Boride Containing Patents (Class 419/12)
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Patent number: 8309018Abstract: Methods of forming bit bodies for earth-boring bits include assembling green components, brown components, or fully sintered components, and sintering the assembled components. Other methods include isostatically pressing a powder to form a green body substantially composed of a particle-matrix composite material, and sintering the green body to provide a bit body having a desired final density. Methods of forming earth-boring bits include providing a bit body substantially formed of a particle-matrix composite material and attaching a shank to the body. The body is provided by pressing a powder to form a green body and sintering the green body. Earth-boring bits include a unitary structure substantially formed of a particle-matrix composite material. The unitary structure includes a first region configured to carry cutters and a second region that includes a threaded pin. Earth-boring bits include a shank attached directly to a body substantially formed of a particle-matrix composite material.Type: GrantFiled: June 30, 2010Date of Patent: November 13, 2012Assignee: Baker Hughes IncorporatedInventors: Redd H. Smith, John H. Stevens, James L. Duggan, Nicholas J. Lyons, Jimmy W. Eason, Jared D. Gladney, James A. Oxford, Benjamin J. Chrest
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Patent number: 8298479Abstract: A process for forming a remateable machined titanium powder base alloy connecting rod using a titanium alloy powder having an average particle size of about 1-20 microns, a mean aspect ratio of about 5 to 300, and a specific surface area of at least about 25 m2/g.Type: GrantFiled: May 12, 2011Date of Patent: October 30, 2012Inventor: Gerald Martino
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Patent number: 8287661Abstract: A method for producing a sintered R-T-B based magnet includes the steps of: providing R-T-B based alloy powders A and B so that the R-T-B based alloy powder B has a particle size D50 that is smaller by at least 1.0 ?m than that of the R-T-B based alloy powder A and that there is a difference ?RH of at least 4 mass % between the higher content of a heavy rare-earth element RH in the R-T-B based alloy powder B and the lower content of the heavy rare-earth element RH in the R-T-B based alloy powder A; mixing these two R-T-B based alloy powders A and B together; compacting the mixed R-T-B based alloy powder to obtain a compact with a predetermined shape; and sintering the compact.Type: GrantFiled: January 14, 2010Date of Patent: October 16, 2012Assignee: Hitachi Metals, Ltd.Inventors: Rintaro Ishii, Futoshi Kuniyoshi
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Publication number: 20120251376Abstract: A process is provided for producing aluminium-titanium-boron grain refining master alloys containing soluble titanium aluminide and insoluble aluminium boride particles, the process comprising mixing aluminium-boron alloy powder and K2TiF6 salt to obtain a blended mixture, heat treating the mixed powder blend thus obtained in an inert gas furnace just below the melting point of aluminium, at approximately 650 degrees Celcius sufficiently long and compacting the heated powder blend in the form of tablets. The cast grain size of an aluminium-7 wt % silicon foundry alloy after inoculation with this master alloy at an addition level of 0.02% Ti was less than 200 microns for contact times of upto 15 minutes.Type: ApplicationFiled: February 27, 2009Publication date: October 4, 2012Applicant: TubitakInventor: Yucel Birol
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Publication number: 20120251375Abstract: A method of producing a Pb-free copper-alloy sliding material containing 1.0 to 15.0% of Sn, 0.5 to 15.0% of Bi and 0.05 to 5.0% of Ag, and Ag and Bi from an Ag—Bi eutectic. If necessary, at least one of 0.1 to 5.0% of Ni, 0.02 to 0.2% P, 0.5 to 30.0% of Zn, and 1.0 to 10.0 mass % of at least one of a group consisting of Fe3P, Fe2P, FeB, NiB and AlN may be added.Type: ApplicationFiled: June 11, 2012Publication date: October 4, 2012Inventors: Hiromi YOKOTA, Ryo Mukai, Shinichi Kato, Nahomi Hamaguchi
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Patent number: 8252225Abstract: A multi-layer precursor material for use in forming hardfacing on a tool including hard particles, metal particles and a polymer. Methods of forming a multi-layer precursor film. Methods of using a precursor material to form hardfacing on a tool, including brazing a precursor material onto a surface of the tool. Intermediate structures for use in forming earth-boring tools including a precursor material covering an internal surface of a body of the tools. Methods of forming earth-boring tools include forming a body having a fluid passageway extending therethrough and covering a surface of the body with a hardfacing material. The surface of the body may be located in a region susceptible to erosion when fluid is caused to flow through the fluid passageway.Type: GrantFiled: March 4, 2009Date of Patent: August 28, 2012Assignee: Baker Hughes IncorporatedInventors: Jimmy W. Eason, Travis E. Puzz
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Patent number: 8222785Abstract: A magnet comprising grains of a ferromagnetic material whose main component is iron and a fluorine compound layer or an oxy-fluorine compound layer of fluoride compound particles of alkali metals, alkaline earth metals and rare earth elements, present on the surface of the ferromagnetic material grains, wherein an amount of iron atoms in the fluorine compound particles is 1 to 50 atomic %.Type: GrantFiled: June 27, 2011Date of Patent: July 17, 2012Assignee: Hitachi, Ltd.Inventors: Matahiro Komuro, Yuichi Satsu, Takao Imagawa
