Boride Containing Patents (Class 419/12)
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Patent number: 5595608Abstract: A permanent magnet which contains R, T and B as main ingredients wherein R is Y or a rare earth element and T is Fe or Fe and Co and has a primary phase of R.sub.2 T.sub.14 B is produced by compacting a mixture of 60 to 95 wt % of a primary phase-forming master alloy and a grain boundary phase-forming master alloy both in powder form and sintering the compact. The primary phase-forming master alloy has columnar crystal grains of R.sub.2 T.sub.14 B with a mean grain size of 3-50 .mu.m and grain boundaries of an R rich phase and contains 26-32 wt % of R. The grain boundary phase-forming master alloy is a crystalline alloy consisting essentially of 32-60 wt % of R and the balance of Co or Co and Fe. In anther form, a permanent magnet which contains R, T and B as main ingredients wherein R is yttrium or a rare earth element, T is Fe or Fe+Co/Ni and has a primary phase of R.sub.2 T.sub.Type: GrantFiled: November 2, 1994Date of Patent: January 21, 1997Assignee: TDK CorporationInventors: Katashi Takebuchi, Shinya Fujito, Shinya Hashimoto, Koichi Yajima
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Patent number: 5595616Abstract: Methods of enhancing oxidation resistance and methods of making molybdenum alloys are provided. In these methods, alloys are prepared by the addition of silicon and boron in amounts defined by the area of a ternary system phase diagram bounded by the points Mo-1.0%Si-0.5%B, Mo-1.0%Si-4.0%B, Mo-4.5%Si-0.5%B, and Mo-4.5%Si-4.0 B. The methods utilize rapid solidification followed by consolidation at below the melting point. The resultant alloys have mechanical properties similar to other high temperature molybdenum alloys while possessing a greatly enhanced resistance to oxidation at high temperature.Type: GrantFiled: June 7, 1995Date of Patent: January 21, 1997Assignee: United Technologies CorporationInventor: Douglas M. Berczik
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Patent number: 5590383Abstract: A porous membrane produced by preparing a slurry made from at least one micropyretic substance and at least one liquid carrier. The slurry is dried into a green form having a desired geometric configuration. Combustion of the green form produces the porous membrane.Type: GrantFiled: August 29, 1994Date of Patent: December 31, 1996Assignee: Micropyretics Heaters International, Inc.Inventors: Jainagesh A. Sekhar, James J. Liu, Naiping Zhu
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Patent number: 5589652Abstract: In the metallic member of the invention, ceramic super fine particles, and solid lubricant particles or short size fibers are dispersed, and the grain size of the ceramic particles is smaller than the solid lubricant particle size or fiber diameter.Type: GrantFiled: February 23, 1994Date of Patent: December 31, 1996Assignee: Hitachi, Ltd.Inventors: Toshiaki Arato, Yasuhisa Aono, Shigeo Tsuruoka, Katsuhiro Komuro
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Patent number: 5590393Abstract: The invention relates to a neutron-absorbing material and to its production process.This material comprises a homogeneous, boron carbide matrix 1 in which are dispersed e.g. pseudospherical, 150 to 500 .mu.m , calibrated clusters 3 of boride such as HfB.sub.2, in order to prevent the propagation of cracks F in the material and improve its thermal shock resistance.Type: GrantFiled: February 7, 1995Date of Patent: December 31, 1996Assignee: Commissariat a l'Energie AtomiqueInventors: Guy M. Decroix, Dominique Gosset, Bernard Kryger
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Patent number: 5584948Abstract: A method is provided for reducing the tendency for thermally induced porosity within a .gamma.' precipitation strengthened nickel-base superalloy which has been processed to obtain a uniform and coarse grain microstructure. This method is particularly useful for forming components such as gas turbine compressor and turbine disk assemblies in which optimal mechanical properties, such as low cycle fatigue and creep resistance, are necessary for operating at elevated temperatures within a gas turbine engine. The method generally entails alloying a .gamma.' precipitation strengthened nickel-base superalloy to have a boron content of not more than about 0.02 weight percent, and then forming a billet by melting an ingot of the superalloy in an argon gas atmosphere and atomizing the molten superalloy using argon gas. The above atomizing technique encompasses both powder metallurgy and spray forming processes.Type: GrantFiled: September 19, 1994Date of Patent: December 17, 1996Assignee: General Electric CompanyInventor: Eric S. Huron
