Abstract: A low profile water distiller has a housing. A steam chamber is located within the housing having a horizontal dimension greater than its vertical height. A condenser is also located within the housing having a horizontal dimension greater than its vertical height. The vertical height of the condenser is generally the same as the vertical height of the steam chamber. A raw water conduit extends in a generally horizontal plane within the housing for delivering water to be distilled into the steam chamber. A steam conduit also extends within the housing for delivering steam from the steam chamber to the condenser. The steam conduit extends in a generally horizontal plane parallel to the generally horizontal plane of the raw water conduit. An air circulation channel within the housing draws cooling air through the condenser in a generally horizontal path parallel to the generally horizontal planes of the raw water conduit and the steam conduit.

Abstract: A water distiller has a steam chamber that includes a tray for containing water to be distilled. Water is conveyed from a source to the tray for distillation. A valve operates in an open position to convey water to the tray and a closed position to block the passage of water to the tray. A heating element means extends in the steam chamber for submersion in the water carried by the tray. The heating element is operable within a range of temperatures to heat the water in the tray. The heating element includes a main body portion having an axis that extends in a plane generally parallel to the water in the tray and a section havign an axis that is deflected above the axis of the main body portion. A heat sink surrounds the deflected section of the heating element means. A heat sensor detects the temperature of the heat sink. A control connects the valve and the heat sensor means. The control closes the valve when the sensed temperature of the heat sink is equal to or less than a predetermined amount.

Abstract: A method of preparing a column for a reaction with distillation process utilizing a solid particulate catalyst includes the steps of providing a plurality of vertically spaced apart distillation devices, coupling these devices with a plurality of vertically extending horizontally spaced catalyst enclosing containers, extending at least some of the containers through at least two successive distillation devices, then loading a particulate catalyst into the containers to form a catalyst bed whereby distillation and catalytic reaction may occur simultaneously in the column. The method also encompasses a process for concurrent catalytic reaction with distillation which includes the foregoing steps as well as the steps of feeding a liquid stream to the column reactor and onto the distillation devices while a vapor stream moves vertically up through the distillation devices while products of reaction and distillation are withdrawn from the reactor.

Abstract: A method of separating and recovering components of a mixture having a gap in the range of miscibility and including organic compounds and water in a pervaporization process with the aid of membranes. The mixture is first separated into an organically loaded water phase and a water-saturated organic phase. Subsequently, the organically loaded water phase and the water-saturated organic phase are separately subjected to parallel, different pervaporization processes, resulting in retentates as water on the one hand and organic liquid on the other hand. The permeates that result during the pervaporization processes are subsequently returned to the mixture that is to be separated.

Abstract: A system for on-site recovery of reusable industrial waste components, such as solvents, from a liquid waste stream includes a trailer that is internally partitioned to separate system components through which the waste stream passes in a first partitioned section of the trailer from support and control components in the second trailer section. Input waste is fed into a horizontal thin-film evaporator within the first trailer section, while steam is fed in a closed loop through the evaporator from the second section of the trailer for evaporating volatile solvents in the waste stream, and thereby separating the volatile solvents from non-volatile liquid and solid components of the waste stream. The evaporated volatile solvents are fed to a heat exchanger, again enclosed within the first partitioned section of the trailer, for recondensation through heat exchange with a coolant fed to the heat exchanger in a closed loop from the second trailer section.

Abstract: A vacuum drying method wherein a solution of a material to be dried which has been adjusted to 1-50 centipoise, is supplied to a steam-heated long tube, solid-vapor mixture of powdery dry material and vapor produced in the tube is blown out under reduced pressure, and the powdery dry material and vapor are separated so as to obtain powdery dry material.

Abstract: Azeotropes of HF and 2,2-dichloro-1,1,1-trifluoroethane and of HF and 2-chloro-1,1,1,2-tetrafluoroethane. Process for the separation of hydrogen fluoride (HF), 2,2-dichloro-1,1,1-trifluoroethane (FC-123), and/or 2-chloro-1,1,1,2-tetrafluoroethane (FC-124) from mixtures containing them by controlling the molar ratio of HF/FC-123 in the mixture prior to subjecting the mixture to azeotropic distillation.

