Michael E. Besse
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Patent number: 8691019Abstract: A process for cleaning a compound semiconductor wafer; the compound semiconductor wafer comprises, taking gallium arsenide (GaAs) as a representative, a group III-V compound semiconductor wafer. The process comprises the following steps: 1) treating the wafer with a mixture of dilute ammonia, hydrogen peroxide and water at a temperature not higher than 20° C.; 2) washing the wafer with deionized water; 3) treating the wafer with an oxidant; 4) washing the wafer with deionized water; 5) treating the wafer with a dilute acid solution or a dilute alkali solution; 6) washing the wafer with deionized water; and 7) drying the resulting wafer. The process can improve the cleanliness, micro-roughness and uniformity of the wafer surface.Type: GrantFiled: October 14, 2011Date of Patent: April 8, 2014Assignee: Beijing Tongmei Xtal Technology Co., Ltd.Inventors: Diansheng Ren, Qinghui Liu
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Patent number: 8652267Abstract: There is disclosed a coated-type silicon-containing film stripping process for stripping off to remove a coated-type silicon-containing film obtained by coating a silicon-containing film composition used in a lithography on a substrate, comprising, at least: a first step of treating the silicon-containing film with an acidic stripping solution containing sulphate ion and/or fluoride ion; and a second step of treating the silicon-containing film with an alkaline stripping solution containing a nitrogen compound. There can be provided a process for allowing a silicon-containing film, which has not been conventionally removed unless dry stripping is adopted, to be removed by a stripping process based on a stripping solution (wet stripping).Type: GrantFiled: November 9, 2009Date of Patent: February 18, 2014Assignee: Shin-Etsu Chemical Co., Ltd.Inventors: Tsutomu Ogihara, Takafumi Ueda, Toshiharu Yano, Shozo Shirai
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Patent number: 8647445Abstract: Cleaning processes for cleaning semiconductor devices or semiconductor tooling during manufacture thereof generally include contacting the semiconductor devices or semiconductor tooling with an antioxidant to form an insoluble adduct followed by solubilizing the adduct with a basic aqueous cleaning solution.Type: GrantFiled: November 6, 2012Date of Patent: February 11, 2014Assignee: International Business Machines CorporationInventors: Vishal Chhabra, John A. Fitzsimmons, Mahmoud Khojasteh, Jennifer Muncy
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Patent number: 8641829Abstract: Disclosed is a substrate processing system, including: a processing chamber to process a substrate; a vaporizing unit to vaporize a material of liquid; a supply system to supply the processing chamber with gas of the material vaporized by the vaporizing unit; an exhaust system to exhaust an atmosphere in the processing chamber; and a cleaning liquid supply system to supply the vaporizing unit with cleaning liquid for cleaning a product deposited in the vaporizing unit, wherein the cleaning liquid supply system supplies at least two kinds of cleaning liquids into the vaporizing unit so that the product can be removed from the vaporizing unit by action of the two kinds of cleaning liquids on the product.Type: GrantFiled: July 15, 2013Date of Patent: February 4, 2014Assignee: Hitachi Kokusai Electric Inc.Inventors: Tomoki Horita, Kazuhiro Hirahara, Hironobu Miya, Atsuhiko Suda, Hirohisa Yamazaki
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Patent number: 8617409Abstract: A protective chuck is magnetically levitated on a substrate with a gas layer between the bottom surface of the protective chuck and the substrate surface. The gas layer protects a surface region of the substrate against a fluid layer covering the remaining of the substrate surface without contacting the substrate, reducing or eliminating potential damage to the substrate surface. The magnetically levitated protective chuck can enable combinatorial processing of a substrate, providing multiple isolated processing regions on a single substrate with different material and processing conditions.Type: GrantFiled: November 22, 2011Date of Patent: December 31, 2013Assignee: Intermolecular, Inc.Inventors: Rajesh Kelekar, Kent Riley Child
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Patent number: 8551252Abstract: Methods for removing residual particles from a substrate are presented including: receiving the substrate including the residual particles; and functionalizing the residual particles with functionalizing molecules, wherein the functionalizing molecules selectively attach with a surface the residual particles, where the functionalizing molecules impart a changed chemical characteristic to the residual particles, and where the changed chemical characteristic facilitates removal of the residual particles from the substrate. In some embodiments, methods further include: before functionalizing, cleaning the substrate, where the cleaning leaves residual particles adhered with a surface of the substrate, and where the residual particles are hydrophilic; and if the surface of the substrate is hydrophobic, performing the functionalizing.Type: GrantFiled: April 3, 2008Date of Patent: October 8, 2013Assignee: Intermolecular, Inc.Inventor: Zachary Fresco