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Publication number: 20120094147Abstract: Provided is a corrosion-resistant and wear-resistant member where a thermal-sprayed layer having corrosion resistance and wear resistance is formed on a surface of a metallic member which is brought into contact with a resin which generates a highly corrosive gas. Also provided is a thermal-spraying powder. The highly corrosion-resistant and wear-resistant member having a thermal-sprayed layer is one obtained by thermally spraying metallic powder on a metallic base material to form a thermal-sprayed layer on a surface of the metallic base material. The member is characterized in that the thermal-sprayed layer is a composite boride cermet of a tetragonal Mo2(Ni,Cr)B2-type or a tetragonal Mo2(Ni,Cr,V)B2-type. The powder for forming a thermal-sprayed layer is made of a composite boride cermet of a Mo2(Ni, Cr)B2-type and comprises 4.0 to 6.5 mass % of boron, 39.0 to 64.0 mass % of molybdenum, and 7.5 to 20.0 mass % of chromium, a balance being 5 mass % or more of nickel and unavoidable elements.Type: ApplicationFiled: March 10, 2009Publication date: April 19, 2012Applicant: TOYO KOHAN CO., LTD.Inventors: Kengo Iwanaga, Yuji Yamazaki, Kourou Hirata
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Patent number: 8157927Abstract: It is an object of the present invention to obtain a highly coercive R-T-B system sintered magnet by making the crystal microstructure of a raw material alloy prepared by strip casting more uniform, thereby making the crushed powder obtained from such raw material alloy more fine and making the size distribution more narrow. The present invention provides a raw material alloy for an R-T-B system sintered magnet containing grains of an R2T14B compound, wherein a P and/or S content is between 100 and 950 ppm. This raw material alloy preferably has a composition comprising 25 to 35% by weight of R, 0.5 to 4% by weight of B, 0.02 to 0.6% of one or both of Al and Cu, 5% by weight or less of Co, and the balance of Fe.Type: GrantFiled: December 23, 2009Date of Patent: April 17, 2012Assignee: TDK CorporationInventors: Yasushi Enokido, Chikara Ishizaka, Gouichi Nishizawa
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Patent number: 8092619Abstract: An R-T-Cu—Mn—B based sintered magnet includes: 12.0 at % to 15.0 at % of R, which is at least one of the rare-earth elements that include Y and of which at least 50 at % is Pr and/or Nd; 5.5 at % to 6.5 at % of B; 0.08 at % to 0.35 at % of Cu; 0.04 at % to less than 0.2 at % of Mn; at most 2 at % (including 0 at %) of M, which is one, two, or more elements that are selected from the group consisting of Al, Ti, V, Cr, Ni, Zn, Ga, Zr, Nb, Mo, Ag, In, Sn, Hf, Ta, W, Au, Pb and Bi; and T as the balance, which is either Fe alone or Fe and Co and of which at most 20 at % is Co if T includes both Fe and Co.Type: GrantFiled: June 11, 2009Date of Patent: January 10, 2012Assignee: Hitachi Metals, Ltd.Inventors: Futoshi Kuniyoshi, Rintaro Ishii, Hiroyuki Tomizawa
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Publication number: 20110262295Abstract: A method of making a hard particle-dispersed metal matrix-bonded composite, includes the steps of mixing hard particles and ductile metal particles to yield a mixture, and sintering the mixture under a pressure of less than 2.0 GPa and at a temperature of less than 1200° C. for a sufficient time to yield the composite. A composite material made by the above method is disclosed.Type: ApplicationFiled: April 21, 2010Publication date: October 27, 2011Inventors: Oleg A. Voronov, Bernard H. Kear
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Patent number: 8043404Abstract: Disclosed herein are extruded titanium metal matrix composites with enhanced ductility. Also disclosed is the extrusion at high extrusion ratio of titanium metal matrix composites produced by powder metal processes. The ductility and machinability of these titanium metal matrix composites extruded at high extrusion ratios combined with their wear resistance and excellent imaging characteristics makes these high extrusion ratio extruded titanium metal matrix composites useful as biological implants, including prosthetic devices. Also disclosed are articles such as orthopedic implants for knee, hip, spine or other biomedical devices, with enhanced properties, made from the disclosed extruded material.Type: GrantFiled: February 17, 2006Date of Patent: October 25, 2011Assignee: Dynamet Technology, Inc.Inventors: Stanley Abkowitz, Susan M. Abkowitz, Harvey Fisher, Patricia J. Schwartz
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Patent number: 8043555Abstract: An earth-boring bit has a steel body and bearing pin for rotatably supporting a cone. The cone has an exterior surface containing rows of cutting elements. The cone and cutting elements are formed of cemented tungsten carbide. The cone may be manufactured by applying pressure to a mixture of hard particles and metal alloy powder to form a billet, then machining the billet to a desired over-sized conical shaped product. Then the conical-shaped product is liquid-phase sintered to a desired density, which causes shrinking to the desired final shape.Type: GrantFiled: December 7, 2009Date of Patent: October 25, 2011Assignee: Baker Hughes IncorporatedInventors: Redd H. Smith, Trevor Burgess, Jimmy W. Eason
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Patent number: 8034153Abstract: A composition for coating sliding or rolling or fretting or impacting members is formed by preparing a composite powder of TiB2 and BN, with a TiB2 to BN ratio ranging from 1:7 to 20:1, and a metallic matrix selected from the group consisting of nickel, chromium, iron, cobalt, aluminum, tungsten, carbon and alloys thereof.Type: GrantFiled: December 21, 2006Date of Patent: October 11, 2011Assignee: Momentive Performances Materials, Inc.Inventors: Robert Marchiando, Jon Leist
