Abstract: The invention relates to a process for the regulation of lyophilization in which the evaporative flux--that is to say, the output of evaporated water transferred on the trap (4)--is measured in a continuous manner, and action is carried out at the temperature of the racks (2) in order to reach, as close as possible, a predetermined optimal flux.

Abstract: A vacuum creating method comprising preparing a chamber for forming a space which can be made so atmospheric and vacuous as to allow a substrate to be directly or indirectly carried in and out of the space, exhausting the chamber, filling the space in the chamber with a CO.sub.2 gas whose vapor pressure becomes larger than 1 atm at ambient temperature but smaller than 10 Torr at a temperature lower than the ambient temperature, carrying the substrate into the chamber, cooling the CO.sub.2 gas to solidify, thereby making an internal pressure in the chamber highly vacuous, carrying the substrate out of the chamber, and heating the solidified dry ice to vaporize thereby returning the internal pressure in the chamber to atmospheric pressure.

Abstract: The lower extremity of each ballscrew (4) is engaged in a nut (6) with a nil pitch equipped with horizontal and parallel throats (7) for receiving balls (8) which cooperate with grooves (9) provided in an extremity sleeve (10) borne by the screw. An imperviousness system is constituted by sintered stainless steel rings mounted onto the upper portion and lower portion of the sleeve and are kept in place by a profiled joint made of a flexible synthetic material.

Abstract: A system for automatically loading and unloading bottles, vials, or other containers into and out of a freeze dryer or other material treating apparatus includes a loading station and a conveyer for bringing bottles to the loading station. A transfer vehicle movable between the loading station and one or more freeze dryers includes a horizontally arranged platen for supporting an entire dryer shelf of bottles. When the vehicle is aligned with the loading station, a pusher bar slides bottles from the loading station onto the vehicle platen. The vehicle then moves to a dryer where the platen aligns itself with one of the dryer shelves. A guide bar at the rear end of a rectangularly shaped lasso or transfer cage moves forwardly pushing the bottles onto the shelf. The forward end of the cage is then raised above the height of the bottles and removed from the dryer. To unload a dryer shelf, the cage enters the dryer above the bottles and the forward end drops down behind them.

Abstract: An automated yarn conditioning apparatus and process is provided. This apparatus and process allows for unconditioned yarn packages to be brought from a source to a yarn conditioning station where they are conditioned and then ejected onto a takeaway conveyor. Yarn conditioning is achieved within an airtight chamber inside of a vessel. The yarn conditioning process used first evacuates the airtight chamber and then injects steam or other conditioning vapor into the airtight chamber while partially elevating the internal chamber pressure and/or temperature. Simultaneously with the conditioning of the yarn packages inside the airtight chamber, unconditioned yarn packages are brought to the conditioning station for placement inside the vessel when the prior conditioning step has been completed.

Abstract: The invention relates to a process and apparatus for desiccation in which the exterior walls of the apparatus are heated and cooled in synchronization with the interior of the apparatus to avoid temperature gradients and inconsistent desiccation of material placed within the apparatus. The apparatus wall temperature regulating means also allows for more accurate sterilization of the apparatus after the desiccation process has been completed.

Abstract: A three step process to season lumber to reduce cracks in the lumber and reduce warping of the lumber. In a first step, the lumber is piled up into a pressure vessel for seasoning. The vessel is charged with saturated steam, the pressure of which fluctuates within the pressure vessel. This is done to enable any contained water within the vessels capillary tubes and cell cavities to evaporate at the same rate. Thereafter, as a second step the lumber is taken out of the pressure vessel in order to allow free water to evaporate from the lumber. The lumber in a third step is placed into the pressure vessel again and charged by a super saturated steam by using a flow of super saturated steam until remaining water is evaporated, thus forming lumber that is seasoned.

Abstract: An improved method and apparatus are provided for subliming solid precursors, and especially organometallic precursors, for use in a chemical vapor deposition (CVD) process. The sublimation apparatus includes a sealed vessel having a vacuum chamber. A quantity of the solid precursor is mixed with a loosely packed particulate material, such as ceramic beads, placed within the vacuum chamber. The vacuum chamber and particulate material are heated. A supply of a carrier gas is directed through the particulate material (particularly through pockets formed in the particulate material) to sublime the precursor which coats the individual particles of particulate material. By agitating the particulate material, a relatively constant sublimation area is maintained. Agitation of the particulate material may be with a mechanical stirrer or by directing an a.c. field through a piezoelectric particulate material.

