Distillation Of Initial Distillate Patents (Class 203/74)
  • Patent number: 4042675
    Abstract: In the production of anhydrous sodium dithionite by reacting sodium formate, an alkaline sodium compound and sulfurous acid anhydride in hydrous methanol, a process for treating the mother liquor, which comprises adding an alkali to the mother liquor left after the separation of the resulting anhydrous sodium dithionite to adjust its pH to at least 8, separating the solids precipitated, and oxidizing the filtrate with an oxidizing agent.
    Type: Grant
    Filed: May 18, 1975
    Date of Patent: August 16, 1977
    Assignee: Mitsui Toatsu Chemicals, Incorporated
    Inventors: Kousuke Yamamoto, Shinji Takenaka, Kazuo Maeda, Michio Mituta
  • Patent number: 4042674
    Abstract: In the production of anhydrous sodium dithionite by reacting sodium formate, an alkaline sodium compound and sulfurous acid anhydride in hydrous methanol, a process for treating the mother liquor, which comprises cooling the mother liquor left after the separation of the resulting anhydrous sodium dithionite to a temperature in the range of +5.degree. to -30.degree. C, and separating the precipitated sodium thiosulfate by filtration.
    Type: Grant
    Filed: May 18, 1976
    Date of Patent: August 16, 1977
    Assignee: Mitsui Toatsu Chemicals Inc.
    Inventors: Kousuke Yamamoto, Shinji Takenaka, Kazuo Maeda
  • Patent number: 4033617
    Abstract: Crude ethylene oxide present in the dilute aqueous solution resulting from the extraction with an aqueous solvent of ethylene oxide from the gaseous stream obtained by catalytic oxidation of ethylene is purified by desorption, liquefaction, distillation in a fractionating column and final desorption treatment to remove absorbed non-condensable gases. The fractionating column is heated by condensation of the water vapor evolved during desorption and a liquid stream of ethylene oxide rich in acetaldehyde is discharged from the bottom, treated to convert a fraction of said acetaldehyde into high-boiling products, distilled to remove the latter as bottoms and returned to the fractionating column.
    Type: Grant
    Filed: July 8, 1976
    Date of Patent: July 5, 1977
    Assignee: Societa' Italiana Resine S.I.R. S.p.A.
    Inventors: Gioacchino Cocuzza, Gianni Torreggiani, Michele Sfregola
  • Patent number: 4021311
    Abstract: Ethylene glycol or 1,2-propylene glycol contained in mixtures with lower carboxylate esters of the glycol is recovered by azeotropic distillation of the mixtures with 1,2,3-trimethyl benzene.
    Type: Grant
    Filed: September 12, 1975
    Date of Patent: May 3, 1977
    Assignee: Halcon International, Inc.
    Inventor: Mitchell Becker
  • Patent number: 4009082
    Abstract: A low boiling water immiscible fluid containing two or more molecular species and having a variable boiling point is contacted in the liquid state with relatively hot or warm water such as surface sea water or geothermal water, thereby generating vapor of immiscible fluid (together with a certain amount of water vapor) which is used to drive a prime mover such as a gas turbine and thereby produce mechanical energy; the exhaust vapor from the prime mover is condensed by direct contact with a relatively cool or cold liquid aqueous phase such as deep sea water or water from a lake or stream or cooling tower to condense the vapor; and the condensate is recycled. Provision is made for ridding water discharged from the system of entrained and dissolved immiscible fluid. By countercurrent flow of the liquid phases and by suitable matching techniques greater efficiency is obtained. The invention is also applicable to heat pumps.
    Type: Grant
    Filed: December 1, 1975
    Date of Patent: February 22, 1977
    Inventor: Calvin Schwartz Smith, Jr.
  • Patent number: 4006190
    Abstract: A sterically hindered enamine (vinyl amine) is reacted with an alkylene oxide followed by hydrolysis of the reaction product to produce a monohydroxyl alkyl aldehyde wherein the hydroxyl group is on the third carbon atom from the carbonyl group, such as 4-hydroxybutanal. The monohydroxyl alkyl aldehyde may be further hydrogenated to produce the corresponding alkanediol, such as 1,4-butanediol.
    Type: Grant
    Filed: March 15, 1976
    Date of Patent: February 1, 1977
    Assignee: Celanese Corporation
    Inventor: Gerald S. Koermer
  • Patent number: 3996112
    Abstract: Ultra high purity hexachlorocyclopentadiene is obtained by a two-stage distillation procedure, in the first stage of which crude hexachlorocyclopentadiene is distilled to separate hexachlorobutadiene as a distillate and in the second stage, ultra high purity hexachlorocyclopentadiene is obtained as a distillate fraction and octachlorocyclopentene is obtained as a distillation residue.
    Type: Grant
    Filed: April 15, 1974
    Date of Patent: December 7, 1976
    Assignee: Hooker Chemicals & Plastics Corporation
    Inventor: George C. Woehr