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Publication number: 20110214529Abstract: A process for forming a remateable machined titanium powder base alloy connecting rod using a titanium alloy powder having an average particle size of about 1-20 microns, a mean aspect ratio of about 5 to 300, and a specific surface area of at least about 25 m2/g.Type: ApplicationFiled: May 12, 2011Publication date: September 8, 2011Inventor: Gerald Martino
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Patent number: 8007714Abstract: The present invention relates to compositions and methods for forming a bit body for an earth-boring bit. The bit body may comprise hard particles, wherein the hard particles comprise at least one of carbide, nitride, boride, oxide, and solid solutions thereof, and a binder binding together the hard particles. The binder may comprise at least one metal selected from cobalt, nickel, and iron and, optionally, at least one melting point reducing constituent selected from a transition metal carbide in the range of 30 to 60 weight percent, boron up to 10 weight percent, silicon up to 20 weight percent, chromium up to 20 weight percent, and manganese up to 25 weight percent, wherein the weight percentages are based on the total weight of the binder.Type: GrantFiled: February 20, 2008Date of Patent: August 30, 2011Assignees: TDY Industries, Inc., Baker Hughes IncorporatedInventors: Prakash K. Mirchandani, Jimmy W. Eason, James J. Oakes, James C. Westhoff, Gabriel B. Collins, John H. Stevens, Steven G. Caldwell, Alfred J. Mosco
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Patent number: 7976643Abstract: A nanocomposite magnet containing an Fe particle in the grain boundary of an Nd2Fe14B compound particle is produced by mixing a dispersion of the Nd2Fe14B compound particle in a solvent containing a surface-active agent and a dispersion of the Fe particle in a solvent containing a surface-active agent, and then supporting the Fe particle on the surface of the Nd2Fe14B compound particle by stirring the mixture of the dispersions while adding an amphiphilic solvent, and then performing the drying and the drying and the sintering.Type: GrantFiled: November 27, 2007Date of Patent: July 12, 2011Assignee: Toyota Jidosha Kabushiki KaishaInventors: Noritsugu Sakuma, Tetsuya Shoji
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Patent number: 7972450Abstract: A magnet comprising grains of a ferromagnetic material whose main component is iron and a fluorine compound layer or an oxy-fluorine compound layer of fluoride compound particles of alkali metals, alkaline earth metals and rare earth elements, present on the surface of the ferromagnetic material grains, wherein an amount of iron atoms in the fluorine compound particles is 1 to 50 atomic %.Type: GrantFiled: February 19, 2010Date of Patent: July 5, 2011Assignee: Hitachi, Ltd.Inventors: Matahiro Komuro, Yuichi Satsu, Takao Imagawa
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Publication number: 20110146348Abstract: Methods of forming larger sintered compacts of PCD and other sintered ultrahard materials are disclosed. Improved solvent metal compositions and layering of the un-sintered construct allow for sintering of thicker and larger high quality sintered compacts. Jewelry may also be made from sintered ultrahard materials including diamond, carbides, and boron nitrides. Increased biocompatibility is achieved through use of a sintering metal containing tin. Methods of sintering perform shapes are provided.Type: ApplicationFiled: June 25, 2010Publication date: June 23, 2011Inventors: DAVID P. HARDING, MARK E. RICHARDS, RICHARD H. DIXON, VICTORIANO CARVAJAL, BAO-KHANG NGOC NGUYEN, GERMAN A. LOESENER, A. BEN CURNOW, TROY J. MEDFORD, TRENTON T. WALKER, JEFFERY K. TAYLOR, BILL J. POPE
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Patent number: 7955526Abstract: A composite material (M) comprising: at least 75% by volume of a mixed electronic conductor compound oxygen anions O<2->(C1) selected from doped ceramic compounds which, at the temperature of use, are present in the form of a crystalline network having ion oxide lattice vacancies and, more particularly, in the form of a cubic phase, a fluorite phase, a perovskite phase, of the aurivillius variety, a Brown-Millerite phase or a pyrochlore phase; and 0.01%-25% by volume of a compound (C2) which is different from compound (C1), selected from oxide-type ceramic materials, non-oxide type ceramic materials, metals, metal alloys or mixtures of said different types of material; and 0%-2.5% by volume of a compound (C3) produced from at least one chemical reaction represented by the equation: xFC1+yFC2 - - - >zFC3, wherein FC1, FC2 and FC3 represent the raw formulae of compounds (C1), (C2) and (C3) and x, y and z represent rational numbers above or equal to 0.Type: GrantFiled: November 5, 2004Date of Patent: June 7, 2011Assignee: L'Air Liquide, Societe Anonyme a Directoire et Conseil de Surveillance pour l 'Etude et l'Exploitation des Procedes Georges ClaudeInventors: Pascal Del Gallo, Thierry Chartier, Gregory Etchegoyen
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Publication number: 20110091345Abstract: A method for producing a high strength aluminum alloy tubing containing L12 dispersoids from an aluminum alloy powder containing the L12 dispersoids. The powder is consolidated into a billet having a density of about 100 percent. The tube is formed by at least one of direct extrusion, Mannesmann process, pilgering, and rolling.Type: ApplicationFiled: October 16, 2009Publication date: April 21, 2011Applicant: United Technologies CorporationInventor: Awadh B. Pandey
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Publication number: 20110064599Abstract: A method for producing a high strength aluminum alloy brackets, cases, tubes, ducts, beams, spars and other parts containing L12 dispersoids from an aluminum alloy powder containing the L12 dispersoids. The powder is consolidated into a billet having a density of about 100 percent. The billet is extruded using an extrusion die shaped to produce the component.Type: ApplicationFiled: September 15, 2009Publication date: March 17, 2011Applicant: UNITED TECHNOLOGIES CORPORATIONInventor: Awadh B. Pandey