Abstract: A spray dryer device for spray drying a sample dissolved in an organic solvent is disclosed, comprising a circulation line in which an inert gas is circulated by a blower, a heater for heating the inert gas to a specified temperature, a main drying chamber provided with a spray nozzle through which the sample dissolved in the organic solvent is sprayed into the inert gas, a collector in which the powdered sample produced in the main drying chamber is collected, and a condenser in which the gaseous organic solvent is condensed and recovered. The powdered sample is obtained in this spray dryer device for spray drying organic solvents by spraying the organic solvent through the spray nozzle into the main drying chamber in which the oxygen concentration is held to a low value by the introduction of the inert gas.

Abstract: An improved method of and apparatus rendering water-based fluid waste stream evaporation operations environmentally and otherwise safe, involving separately and independently existing the hot gas stream produced by fuel combustion and the vaporized fluid-air exhaust stream resulting from heat-vaporizing of the fluid, independently directing the streams in opposite directions toward one another and to a common region, and applying fan suction immediately at said region to exert the sole control of withdrawing the streams simultaneously.

Abstract: A low-pressure desalinization in a water chamber having an open end submerged in a water supply such as an ocean. An air exhaust pump draws air out of the water chamber to lower the surface tension of an upper stratum of water, which is thereby converted to vapor and subsequently condensed to nonsalinated water and collected in a U-shaped trap with a pair of sealing, closable valve. Although specifically designed for desalinization purposes, the apparatus may be used for distilling non-potable fresh water to potable fresh water. The system may also be used to de-water sludge in paper producing plants and also in the diary industry and other projects where large amounts of water need to be drawn off. The system would be appropriate in municipal water systems also as an odor controlling entity, in milk concentrate, maple syrup operations or cheese factories. Moreover, a velocity enhancing parabolic channel is disclosed for efficiently utilizing the potential energy of the fresh water.

Abstract: The disclosure relates to a solar-operated apparatus to purify and/or desalinate water. Several embodiments are disclosed, each of which substantially derives its source of heat from solar energy. The apparatus includes a unique design of the evaporating collector dome which is provided with a smooth interior surface to permit collection of increased amounts of distillate. The apparatus exterior is provided with a black surface to serve as a black body and so absorb increased amounts of the sun's energy. Additionally, that same exterior is coated with a film of infra-red absorbing material (STET) to further increase solar-energy absorption. To further improve the system's efficiency, various external tubing designs are utilized to preheat the load prior to its entry into the evaporating chamber. The distillate-collecting vessel is a downwardly-extending dome. This increases the volume while at the same time reducing re-evaporation by minimizing the exposed surface area.

Abstract: A method and apparatus for automatically and sequentially distilling batches of water having substantially equal volumes in a plurality of distillation cycles, one batch in each cycle. During each cycle, water is admitted to a boiler tank for a fixed interval of time to form a batch in the tank. The batch of water in the tank is then vigorously boiled while venting the tank through a pipe to the atmosphere. The vigorous boiling is terminated when the temperature within the vent pipe reaches the boiling point of pure water. Upon termination of the vigorous boiling phase, a gentle boiling phase is initiated, the vent pipe is closed, and vapor in the tank is admitted to a condenser. The condenser condenses the vapor to obtain distilled water which is collected in a collection device. The gentle boiling phase continues until the level of water in the tank recedes to the level of a heater in the tank.

Abstract: An apparatus for feeding gas into a heated saline solution for pressure measurement or to pump this solution. The gas is introduced into the solution through a gas bubbling-in pipe having a gas outlet opening. The gas is heated prior to being introduced into the solution and is charged with moisture until the saturation of the gas comes close to or corresponds to the saturation conditions in the solution at the gas outlet opening. This minimizes clogging by crystallization at the feeder pipes carrying the measuring or purge gas.

Abstract: The column for distillation of charge products which form a heavier liquid phase and a lighter liquid phase and connected sump circulating boiler are provided with a liquid impermeable collecting bottom plate located in a lower part of the column. The bottom plate has a discharge passage and the column is provided with a liquid withdrawal outlet arranged closely underneath the collecting bottom plate but above the lower end of the discharge passage so that the heavier phase can be prevented from reaching the liquid withdrawal outlet by gravity. One pipe connects the sump circulating boiler with the liquid withdrawal outlet to provide a free flow of liquid from the column to the sump circulating boiler for heating and another pipe connects the column with the sump circulating boiler above the collecting bottom plate so that the reheated liquid can flow from the sump circulating boiler to the column without a circulating pump.

