With Measuring, Testing Or Inspecting Patents (Class 203/1)
  • Patent number: 5496447
    Abstract: A distilling apparatus for distillation of water, including a condensing chamber divided into an upper holding space for receiving water from a water source and a lower holding chamber for condensing steam into water, a heating chamber controlled to heat water from the upper holding space into steam and having a steam outlet connected to the lower holding space for guiding steam into the lower holding space for condensing, a hot water chamber, which receives condensed water from the lower holding space of the condensing chamber, and a cold water chamber, which receives distilled water from the hot water chamber and cools it down by an electronic cooler.
    Type: Grant
    Filed: March 10, 1995
    Date of Patent: March 5, 1996
    Inventor: Chin-Tu Wang
  • Patent number: 5492602
    Abstract: A distiller for producing potable water employs a metal boiler tray having a cover member in which there is an inlet for raw water and which together form a steam chamber having an outlet for steam. The boiler tray bottom has a plurality of steps including a highest, an intermediate and a lowest level step which are all covered with water at the beginning of a distillation cycle. The temperature of the highest level step is monitored with a sensor. A rise in the temperature of the highest level step by a predetermined amount above the boiling temperature of water indicates that the highest and intermediate level steps have become dry. This results in a signal to a controller to open a valve and admit replenishment raw water whose amount is dependent on valve open time. Steam evolved from the boiler tray is conducted through a first check valve in the cover member to demister chamber when the mist or carryover water in the steam impinges on a baffle and is separated from the steam as condensate.
    Type: Grant
    Filed: September 10, 1993
    Date of Patent: February 20, 1996
    Assignee: Emerson Electric Co.
    Inventors: Jonathan C. Vogelman, William F. Strutz
  • Patent number: 5484510
    Abstract: A water distillation apparatus and method include an improved control system for operation and maintenance, condensers with plastic to metal seals between a plastic condenser manifold and metallic cooling tubes, and a filter with steam bypass to allow for easy sterilization of the filter and remaining distillation system. The control system includes a three pronged probe assembly for monitoring conditions within an evaporation chamber. One of the three probes monitors steam conductivity and provides a steam fault signal to indicate an upper level of contaminants in the steam. A purge pump is responsive to fault signals, including the steam fault signal, to pump water from the evaporation chamber.
    Type: Grant
    Filed: October 26, 1993
    Date of Patent: January 16, 1996
    Assignee: Dew Enterprises, Inc.
    Inventors: Micheal O. Hartman, Dale J. Kinder, Randy E. Rainey, Arthur R. Helmich, Daniel E. Willis
  • Patent number: 5472576
    Abstract: A method for the production of an industrial diluent which includes the steps of heating a liquid waste from a facility that manufactures coatings, inks, lacquers, adhesives, or dyes in a mixer-reactor to generate a vapor, flowing the vapor into a distillation column, distilling the vapor to form distillation components, and transferring each component to a tank designated for such component. The method may include the additional steps of mixing at least two of the components in a predetermined amount, and thoroughly mixing the liquid waste during the heating step. The heating step is preferably effected by applying heat substantially uniformly to the liquid waste.
    Type: Grant
    Filed: May 7, 1992
    Date of Patent: December 5, 1995
    Inventor: Anwar E. Berberi
  • Patent number: 5466344
    Abstract: A pollution control apparatus (10) for controlling water-based liquid waste includes a vacuum distillation vessel (14) for separating water-based liquid waste into a distilled water component and a pumpable sludge component. A pH control system (12) allows the vacuum distillation vessel (14) to operate at maximum efficiency, and a purification system (22) allows the distilled water component to be purified to a level capable for reuse in chemistry, or else suitable for direct discharge into a municipal sewer. A microprocessor allows the apparatus (10) to operate automatically.
    Type: Grant
    Filed: April 11, 1994
    Date of Patent: November 14, 1995
    Assignee: Houston Fearless 76, Inc.
    Inventor: Paul A. Lindke
  • Patent number: 5464531
    Abstract: A water purification device mounted within a housing adapted to be positioned on an existing water cooler/dispenser has a valve control member extending from the base of the housing and is positionable within the water reservoir of the dispenser to control the release of purified water from the device to the reservoir. The device includes a feedwater tank into which supply water is fed and which feeds water to a water level control tank which communicates with the bottom of a boiler which is maintained at the same level as the water in the control tank. The control tank includes a control valve which maintains the water in it to a predetermined level above the level of the heating element in the boiler. The boiler is connected to condenser coils for condensing vaporized water from the boiler to form distilled water which is directed through a carbon filter to a distillate storage tank where the purified water is stored until required by the water cooler/dispenser.