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Patent number: 7906222Abstract: A sliding material has a sintered layer formed atop a backing plate. The sintered layer contains 5-15 mass % of Bi nonuniformly distributed in a Cu—Sn alloy matrix consisting essentially of 8-12 mass % of Sn and a remainder of Cu. The sliding material can be manufactured by nonuniformly mixing Cu—Sn alloy powder and Bi powder, dispersing the mixed powder on a backing plate, and sintering the mixed powder to form a sintered layer on the backing plate. The sliding material does not undergo seizing and does not have separation of the sintered layer from the backing plate even when used in severe conditions such as in hydraulic equipment or construction equipment.Type: GrantFiled: July 10, 2007Date of Patent: March 15, 2011Assignee: Senju Metal Industry Co., Ltd.Inventors: Sinzo Nakamura, Naoki Sato, Toshio Hakuto
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Patent number: 7892480Abstract: Dental prostheses are fabricated as a metallic alloy body by a technique that produces scrap alloy. Suitable gold base alloys have only base metal alloying additions which are more readily oxidized than gold and when combined with the gold can be age hardened. Exemplary metals include titanium, zirconium, yttrium and chromium. Scrap from fabricating a dental prosthesis is melted in air so that the base metals are all oxidized and substantially pure gold is reclaimed for reuse in new alloys.Type: GrantFiled: January 25, 2007Date of Patent: February 22, 2011Assignee: The Argen CorporationInventor: Paul J. Cascone
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Patent number: 7879286Abstract: A method of producing a high strength, high stiffness and high ductility titanium alloy, comprising combining the titanium alloy with boron so that the boron concentration in the boron-modified titanium alloy does not exceed the eutectic limit. The carbon concentration of the boron-modified titanium alloy is maintained below a predetermined limit to avoid embrittlement. The boron-modified alloy is heated to a temperature above the beta transus temperature to eliminate any supersaturated excess boron. The boron-modified titanium alloy is deformed at a speed slow enough to prevent microstructural damage and reduced ductility.Type: GrantFiled: June 7, 2006Date of Patent: February 1, 2011Inventors: Daniel B. Miracle, Seshacharyulu Tamirisakandala, Radhakrishna B. Bhat, Dale J. McEldowney, Jerry L. Fields, William M. Hanusiak, Rob L. Grabow, C. Fred Yolton, Eric S. Bono
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Publication number: 20110002804Abstract: The present invention includes consolidated hard materials, methods for producing them, and industrial drilling and cutting applications for them. A consolidated hard material may be produced using hard particles such as B4C or carbides or borides of W, Ti, Mo, Nb, V, Hf, Ta, Zr, and Cr in combination with an iron-based, nickel-based, nickel and iron-based, iron and cobalt-based, aluminum-based, copper-based, magnesium-based, or titanium-based alloy for a binder material. Commercially pure elements such as aluminum, copper, magnesium, titanium, iron, or nickel may also be used for the binder material. The mixture of the hard particles and the binder material may be consolidated at a temperature below the liquidus temperature of the binder material using a technique such as rapid omnidirectional compaction (ROC), the CERACON™ process, or hot isostatic pressing (HIP). After sintering, the consolidated hard material may be treated to alter its material properties.Type: ApplicationFiled: September 13, 2010Publication date: January 6, 2011Applicant: BAKER HUGHES INCORPORATEDInventors: Jimmy W. Eason, James C. Westhoff, Roy Carl Lueth
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Patent number: 7829013Abstract: The present invention includes consolidated hard materials, methods for producing them, and industrial drilling and cutting applications for them. A consolidated hard material may be produced using hard particles such as B4C or carbides or borides of W, Ti, Mo, Nb, V, Hf, Ta, Zr, and Cr in combination with an iron-based, nickel-based, nickel and iron-based, iron and cobalt-based, aluminum-based, copper-based, magnesium-based, or titanium-based alloy for a binder material. Commercially pure elements such as aluminum, copper, magnesium, titanium, iron, or nickel may also be used for the binder material. The mixture of the hard particles and the binder material may be consolidated at a temperature below the liquidus temperature of the binder material using a technique such as rapid omnidirectional compaction (ROC), the CERACON™ process, or hot isostatic pressing (HIP). After sintering, the consolidated hard material may be treated to alter its material properties.Type: GrantFiled: June 11, 2007Date of Patent: November 9, 2010Assignee: Baker Hughes IncorporatedInventors: Jimmy W. Eason, James C. Westhoff, Roy Carl Lueth
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Patent number: 7776256Abstract: Methods of forming bit bodies for earth-boring bits include assembling green components, brown components, or fully sintered components, and sintering the assembled components. Other methods include isostatically pressing a powder to form a green body substantially composed of a particle-matrix composite material, and sintering the green body to provide a bit body having a desired final density. Methods of forming earth-boring bits include providing a bit body substantially formed of a particle-matrix composite material and attaching a shank to the body. The body is provided by pressing a powder to form a green body and sintering the green body. Earth-boring bits include a unitary structure substantially formed of a particle-matrix composite material. The unitary structure includes a first region configured to carry cutters and a second region that includes a threaded pin. Earth-boring bits include a shank attached directly to a body substantially formed of a particle-matrix composite material.Type: GrantFiled: November 10, 2005Date of Patent: August 17, 2010Assignee: Baker Huges IncorporatedInventors: Redd H. Smith, John H. Stevens, James L. Duggan, Nicholas J. Lyons, Jimmy W. Eason, Jared D. Gladney, James A. Oxford, Benjamin J. Chrest