Abstract: A microdistillation column for the quantitative steam distillation of cyanide, phenolic compounds, hydrogen fluoride, ammonia, sulfites and other volatile analyte compounds from samples of environmental waters and sludge for their subsequent analysis involves volatilizing the water in the sample tube of the microdistillation column. The pressure which develops due to the water vapor forces all volatile compounds from the water sample, including the water itself, through a hydrophobic membrane and into the collector tube of the microdistillation column. The volatile compounds and the water vapor condense in the cooler collector tube and are quantitatively trapped and retained over the membrane. Relatively small samples may be distilled in the column.

Abstract: A control for a water distillation apparatus admits untreated feed water to the boiling tank in response to a demand for the production of distilled water and operates the heater to produce steam. Level probes in the boiling tank monitors the level of untreated water in the boiling tank and admits more feed water as necessary. When demand for production of distilled water has ceased, the heater is deenergized and the boiling tank is filled to dilute the residual water in the tank and lower its temperature prior to drainage to prevent damage to a plastic house drain. In a preferred embodiment, feed water is admitted to the boiling tank in large batches and the production of distilled water continues uninterrupted until the entire batch is distilled to conserve heat energy even if demand ceases during such batch distillation. A cleaning mode is provided to remove scale from the interior of the boiling tank with a simplified manual cleaning procedure.

Abstract: A method of treating photographic process waste liquor through concentration by evaporation, including heating an upper part of photographic process waste liquor to concentrate by evaporation the photographic process waste liquor in such a manner that the difference between the temperature of the photographic process waste liquor in the vicinity of the heated part and the temperature at a bottom part of the photographic process waste liquor may become 5.degree. C. or more, and causing a solute in the photographic process waste liquor to settle.

Abstract: A method for treating photographic process waste liquor by evaporation to concentrat the waste liquor. The method includes evaporating with a heating device which has a heat density of about 17.2 kcal/cm.sup.2 or less; and intermittently feeding the waste liquor to maintain a predetermined liquid level in the vessel. By controlling the heating and/or the liquid level in the evaporation vessel, odors are controlled while efficiency is maintained.

Abstract: A distillation type of water purification system has a raw water inlet valve for admitting raw water continuously to a boiling tank at a rate greater than the rate at which raw water is converted to treated water. A drain valve located at the bottom of the boiling tank is energized by a raw water level sensing means whenever the raw water level reaches a predetermined level, to discharge water from the boiling tank. Treated water is stored in a storage tank having a pump for discharging treated water to the user upon demand. A single conductivity sensor in the storage tank controls the pump to allow it to operate only if the sensed conductivity is above a first predetermined value but not at or above a second predetermined value greater than the first value. An improved condenser has two sets of tubes, each set is arranged in a pair of planes oriented transverse the flow of cooling air with the tubes parallel. The internal cross-sectional area of one set is about twice that of the other.

Abstract: A water distillation apparatus has an outer chamber and an inner chamber suspended within the outer chamber by support arms. The inner chamber suspends a heating element to create steam. Heat is transferred from the inner chamber to the outer chamber, wherein the heated water in the outer chamber is allowed to degassify. Degassification removes unpleasant tasting chemicals from the water before distillation. Openings are provided for air circulation to remove the gasses. A condenser is also suspended by the support arms. The stem exits the inner chamber and goes into the condenser. A fan provides air circulation through the condenser. The outer chamber is not penetrated by any openings, thereby precluding the possibility of any leaks. The support arms bear on the outer chamber walls; the inner chamber is removed from the outer chamber for cleaning simply by lifting up. In one embodiment the outer and inner chambers are made of a ceramic material to better regulate heat transfer.