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Patent number: 5581798Abstract: According to the invention there now is provided a method of producing a sintered titanium based carbonitride alloy with 3-25 weight % binder phase with extremely good properties at intermittent machining of materials difficult to machine. The method relates to the use of a raw material comprising a complex cubic carbonitride containing the main part of the metals from groups IV and V of the periodic system and carbon and nitrogen to be found in the finished alloy whereby said alloy has the composition0.86.ltoreq.X.sub.IV .ltoreq.0.970.44.ltoreq.X.sub.C .ltoreq.0.55where X.sub.IV is the molar ratio of the group IV elements of the alloy and X.sub.C is the molar ratio of carbon.Type: GrantFiled: May 11, 1995Date of Patent: December 3, 1996Assignee: Sandvik ABInventors: Gerold Weinl, Rolf Oskarsson
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Patent number: 5568653Abstract: According to the invention there now is provided a method of producing a sintered titanium based carbonitride alloy with 3-25 weight-% binder phase with extremely good properties at semifinishing operations at turning. The method relates to the use of a raw material consisting of a complex cubic carbonitride comprising the main part of the metals from groups IV and V of the periodic system and carbon and nitrogen to be found in the finished alloy whereby said alloy has the composition0.85.ltoreq.X.sub.IV .ltoreq.0.990.58.ltoreq.X.sub.C .ltoreq.0.69where X.sub.IV is the molar ratio of the group IV elements of the alloy and X.sub.C is the molar ratio of carbon.Type: GrantFiled: May 11, 1995Date of Patent: October 22, 1996Assignee: Sandvik ABInventors: Gerold Weinl, Rolf Oskarsson
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Patent number: 5561831Abstract: According to the invention there now is provided a method of producing a sintered titanium based carbonitride alloy with 3-25 weight-% binder phase with extremely good properties at fine to medium coarse milling. The method relates to the use of a raw material consisting of a complex cubic carbonitride comprising the main part of the metals from groups IV and V of the periodic system and carbon and nitrogen to be found in the finished alloy whereby said alloy has the composition0.89.ltoreq.X.sub.IV .ltoreq.0.970.52.ltoreq.X.sub.C .ltoreq.0.61where X.sub.IV is the molar ratio of the group IV elements of the alloy and X.sub.C is the molar ratio of carbon.Type: GrantFiled: May 11, 1995Date of Patent: October 1, 1996Assignee: Sandvik ABInventors: Ake Ostlund, Rolf Oskarsson
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Patent number: 5561830Abstract: According to the invention there now is provided a method of producing a sintered titanium based carbonitride alloy with 325 weight-% binder phase with extremely good properties at extremely fine machining with high cutting speeds and low feeds. The method relates to the use of a raw material comprising a complex cubic carbonitride containing the main part of the metals from groups IV and V of the periodic system and carbon and nitrogen to be found in the finished alloy whereby said alloy has the composition0.87.ltoreq.X.sub.IV .ltoreq.0.990.66.ltoreq.X.sub.C .ltoreq.0.76where X.sub.IV is the molar ratio of the group IV elements of the alloy and X.sub.C is the molar ratio of carbon.Type: GrantFiled: May 11, 1995Date of Patent: October 1, 1996Assignee: Sandvik ABInventors: Gerold Weinl, Rolf Oskarsson
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Patent number: 5561827Abstract: A nickel-base superalloy article has a coating having a composition, in weight percent, of from about 10 to about 20 percent cobalt, from about 14 to about 25 percent chromium, from about 2 to about 12 percent aluminum, from 0 to about 0.2 percent yttrium, from about 0.001 to about 3 percent boron, from about 1 to about 10 percent silicon, balance nickel and incidental impurities. The coating is preferably applied by mixing together two powders, one with a higher solidus temperature and one with a lower solidus temperature, whose net composition is that of the coating. The powder mixture is compacted with a binder, applied to a surface of the article, and heated to a temperature above the lower solidus temperature.Type: GrantFiled: December 28, 1994Date of Patent: October 1, 1996Assignee: General Electric CompanyInventors: Jim D. Reeves, David E. Budinger, Robert A. Anderson