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Patent number: 7771649Abstract: Disclosed herein is a method of producing an ultrafine crystalline TiN/TiB2 composite cermet. In the method, titanium nitride (TiN)/titanium boride (TiB2)/stainless steel composite nanopowder is produced through a reaction milling process using titanium (Ti), boron nitride (BN), and stainless steel powders as raw material powders, and the resulting composite nanopowder is liquid-phase sintered. The method comprises a first step of mixing titanium powder and boron nitride powder at a molar ratio of 3:2, a second step of mixing 5-60 wt % stainless steel powder and the powder mixture, a third step of feeding the powder mixture along with a ball having a predetermined diameter into a jar and conducting a high energy ball milling process to produce titanium nitride/titanium boride/stainless steel composite nanopowder, and a fourth step of shaping and sintering the resulting composite nanopowder.Type: GrantFiled: November 19, 2007Date of Patent: August 10, 2010Assignee: Korea Institute of Science and TechnologyInventors: Jae Hyeok Shim, Ji Woo Kim, Young Whan Cho
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Publication number: 20100154587Abstract: Methods of fabricating bodies of earth-boring tools include mechanically injecting a powder mixture into a mold cavity, pressurizing the powder mixture within the mold cavity to form a green body, and sintering the green body to a desired final density to form at least a portion of a body of an earth-boring tool. For example, a green bit body may be injection molded, and the green bit body may be sintered to form at least a portion of a bit body of an earth-boring rotary drill bit. Intermediate structures formed during fabrication of an earth-boring tool include green bodies having a plurality of hard particles, a plurality of matrix particles comprising a metal matrix material, and an organic material that includes a long chain fatty acid derivative. Structures formed using the methods of fabrication are also disclosed.Type: ApplicationFiled: December 22, 2008Publication date: June 24, 2010Inventor: Jimmy W. Eason
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Patent number: 7731776Abstract: Multimodal cermet compositions comprising a multimodal grit distribution of the ceramic phase and method of making are provided by the present invention. The multimodal cermet compositions include a) a ceramic phase and b) a metal binder phase, wherein the ceramic phase is a metal boride with a multimodal distribution of particles, wherein at least one metal is selected from the group consisting of Group IV, Group V, Group VI elements of the Long Form of The Periodic Table of Elements and mixtures thereof, and wherein the metal binder phase comprises at least one first element selected from the group consisting of Fe, Ni, Co, Mn and mixtures thereof, and at least second element selected from the group consisting of Cr, Al, Si and Y, and Ti.Type: GrantFiled: December 2, 2005Date of Patent: June 8, 2010Assignee: ExxonMobil Research and Engineering CompanyInventors: ChangMin Chun, Narasimha-Rao V. Bangaru, Neeraj S. Thirumalai, Hyun-Woo Jin, Jayoung Koo, John R. Peterson, Robert L. Antram, Christopher J. Fowler, Emery B. Lendvai-Lintner
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Patent number: 7730755Abstract: The present invention relates to a process of producing a permanent magnet, which includes extruding a preform to form a plate-shaped permanent magnet, in which the preform is extruded in such a way that a dimension of a cross section of the preform is reduced in an X-direction and enlarged in a Y-direction perpendicular to the X-direction. The present invention also relates to a plate-shaped permanent magnet formed by extruding a preform, in which the preform is extruded in such a way that a dimension of a cross section of the preform is reduced in an X-direction and enlarged in a Y-direction perpendicular to the X-direction, whereby the permanent magnet has a strain ratio ?2/?1 with respect to the preform in a range of 0.2 to 3.5, in which ?1 is a strain in the direction of the extrusion of the preform and ?2 is a strain in the Y-direction.Type: GrantFiled: August 31, 2007Date of Patent: June 8, 2010Assignee: Daido Tokushuko Kabushiki KaishaInventors: Junichi Esaki, Hiroaki Yoshida, Sachihiro Isogawa
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Patent number: 7691173Abstract: The present invention includes consolidated hard materials, methods for producing them, and industrial drilling and cutting applications for them. A consolidated hard material may be produced using hard particles such as B4C or carbides or borides of W, Ti, Mo, Nb, V, Hf, Ta, Zr, and Cr in combination with an iron-based, nickel-based, nickel and iron-based, iron and cobalt-based, aluminum-based, copper-based, magnesium-based, or titanium-based alloy for the binder material. Commercially pure elements such as aluminum, copper, magnesium, titanium, iron, or nickel may also be used for the binder material. The mixture of the hard particles and the binder material may be consolidated at a temperature below the liquidus temperature of the binder material using a technique such as rapid omnidirectional compaction (ROC), the CERACON® process, or hot isostatic pressing (HIP). After sintering, the consolidated hard material may be treated to alter its material properties.Type: GrantFiled: September 18, 2007Date of Patent: April 6, 2010Assignee: Baker Hughes IncorporatedInventors: Jimmy W. Eason, James C. Westhoff, Roy Carl Lueth