    Type: Grant
    Filed: October 14, 1993
    Date of Patent: November 7, 1995
    Assignee: Market Design & Development, Inc.
    Inventor: Ralph G. Greene
  • Patent number: 5464504
    Abstract: In a distillation column, which for control purposes cannot tolerate the inherent dead time between analysis of consecutive samples in chromatograph analyzers, the chromatograph output is frequently corrected by inferring a dynamic correction based on the temperature change of a selected tray in the column. The dynamic correction applied to the distillation analyzer essentially eliminates the inherent dead time for obtaining a chromatograph analysis, and accordingly increased the rapidity of response of the column controls which rely on chromatograph analysis.
    Type: Grant
    Filed: December 2, 1993
    Date of Patent: November 7, 1995
    Assignee: Phillips Petroleum Company
    Inventor: Martin H. Beauford
  • Patent number: 5443695
    Abstract: The invention relates to an improved method and a novel apparatus for the concentration, separation, and purification of contaminated chemical compounds, wherein the chemical compound is less volatile than the contaminant. The distillation is performed using constant, predetermined distillation parameters.
    Type: Grant
    Filed: February 26, 1993
    Date of Patent: August 22, 1995
    Assignee: Athens Corporation
    Inventor: Wallace I. Yuan
  • Patent number: 5431779
    Abstract: An evaporator control method for a salt manufacturing plant includes the steps of: measuring the speed of sound of in a raw solution of salt which additionally includes magnesium chloride and calcium chloride accommodated in an evaporator; calculating the combined concentration of magnesium chloride and calcium chloride according to the speed of sound based on a calibration curve; and controlling a condition of the raw solution in the evaporator according to the combined concentration of magnesium chloride and calcium chloride.
    Type: Grant
    Filed: March 22, 1993
    Date of Patent: July 11, 1995
    Assignee: Japan Tobacco, Inc.
    Inventor: Norio Kawata
  • Patent number: 5368698
    Abstract: A water distillation apparatus includes a cylindrical housing with a first cover thereon, a pair of spaced apart funnel-shaped partitions, a second cover on the uppermost partition and a skirt extending downwardly from the periphery of the cover and the uppermost partition to a location above the bottom of the housing, the partitions and skirt dividing the interior of the housing into an inlet reservoir chamber for cold water above the first partition, a lower boiling chamber beneath the second partition and an inclined condensation passage between the partitions. Cold water is introduced through a pipe and solenoid valve into the bottom of the reservoir chamber for overflow through an opening in the second cover into the boiling chamber. A heater in the boiling chamber heats the water to produce steam which rises, passing into the condensation passage and flowing downwardly to a central drain for discharge into a distilled water reservoir beneath the housing.
    Type: Grant
    Filed: March 11, 1994
    Date of Patent: November 29, 1994
    Assignee: Big Iron Drilling Ltd.
    Inventors: George R. Field, Wallace B. Bolte, Norman N. Pepin
  • Patent number: 5352415
    Abstract: A novel control system is provided to control the liquid levels in a reactor-flasher combination used particularly for the carbonylation of methanol to acetic acid. Liquid level control is achieved by proportional controllers or other controllers which do not continuously seek zero off-set from the desired level and which proportionally change the liquid flow rates from the respective reactor and flasher. An adjustment can be made to the level controllers to change the liquid flow rates by a function generator which adjusts the flow rate, according to an empirically derived function which correlates changes in methanol feed rate to liquid flow rates from the reactor and flasher.
    Type: Grant
    Filed: September 29, 1993
    Date of Patent: October 4, 1994
    Assignee: Hoechst Celanese Corporation
    Inventor: Shinya Ochiai
  • Patent number: 5348622
    Abstract: This disclosure relates to an improved solar water purification system and process wherein the evaporating, condensing and distillate collecting chambers are located underground to assist in the evaporation and condensation process. The system includes three computer controlled preheaters which are constantly monitored to determine the temperature of the load therein. The cycling and recycling of the load relative to the load tank and the three preheaters is controlled by the computer for optimum system efficiency. One of the three preheaters is located underground, while a second preheater is located externally as a solar preheater and the third preheater is an outside gas, oil or waste heat fired preheater. In addition to producing pure water through the evaporation process, there is disclosed a system and process whereby various contaminants may be captured for further processing, storage and exploitation.