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Patent number: 5552108Abstract: According to the invention there now is provided a method of producing a sintered titanium based carbonitride alloy with 3-25 weight-% binder phase with extremely good properties at extreme fine machining when turning with high cutting rates. The method relates to the use of a raw material comprising a complex cubic carbonitride containing the main part of the metals from groups IV and V of the periodic system and carbon and nitrogen to be found in the finished alloy whereby said alloy has the composition0.86.ltoreq.X.sub.IV .ltoreq.0.990.74.ltoreq.X.sub.C .ltoreq.0.83where X.sub.IV is the molar ratio of the group IV elements of the alloy and X.sub.C is the molar ratio of carbon.Type: GrantFiled: May 11, 1995Date of Patent: September 3, 1996Assignee: Sandvik ABInventors: Gerold Weini, Rolf Oskarsson
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Patent number: 5541006Abstract: Methods for making, methods for using and articles comprising ferromagnetic cermets, preferably cemented carbides and more preferably tungsten carbide, having at least two regions exhibiting at least one property that differs are discussed. The multiple-region cermets are particularly useful in wear applications. The cermets are manufactured by juxtaposing and densifying at least two powder blends having different properties (e.g., differential carbide grain size or differential carbide chemistry or differential binder content or differential binder chemistry or differential magnetic saturation or any combination of the preceding). Preferably, a first region of the cermet comprises a first hard component having a prescribed binder content and a first magnetic saturation and a second region, juxtaposing or adjoining the first region, comprising a second binder content different than the binder content of the first region and a second magnetic saturation different than that of the first region.Type: GrantFiled: December 23, 1994Date of Patent: July 30, 1996Assignee: Kennametal Inc.Inventor: Edward V. Conley
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Patent number: 5536485Abstract: A powder of diamond or high-pressure phase boron nitride core particles charged into a coating space as it is dispersed, and a precursor of a coat forming substance allowed to contact and/or impinge against the particles in the powder of core particles so that their surfaces are covered with the coat forming substance, thereby preparing coated diamond or high-pressure phase boron nitride particles which are subsequently sintered. The thusly produced diamond of high-pressure phase boron nitride sinter is composed of coated core particles of high performance that are superhard, uniform, dense and sintered firmly, and which have a controlled microstructure.Type: GrantFiled: August 11, 1994Date of Patent: July 16, 1996Assignees: Agency of Industrial Science & Technology, Nisshin Flour Milling Co., Ltd., Reed Co., LtdInventors: Shoichi Kume, Haruo Yoshida, Yukiyoshi Yamada, Tadashi Fuyuki, Satoshi Akiyama, Yoshiaki Hamada, Eisuke Kuroda, Tadakatsu Nabeya, Yukio Sumita, Kenichi Kimura
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Patent number: 5534086Abstract: A dispersion-strengthened copper alloy is disclosed having an exceptional combination of strength, ductility, and thermal conductivity. The copper alloy comprises: copper, 0.01 to 2.0 weight % boron and 0.1 to 6.0 weight % cobalt, and cobalt-boride disperoids that range in size between 0.025 and 0.25 microns in diameter. A copper alloy is made by rapid solidification of the melt into a powder. Strong, thermally conductive articles can be made by compacting the powder at temperatures below the melting temperature of the copper alloy, and optionally warm working, cold working, and annealing.Type: GrantFiled: May 1, 1995Date of Patent: July 9, 1996Assignee: United Technologies CorporationInventor: James S. Andrus
