Abstract: Disclosed is a polyol/polyisocyanate adhesive system having an isocyanate component and a catalyzed component which form a heat-cured composition when admixed and heated above a threshold temperature. The catalyzed component has a hydroxyl-functional component catalyzed with a catalyst combination of a heat-activatable amine or amine-like catalyst which is activated at temperatures above the threshold temperature, and an activatable complexed metal catalyst comprising the reaction product of tin or bismuth catalysts, or a mixture thereof, and a molar excess of a mercapto compound complexing agent. The catalyst combination is effective to maintain the processibility of the system at ambient temperatures while promoting the rapid cure of the system when heated above the threshold temperature.

Abstract: A circuit component built-in module of the present invention includes an insulating substrate formed of a mixture comprising 70 wt % to 95 wt % of an inorganic filler and a thermosetting resin, a plurality of wiring patterns formed on at least a principal plane of the insulating substrate, a circuit component arranged in an internal portion of the insulating substrate and electrically connected to the wiring patterns, and an inner via formed in the insulating substrate for electrically connecting the plurality of wiring patterns. Thus, a highly reliable circuit component built-in module having high-density circuit components can be obtained.

Abstract: The mounting of semiconductor chips onto a flexible substrate takes place in three steps: Firstly, at a dispensing station, adhesive is applied to predetermined substrate sites on the substrate. Then, at a bonding station, semiconductor chips are placed onto the substrate sites. Finally, curing of the adhesive takes place. In accordance with the invention, the substrate is fixed onto a level support surface by means of vacuum during the hardening of the adhesive.

Abstract: A processes for adhering a vulcanized rubber to a vulcanized rubber or an unvulcanized rubber. Adhesion of vulcanized rubbers to each other is conducted by using at least one of the vulcanized rubbers before vulcanization thereof according to steps of: (1) laminating a sheet material which can easily be peeled from a surface of a rubber after vulcanization to a rough surface of the rubber before vulcanization, (2) vulcanizing a resultant laminate, (3) removing the sheet material from the vulcanized laminate immediately before adhesion of the vulcanized rubber in the laminate to another vulcanized rubber, and (4) adhering the vulcanized rubbers to each other according to a method of adhesion. The adhering of the vulcanized rubbers to each other is also conducted by using a rubber composition for adhesion inserted between the vulcanized rubbers without procedures using the sheet material.

Abstract: Resin compositions are provided which are used in combination with fibers to form self-adhesive prepreg sheets that are applied to core materials to form sandwich panels. The prepreg resin includes a thermoset resin, a curing agent and a viscosity control agent. The prepreg resin further includes certain thermoplastic particles which are used to control the flow characteristics of the prepreg resin and the formation of fillets during bonding of the prepreg to the core material.

Abstract: A semiconductor chip module uses a silicone adhesive between the semiconductor chip and a cap, said adhesive having sufficient bond strength to secure said cap to said chip without additional mechanical constraint while providing a direct thermally conductive path and permitting sufficient heat flow from said chip to said cap to maintain steady state operation of said semiconductor chip. The preferred silicone adhesive comprises a primerless, two-part polysiloxane-based adhesive made by reacting polydimethyl siloxane, an organosilicon compound, a polysiloxane, and a silane, in the presence of a catalyst.

Abstract: This invention relates to water-dispersible polyisocyanates obtained by reacting a) at least one bishydroxy-functional compound of the formula (I) HO—R1,—[O—CR2R3—O—R1]n—OH  (I)  wherein R1, R2, R3, and n are defined herein, with b) at least one polyisocyanate of the formula (II) Q[NCO]q  (II)  wherein Q and q are defined herein, and subsequently, in any order, with c) at least one monofunctional polyether alcohol of the formula (III) R4—[O—R5]m—O—H  (III)  wherein R4, R5, and m are defined herein, and optionally with d) at least one compound of the formula (IV) H—O—[R5—O]o—N+R6R7R8 X−  (IV)  wherein R5, R6, R7, R8, O, and X− are defined herein.

Abstract: Retroreflective sheeting includes a body layer having a structured surface with recessed faces forming cube corner cavities. A reflective film is disposed at least on the recessed faces, and a fill material fills the cube corner cavities. The fill material comprises radiation-curable materials, adhesives, or both, and preferably transparent radiation-curable pressure-sensitive adhesives. The fill material preferably forms a continuous layer covering both the recessed faces and upper portions of the structured surface. A transparent cover layer preferably contacts the fill material layer.