    Type: Grant
    Filed: September 14, 1993
    Date of Patent: September 20, 1994
    Inventors: David Deutsch, Thomas C. Flores
  • Patent number: 5348623
    Abstract: An automatic water heating and distilling apparatus is provided having a hot water reservoir, an evaporator tank, a condenser, a distilled water reservoir and a control mechanism. Water is boiled within the evaporator tank generating steam which is condensed in the condenser to form distilled water. The heat rejected during condensation is transferred into the hot water reservoir. The distilled water reservoir has an input coupled to the condenser, an output for distilled water, and an overflow so that excess distilled water is returned to the evaporator tank. The control mechanism automatically regulates the operation of a heater within the evaporator to maintain the water in the hot water reservoir within a selected operating range. Various alternative embodiments are also described including a hot water heating apparatus utilizing an enclosed heat transfer device partially filled with liquid having a boiling point above the selected temperature for the water to be heated.
    Type: Grant
    Filed: September 30, 1992
    Date of Patent: September 20, 1994
    Assignee: Terrill Designs, Inc.
    Inventor: Michael E. Salmon
  • Patent number: 5340444
    Abstract: A circulation cooler (10) has a heat exchanger (12) in a housing (11) that contains a cooling liquid and is detachably connected by its forward flow (13) to an inlet line (5), and by its return line (14) to the outlet (6) of a condenser (4) of a distillation apparatus (1). The circulation cooler (10) moreover has a vacuum pump (21) inside its housing (11) and an absorber (28) outside its housing (11). A second condenser (24) is interposed along the cooling agent inlet line (13) between the circulation cooler (10) and the condenser (4) of the distillation apparatus (1), and is connected to a vacuum line (27). The cooling liquid (25) flows successively to the heat exchanger ( 12) through the two condensers (24, 4) , then back to the heat exchanger (12). In both condensers, which are under a vacuum through common vacuum line (26, 27) , the condensation of the liquid substances is effected in the form of main condensation and aftercondensation phases.
    Type: Grant
    Filed: June 22, 1993
    Date of Patent: August 23, 1994
    Assignee: Peter W. D. van der Heijden Laborbedarf
    Inventor: Peter W. D. van der Heijden
  • Patent number: 5336376
    Abstract: In a distillation column with vaporous sidestream removal, the vaporous product removed is condensed in a condenser. The vapor pipe provided for the removal of product opens into a dip tank of which the upper end is connected to the condenser while its lower end is connected to a discharge pump. Inert gas present in the condensate is returned to the column above the sidestream removal through an inert gas pipe arranged at the upper end of the condenser.
    Type: Grant
    Filed: April 27, 1993
    Date of Patent: August 9, 1994
    Assignee: Bayer Aktiengesellschaft
    Inventors: Siegfried Taurat, Heinrich Steude, Ludwig Deibele, Heinz-Jurgen Alpers
  • Patent number: 5334291
    Abstract: An apparatus for removing non-volatile residues and impurities from a used solvent includes a self-scrubbing heating distillation subassembly for separating purified solvent for reuse and a controlled waste collector subassembly for overflowing concentrated residues and impurities stripped from the used solvent into an easy-to-service container. The apparatus may be disposed in a parallel in-line relationship with a circulating solvent flow circuit, such as in a dry cleaning operation, to continuously withdraw and purify aliquot portions of the circulating solvent stream, returning good solvent back to the flow circuit and concentrating non-volatile residues and impurities to a removable, environmentally sound serviceable container.
    Type: Grant
    Filed: July 9, 1993
    Date of Patent: August 2, 1994
    Assignee: Safety-Kleen Corp.
    Inventors: Gilbert Gavlin, William M. Langdon, deceased, Boris Goltsin, Gunther Erlebacher, Douglas A. Larson
  • Patent number: 5314587
    Abstract: A method and apparatus are disclosed wherein a standpipe mounted in an accumulator outside the operating zone of a distillation column is used in conjunction with a liquid level controller to measure condensate collected in the accumulator and to change the amount of energy provided to the distillation column in response to changes in the level of condensate collected in the accumulator.
    Type: Grant
    Filed: January 13, 1993
    Date of Patent: May 24, 1994
    Assignee: Union Carbide Chemicals & Plastics Technology Corporation
    Inventor: Gerald L. Smith
  • Patent number: 5308452
    Abstract: A waste photopolymer plate washout fluid solvent distillation apparatus includes a single enclosure enclosing a waste washout fluid container, a recovered solvent container, and a distillation unit in which waste washout is distilled by application of heat and vacuum pressure to the waste washout, and by supplying a metered supply of a surrogate solvent to the distilled waste washout as a desired solvent is distilled from the waste washout. The apparatus, by supplying the surrogate solvent to the waste washout as the desired solvent is distilled from the waste washout, enables a greater percentage of the desired solvent to be recovered from the waste washout than has been heretofore possible with prior art apparatus, and also enables the waste washout to be disposed of as a liquid.
    Type: Grant
    Filed: January 31, 1992
    Date of Patent: May 3, 1994
    Assignee: Progressive Recovery, Inc.