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Patent number: 5527504Abstract: To a fine R-Fe-B alloy powder comprised predominantly of 10-30 atomic % of R (wherein R stands for at least one elements selected from rare earth elements including yttrium), 2-28 atomic % of B, and 65-82 atomic % of Fe in which up to 50 atomic % of Fe may be replaced by Co, at least one boric acid ester compound such as tributyl borate is added as a lubricant in a proportion of 0.01%-2% by weight and mixed uniformly before, during, or after fine grinding of the alloy powder. The resulting powder mixture is compacted by compression molding in a magnetic field and the green compacts are sintered and aged. Compression molding can be performed continuously without need of mold lubrication, and the resulting magnets have improved magnet properties with respect to residual flux density, maximum energy product, and intrinsic coercive force.Type: GrantFiled: May 9, 1995Date of Patent: June 18, 1996Assignees: Sumitomo Metal Industries, Ltd., Sumitomo Special Metals Co. Ltd.Inventors: Yoshihisa Kishimoto, Nobushige Hiraishi, Wataru Takahashi, Masakazu Ohkita, Naoyuki Ishigaki, Yutaka Matsuura
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Patent number: 5520880Abstract: This invention relates to a method for producing a self-supporting body comprising the steps of:(a) forming a permeable mass comprising at least one solid-phase oxidant selected from the group consisting of the halogens, sulphur and its compounds, metals, metal oxides other than the silicates, and metal nitrides other than those of boron and silicon;(b) orienting said permeable mass and a source of said parent metal relative to each other so that formation of said oxidation reaction product will occur into said permeable mass;(c) heating said source of parent metal to a temperature above the melting point of said parent metal but below the melting point of said oxidation reaction product to form a body of molten parent metal;(d) reacting said body of molten parent metal with said at least one solid-phase oxidant at said temperature to permit said oxidant at said temperature to permit said oxidation reaction product to form; and(e) maintaining at least a portion of said at least one oxidation reaction productType: GrantFiled: September 19, 1994Date of Patent: May 28, 1996Assignee: Lanxide Technology Company, LPInventors: William B. Johnson, Eugene S. Park, Gerhard H. Schiroky, Danny R. White, Terry D. Claar
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Patent number: 5520879Abstract: A sintered titanium alloy is composed of a titanium matrix or titanium alloy matrix and hard particles dispersed in the matrix, the sintered titanium alloy comprises: 4-8 mass % of aluminum (Al); 2-6 mass % of vanadium (V); 0.15-0.8 mass % of oxygen (O); at least one element selected from the group consisting of 0.2-9 mass % of boron (B), 0.5-3 mass % of at least one of molybdenum (Mo), tungsten (W), tantalum (Ta), zirconium (Zr), niobium (Nb), and hafnium (Hf), 0.05-2 mass % of at least one of Ia Group elements, IIa Group elements, and IIIa Group elements, 0.05-0.5 mass % of at least one of halogens; with the balance being titanium (Ti) and inevitable impurities.Type: GrantFiled: January 11, 1995Date of Patent: May 28, 1996Assignee: Kabushiki Kaisha Toyota Chuo KenkyushoInventors: Takashi Saito, Tadahiko Furuta
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Patent number: 5516483Abstract: A process of forming a sintered article for powder metal comprising blending carbon and ferro alloys and lubricant with compressible elemental iron powder, pressing said blended mixture to form sintering said article, and then high temperature sintering said article in a reducing atmosphere to produce a sintered article having a high density from a single compression.Type: GrantFiled: February 8, 1994Date of Patent: May 14, 1996Assignee: Stackpole LimitedInventors: Rohith Shivanath, Peter Jones, Danny T. D. Thieu