Abstract: A distillation apparatus including a pair of vertical lower vessels each open at its upper end, and a pair of elongate upper vessels each having an open lower end, slidably mounted in a respective one of the lower vessels. A heat exchanger is mounted in each of the upper vessels, with the upper end of one upper vessel being connected to the inlet of the heat exchanger in the other vessel, and vice versa. A reciprocating drive mechanism drives the two upper vessels up and down in opposite directions so as to simultaneously effect compression in the space above the liquid level in the downwardly moving vessel while expanding the space above the liquid in the other vessel, driving vapor from the downwardly moving vessel into the heat exchanger in the other vessel, where it condenses.

Abstract: A water distiller is provided which is used in conjunction with a hot water heater where normally wasted energy is used to preheat the hot water heater inlet. The distiller includes a heat storage tank, an evaporator tank having a water inlet, a heater and a steam outlet, and a first and second heat exchanger located within the heat storage tank. Steam generated in the evaporator tank passes through the first heat exchanger and condenses, forming distilled water. The heat rejected during condensation is absorbed within the heat storage tank. The second heat exchanger is used to preheat the water flowing to the hot water heater inlet by passing the water through the second heat exchanger on an as needed basis where it absorbs heat from the heat storage tank.

Abstract: Process for the separation of hydrogen fluoride (HF), 2,2-dichloro-1,1,1-trifluoroethane (FC-123), and/or 2-chloro-1,1,1,2-tetrafluoroethane (FC-124) from mixtures containing them by controlling the molar ratio of HF/FC-123 in the mixture prior to subjecting the mixture to azeotropic distillation.

Abstract: A modular water distillation apparatus includes a distillation unit which may be manually operated by adding water manually to the steam generator. The apparatus further includes an add-on holding tank and an add-on control unit which mounts to the holding tank and provides automatic control of the distillation unit by providing feedwater to the steam generator when the steam generator is deenergized and the holding tank is not full. The add-on control further includes a power receptacle for an add-on distilled water demand pump.

Abstract: An apparatus for treating a waste solution generated when a photosensitive material is processed by an automatic developing machine includes a waste solution reservoir which is maintained at a constant level. A drum, partially immersed in the waste solution, is rotated to coat its surface. The drum is heated to produce a waste vapor. The waste vapor is condensed by a condenser and filtered and solid wastes are scraped from the surface of the drum. The condenser has a drain tank for collecting condensate and a non-condensable gas component. The interior of the drain tank is sealed to form an air tight seal and has a vent for exhausting the non-condensable gas component from the interior portion to the outside. The air vent includes an absorption tower to treat the non-condensable gas component.

Abstract: The vacuum column system distills liquid under partial vacuum conditions. The system rigorously splashes and boils liquid in a boiler chamber so as to form vapor and a rising mist from the splashing liquid. The vapor and mist rise in a circularly converging path through a mist collector. The heavier mist strikes the surfaces of the mist collector and deposits on those surfaces, thereby separating itself from the vapor. The vapor is then drawn to a condensor chamber where droplets of treated liquid are sprayed through it and fall into a shallow pool of treated liquid. The droplets seed condensation of the vapor directly onto the droplets. Also, the droplets assist in encapsulating bubbles of vapor in the pool as the droplets fall into the pool. The bubbles are then entrained with other treated liquid of the pool as the treated liquid is drawn from the pool down an entrainment conduit.

Abstract: An apparatus for supplying both hot water and distilled water includes a water distillation unit having a steam generator, a condenser connected with the steam generator for converting steam into distilled water and a holding tank for receiving distilled water from the condenser. The condenser is in heat transfer relation to the interior of a water heater tank. Water level monitors are provided for monitoring the level of water in the steam generator and the holding tank and temperature sensors sense the temperature of water in the steam generator and water heater tank. When the level of water in the holding tank is above a predetermined value, the steam generator is de-energized and feed water is admitted to the steam generator to dilute the contents to a safe temperature before the contents are discharged to drain.

Abstract: A distillation type of water purification system has a raw water inlet valve for admitting raw water continuously to a boiling tank at a rate greater than the rate at which raw water is converted to treated water. A drain valve located at the bottom of the boiling tank is energized by a raw water level sensing device whenever the raw water level reaches a predetermined level, to discharge water from the boiling tank. Treated water is stored in a storage tank having a pump for discharging treated water to the user upon demand. A single conductivity sensor in the storage tank controls the pump to allow it to operate only if the sensed conductivity is above a first predetermined value but not at or above a second predetermined value greater than the first value. An improved condenser has two sets of tubes, each set is arranged in a pair of planes oriented transverse the flow of cooling air with the tubes parallel. The internal cross-sectional area of one set is about twice that of the other.