    Inventors: Daniel B. Marks, Donald G. Fluchel
  • Patent number: 5306397
    Abstract: The apparatus is located almost completely under the surface of the sea. The vacua in the de-aeration and the evaporation chambers are generated by a vacuum pump and are maintained by the effects of a pressure reduction device at the inlet for warm seawater and a lifting pump at the outlet for brine. The de-aerator and the evaporator are laid out as heat exchangers and penetrated by heating tubes, which are flowed through passively by warm seawater. The immersion tube forming the steam compartment which is suspended vertically in the sea serves as a condenser. The condenser is cooled passively by cold seawater. The attachment to the bottom of the sea is performed by a single point mooring construction via an anchor chain at an anchor weight. The elevation of the water production unit is controlled automatically by means of an air chamber and an air compressor.
    Type: Grant
    Filed: October 28, 1992
    Date of Patent: April 26, 1994
    Assignee: PI Praktische Informatik GmbH
    Inventor: Edgar Schmidt
  • Patent number: 5304286
    Abstract: To provide a balanced supply of distilled water and undistilled hot water for a household, a condenser coil communicates at one end with a steam generator located above a hot water heater and at its other end well the holding tank of a distilled water system, with a condenser entering the hot water heater near the bottom. The steam generator power input matches the power needed to meet the recovery rate to satisfy undistilled hot water demand under normal conditions. The condenser includes a plurality of loops grouped together so a line drawn from top to bottom through them is no longer than 5 inches. The length of the loops is at least 6 inches and the tubes have inside diameters between 1/4 inch and 5 inches and a total area of at least 25 square inches. Near the outlet of the condenser, the tube bends upwardly by approximately a diameter to create a water holding portion in the lower most loop of the condenser to restrain condensate and maximize heat transfer.
    Type: Grant
    Filed: November 1, 1989
    Date of Patent: April 19, 1994
    Inventor: David G. Palmer
  • Patent number: 5304287
    Abstract: A microdistillation method for the quantitative steam distillation of cyanide, phenolic compounds, hydrogen fluoride, ammonia, sulfites and other volatile analyte compounds from samples of environmental waters and sludge for their subsequent analysis involves volatilizing the water in the sample tube of a microdistillation column. The pressure which develops due to the water vapor forces all volatile compounds from the water sample, including the water itself, through a hydrophobic membrane and into the collector tube of the microdistillation column. The volatile compounds and the water vapor condense in the cooler collector tube and are quantitatively trapped and retained over the membrane. Relatively small samples may be distilled.
    Type: Grant
    Filed: February 7, 1991
    Date of Patent: April 19, 1994
    Assignee: Lachat Instruments
    Inventor: Scott Stieg
  • Patent number: 5296103
    Abstract: A method for the fractional distillation of a mixture of at least two compounds with different boiling points, a rising flow of vapor is brought into intimate contact with a descending flow of liquid obtained within a column (1) by the partial condensation of the flow of vapor itself by heat exchange with a cooled surface which extends through a filling (37).
    Type: Grant
    Filed: May 13, 1992
    Date of Patent: March 22, 1994
    Assignee: T.I.I. Tecnologie Industriali Innovative S.n.c. di Rosa Corigliano e.C.
    Inventor: Gianclaudio Masetto
  • Patent number: 5290402
    Abstract: An automatic cold/hot distilled water fountain which automatically performs water boiling, condensing, storing and heating processes to provide purified cold/hot drinking water, mainly composed of a distilling chamber, a condensing mechanism, a water reservoir and a heating box, whereby by the automatic control system designed for the water fountain, the water is controllably supplied into the distilling chamber and distilled therein and the distilled water is then collected and stored in the water reservoir to be directly discharged therefrom as a purified cold drinking water or further heated by the heating box to serve as hot drinking water. By the above arrangement, the amount of the water stored in the water fountain is properly kept within a predetermined range and what is most important is the safety and hygiene in water drinking is insured.
    Type: Grant
    Filed: May 10, 1993
    Date of Patent: March 1, 1994
    Inventor: Yao K. Tsai
  • Patent number: 5286350
    Abstract: A water distiller includes a raw water chamber for storing raw water, a main vaporization tank coupled with the raw water chamber for vaporizing raw water, a condensation device coupled with the main vaporization tank for condensing steam from the main vaporization tank, and a distilled water chamber communicated with the condensing conduit unit for accepting and storing distilled water. An auxiliary vaporization tank is communicated with the main vaporization tank and is mounted on the top end portion of the main vaporization tank. Each of the main and auxiliary vaporization tanks has a generally conical top wall which has a lower end portion that is provided with an annular water collecting groove formed in the inner surface thereof. Each of the water collecting grooves has a bottom wall which has a discharge opening formed therethrough.