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Patent number: 8529707Abstract: Provided is a liquid processing apparatus in which a target substrate is horizontally held on a substrate holding unit and rotated around a vertical shaft, and the chemicals are supplied from a chemical supplying unit to the bottom surface of the target substrate that is rotating. In particular, the liquid processing apparatus performs a first step in which the chemicals are supplied to the target substrate while rotating the target substrate at a first rotation speed, a second step in which the supply of the chemicals is halted and the chemicals are thrown off by rotating the target substrate at a second rotation speed higher than the first rotation speed, and a third step in which the rinse liquid is supplied to the target substrate while rotating the target substrate at a third rotation speed equal to or lower than the first rotation speed.Type: GrantFiled: June 13, 2011Date of Patent: September 10, 2013Assignee: Tokyo Electron LimitedInventor: Hiromitsu Namba
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Patent number: 8486200Abstract: The present invention discloses a method of washing ware, in particular in an automatic domestic or institutional ware washing machine, using a detergent composition containing a cationic starch. This eliminates the need for a surfactant in the rinse step. The cationic starch provides a layer of cationic starch on the ware so as to afford a sheeting action in an aqueous rinse step without any added rinse agent.Type: GrantFiled: November 28, 2012Date of Patent: July 16, 2013Assignee: Diversey, Inc.Inventors: Antonius Maria Neplenbroek, Julie Jessica Beau, Florian Romain Marie Raphanel
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Patent number: 8470730Abstract: Disclosed is a method for producing a catalyst, in which physical properties of a dried material or a calcined material in a production process of the catalyst are stable and a change in at least one of a catalyst activity and a selectivity to a target product is small and hence reproducibility of the catalyst is excellent. The present invention is a method for producing a catalyst containing molybdenum, bismuth, and iron, which contains the steps of washing a surface of at least one device equipped in an apparatus for the production of catalyst, to which a solid matter adheres, with a basic solution, and producing the catalyst with the apparatus for the production of catalyst thus washed.Type: GrantFiled: July 5, 2006Date of Patent: June 25, 2013Assignee: Mitsubishi Rayon Co., Ltd.Inventors: Masahide Kondo, Masanori Nitta, Hiroyuki Naitou, Toru Kuroda, Seiichi Kawato
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Patent number: 8460474Abstract: A method of cleaning semiconductor wafers using an acid cleaner followed by an alkaline cleaner to clean contaminants from the materials is provided. The acid cleaner removes substantially all of the metal contaminants while the alkaline cleaner removes substantially all of the non-metal contaminants, such as organics and particulate material.Type: GrantFiled: January 13, 2010Date of Patent: June 11, 2013Assignee: Rohm and Haas Electronic Materials LLCInventors: Robert K. Barr, Raymond Chan, Matthew L. Moynihan
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Patent number: 8398781Abstract: A method of cleaning equipment such as heat exchangers, evaporators, tanks and other industrial equipment using clean-in-place procedures and a pre-treatment solution prior to the conventional CIP cleaning process. The pre-treatment step improves the degree of softening of the soil, and thus facilitates its removal. The pre-treatment solution can be a strong acidic solution, a strong alkaline solution, or comprise a penetrant. A preferred strong acidic solution is an acid peroxide solution. In some embodiments, the pre-treatment may include no strong alkali or acid ingredient; rather, the penetrant provides acceptable levels of pre-treatment.Type: GrantFiled: August 27, 2004Date of Patent: March 19, 2013Assignee: Ecolab USA Inc.Inventors: Brandon Leon Herdt, Peter J. Fernholz
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Patent number: 8343286Abstract: The present invention discloses a method of washing ware, in particular in an automatic domestic or institutional ware washing machine, using a detergent composition containing a cationic starch. This eliminates the need for a surfactant in the rinse step. The cationic starch provides a layer of cationic starch on the ware so as to afford a sheeting action in an aqueous rinse step without any added rinse agent.Type: GrantFiled: December 1, 2009Date of Patent: January 1, 2013Assignee: Diversey, Inc.Inventors: Antonius Maria Neplenbroek, Julie Jessica Beau, Florian Romain Marie Raphanel