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Patent number: 5514224Abstract: Isotropic hot pressed iron-rare earth metal permanent magnets are provided wherein the hot pressed permanent magnet exhibits magnetic remanences of at least about 9 kG, and most typically about 10 kG. Preferred compositions include a relatively low rare earth content coupled with an optimal amount of boron. The preferred composition is, on a weight percent basis, from about 5 to about 25 percent rare earth, most preferably about 10 to about 20 percent rare earth, from about 0.5 to about 4.5 percent boron, most preferably from about 0.8 to about 4.0 percent boron, wherein the total combination of the rare earths and boron ranges from about 9 percent to about 26 percent, most preferably from about 12 percent to about 22 percent, and optionally from about 2 percent to about 16 percent cobalt, with the balance being essentially iron.Type: GrantFiled: November 5, 1993Date of Patent: May 7, 1996Assignee: Magnequench International, Inc.Inventor: Viswanathan Panchanathan
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Patent number: 5509975Abstract: A soft magnetic bulky alloy according to the present invention is obtained by forming under pressure a powder and granule material mainly made of a Fe-M-B based amorphous alloy containing Fe, B and M where M is at least one element selected from a group consisting of Ti, Zr, Hf, V, Nb, Ta, Mo and W. In the soft magnetic bulky alloy, an amorphous alloy phase and a bcc phase with fine grain sizes of 30 nm or below are present in a mixed state, or the bcc phase with fine grain sizes of 30 nm or below is mainly present. The present invention also discloses a method of manufacturing such a soft magnetic bulky alloy.Type: GrantFiled: September 27, 1994Date of Patent: April 23, 1996Assignees: Alps Electric Co., Ltd., Tsuyoshi Masumoto, Akihisa InoueInventors: Akinori Kojima, Katsuaki Hangai, Shoji Yoshida, Akihiro Makino, Tsuyoshi Masumoto, Akihsia Inoue
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Patent number: 5494634Abstract: Graphite or carbon particles with a graphitic skin are intercalated with a compound including an oxidized form of a metal and then reduced in a hydrogen atmosphere. This process reduces the driving force for the galvanic reaction between the particles and active metals in aqueous environments. The particles may be present as a reinforcement for a metal matrix (e.g., graphite/aluminum metal matrix composites) or as a reinforcement for a non-metallic material (e.g., graphite/polyimide, graphite/polyester or graphite/cyanate composites). In the latter case, the composite is adjacent to a metal in a structure.By way of example, the graphite or carbon particle may be a fiber, the metal subject to attack may be aluminum or magnesium, and the intercalation compound may be NiCl.sub.2.Type: GrantFiled: January 15, 1993Date of Patent: February 27, 1996Assignee: The United States of America as represented by the Secretary of the NavyInventors: Alan S. Edelstein, Richard K. Everett, Patricia P. Trzaskoma, Benji Maruyama
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Patent number: 5489343Abstract: An R-Fe-B-based, sintered magnet, wherein R is one or more of rare earth elements including Y, is produced by the method including the steps of mixing fine R-Fe-B-based magnet powder with a mineral oil and/or a synthetic oil having a fractional distillation temperature range of 150.degree.-400.degree. C. and a kinetic viscosity of 10 cSt or less to prepare a mixture; charging the mixture under pressure into a die cavity equipped with a filter, to which an orientated magnetic field is applied, while removing a mineral oil and/or a synthetic oil from the mixture; compressing the mixture in the die cavity to carry out a wet molding while orientating the powder to prepare a green body; heating the green body to a temperature up to 500.degree. C. at a speed of 10.degree. C./min or less under pressure of 10.sup.-1 Torr or less for 30 minutes or more to remove a mineral oil and/or a synthetic oil from the green body; and then sintering the green body.Type: GrantFiled: January 27, 1994Date of Patent: February 6, 1996Assignee: Hitachi Metals, Ltd.Inventors: Kimio Uchida, Masahiro Takahashi, Masamichi Ozaki, Akira Kikuchi
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Patent number: 5478409Abstract: It is an object of the present invention to provide a method of producing sintered- or bond- rare earth element.iron.boron magnets obtainable easily and superior in magnetic properties with stable performance. The method of producing sintered rare earth element.iron.boron magnets according to the present invention is characterized by that it comprises steps of mixing in a scheduled ratio an acicular iron powder coated with a coating material, a rare earth element powder coated with a coating material and a boron powder coated with a coating material, and subjecting the mixture to compression molding followed by sintering of the molded mixture in the presence of a magnetic field. The method of producing bond rare earth element.iron.Type: GrantFiled: October 13, 1994Date of Patent: December 26, 1995Assignees: Kawasaki Teitoku Co., Ltd., Komeya Inc., Sanei Kasei Co., Ltd.Inventor: Yasunori Takahashi