    Type: Grant
    Filed: December 14, 1992
    Date of Patent: February 15, 1994
    Inventor: Shan-Meng Huang
  • Patent number: 5286351
    Abstract: A water distiller is provided which is used in conjunction with a hot water heater where normally wasted energy is used to preheat the hot water heater inlet. The distiller includes a heat storage tank, an evaporator tank having a water inlet, a heater and a steam outlet, and a first and second heat exchanger located within the heat storage tank. Steam generated in the evaporator tank passes through the first heat exchanger and condenses, forming distilled water. The heat rejected during condensation is absorbed within the heat storage tank. The second heat exchanger is used to preheat the water flowing to the hot water heater inlet by passing the water through the second heat exchanger on an as needed basis where it absorbs heat from the heat storage tank.
    Type: Grant
    Filed: May 15, 1991
    Date of Patent: February 15, 1994
    Assignee: Terrill Designs, Inc.
    Inventor: Michael E. Salmon
  • Patent number: 5281309
    Abstract: A water purification device mounted within a housing adapted to be positioned on an existing water cooler/dispenser has a valve control member extending from the base of the housing and is positionable within the water reservoir of the dispenser to control the release of purified water from the device to the reservoir. The device includes a feedwater tank into which supply water is fed, either automatically, or manually. The feedwater tank, when the water is above a minimal level, feeds water to an anti-backflow control housing which communicates the water from the feedwater tank to the bottom of a boiler which is maintained at the same level as the water in the feedwater tank without the use of a float within the boiler. The anti-backflow housing includes a check valve in the form of a ball that prevents the backflow of heated water from the boiler into the feedwater tank.
    Type: Grant
    Filed: June 23, 1992
    Date of Patent: January 25, 1994
    Assignee: Market Design & Development, Inc.
    Inventor: Ralph G. Greene
  • Patent number: 5277759
    Abstract: To decrease the sulfur emissions of a sulfate cellulose mill, black liquor is heated before the last effect of the evaporation at a temperature higher than the cooking temperature of the sulfate cook and the sulfidity of white liquor is adjusted by adjusting the temperature and/or retention time of the heat treatment so that a predetermined amount of sulfur compounds are separated from the gaseous black liquor. Preferably, the sulfur containing gas is thereafter divided into different fractions and separately combusted.
    Type: Grant
    Filed: November 16, 1990
    Date of Patent: January 11, 1994
    Assignee: A. Ahlstrom Corporation
    Inventor: Krister Sannholm
  • Patent number: 5273719
    Abstract: A liquid evaporator includes an air-tight outer container containing liquid therein, the liquid container having support legs adjacent the bottom surface thereof; an inner container mounted on the legs for partitioning the interior space of the outer container, the inner container having a wall made of insulating material; and a heater fixed to an upper portion of the outer container and positioned inside the inner container. The liquid evaporator may be combined with a deodorizing device for forming a urine treating device, wherein the urine treating device includes a deodorizing housing having an upper portion provided with a secondary heater therein, a catalyst surrounding the secondary heater, a blower provided outside the housing, and a diffusion pipe provided at the upper portion of the housing.
    Type: Grant
    Filed: June 22, 1992
    Date of Patent: December 28, 1993
    Assignee: Japanic Corporation
    Inventors: Mitsuhiro Kishi, Toyohiko Sunaoka
  • Patent number: 5271810
    Abstract: A distillation device for separating a liquid mixture from contaminants contained therein. The device partially cools, using an air radiator or equivalent passive heat-exchange device, a fluid of that contains at least one component of the mixture to be separated; the temperature of the fluid does not fall the ambient air temperature, thus preventing condensation on the heat exchanger. The partially cooled fluid is introduced into an aspirator and combined therein with a gaseous stream produced by heating the mixture to boiling in a separate chamber. Because of the high surface area of contact between vapor and aspirated liquid, the heat transfer is completely effective to condense the gaseous mixture, which settles into a pool. The components can then be separated mechanically or by gravity.
    Type: Grant
    Filed: June 19, 1992
    Date of Patent: December 21, 1993
    Assignee: Environmental Solvents Corporation
    Inventors: Gene E. Keyser, Robert L. Klopfenstein
  • Patent number: 5262013
    Abstract: A coolant recycling apparatus has a boiler and condenser for distilling a glycol and water from a used coolant. The glycol and water are recombined in a mixing tank to form a mixture having a desired ratio of water to glycol, and an inhibitor is added to the mixture to obtain a fresh coolant mixture ready for use in an engine cooling system. Contaminants in the used coolant are concentrated to form a sludge.