Abstract: A vacuum drying apparatus characterized by a means for pre-heating a product by hot air, provided to a vacuum container having a heater housed therein.

Abstract: The invention relates to a process and an apparatus for drying sludge, in particular sewage sludge, or moist bulk material, wherein the material to be dried is heated by supplying energy by means of an electromagnetic alternating field generated between electrodes in a sealed pressurized vessel at an overpressure and the material moisture evaporated by the heating is used as heat transfer medium for heating the material to be dried in a step which is separate from the heating in the electromagnetic alternating field. In this process, the material to be dried is received with electrically insulated contiguous contact with the electrodes located in the pressurized vessel at least for a dwell time which is necessary for the heating and is then subjected to a flash drying.

Abstract: The invention relates to an apparatus for carrying out a process for aftertreating garments cleaned dried by means of at least one organic solvent such as for example perchlorethylene and/or other chlorinated hydrocarbons or the like, in which, for the purpose of removing solvent residues after their actual drycleaning, the garments, while being hung up for airing and/or preferably smoothing, are treated with steam and/or air.

Abstract: An apparatus and method are described for delivering hygroscopic, corrosive chemicals such as hydrogen chloride from a source such as a tube trailer to a use point such as a semiconductor fabrication tool minimizing infiltration of moisture, and entrainment of particulates, while still reducing moisture contents below 100 parts per billion and achieving appropriate pressure drops without two phase flow.

Abstract: To permit the use of combustible and potentially explosive solvents used in dry-cleaning operations, based on hydrocarbon compounds, the dry-cleaning machine is formed with an explosion-resistant housing (8) surrounding a perforated, rotatable drum (1) into which the goods are introduced. After carrying out the normal dry-cleaning procedure, and draining of dry-cleaning solvent, a vacuum pump generates an under-pressure, in the order of below 500 mbar, and preferably about 230 mbar, while heating the mixture to effect drying. A cooling coil, located at a lower portion of the machine, provides for condensation of solvent out of the solvent-air mixture and, after the major portion of the solvent has been evaporated, the heat exchanger is switched over to cooling for final condensation of any remanent solvent. The vacuum continues to be maintained, so that the boiling point of solvent, due to the under-pressure, is lowered by at least 40.degree. C., and preferably 50.degree. C.

Abstract: A vacuum drying apparatus for refuse or the like includes a drying vessel which receives a material, e.g., refuse, to be dried; a heat recoverer connected to the drying vessel through a steam discharge passage extending from the upper portion of the drying vessel; means for exhaust and drainage mounted to the heat recoverer; a heat pump; a radiator provided in the heat pump; heat exchanger for the drying vessel which introduces the heat of a refrigerant flowing through a piping of the heat pump into the drying vessel; and heat exchanger for the heat recoverer which introduces the heat of the refrigerant flowing through the piping of the heat pump into the heat recoverer. The refrigerant piping of the heat pump is capable of being switched over from a flow of the refrigerant through a circulation system for heating the drying vessel and cooling the heat recoverer, and discarding the heat generated by the radiator.

Abstract: This invention discloses a simple and inexpensive household implement to blot grease from one lot of prepared solid foodstuff, particularly deep-fried articles. It comprises an air-evacuating pump connected to a openable, closable, disposable, and flexible plastic bag interiorly lined with a layer of flexible liquid-absorbing material. Upon activation of said pump, blotting action occurs after the closed bag and the layer of liquid-absorbing are packed tightly against the greasy articles.

Abstract: This invention relates to a vacuum processing apparatus having vacuum processing chambers the insides of which must be dry cleaned, and to a method of operating such an apparatus. When the vacuum processing chambers are dry-cleaned, dummy substrates are transferred into the vacuum processing chamber by substrates conveyor means from dummy substrate storage means which is disposed in the air atmosphere together with storage means for storing substrates to be processed, and the inside of the vacuum processing chamber is dry-cleaned by generating a plasma. The dummy substrate is returned to the dummy substrate storage means after dry cleaning is completed. Accordingly, any specific mechanism for only the cleaning purpose is not necessary and the construction of the apparatus can be made simple.