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Publication number: 20100061874Abstract: A nanocomposite magnet containing an Fe particle in the grain boundary of an Nd2Fe14B compound particle is produced by mixing a dispersion of the Nd2Fe14B compound particle in a solvent containing a surface-active agent and a dispersion of the Fe particle in a solvent containing a surface-active agent, and then supporting the Fe particle on the surface of the Nd2Fe14B compound particle by stirring the mixture of the dispersions while adding an amphiphilic solvent, and then performing the drying and the drying and the sintering.Type: ApplicationFiled: November 27, 2007Publication date: March 11, 2010Applicant: TOYOTA JIDOSHA KABUSHIKI KAISHAInventors: Noritsugu Sakuma, Tetsuya Shoji
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Publication number: 20100040500Abstract: A method of preparing a titanium-based metal matrix composite. In one form, titanium hydride can be added to substantially pure titanium, an alloying material and a source of boron such that a mixture of these materials can be compacted and sintered in a powder metallurgy process to produce a component made up of a titanium boride reinforced titanium alloy. In another form, the substantially pure titanium, alloying material and source of boron could be vigorously mixed (with or without the titanium hydride) to such an extent that oxide films that may have built up on the titanium precursor can be removed to minimize the presence of oxygen in the manufactured component.Type: ApplicationFiled: December 13, 2007Publication date: February 18, 2010Applicant: GM GLOBAL TECHNOLOGY OPERATIONS, INC.Inventors: Yucong Wang, Richard David Ricchi, Lian Zhou, Yinjiang Wu, Qingwen Duan, Tuanwei Yang
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Publication number: 20100028190Abstract: A method of preparing a titanium-based metal matrix composite component. The method includes combining a titanium alloy-based matrix and a titanium-based ceramic reinforcement to form one or more mixtures, placing the mixture or mixtures into a mold, compacting the mixture or mixtures by shock loading, and sintering the compacted mixture or mixtures. In one form, the various mixtures may include differing levels of reinforcement concentration. In this way, different portions of a component produced by the present method may be made up of different mixtures from other portions of the manufactured component, thereby facilitating tailored mechanical or related structural properties.Type: ApplicationFiled: July 31, 2008Publication date: February 4, 2010Applicant: GM GLOBAL TECHNOLOGY OPERATIONS, INC.Inventor: Yucong Wang
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Publication number: 20100021334Abstract: An element such as Cr is caused to dissolve sufficiently in a base-material metal (Cu) in a solid solution state at a high temperature and a material in a supersaturated condition is obtained by performing quenching. After that, a strain is applied to this material and this material is subjected to aging treatment at a low temperature simultaneously with or after the application of this strain. As a result of this, it is possible to obtain a copper alloy having properties desirable as an electrode material, for example, a hardness of not less than 30 HRB, an electrical conductivity of not less than 85 IACS %, and a thermal conductivity of not less than 350 W/(m·K).Type: ApplicationFiled: May 5, 2009Publication date: January 28, 2010Applicant: HONDA GIKEN KOGYO KABUSHIKI KAISHAInventors: Mitsuhiro Funaki, Hiroki Baba, Shinya Ohyama, Toshiyuki Horimukai
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Patent number: 7645349Abstract: A sintered permanent magnet having a composition comprising, by mass, 27-33.5% of R, which is at least one of rare earth elements including Y, 0.5-2% of B, 0.002-0.15% of N, 0.25% or less of O, 0.15% or less of C, and 0.001-0.05% of P, the balance being Fe, wherein it is in the shape of a ring having an outer diameter of 10-100 mm, an inner diameter of 8-96 mm, and a height of 10-70 mm, with a plurality of magnetic poles axially extending on an outer circumferential surface. The distribution of a surface magnetic flux density B0 on magnetic poles in an axial direction of the ring magnet is in a range of 92.5% or more of the maximum of B0.Type: GrantFiled: October 10, 2006Date of Patent: January 12, 2010Assignee: Hitachi Metals, Ltd.Inventors: Nobuhiko Fujimori, Kazuhiro Sonoda, Takashi Tsukada, Junji Matsushima, Yasushi Kimura, Satoru Kikuchi
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Patent number: 7618497Abstract: An R-T-B system rare earth permanent magnet, which comprises main phase grains consisting of R2T14B compounds and a grain boundary phase having a higher amount of R than the above described main phase grains, and which satisfies AVE(X)/Y=0.8 to 1.0; and (X/Y)max/(X/Y)min=2.0 to 13.0, wherein X represents (weight ratio of heavy rare earth elements)/(the weight ratio of all rare earth elements) for a given number of the above described main phase grains Y represents (weight ratio of heavy rare earth elements)/(weight ratio of all rare earth elements) for the sintered body as a whole; AVE(X) represents the mean value of X obtained for the given number of main phase grains; (X/Y)min represents the minimum value of (X/Y) obtained for the given number of main phase grains; and (X/Y)max represents the maximum value of (X/Y) obtained for the given number of main phase grains.Type: GrantFiled: June 24, 2004Date of Patent: November 17, 2009Assignee: TDK CorporationInventors: Eiji Kato, Chikara Ishizaka