    Type: Grant
    Filed: July 17, 1991
    Date of Patent: November 16, 1993
    Assignee: Amalgamated Technologies, Inc.
    Inventors: Roy E. Beal, Scott A. McCracken
  • Patent number: 5260865
    Abstract: In a fractional distillation process which performs a binary or limited multicomponent separation, and in which it is desired to maintain composition set points for dual product streams, a computer is programmed for applying model based control. Multivariable, noninteracting control of the distillation process is achieved by utilizing a nonlinear model, which calculates process vapor and distillate flow rates required to maintain product set points. The model, which applies tray-to-tray calculation essentially derived from a McCabe-Thiele analysis, is periodically updated by adjusting tray efficiency based on steady state composition measurements to keep the model in pace with changing process conditions.
    Type: Grant
    Filed: April 1, 1991
    Date of Patent: November 9, 1993
    Inventors: Martin H. Beauford, Jackie C. Watts, James B. Riggs
  • Patent number: 5259931
    Abstract: A system for removing volatile constituents (e.g., hydrocarbons) from a liquid (e.g., water) containing the same by which there is a continuous countercurrent contact between the liquid and a forced air flow. Water collected in a reservoir is continuously pumped to the top of a stripping tower where it is dispersed downwardly over packing material. A blower forces air upwardly in the tower so as to remove the volatile constituents that exit the tower with the exit air. Since the water flow is continuous, multiple passes occur through the tower to enhance separation efficiency. Water from the base of the tower returns to the reservoir via overflow from a standpipe. A lower liquid level sensor in the reservoir initiates operation of the water pump to the tower, and an upper liquid level sensor initiates operations of another pump for pressure discharge from the base of the tower to an exterior site.
    Type: Grant
    Filed: February 3, 1992
    Date of Patent: November 9, 1993
    Inventor: James R. Fox
  • Patent number: 5248393
    Abstract: A compact solvent reprocessing system for use in a limited physical area. Solvents to be reprocessed is contacted by deionized water in a water wash column and delivered to a distillation column where waste solvent is separated from materials that boil at a higher temperature than the waste solvent. Distilled solvent is delivered to a drying column and final filters for removal of any other foreign materials. The modular solvent reprocessing system to reclaim/recycle high purity solvents on-site at a manufacturing facility. A system includes a pumpless pressurized tank solvent transfer units, storage tanks, liquid-liquid extraction column, distillation columns, submicron filtration units, and water and acid adsorption columns arranged as necessary to produce ultra-high purity solvents from waste solvent streams. The systems are packaged in modular assemblies with secondary containment to meet U.S. EPA requirements.
    Type: Grant
    Filed: January 31, 1990
    Date of Patent: September 28, 1993
    Assignee: S&K Products International, Inc.
    Inventors: J. Randolph Schumacher, Gregory E. Carr, Martin J. Striefler
  • Patent number: 5242548
    Abstract: An improved distillation device (1) which uses a combination of centrifugal and positive displacement pumps to purify raw liquid in an area of limited space. The device (1) includes evaporation assembly (2) having a boiling chamber (5), a valve and float switches (15, 16, 17) for maintaining the liquid level (20) in the boiling chamber (5) at a predetermined level, and connecting conduit (21) for directing vapor to a condensation apparatus (3). The condensation assembly (3) includes a condensation chamber (6), a collection chamber (7), and at least one bubble tube (22) connecting the two chambers (6, 7). Leading from the collection chamber (7) is first transfer conduit (50), a tube (51) for permitting vapor to bleed from the collection chamber (7) back to condensation chamber (6), and second transfer conduit (52) for returning only distillate from collection chamber (7) to condensation chamber (6) to cool condensation chamber (6).
    Type: Grant
    Filed: January 4, 1993
    Date of Patent: September 7, 1993
    Inventor: Philip G. Youngner
  • Patent number: 5240560
    Abstract: A wastewater evaporator system is provided for evaporating wastewater at a rate of about seven gallons per hour. Such system includes a heater, a blower, a plurality of honeycombed plates, a drive element including an electric motor, and a tank. Such system improves the environment and allows safe, reliable, and economical disposal of wastewater.
    Type: Grant
    Filed: July 19, 1991
    Date of Patent: August 31, 1993
    Inventor: Marshall W. Gregory
  • Patent number: 5236555
    Abstract: The invention relates to a distillation method and an apparatus for the concentration and purification of water-containing liquid chemicals. The distillation is performed using constant, predetermined distillation parameters.
    Type: Grant
    Filed: October 24, 1991
    Date of Patent: August 17, 1993
    Assignee: Athens Corp.