Abstract: A colloidal substance is injected into a vacuum chamber to be dehydrated therein. The dehydrated substance is extracted from the vacuum chamber by a screw extruder disposed at a bottom of the vacuum chamber. A gas resulting from the dehydration is drawn from the vacuum chamber into a surface condenser to be cooled through an indirect heat exchange with cooling water. After the dehydration of the substance, the extraction of the dehydrated substance and the cooling of the gas are carried out in parallel.

Abstract: A process and apparatus are described for rapidly drying a wet, porous gel monolith of glass or ceramic, at subcritical temperatures without inducing any cracking of the gel. The wet gel is immersed in a liquid solvent in a chamber, and the liquid solvent is then heated and expelled from the chamber. Further heating, with or without the presence of a flowing inert gas, fully dries the wet gel. When an inert gas is used, the gas is delivered to the chamber with a controlled solvent partial vapor pressure, to correspondingly control the driving force for drying the gel.

Abstract: The present invention discloses a method and an apparatus for drying granular materials by submitting them to dielectric heating by means of electromagnetic waves such as microwave, high frequency, etc. The granular materials to be dried are heated to the prescribed temperature with electromagnetic waves under a reduced pressure of a range not producing any glow discharge and then dried to the prescribed moisture percentage while passing through a pressure reducing process of a vacuum of higher degree. An apparatus for it is provided with a reduced pressure drying tank (1) having an electromagnetic wave generator (2), a main drying tank (30) communicated with said reduced pressure drying tank (1), and suction air sources (20), (20') which are provided respectively in the reduced pressure drying tank (1) and the main drying tank (30).

Abstract: In order to provide a vacuum degreasing-drying method by which extremely small, precision metal products can be degreased and dried quickly and completely without using organic solvents, according to the present invention, an object 112 to be rinsed is put in a vacuum drier 110 after being rinsed with a hydrocarbon cleaning agent and then the air in the vacuum drier 110 is evacuated so as to degrease and dry the object thus rinsed.

Abstract: A carton is provided for holding wet books and like materials during transport to and processing at a freezing and freeze drying or vacuum drying facility. The carton is fabricated as a laminated corrugated carton from a high density polymer that may be stored in a flat condition, assembled to hold the books or like and after their processing collapsed for storage. The carton have openings throughout to facilitate extraction of fluids. The cartons are reusable as many as 20 times or more.

Abstract: The apparatus for draining dyed yarn on yarn bobbins includes a vacuum pump; a hollow dye carrier insert for carrying a plurality of yarn bobbins having yarn to be drained thereon, an interior volume of this dye carrier insert being connectable to the vacuum pump and structured so that, when at least a partial vacuum is produced in the interior volume by the vacuum pump, air is drawn through the yarn on the bobbins into the interior volume; a vacuum tank connected to the vacuum pump for producing a vacuum as ballast and having a capacity not less than the interior volume of the dye carrier insert; a coupling device for receiving the dye carrier insert on which the yarn bobbins are mounted; a bell releasably mountable on the coupling device to enclose the dye carrier insert carrying the yarn bobbins in a vacuum-tight manner and a connecting pipe with a valve connecting the coupling device to the vacuum tank and operable so as to be able to form the partial vacuum in the dye carrier insert for draining the yarn

Abstract: A device for drying articles such as semiconductor wafers comprising a vacuum process chamber for holding articles to be dried; a vapor generator substantially isolated from the process chamber for supplying a substance such as isopropyl alcohol in vapor form to the process chamber; a heater for heating the walls of the process chamber to discourage the substance vapor from condensing on the inside walls of the process chamber. The device can also be used for rinsing and cleansing articles prior to drying.

Abstract: This invention relates to a vacuum processing apparatus having vacuum processing chambers the insides of which must be dry cleaned, and to a method of operating such an apparatus.