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Publication number: 20120312332Abstract: A liquid processing apparatus 1 comprises a casing 5, a substrate holding mechanism 20 that holds a wafer (substrate to be processed) W, a process-liquid supplying mechanism 30 that supplies a process liquid, a draining cup 12 that receives a process liquid, and a draining pipe 13 that discharges a process liquid outside. The process-liquid supplying mechanism 30 includes a first chemical-liquid supply mechanism that supplies a hydrofluoric process liquid, and a drying-liquid supplying mechanism that supplies an organic solvent for drying a wafer W. A control part 50 causes the first chemical-liquid supplying mechanism to supply a hydrofluoric process liquid, and then causes the drying-liquid supplying mechanism to supply an organic solvent. In addition, before the control part 50 causes the drying-liquid supplying mechanism to supply an organic solvent, the control part causes a cleaning mechanism 10 to remove an alkaline component in a casing 5.Type: ApplicationFiled: August 22, 2012Publication date: December 13, 2012Applicant: TOKYO ELECTRON LIMITEDInventors: Teruomi MINAMI, Norihiro ITO, Yuji KAMIKAWA
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Publication number: 20120312331Abstract: This invention relates to a method of preprocessing a magnesium alloy for electroplating, including pickling the magnesium alloy with an ethyleneglycol-nitric acid solution.Type: ApplicationFiled: December 6, 2011Publication date: December 13, 2012Applicants: Pusan National University Industry-University Cooperation Foundation, HYUNDAI MOTOR COMPANYInventors: Hyung Sop Yoon, Won Sub Chung, Jung Hoon Lee
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Patent number: 8317993Abstract: A plating apparatus has a steam treatment chamber configured to perform a steam treatment using steam on a surface of a substrate, and a plating chamber configured to plate the surface of the substrate subjected to the steam treatment. The plating apparatus also has an acid treatment chamber configured to bring the surface of the substrate subjected to the steam treatment into contact with an acid liquid. The plating apparatus includes a frame housing the steam treatment chamber, the acid treatment chamber, and the plating chamber.Type: GrantFiled: August 18, 2009Date of Patent: November 27, 2012Assignee: Ebara CorporationInventors: Fumio Kuriyama, Rei Kiumi, Nobutoshi Saito, Takashi Takemura, Masaaki Kimura, Sachiko Takeda, Yugang Guo
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Patent number: 8298341Abstract: A method is used for removing a metal contaminant deposited on a quartz member selected from the group consisting of a reaction tube, wafer boat, and heat-insulating cylinder of a vertical heat processing apparatus for a semiconductor process. The method includes obtaining the quartz member unattached to the vertical heat processing apparatus; then, performing diluted hydrofluoric acid cleaning of cleaning the quartz member by use of diluted hydrofluoric acid; then, performing first purified water cleaning of cleaning the quartz member by use of purified water; then, performing hydrochloric acid cleaning of cleaning the quartz member by use of hydrochloric acid; and then, performing second purified water cleaning of cleaning the quartz member by use of purified water.Type: GrantFiled: April 28, 2009Date of Patent: October 30, 2012Assignee: Tokyo Electron LimitedInventors: Hitoshi Katoh, Tsuneyuki Okabe, Kohichi Orito, Takashi Chiba
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Patent number: 8277564Abstract: A method for removing a hardened photoresist from a semiconductor substrate. An example method for removing a hardened photoresist layer from a substrate comprising a low-? dielectric material preserving the characteristics of the low-?dielectric material includes: a)—providing a substrate comprising a hardened photoresist layer and a low-? dielectric material at least partially exposed; b)—forming C?C double bonds in the hardened photoresist by exposing the hardened photoresist to UV radiation having a wavelength between 200 nm and 300 nm in vacuum or in an inert atmosphere; c)—breaking the C?C double bonds formed in step b) by reacting the hardened photoresist with ozone (O3) or a mixture of ozone (O3) and oxygen (O2) thereby fragmenting the hardened photoresist; and d)—removing the fragmented photoresist obtained in step c) by wet processing with cleaning chemistries.Type: GrantFiled: September 17, 2009Date of Patent: October 2, 2012Assignee: IMECInventors: Quoc Toan Le, Els Kesters, Guy Vereecke
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Patent number: 8246758Abstract: The present invention relates to medium chain peroxycarboxylic acid compositions of neutral or alkaline pH, to methods of making these compositions, and to methods employing these compositions. The methods include methods of cleaning. The compositions include cleaning compositions.Type: GrantFiled: December 17, 2010Date of Patent: August 21, 2012Assignee: Ecolab USA Inc.Inventors: Victor F. Man, Gina M. Danielson, Nathan D. Peitersen, Mark R. Altier
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Publication number: 20120192901Abstract: The present invention discloses methods of neutralizing apatite surfaces, for example after a flow-through collection of a target and prior to cleaning the chromatography solid support.Type: ApplicationFiled: February 1, 2012Publication date: August 2, 2012Applicant: Bio-Rad Laboratories, Inc.Inventor: Larry J. Cummings