Abstract: An electronic control and dosing system for desalinators (10) has a baffle, disposed between the evaporation and condensation chambers, fitted with probes (70, 71) which detect the presence of liquid created by entrained bubbles, that pass through the holes in the baffle. A control circuit (72), connected to the probes (70,71), closes a solenoid valve (62) to shut off the supply of feed water to the desalinator (10) until the threat of entrainment has passed. A foaming and/or scale inhibiting polymer, contained in a tank (64), is periodically introduced to the feed water inlet line (63) by a solenoid valve (65) controlled by a timer circuit (66).

Abstract: Diastereomers can be separated with good industrial success with the aid of extractive distillation. The separation process is characterized in that an auxiliary which changes the partial pressure of the various diastereomers to be separated to a different degree and thus allows easier separation of the diastereomers by distillation is added during the distillation. Using the present process diastereomic cis/trans-permetric acid methyl esters and mixtures of menthol and isomenthol can be separated with isolation of 99% pure product.

Abstract: A steam distillation apparatus is provided which has a column body, a head connected to one end of the column body which has a diameter larger than the column body, a sump connected to the other end of the column body and contact elements disposed within the column body which are positioned and arranged to avoid formation of preferential pathways for the steam passing through the column body while providing for ready flow of the material being steam distilled through the column body. The connection of the head and column body may be frustoconical in shape such that its diameter diminishes from a diameter corresponding with that of the head at its connection with the head to a diameter corresponding with that of the column body at its connection with the column body. A collar is positioned at the connection of the neck and column body and extends into the head to define an annular space between the neck and collar.

Abstract: A method for concentrating salt water. Salt water is separated from oil-water mixture which has been produced from a well. Salt water is introduced into a recirculating weir and mixed with more concentrated brine. Brine is recirculated through a thermal syphon apparatus. Recirculation includes passing brine, including some salt water, from weir into boiler vessel. Brine is heated within boiler vessel to a boiling temperature whereby brine, while boiling, generates steam which passes up out of weir. All of foregoing steps are performed at atmospheric pressure. The density of brine is sensed at a location in the lower vicinity of weir. Concentrated brine is released from lower vicinity when density at sensed temperature is at a level corresponding to a brine concentration near the precipitation of salt from solution. Salt water and brine is passed through a magnetic water treating unit. The concentrated brine, as released, is passed into a holding vessel.

Abstract: A laboratory apparatus for continuously producing high purity distilled water includes a distillation flask, a carboy and condenser unit. A double walled microwave oven with a spacing between the walls, large enough to accommodate piping and valving means for controlling the flow of water to the distillation flask. The microwave oven supplies the heat to the system.

Abstract: A vacuum evaporator is provided which is connected to the casing of a driving motor for rotating the evaporator piston, wherein the driving motor is vertically adjustable mounted on a bolt fixedly mounted on a pedestal. A supporting sleeve which is freely displaceable on the bolt supports the driving motor thereon and a lever arm supports this sleeve and is articulated on the pedestal. A thread drive is coupled to the lever arm by means of a coupling sleeve arranged on the lever arm and wherein the lever arm is pivotable by the thread drive and the thread drive is adjustable by means of a geared motor.

Abstract: Distilling equipment comprising evaporation apparatus (2) including a boiling chamber (6) and equipment and conduits (46-59, 62, 63, 65-71) for supplying raw liquid to the boiling chamber at a predetermined level (43), a plurality of serial condensation stages (10, 20, 30), the first stage (10) connected to the top (7) of the boiling chamber (6) to receive gas therefrom and condense the gas by contact with cold recycled distillate from the final condensation stage (30), each stage having vertical vacuum producing bubble tubes (15, 25, 35) through which distillate and gas bubble (17) pass downward to a collection vessel (16, 26), gas carrier tubes (19, 29) which carry gas from each collection vessel (16, 26) to the condensation chamber (21, 31) of the following stage, and pump (41, 42) in cooperating conduits (18, 22, 28, 32) for pumping distillate free of gas from each collection chamber (16, 26) to the condensation chamber (21, 31) of the following stage.