    Inventor: Wallace I. Yuan
  • Patent number: 5225048
    Abstract: The invention relates to a distillation method and an apparatus for the concentration and purification of water-containing liquid chemicals. The distillation is performed using constant, predetermined distillation parameters.
    Type: Grant
    Filed: January 29, 1991
    Date of Patent: July 6, 1993
    Assignee: Athens Corp.
    Inventor: Wallace I. Yuan
  • Patent number: 5221441
    Abstract: A method and apparatus for conducting a catalytic distillation process is provided which allows for maintaining a liquid level in selected portions of the catalyst bed. Three particular processes disclosed are the production of methyl tertiary butyl ether, tertiary butyl alcohol and cumene.
    Type: Grant
    Filed: October 4, 1991
    Date of Patent: June 22, 1993
    Assignee: Chemical Research & Licensing Company
    Inventor: Lawrence A. Smith, Jr.
  • Patent number: 5217581
    Abstract: A distillation system where a saline fluid (10) is pumped into a pressure vessel (14), through a counterflow heat exchanger (16) and heated to boiling. A salt free distillate (20) is separated from the saline fluid (10). The concentrate valve (24) and the distillate valve (26) restrict egress flow. The concentrate valve (24), the distillate valve (26) and the heater (18) are controlled by a computer control system (32) to attain and maintain a desired value of the Ewing Number. The Ewing Number is a dimensionless measure of performance defined as the heat of vaporization of the distillate (20) at standard atmospheric conditions times the distillate (20) mass flow divided by the system power input.
    Type: Grant
    Filed: August 5, 1992
    Date of Patent: June 8, 1993
    Inventor: Frank A. Ewing
  • Patent number: 5207869
    Abstract: A liquid waste reduction system uses an evaporator having two packed columns. A reservoir of the evaporator has three level sensor which monitor the fluid level in the reservoir. An input pump delivers waste liquid to the reservoir. When the fluid level has exceeded a low level, a control unit powers an output pump which pumps liquid from the base of the reservoir to an external storage unit. A distributor pump pumps liquid from the reservoir to the top of the packed columns. A blower forces air upward through the packing material to evaporate water from the liquid. When the fluid level has exceeded a high level, the control unit switches on a heating element which heats the air delivered from the blower to the second packed column, thus accelerating the evaporation process. When the fluid level has exceeded the maximum level, the control unit deactivates the input pump to prevent flooding of the evaporator unit.
    Type: Grant
    Filed: February 20, 1991
    Date of Patent: May 4, 1993
    Assignee: Clivus Multrum, Inc.
    Inventors: H. David Harmoning, Guy Marchesseault
  • Patent number: 5205909
    Abstract: A method and apparatus are disclosed wherein a standpipe mounted in an accumulator outside the operating zone of a distillation column is used in conjunction with a liquid level controller to measure condensate collected in the accumulator and to change the amount of energy provided to the distillation column in response to changes in the level of condensate collected in the accumulator.
    Type: Grant
    Filed: December 4, 1991
    Date of Patent: April 27, 1993
    Assignee: Union Carbide Chemicals & Plastics Technology Corporation
    Inventor: Gerald L. Smith
  • Patent number: 5203969
    Abstract: A method of separating and recovering components of a mixture having a gap in the range of miscibility and having organic compounds and water in a pervaporization process with the aid of membranes. The mixture is first separated into an organically loaded water phase and a water-saturated organic phase. Subsequently, the organically loaded water phase and the water-saturated organic phase are separately subjected to parallel, different pervaporization processes, resulting in retentates as water on the one hand and organic liquid on the other hand. The permeates that result during the pervaporization processes are subsequently returned to the mixture that is to be separated.
    Type: Grant
    Filed: October 7, 1991
    Date of Patent: April 20, 1993
    Assignee: GKSS-Forschungszentrum Geesthacht GmbH
    Inventors: Axel Wenzlaff, Dieter Behling, Karl W. Boddeker
  • Patent number: 5188710
    Abstract: A continuous water distillation system has a steam chamber assembly and a condenser assembly for making steam and condensing the steam into purified water. An associated holding tank collects the purified water for dispensing upon user demand. The quantity of purified water is continuously sensed in the holding tank. A controller coordinates the operation of the steam chamber assembly and the purified water delivery mechanism to dispense purified water from the holding tank upon demand and automatically make and replenish the supply of purified water. In one arrangement, a first sensor continuously senses the purity of the water collected in the holding tank, while a second sensor continuously senses the purity of the water entering the steam chamber assembly. In another arrangement, the condenser assembly includes a cooling fan with a replaceable air filter, and the purified water dispenser includes an inline water filter.