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Patent number: 5476632Abstract: A process of forming a sintered article of powder metal comprising: selecting elemental iron powder; determining the desired properties of said sintered article and selecting, a quantity of carbon, and ferro alloy from the group of ferro manganese, ferro chromium, ferro molybdenum, ferro vanadium, ferro silicon and ferro boron; grinding said ferro alloy to a mean particle size of approximately 8 to 12 microns; introducing a lubricant while blending the carbon, ferro alloy, with said elemental iron powder; pressing the mixture to form the article; and then high temperature sintering the article at a temperature between 1,250.degree. C. and 1,350.degree. C. in a neutral or reducing atmosphere; so as to produce the sintered article of powdered metal; and includes the product formed thereby.Type: GrantFiled: January 14, 1994Date of Patent: December 19, 1995Assignee: Stackpole LimitedInventors: Rohith Shivanath, Peter Jones
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Patent number: 5470524Abstract: A method is provided for manufacturing a bladed ring for drum-shaped rotors of turbomachinery, especially rotors for axial compressors of gas turbine engines. The bladed ring is to be manufactured by hot isostatic pressing (HIP) and the fiber rings are formed in a metallic powder material for the bladed ring arranged in a circumferential direction. The fiber rings are bonded with spacing therebetween. The fiber rings are reinforced by fibers embedded in a metal matrix. The bladed ring prefabricated in this fashion by HIP is machined down to its required dimensions.Type: GrantFiled: June 14, 1994Date of Patent: November 28, 1995Assignee: MTU Motoren- Und Turbinen-Union Muenchen GmbHInventors: Wolfgang Krueger, William Wei
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Patent number: 5460640Abstract: A fully dense ceramic-metal body including 40-88 v/o of an oxide hard phase of, in v/o of the body, 4-88 v/o M-aluminum binary oxides, where the binary oxide has a C-type rare earth, garnet, .beta.-MAl.sub.11 O.sub.18, or perovskite crystal structure, and M is a lanthanide or indium, and 0-79 v/o .alpha.-alumina; about 10-50 v/o of a hard refractory carbide, nitride, or boride as a reinforcing phase; and about 2-10 v/o of a dispersed metal phase combining Ni and Al mostly segregated at triple points of the microstructure. The preferred metal phase contains a substantial amount of the Ni.sub.3 Al ordered crystal structure. In the preferred body, the reinforcing phase is silicon carbide partially incorporated into the oxide grains, and bridges the grain boundaries. The body including a segregated metal phase is produced by densifying a mixture of the hard phase components and the metal component, with the metal component being present in the starting formulation as Ni powder and Al powder.Type: GrantFiled: August 17, 1992Date of Patent: October 24, 1995Assignee: Valenite Inc.Inventor: Sergej-Tomislav Buljan
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Patent number: 5460775Abstract: The invention provides aluminum sintered alloys with high dimensional accuracy and high density which are superior in mechanical and physical characteristics as well as wear resistance, and a method of producing such alloys not by plastic working but by atmospheric sintering with high economy. Rapidly solidified aluminum alloy powder resulting from solidifying aluminum alloy molten metal containing 0.4 to 4.0% by weight of Mg at a solidification rate of 10.sup.2 .degree. C./sec or more is press molded in the cold, after annealing in the temperature range of 250 to 450.degree. C. if necessary, and then the molded product is sintered by generating nitrogen compounds on the powder surface at atmospheric pressure with a nitrogen partial pressure of 0.8 atm or more and a steam partial pressure of 0.01 atm or less in which a reducing gas component has been added as a nitrogen-combining acceleration gas component by 0.01 atm or more. Thus, a nitrogen-combined aluminum sintered alloy containing 0.4 to 4.Type: GrantFiled: July 2, 1993Date of Patent: October 24, 1995Assignee: Sumitomo Electric Industries, Ltd.Inventors: Tetsuya Hayashi, Yoshinobu Takeda