Abstract: The invention relates to a rotary evaporator for carrying out a processor-controlled distilling operation. A rotary flask (5), a condenser (8) and a distillate collector receptacle (10) of the rotary evaporator (1) are continually kept under vacuum.According to the invention, the automatically controlled supply of a sample solution to the rotary flask is accomplished by means of a metering receptacle adapted to have the sample solution supplied thereto from a supply container for temporary transitory storage therein prior to transfer of the solution to the vacuum system, or the rotary flask (5), respectively. For discharging the distillate from the distillate collector receptacle (14), an outlet valve associated therewith is operable to connect the collector receptacle to a vacuum conduit (26) for the discharge of the distillate. This provision offers the advantage of permitting substantially discharge of the distillate without requiring the vacuum system to be vented.

Abstract: Vapor and liquid contact structure for distillation, fractionation, rectification, absorption, and the refining, in a column, of various liquid materials such as petroleum, chemical, and alcohol solutions. Provision is made for the inclusion of vertically-spaced bubble plate chambers, having respective liquid/vapor contact devices, to accommodate contact of counter-current flows of reflux liquid and vapors. Downcomer means including slanted ramps, disposed outside of the vapor conduit-defining interior, define elongate downcomer structure for liquid flow and thereby, i.e., by such slanted construction, reduce froth or foam passing to a next lower contact device, eliminating unwanted counter-current gas entrainment between contact devices. Liquid flow rates over exit weirs beyond 30 gpm/inch are obtained. Downcomer reflux reservoir depth can be adjusted by an adjustable gate proximate the slot opening to a given contact device.

Abstract: In a fractional distillation process, the operation of a reflux pump in the process is enhanced by providing that liquid discharged from the reflux pump is returned directly to the reflux pump suction during the periods when the liquid reflux supply from the fractional distillation process is not sufficient to keep the reflux pump in constant operation.

Abstract: A method and apparatus of controlling a rotating vacuum evaporation system is disclosed. The rotating flask, containing the medium to be evaporated, is buoyantly supported in a liquid bath and the relative elevation between the flask and the liquid level in the bath is measured. The relative elevation is utilized as the control signal to control the addition of fluid medium to the flask, and to shut off the system when desired.

Abstract: Apparatus and method for using a heated waste gas stream to evaporate a volatile component such as water or a solvent from a liquid solution comprises a flue to feed the gas stream from the source of heated gas; a container having an inner chamber to hold the liquid for evaporation of the volatile compound and an outer chamber connected to the flue which forms a gas channel substantially surrounding the inner chamber through which at least a portion of the gas stream flows to supply heat to the inner chamber and evaporate the volatile component of the liquid solution; an inlet to feed the liquid solution into the inner chamber; upper and lower liquid level sensors to control the quantity of liquid solution fed into the inner chamber to establish a liquid level therein; a sparger for agitating the liquid solution in the inner chamber; a sump below the container and connected to the flue to receive any condensate from the gas stream and any liquid leaking from the inner chamber; an outlet to combine, vent and d

Abstract: A computer control system for automatically optimizing the temperature of the feed supplied to a distillation column from a fuel fired preheat furnace, wherein the furnace temperature is manipulated in response to a measured ratio of distillate flow (D) from the tower to fuel flow (F) to the furnace. The D/F ratio is maximized by periodically comparing the present value of D/F to the previous value and incrementally increasing the furnace temperature as long as the D/F ratio increases. When no change is detected or the D/F ratio starts to decrease the furnace temperature is incrementally decreased until the D/F ratio again increases and reverses the control action once more.

Abstract: Cut point is controlled in a distillation process by monitoring the partial pressure in a stripper.

Abstract: Process and apparatus for the preliminary determination of the efficiency of the trays of distillation and/or absorption columns in order to establish the actual tray number of the columns, as well as for those columns the tray number of which was determined thereby. Each column section of different geometry or load is loaded with a set of trays (12) with air water system consisting at least of two trays having identical geometry (13,13a) and one air distributor (14). On the basis of the recognition that each set of trays (12) may be regarded as a cascade consisting of mixers which include series-connected mixers formed from the trays (13,13a), the liquid content of which is mixed by ascending vapor, or gas, in this case by air.