Abstract: A method for fabricating a stringer-stiffened shell structure using fiber composite materials involves the following steps. A fiber reinforced skin member having a specified surface curvature is laid onto a correspondingly curved mold surface of a shell mold. Stringer core blanks are cut from a cured plate of fiber composite material, whereby each blank has a narrow edge with a curvature matching the curvature of the skin member. These stiff pre-cut blanks are arranged extending along and vertically protruding from the skin member, with the narrow edges of the blanks lying in contact along the skin surface. An auxiliary frame is placed around the perimeter of the shell mold, and the ends of the stringer core blanks are received in slots in the frame to hold the blanks in proper positions.

Abstract: A method of manufacturing a bonded friction product, such as an automobile brake shoe, and apparatus therefor, includes forming a plastic inner lining element of uncured or green thermosetting resin binder containing friction modifiers and reinforcements and bonding the element to a shoe platform by way of an adhesive resin in a heat and pressure regime which cures the resin binder and adhesive. The need for a closed mold and/or venting stops is avoided by a stabilizing press (50) which includes a heated bed (53) between guide plates (56, 57) that has a recess (52) of less thickness than the lining element (16) to receive such lining element in its green state. The guide plates are spaced slightly further apart than the width of a shoe platform which is, having been preheated, brought down onto the lining element and pressed by a pneumatic ram (70), the loosely sliding shoe body (11) comprising a non-sealing closure member of the press.

Abstract: A vinyl graphic marking film or label coated with a pressure sensitive acrylic adhesive designed to achieve high or permanent adhesion to polymeric low energy surfaces is disclosed. In addition to good adhesion to low energy surfaces, the graphic marking film or label may have microperforated or micro-rough edges which initiate tearing when removal is attempted. The article maintains flexibility and film strength for easy fabrication in graphic marking film or label manufacture.

Abstract: A surface material is provided with a first adhesive layer formed by applying a first adhesive composed of a soluble self-digesting adhesive to an adhesive surface and a second adhesive layer formed by applying a second adhesive composed of a two-part synthetic resin contact adhesive to the upper surface of the first adhesive layer. A base material is provided with a base material adhesive layer formed by applying a second adhesive composed of a two-part synthetic resin contact adhesive to an adhesive surface, and having a composition of adhering the second adhesive layer of the surface material and the base material adhesive layer of the base material.

Abstract: Disclosed are a method for manufacturing a solid polymer electrolyte film/electrode composite, in which a porous electrode made from an electochemically active substance is used as an electrode and the pressure inside the porous electrode is reduced in order to fix the solid polymer electrolyte (SPE) film or pre-solid polymer electrolyte (pre-SPE) film to the porous electrode, a battery obtained by impregnating the electrode in the solid polymer electrolyte film/electrode composite with an electrolytic solution under reduced pressure and a method for producing such. The invention provides a thin, uniform film-shaped solid polymer electrolyte/electrode composite with ease. The battery fabricated with the composite is free of defects such as short, has high performance and, hence, is useful.

Abstract: A method of preparing a stain resistant and water repellant textile fabric comprising: a) treating a textile fabric with an aqueous primary treatment composition comprising at least about 5 weight percent of a fluorochemical textile treating agent, based on the weight of the primary treatment composition; b) drying the treated fabric at an elevated temperature to obtain a primarily treated fabric; c) providing a polymeric film on one side of the primarily treated fabric, the film comprising an aqueous secondary treatment composition comprising at least about 4 weight percent of a fluorochemical textile treating agent, based on the weight of the secondary treatment composition; and d) drying the treated fabric with the film at an elevated temperature to obtain a secondarily treated fabric.

Abstract: The present invention provides a room-temperature curable, reinforced thermosetting epoxy resin composition. The composition includes an epoxy resin first component, and an epoxy resin hardener second component. The epoxy resin component includes an epoxy resin, and may further include an inorganic and/or organic filler component, such as a structural reinforcement component. The epoxy resin hardener component includes an amine-based hardener, and may further include an inorganic and/or organic filler component. Cured reaction products of the composition demonstrate at about room temperature an adhesive strength of at least about 6500 psi, such as about 8000 to about 10000, and a fracture toughness of at least about 10 in-lbs/in2, such as about 20 to about 35 in-lbs/in2. In addition, the cured reaction products of the composition demonstrate a creep resistance at about room temperature at least about 6000 psi of at least about 1 hour.