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Patent number: 5455001Abstract: A method for manufacturing an intermetallic compound comprises (a) preparing a powder, (b) canning said powder in a tube, (c) executing a first heat treatment to said tube-canned powder, and (d) treating said tube-canned powder for obtaining an intermetallic compound. This invention offers a simple, efficient, and inexpensive method for producing an intermetallic compound possessing excellent mechanical properties.Type: GrantFiled: July 7, 1994Date of Patent: October 3, 1995Assignee: National Science CouncilInventor: Chen-Ti Hu
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Patent number: 5447578Abstract: This invention provides permanent magnets that are excellent not only in magnetic properties but also corrosion resistance by using two magnetically useful phases, i.e., RE.sub.2 TM.sub.14 B phase having a high residual magnetic flux density and a low melting point RE-TM' phase or RE-TM'-B phase which enhances the sinterability and possesses a cleaning action against grain boundaries of the RE.sub.2 TM.sub.14 B main phase. Further the invention provides a method for forming an electrochemically noble composition as a starting material to prepare a two phase magnet.Type: GrantFiled: June 28, 1994Date of Patent: September 5, 1995Assignee: Kawasaki Steel CorporationInventors: Yukiko Ozaki, Michio Shimotomai, Yasutaka Fukuda, Akira Fujita, Yoko Kitano, Junichi Shimomura
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Patent number: 5447681Abstract: A method for manufacturing a metal graphite brush comprises steps of preparing natural graphite powders of 60-70 wt %, electrolytic copper powders of 30-40 wt %, molybdenum disulfide and lead of 2.5 wt % and the mixed resin of novolak phenol resin and furfural resin powders of 1-15 wt % which are adhesives, wet-mixing graphite powders with adhesives, pulverizing mixed powders to diameters of less than 200 .mu.m, press-molding all the powders under a pressure of 2-3 ton/cm.sup.2 and heating at a temperature 700.degree. C., and attaching a lead wire thereto, simultaneously, wherein the average particle distribution of the powders is 27 .mu.m. The compound ratio of graphite powders: copper powders: molybdenum disulfide: lead is 62.5 wt %: 35 wt %: 1.5 wt %: 1.0 wt %, the adhesives comprising the mixed resin of novolak phenol resin and furfural resin by 50:50 is added by a weight ratio of 7.5 wt % to the graphite powders.Type: GrantFiled: December 27, 1993Date of Patent: September 5, 1995Assignee: Mando CorporationInventors: Chung Tai Seung, Kim Seong Soo, Lee Jae Sung
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Patent number: 5439744Abstract: This invention relates generally to a novel directed metal oxidation process which is utilized to produce self-supporting bodies. In some of the more specific aspects of the invention, a parent metal (e.g., a parent metal vapor) is induced to react with at least one solid oxidant-containing material to result in the directed growth of a reaction product which is formed from a reaction between the parent metal and the solid oxidant-containing material. The inventive process can be utilized to form bodies having substantially homogeneous compositions, graded compositions, and macrocomposite bodies.Type: GrantFiled: February 25, 1993Date of Patent: August 8, 1995Assignee: Lanxide Technology Company, LPInventors: Terry D. Claar, Vilupanur A. Ravi, Philip J. Roach
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Patent number: 5439499Abstract: A cermet useful in the fabrication of metal cutting, rockdrilling and mineral tools, as well as wear parts. The cermet comprises (i) a hard phase of a simple boride of a transition metal, a mixture of simple borides of transition metals, or a mixed boride of transition metals; (ii) a binder phase of Fe, Ni, Co, Cr, or alloys thereof; (iii) a dispersion of particles of oxides of transition metals in which the oxygen can be replaced by nitrogen and/or carbon; and (iv) a dispersion of oxides of metals chosen from aluminum and Group IIA and IIIA metals.Type: GrantFiled: February 26, 1993Date of Patent: August 8, 1995Assignee: Sandvik ABInventors: Henri Pastor, Colette Allibert, Laurent Ottavi, Manuel Albajar, Francisco Castro-Fernandez