Abstract: The present invention provides a process for freeze drying of especially biologically or pharmaceutical material under sterile conditions, wherein the material to be dried is introduced into a container the sides of which consist at least partly of a hydrophobic, porous, micro-organism-impermeable, water vapor-permeable membrane, the container is tightly closed and the material is subsequently freeze dried in the closed container under the usual conditions. The present invention also provides a container for freeze drying materials under sterile conditions, wherein the sides of the container consist at least partly of a hydrophobic, porous, germ-impermeable, water vapor-permeable membrane.

Abstract: A gas supply system includes a gas source containing a process gas to be supplied in a reduced-pressure container, a piping unit including a metallic pipe through which the process gas circulates and arranged between the gas supply source and the reduced-pressure container, and a duct formed of a metallic and/or nonmetallic pipe and arranged between the piping unit and the reduced-pressure container. At least part of the duct is formed of an austenitic stainless steel containing 6% or more of molybdenum by weight.

Abstract: This invention relates to a vacuum drying apparatus for continuously drying treated articles subjected to washing treatment with water such as electronic components. A plurality of vacuum tanks each incorporating therein heaters are disposed concyclically on a rotary table, and a carry-in apparatus for carrying in treated articles washed with water and a carry-out apparatus for carrying out dried treated articles are disposed in a carry-in/out zone of the treated articles. Furthermore, hot air heating devices for blowing hot air to the treated articles subjected to water washing treatment are disposed in the carry-in apparatus.

Abstract: A chemical vapor trap for selectively removing harmful corrosive contaminants, such as water and acetic acid vapors, from an evacuating vapor phase in a vacuum drying system is provided. The chemical vapor trap includes a condenser section effective to convert a high temperature incoming heated sample liquids and heated vapor phase into a liquid phase condensate and a relatively lower room temperature stripped vapor phase. Liquid condensate including water and acetic acid are trapped below a chemical blanket or sealing layer which prevents re-vaporization or boiling of removed corrosive volatile contaminants from the vapor phase entering the vacuum pumps, promoting improved pump performance and extend pump service life.

Abstract: A method and apparatus for removing vaporizable components from polymeric products effects uniform distribution of heat over such products contained within a chamber. The apparatus includes a heated chamber having support means for supporting the products within the chamber. Omnidirectional multi-point gas dispersion means located within the chamber uniformly disperse heated gas over the product. The vaporizable components are evacuated from the chamber along with the gas. The product can be rotated during treatment to ensure uniform exposure of the product to heat and gas.

Abstract: A solar sanitary dryer bag to be used for drying and exterminating tiny worms and insects existing in a mattress or the like, characterized by having an opening for vacuuming the bag and having a black layer therein for effectively absorbing the solar heat.

Abstract: A vacuum structure arranged for mounted securement to an associated hair clipper assembly is provided in operative communication with a vacuum pump to direct severed and trimmed hair into an associated container. The apparatus includes a rigid air inlet housing arranged for mounting to the hair clipper assembly having a downwardly canted inlet nozzle to include a nozzle valve plate mounted to effect air flow into the nozzle.

Abstract: Continuous freeze drying apparatus composed of a vessel whose internal chamber houses a cooled revolving cylinder on which a nebulizer sprays the material to be freeze dried.A scraping blade, grazing the freezed material, removes it making it fall onto revolving holed planes heated by heating elements interposed between these revolving planes, in order to obtain a quick sublimation of the substance to be freeze dried.

Abstract: A method and an apparatus for drying a wet work, for example, subsequent to a washing operation, in which a work is dried in an accelerated and precise manner free of stains or spots by means of: a hot D.I. water drying section 1 adapted to heat a work by immersion in hot D.I. water 11 and then to pull out the work for drying same; a vacuum drying section 2 adapted to dry off residual moisture on the work in a vacuum vessel under reduced pressure; and a work transfer means arranged to transfer the work from the hot D.I. water drying section 1 to the vacuum drying section 2.