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Patent number: 7618496Abstract: A radial anisotropic sintered magnet formed into a cylindrical shape includes a portion oriented in directions tilted at an angle of 30° or more from radial directions, the portion being contained in the magnet at a volume ratio in a range of 2% or more and 50% or less, and a portion oriented in radial directions or in directions tilted at an angle less than 30° from radial directions, the portion being the rest of the total volume of the magnet. The radial anisotropic sintered magnet has excellent magnet characteristics without occurrence of cracks in the steps of sintering and cooling for aging, even if the magnet has a shape of a small ratio between an inner diameter and an outer diameter.Type: GrantFiled: September 20, 2005Date of Patent: November 17, 2009Assignee: Shin-Etsu Chemical Co., Ltd.Inventors: Koji Sato, Mitsuo Kawabata, Takehisa Minowa
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Patent number: 7556668Abstract: The present invention includes consolidated hard materials, methods for producing them, and industrial drilling and cutting applications for them. A consolidated hard material may be produced using hard particles such as B4C or carbides or borides of W, Ti, Mo, Nb, V, Hf, Ta, Zr, and Cr in combination with an iron-based, nickel-based, nickel and iron-based, iron and cobalt-based, aluminum-based, copper-based, magnesium-based, or titanium-based alloy for the binder material. Commercially pure elements such as aluminum, copper, magnesium, titanium, iron, or nickel may also be used for the binder material. The mixture of the hard particles and the binder material may be consolidated at a temperature below the liquidus temperature of the binder material using a technique such as rapid omnidirectional compaction (ROC), the CERACON™ process, or hot ecstatic pressing (HIP). After sintering, the consolidated hard material may be treated to alter its material properties.Type: GrantFiled: December 4, 2002Date of Patent: July 7, 2009Assignee: Baker Hughes IncorporatedInventors: Jimmy W. Eason, James C. Westhoff, Roy Carl Lueth
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Patent number: 7553563Abstract: The invention concerns a composite material consisting of intermetallic phases and ceramic, in particular in the form of a coating on metallic substrates, as well as an arc wire spraying process for production of the composite material in which the intermetallic phases and the ceramics to be deposited are newly formed during the deposit process from the components of the supplied wires by chemical reaction. The invention further concerns wear resistant layers formed by the composites, tribologic layers and plating or hard-facing materials.Type: GrantFiled: February 9, 2004Date of Patent: June 30, 2009Assignee: Daimler AGInventors: Stefan Grau, Michael Scheydecker, Karl Weisskopf
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Publication number: 20090129962Abstract: Disclosed herein is a method of producing an ultrafine crystalline TiN/TiB2 composite cermet. In the method, titanium nitride (TiN)/titanium boride (TiB2)/stainless steel composite nanopowder is produced through a reaction milling process using titanium (Ti), boron nitride (BN), and stainless steel powders as raw material powders, and the resulting composite nanopowder is liquid-phase sintered. The method comprises a first step of mixing titanium powder and boron nitride powder at a molar ratio of 3:2, a second step of mixing 5-60 wt % stainless steel powder and the powder mixture, a third step of feeding the powder mixture along with a ball having a predetermined diameter into a jar and conducting a high energy ball milling process to produce titanium nitride/titanium boride/stainless steel composite nanopowder, and a fourth step of shaping and sintering the resulting composite nanopowder.Type: ApplicationFiled: November 19, 2007Publication date: May 21, 2009Applicant: KOREA INSTITUTE OF SCIENCE AND TECHNOLOGYInventors: JAE HYEOK SHIM, JI WOO KIM, YOUNG WHAN CHO
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Patent number: 7501081Abstract: A nanostructured monolithic titanium boride (TiB) material and methods of forming such a material are disclosed and described. This material has a room-temperature four-point flexural strength about three times that of commercially available titanium diboride (TiB2). The achievement of nanostructured internal microstructural arrangement having a network of interconnected titanium monoboride whiskers affords a very high strength to this material above some of the best ceramic materials available in the market. The material contains a small amount of titanium and a densifier, but it is largely made of TiB phase with substantially no TiB2. The nanostructured monolithic titanium boride material can be formed by high temperature processing of a powder precursor having carefully selected weight and size distributions of titanium powder, titanium diboride powder, and densifier powder.Type: GrantFiled: January 25, 2007Date of Patent: March 10, 2009Assignee: University of Utah Research FoundationInventor: K. S. Ravi Chandran
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Publication number: 20090041609Abstract: The invention relates to manufacturing the flat or shaped titanium matrix composite articles having improved mechanical properties such as lightweight plates, sheets for aircraft and automotive applications, heat-sinking lightweight electronic substrates, armor plates, etc. High-strength discontinuously-reinforced titanium metal matrix composite (TMMC) comprises (a) titanium matrix or titanium alloy as a major component, (b) ceramic and/or ?50 vol. % intermetallic hard particles dispersed in matrix, (c) complex carbide- and/or boride particles at least partially soluble in matrix at sintering or forging temperatures such as ?50 vol. % AlV2C, AlTi2Si3, AlTi6Si3, VB2, TiVSi2, TiVB4, Ti2AlC, AlCr2C, TiAlV2, V2C, VSi2, Ta3B4, NbTiB4, Al3U2C3 dispersed in matrix. Method for manufacturing these TMMC materials is disclosed. Sintered TMMC density exceeds 98% and closed discontinuous porosity allows performing hot deformation in air without encapsulating.Type: ApplicationFiled: August 7, 2007Publication date: February 12, 2009Inventors: Volodymyr A. Duz, Vladimir S. Moxson, Alexander E. Shapiro