Abstract: A description is given of a method of crosslinking radiation-crosslinkable pressure-sensitive adhesive films by controlled-dose exposure to actinic radiation, which involves exposing the film surface to a regular or irregular radiation pattern made up of regions of different intensity. The method permits a more precise adjustment of the adhesion—in particular, the adhesion of flexible films on a substrate.

Abstract: A synthetic wood material and method are disclosed, including providing a plurality of continuous glass fibers oriented substantially in the longitudinal axis and coated with a resorcinol modified phenolic resin binder substantially free from catalyst. In one aspect, the synthetic wood material is oxidatively treated to restore color. In one aspect, the fibers and binder are precoated with a furfuryl alcohol resin prior to the pultrusion step to form the synthetic wood.

Abstract: Adhesive coating film consisting of a) a radiation-cured coat which comprises from 40 to 90% by weight, preferably from 50 to 60% by weight, of urethane acrylate, from 0 to 20% by weight, preferably from 10 to 15% by weight, of polyether acrylate, from 10 to 50% by weight, preferably from 25 to 40% by weight, of reactive diluent, from 0 to 30% by weight of pigments from 0 to 10% by weight, preferably from 2 to 5% by weight, of a carboxy-functional (meth)acrylic esther [sic], from 0 to 10% by weight of other customary coatings fillers, and in the case of curing with UV radiation, from 0 to 10% by weight, preferably from 3 to 6% by weight, of photoinitiator, and b) which carries on one side an adhesive composition which has free NCO groups in the freshly applied adhesive composition, can be plastified thermally, especially under the intended processing conditions, and has a markedly weak surface tack.

Abstract: A batt of acoustical/thermal insulation for use in insulating appliances, compressors, machines and the like is disclosed. The batt comprises a fiberglass blanket and a release liner assembly. The liner assembly features a carrier sheet for supporting layers or coatings of adhesive on opposite broad surfaces thereof. One adhesive coated surface of the carrier sheet is releasably adhesively attached to a conventional release liner which is coated with an adhesive release agent. The other adhesively coated surface is joined to exposed fibers of a surface portion of the fiberglass blanket while the adhesive coating is in a heated, uncured, liquid state so as to immerse surface fibbers of the blanket in the adhesive. The carrier sheet adds stability to the resulting laminate structure and prevents surface fibers from being torn from the blanket when the release liner is removed from the carrier at the time of placement of the batt in service. A method for forming the batt is also disclosed.

Abstract: A method of attaching a flexible plastic film having electronic circuit traces to a rigid plastic substrate. The film and substrate are made from different incompatible plastic materials that do not bond to one another and have different CTE. The use of different or incompatible materials is useful where the properties of the backing structure and film are selected to achieve different results. For example, the flexible film may be selected from a material that provides a high melting point to withstand soldering while the backing material is selected from a low-cost and light weight plastic material that has a lower melting point. The film has conductive traces on at least one surface thereof and a backing surface. A heat activated adhesive is applied to the backing surface. The film is placed within an open injection mold and the mold is closed. A hot plastic resin is injected into the mold adjacent the adhesive.

Abstract: A process and apparatus are provided for preparing a release layer suitable for facilitating release of green ceramic laminates from a lamination fixture. The process comprises applying an electrostatic charge to at least one variably electrostatically chargeable portion of at least one lamination fixture and dispensing a layer of ceramic particulates, glass particulates or glass-ceramic particulates onto the charged portion of the lamination fixture to form a release layer on the lamination fixture. The apparatus provides a particulate dispenser for dispensing a layer of particulates of ceramic, glass, or ceramic-glass mixture, at least one lamination fixture having at least one variably electrostatically chargeable portion disposed in particulate receiving communication with the particulate dispenser; and a variable voltage electrostatic generator in electrical communication with the at least one chargeable portion of the lamination fixture.

Abstract: Novel liquid crystal polymer coatings and methods of applying the same. The liquid crystal polymers (LCPs) comprise high-melting point thermal plastics selected from the group consisting of co-polyesters, co-polyesteramides, or multiple monomer wholly aromatic polyesters. In the preferred embodiment, the LCPs may be chemically modified to provide greater hardness. The method of the present invention involves the thermal spraying of an LCP on the tooling used for curing composite structures.