Abstract: In the drying of solvents-containing material in a vacuum concentrator and which involves condensation of evolved solvents in a cold trap, simplified and inexpensive flow blocking devices are provided intervening an outlet of the cold trap and an inlet to the vacuum pump with which the concentrator is evacuated. The flow blocking practiced allows cryopumping effect to ensue between the concentrator and cold trap such being the agency by which solvent vapor outflows from the concentrator and is recovered by condensation thereof in the cold trap. Near complete solvent recovery can be achieved and carryover of solvent to the vacuum pump is reduced to insignificant measure. In one form, flow blocking is attained by use of a simple pressure differential valve.

Abstract: An apparatus and method is provided using a standard sized and shaped roll-off trash container sealed to contain contaminated soils to be treated with a central lengthwise vacuum tube to draw off vapors through a blower with air intake tubing aligned along the lengthwise side walls to distribute air to the soil mass with valve controls on the intake openings with the container having an openable side to dump the cleansed soil after treatment.

Abstract: A treating apparatus for drying wet sludge in batches or continuous feed which is circulated through the apparatus. The apparatus includes conveyor means for circulating the wet sludge in a closed loop and means for heating and circulating the dryer air around and about the conveyor means without contacting the sludge itself. It also includes means for heating and circulating cleaning air through the sludge to dry the sludge as it is circulating in the closed loop. A sensor is provided for determining the moisture content of the sludge and means are provided for discharging the sludge from the conveyor circulating means when the moisture content in the sludge reaches a predetermined level. A measured amount of cleaning air is drawn into the conveyor means from the atmosphere and circulates through the sludge itself to assist in drying and cleaning the sludge. This air is then withdrawn from the interior of the conveying means and exhausted through a cleaning means into the atmosphere.

Abstract: A pressure sealed chamber such as a load lock for a apparatus for processing substrates is provided with a guide plate spaced from a substrate supported therein so as to form a gap which covers the substrate surface to be protected from particulate contamination. During the filling of the chamber and during the evacuation of the chamber, by either pumping or venting, clean gas is introduced through an orifice in the center of the plate so as to flow outwardly from the edge of the gap at a pressure sufficient to deflect or otherwise reduce the number of turbulent gas borne particulates in the chamber from entering the gap and contaminating the surface to be protected of the substrate. During the filling of the chamber, all or some of the gas filling the chamber is introduced through the gap. During the evacuation of the chamber, gas is introduced through the gap at a flow rate less that of the evacuating gas.

Abstract: A condenser for removing vapor from freeze dryers and other vessels includes a three-stage cyclonic or turbine-like vapor distributor mounted for rotation about the axis of an elongated horizontal delivery tube extending through the axial center of the condenser chamber. The delivery tube mounts end and radial spray nozzles for selectively spraying cleansing fluid and sterilizing steam onto the interior surfaces of all components within the condenser chamber, including a plurality of condenser members arranged in radially offset configuration about the delivery tube in an optically dense configuration which requires vapors to impact the cold surfaces of the condenser members before contacting the inner surface of the enclosing condenser chamber. Optical density is achieved by providing the condenser member as sheets of metal formed with a serpentine passageway between them for the circulation of a coolant.

Abstract: A vacuum drying method and wherein a feed liquid is sprayed into a solvent vapor before being introduced into a vacuum chamber for vacuum evaporation, whereby a powder having spherical particles is produced. Moreover, the amount of solvent remaining in the powder obtained is small.

Abstract: Metallic workpieces, such as surgical needles, which have been washed with an aqueous solution are dried by subjecting the workpieces to heat and reduced pressure in the presence of an inert gas.

Abstract: In a freeze-drying method, liquid substances to be dried are sprayed into a stream of cold gas, usually air, at ambient pressure creating a collection of small frozen particles that are metered through a vacuum lock into a vacuumized vertical tower having heated walls and, as the particles fall through the vacuum in the tower to its bottom, radiant heat from the tower walls causes the ice contained in the particles to sublime. The resulting sublimed vapor is removed from the tower by low temperature condensation while the dried particles are collected at the bottom and transferred through another vacuum lock into a container. The operation is continuous and fast, providing significant advantages compared to prior known freeze-drying operations.

Abstract: Peanuts with a moisture content of from 6% to 15% are subjected to vacuum drying and/or roasting in a chamber using microwave energy to ensure penetration of the kernel. Aflatoxin compounds are destroyed and/or driven off with the vapors exiting the vacuum chamber.