    Type: Grant
    Filed: January 18, 1991
    Date of Patent: February 23, 1993
    Assignee: Emerson Electric Co.
    Inventors: Thomas J. Weber, Dale L. Garrison, Richard E. Forrest, William F. Strutz
  • Patent number: 5178734
    Abstract: A water distilling apparatus (10) which includes vertically stacked components, i.e. an uppermost water storage tank (12), an intermediate boiling tank (14) and a lowermost condensing unit (16). Stacking of the distiller components creates a space efficient design with ready access to the respective components. The preferred apparatus (10) is also equipped with a small, dedicated water conditioning unit (20) situated between the main solenoid water valve (94) and the inlet of the boiling tank (14).
    Type: Grant
    Filed: February 16, 1990
    Date of Patent: January 12, 1993
    Assignee: International Water Technologies, Inc.
    Inventor: David G. Palmer
  • Patent number: 5174864
    Abstract: Controlled heating unit for extracting solvent from sludge by distillation, in particular for dry-cleaning machines, having a sludge tank with a flattened shape which is arranged at the base of a sealed box-like chamber and above which inlets for microwaves generated by a microwave source are present, a mixer for the sludge to be treated, at least one sludge temperature sensor which switches off the microwave source when the sludge reaches a temperature which is proximate to the degradation temperature of the solvent.
    Type: Grant
    Filed: October 16, 1990
    Date of Patent: December 29, 1992
    Assignee: Sodibo S.p.A.
    Inventors: Tommaso Arbizzani, Gualtiero Ghelardini
  • Patent number: 5160580
    Abstract: An evaporating process that alternate between different modes of operation, according to the characteristics of the product handled; the product is either force fed into the tube nest, or cascaded through it in a free-falling film.
    Type: Grant
    Filed: January 3, 1990
    Date of Patent: November 3, 1992
    Assignee: Fenco S.p.A.
    Inventor: Carlo Sassi
  • Patent number: 5156706
    Abstract: A vertical tube evaporation process for the concentration of saline water and other liquids, including the addition of an anionic mono-molecular dispersant thereto which interacts with materials precipitated during concentration and inhibits the formation of scale or fouling depositions on evaporator surfaces, and wherein the additive is incorporated into the precipitated materials and improves their removal during the descaling or defouling of evaporator surfaces by rendering such precipitates redispersable in fresh water or in a non-saturated liquid used for descaling or defouling of evaporator surfaces.
    Type: Grant
    Filed: April 29, 1988
    Date of Patent: October 20, 1992
    Inventor: Hugo H. Sephton
  • Patent number: 5139620
    Abstract: Evaporation of saline water in a desalinization process, or evaporation of other types of liquid such as black liquor from paper pulp processing, is accomplished utilizing a multiple effect evaporator. Each effect includes one or more (e.g. first and second) sets of horizontally elongated dimpled plate evaporator elements. Horizontally flowing heating fluid, such as steam, is introduced to the internal passage of at least the second set in all the effects, and a head of circulation liquid is provided to cause liquid being evaporated to flow downwardly from the head over the external surfaces of the sets of dimpled plates in a thin film. The vapor evaporated is drawn through a demistor and is used as the heating fluid for the next effect. Recirculating liquid that has not evaporated and liquid separated by the demisting process are recirculated to the head associated with each effect. Clean condensate--such as distilled water--is withdrawn from the last effect.
    Type: Grant
    Filed: August 13, 1990
    Date of Patent: August 18, 1992
    Assignee: Kamyr, Inc.
    Inventors: Carl E. Elmore, Kyle Infante
  • Patent number: 5122234
    Abstract: This invention is a continuous process for preparing phenol having improved clarity when dispersed in water. The phenol is prepared from crude phenol being the product of decomposition of cumene hydroperoxide and having previously been distilled to remove large portions of acetone, cumene and alphamethyl styrene.
    Type: Grant
    Filed: February 4, 1991
    Date of Patent: June 16, 1992
    Assignee: Allied-Signal Inc.
    Inventors: Saul L. Elishewitz, Clifford M. Gilpin, III, Gerald E. Hollenbach, John J. Santarsiero, II, William J. Moffatt, David B. Lebowitz, Dodd S. Smith, Larry B. Wolf
  • Patent number: 5120403
    Abstract: A method and apparatus for conducting a catalytic distillation process is provided which allows for maintaining a liquid level in selected portions of the catalyst bed. Three particular processes disclosed are the production of methyl tertiary butyl ether, tertiary butyl alcohol and cumene.
    Type: Grant
    Filed: April 8, 1991
    Date of Patent: June 9, 1992
    Assignee: Chemical Research & Licensing Company
    Inventor: Lawrence A. Smith, Jr.