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Patent number: 7459105Abstract: A nanostructured monolithic titanium boride (TiB) material and methods of forming such a material are disclosed and described. This material has a room-temperature four-point flexural strength about three times that of commercially available titanium diboride (TiB2). The achievement of nanostructured internal microstructural arrangement having a network of interconnected titanium monoboride whiskers affords a very high strength to this material above some of the best ceramic materials available in the market. The material contains a small amount of titanium, but it is largely made of TiB phase with substantially no TiB2. The nanostructured monolithic titanium boride material can be formed by high temperature processing of a powder precursor having carefully selected weight and size distributions of titanium and titanium diboride powders. Potential applications of this material can include wear resistant components such as die inserts for extrusion dies, nozzles, armor, electrodes for metal refining etc.Type: GrantFiled: July 7, 2005Date of Patent: December 2, 2008Assignee: University of Utah Research FoundationInventor: K. S. Ravi Chandran
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Patent number: 7435376Abstract: A composite of a metal matrix with one or more incorporated secondary phases is referred to as a metal matrix composite (MMC). Secondary phase refers to all the particles or fibers which have a different composition than the metal matrix, and which are incorporated therein. As incorporation phases, elements and compounds are possible which, as a result of their material characteristics, are suited for improving individual properties of the metal matrix. Besides an improvement in individual properties of the pure metal matrix as a result of the incorporated secondary phase, certain properties of the metal are also degraded, in particular by particles having a size of 1 to 50 ?m. For example, the elongation at break decreases, the strength may decrease, or the tribology may become less favorable.Type: GrantFiled: December 15, 2003Date of Patent: October 14, 2008Assignee: CeramTec AGInventors: Dirk Rogowski, Ilka Lenke, Dieter Theil
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Publication number: 20080202820Abstract: The present invention includes consolidated hard materials, methods for producing them, and industrial drilling and cutting applications for them. A consolidated hard material may be produced using hard particles such as B4C or carbides or borides of W, Ti, Mo, Nb, V, Hf, Ta, Zr, and Cr in combination with an iron-based, nickel-based, nickel and iron-based, iron and cobalt-based, aluminum-based, copper-based, magnesium-based, or titanium-based alloy for the binder material. Commercially pure elements such as aluminum, copper, magnesium, titanium, iron, or nickel may also be used for the binder material. The mixture of the hard particles and the binder material may be consolidated at a temperature below the liquidus temperature of the binder material using a technique such as rapid omnidirectional compaction (ROC), the Ceracon™ process, or hot isostatic pressing (HIP). After sintering, the consolidated hard material may be treated to alter its material properties.Type: ApplicationFiled: September 18, 2007Publication date: August 28, 2008Applicant: BAKER HUGHES INCORPORATEDInventors: Jimmy W. Eason, James C. Westhoff, Roy Carl Lueth
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Publication number: 20080193319Abstract: An article made of constituent elements is prepared by furnishing at least one nonmetallic precursor compound, wherein all of the nonmetallic precursor compounds collectively contain the constituent elements. The constituent elements include a titanium-base metallic composition, boron present at a level greater than its room-temperature solid solubility limit, and, optionally, a stable-oxide-forming additive element present at a level greater than its room-temperature solid solubility limit. The precursor compounds are chemically reduced to produce a material comprising a titanium-base metallic composition having titanium boride particles therein, without melting the titanium-base metallic composition. The titanium-base metallic composition having the titanium boride particles therein is consolidated without melting.Type: ApplicationFiled: April 18, 2008Publication date: August 14, 2008Applicant: GENERAL ELECTRIC COMPANYInventors: Andrew Philip WOODFIELD, Eric Allen OTT, Clifford Earl SHAMBLEN, David Alan UTAH, Alan Glen TURNER, Michael Francis Xavier GIGLIOTTI
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Patent number: 7396506Abstract: A method is described for the preparation of superconductor massive bodies of MgB2, having a density close to the theorical value, which comprises the following passages: mechanical activation of crystalline boron with the formation of activated powders; formation of a porous preform of said powders; assembly of the porous boron preform and massive precursors of metallic magnesium in a container and sealing thereof in an atmosphere of inert gas or with a low oxygen content; thermal treatment of the boron and magnesium as assembled above, at a temperature higher than 700° C. for a time greater than 30 minutes, with the consequent percolation of the magnesium, in liquid phase, through the activated crystalline boron powders.Type: GrantFiled: May 10, 2002Date of Patent: July 8, 2008Assignee: Edison, S.p.AInventors: Giovanni Giunchi, Sergio Ceresara