Abstract: In a reproduction machine wherein thermoplastic marking particles are permanently fixed to a receiver member by application of heat in a fusing assembly as the receiver member is transported along a travel path, an improved device for cooling the receiver member. The improved cooling device comprises a thermally conductive guide plate located in juxtaposition with the receiver member travel path downstream, in the direction of receiver member travel, of the fusing assembly. A plurality of heat transfer fins extend from the guide plate on the opposite side thereof from the travel path. The heat transfer fins are oriented in a direction parallel to the direction of travel of a receiver member along the travel path. Cooling air is directed over the heat transfer fins to dissipate heat from a receiver member moving along the travel path.

Abstract: A system, apparatus and methods are described for the treatment of fibrous materials and, in particular, works of art on paper, with aqueous treating fluids introduced to a treatment chamber by means of an ultrasonic humidifier creating contact between the fibrous materials being treated and an absorbent material beneath it through air pressure, and drawing filtered air through the material being treated to dry the material by means of an underlying vacuum.

Abstract: Spray-freeze-drying systems and methods are disclosed for converting a wide variety of liquid substances into dry powder that may be reconstituted into the original substance by addition of water or other liquid that had been removed therefrom. Such systems and methods involve repetitive cycles of four operational steps, i.e., freezing, drying, defrosting and resetting and are characterized by: spraying the liquid substance downwardly in a vessel while surrounding the spray with a downward flow of process gas during the freezing step and by utilizing a heat pump for energy recapture to increase efficiency of operation.

Abstract: A pressure sealed chamber such as a load lock for a apparatus for processing substrates is operated with a guide plate spaced from a substrate supported therein so as to form a gap which covers the substrate surface to be protected from contamination by moisture condensing in the chamber during the rapid evacuation thereof. During the evacuation of the chamber, by either pumping or venting, clean dry gas is introduced through an orifice in the center of the plate so as to flow outwardly from the edge of the gap at a pressure sufficient to displace or otherwise prevent gas borne moisture condensate in the chamber from entering the gap and contaminating the surface to be protected of the substrate. During the evacuation of the chamber, gas is introduced through the gap at a flow rate less that of the evacuating gas.

Abstract: A vacuum dryer that has upper and lower platens brought together against the load handled by the application of a vacuum. A manifold, with means for producing a pressure within the manifold different from atmospheric, is used to seal one platen against the other. A flexible means joins the manifold to a platen whereby they are relatively displaceable.

Abstract: The subject invention provides a freeze dryer apparatus having an interim condensing system, preferably a refrigeratable condensing surface. The interim condensing system condenses vapors within the product chamber of the freeze dryer apparatus when the main condenser coil, which normally condenses vapors within the product chamber, needs to be defrosted. The refrigeratable condensing surface is preferably mounted inside the product chamber.

Abstract: Apparatus and method is set forth for treating a flat substrate (10), more particularly a semiconductor wafer in the manufacture of integrated circuits, under reduced pressure comprising a vacuum chamber (2a, 2b) provided with a substrate support (11) having a body (11a) with heating and/or cooling means (12) and a supporting surface (11b) at which a plurality of injection openings (20) is present communicating with an injection space (12) and a supplementary gas inlet (28), through which injection openings a gas is supplied between the substrate and the supporting surface for forming a heat-exchanging gas cushion therebetween.

Abstract: An apparatus is described for vacuum degassing and curing a spin-on-glass layer on an article. The machine has a chamber into which an article, such as at least one or more semiconductor wafers are moved by appropriate means. Means are provided for causing the chamber to be evacuated and for continuing to maintain the vacuum at less than about 100 mtorr. The temperature of the article is maintained at a substantially constant level within a first range of temperature by appropriate means during the vacuum degassing. Means are provided to ramping the temperature at a controlled rate from the first range of temperature up to the desired second range of temperature for curing of the spin-on-glass layer. The temperature of the article is maintained at a substantially constant level within the second range of temperature by suitable means for the curing. Means are provided to allow a constant inert gas flow to fill the chamber under the vacuum conditions during the operation.