Abstract: A water distiller assembly which provides for an efficient distillation process wherein steam generated in a boiling chamber is delivered to a steam condensing chamber where steam condensation is carried out by the combined effect of water cooling and air cooling. The resulting distilled water is stored in the steam condensing chamber where it is kept hot by the incoming steam for hot serving while at the same time helps in condensing the steam it comes into contact with. Water vapor emanating from the surface of the hot coolant water is also condensed and collected. Operating temperature of the coolant water may be adjusted to suit room temperature demands. The distillation process is made automatic, continuous and self-limiting by the use of two simple float controls and a thermostatic water outlet valve.

Abstract: The present invention provides a process for the separation of materials obtained by means of high pressure extraction from an extraction agent, wherein extraction agent loaded with extracted material is passed from below into a separator comprising a head (2), a bottom (3), a runback pipe (4) and a heat exchanger (1) in the form of one or more pipes and extract recycled in a forced circulation via the head (2) and the runback pipe (4) to the bottom (3) and there either discharged and/or returned to the heat exchanger (1), the extraction agent evaporated in the heat exchanger being removed via a filter (11) on the head (2).

Abstract: A vacuum distillation system uses a tower having an open bottom submerged within a tank of solution exposed to atmospheric pressure. The solution within the tower is elevated to barometric level by a high vacuum or low absolute pressure on the tower top. As solution flows through the open bottom and upward, the solution is heated and then cooled to cause degasification and precipitation, and then withdrawn from the tower top. The treated solution is flowed to a vaporization chamber that is subjected to a low absolute pressure. A heater maintains the solution at a selected chamber temperature above the boiling point of water at the selected chamber pressure. The chamber pressure and temperature may be selected as desired to yield the purest water distillate for almost any solution of water and impurities. Water vapor is pumped from the vaporization chamber by a vapor pump to a condenser, where condensation results from increased pressure and decreased temperature.

Abstract: An oven for heating a distillable material in a preselected gas atmosphere. The oven comprises an inner heating chamber adapted to receive a spherical gravity lid, the heating chamber being connected to and in communication with a gas exhaust tube having a condensate trap at the termination thereof. The inner heating chamber is also in communication with and surrounded by an outer gas flow chamber, the outer gas flow chamber having a plurality of heater elements therein. The gas exhaust tube is surrounded by an ante chamber which is in communication with the outer chamber. The heater elements are continuously monitored by a programmable controller and a thermocouple in communication therewith. During oven operation, a purge gas is introduced to the ante chamber and flows therefrom into the outer gas flow chamber around the heater elements and into the top of the inner heating chamber.

Abstract: The Reid Vapor Pressure of a hydrocarbon mixture consisting essentially of hydrocarbons selected from the same series is determined based on the actual temperature and vapor pressure of the hydrocarbons mixture. The thus determined Reid Vapor Pressure may be compared to a set point for the Reid Vapor Pressure with the results of the comparison being utilized to maintain the actual Reid Vapor Pressure substantially equal to the desired Reid Vapor Pressure.

Abstract: A method of vaporizing a multicomponent liquid, such as a hydrogen peroxide and water solution, for injection into a vacuum chamber including the steps of metering successive predetermined increments of the liquid at a predetermined rate onto a heated surface in a vaporization chamber. Upon exposure to the heated surface, each liquid increment is substantially instantaneously vaporized before the next succeeding liquid increment is metered onto the heated surface to produce a multicomponent vapor increment having substantially the same weight percent composition as the multicomponent liquid increment. Each vapor increment is passed into the vacuum chamber.

Abstract: A method of vaporizing a multicomponent liquid, such as a hydrogen peroxide and water solution, for injection into a vacuum chamber including the steps of metering successive predetermined increments of the liquid at a predetermined rate onto a heated surface in a vaporization chamber. Upon exposure to the heated surface, each liquid increment is substantially instantaneously vaporized before the next succeeding liquid increment is metered onto the heated surface to produce a multi-component vapor increment having substantially the same weight percent composition as the multicomponent liquid increment. Each vapor increment is passed into the vacuum chamber.