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Patent number: 5437833Abstract: This invention relates generally to a novel method of manufacturing a composite body, such as a ZrB.sub.2 --ZrC--Zr (optional) composite body, by utilizing a post-treatment process and to the novel products made thereby. More particularly, the invention relates to a method of modifying a composite body comprising one or more boron-containing compounds (e.g., a boride or a boride and a carbide) which has been made by the reactive infiltration of a molten parent metal into a bed or mass containing boron carbide, and optionally one or more inert fillers, to form the body.Type: GrantFiled: March 25, 1994Date of Patent: August 1, 1995Assignee: Lanxide Technology Company, LPInventors: Terry D. Claar, Gerhard H. Schiroky, William B. Johnson
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Patent number: 5435966Abstract: This invention relates generally to a novel method for removing metal from a formed self-supporting body. A self-supporting body is made by reactively infiltrating a molten parent metal into a bed or mass containing a boron donor material and a carbon donor material (e.g., boron carbide) and/or a boron donor material and a nitrogen donor material (e.g., boron nitride) and, optionally, one or more inert fillers. Once the self-supporting body is formed, it is then subjected to appropriate conditions which causes metallic constituent contained in the self-supporting body to be at least partially removed.Type: GrantFiled: January 11, 1993Date of Patent: July 25, 1995Assignee: Lanxide Technology Company, LPInventors: William B. Johnson, James C. Wang
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Patent number: 5409518Abstract: A sintered titanium alloy is composed of a titanium matrix or titanium alloy matrix and hard particles dispersed in the matrix, the sintered titanium alloy comprises: 4-8 mass % of aluminum (Al); 2-6 mass % of vanadium (V); 0.15-0.8 mass % of oxygen (O); at least one element selected from the group consisting of 0.2-9 mass % of boron (B), 0.5-3 mass % of at least one of molybdenum (Mo), tungsten (W), tantalum (Ta), zirconium (Zr), niobium (Nb), and hafnium (Hf), 0.05-2 mass % of at least one of Ia Group elements, IIa Group elements, and IIIa Group elements, 0.05-0.5 mass % of at least one of halogens; with the balance being titanium (Ti) and inevitable impurities.Type: GrantFiled: November 8, 1991Date of Patent: April 25, 1995Assignee: Kabushiki Kaisha Toyota Chuo KenkyushoInventors: Takashi Saito, Tadahiko Furuta
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Patent number: 5405455Abstract: Disclosed is a novel method for the preparation of a rare earth-based permanent magnet by the so-called two-alloy process in which powders of two kinds of rare earth-containing magnetic alloys each having a different composition from the other are blended together in a specified proportion and the powder blend is shaped in a magnetic field into a green body which is sintered. In the invention, the first magnetic alloy has a composition of the formula R.sub.2 T.sub.14 B, in which R is a rare earth element selected from the group consisting of neodymium, praseodymium, dysprosium and terbium and T is iron or a combination of iron and cobalt, while the second alloy has a composition of the formula R.sub.a Fe.sub.b Co.sub.c B.sub.d M.sub.Type: GrantFiled: September 13, 1993Date of Patent: April 11, 1995Assignee: Shin-Etsu Chemical Co. Ltd.Inventors: Matou Kusunoki, Takehisa Minowa, Masao Yoshikawa
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Patent number: 5403790Abstract: This invention relates generally to a novel method of manufacturing a composite body. More particularly, the present invention relates to a method for modifying the resultant properties of a composite body, by, for example, minimizing the amount of porosity present in the composite body. Moreover, additives, whether used alone or in combination, (1) can be admixed with the permeable mass, (2) can be mixed or alloyed with the parent metal, (3) can be placed at an interface between the parent metal and the preform or mass of filler material, (4) or any combination of the aforementioned methods, to modify properties of the resultant composite body. Particularly, additives such as VC, NbC, WC, W.sub.2 B.sub.5, TaC, ZrC, ZrB.sub.2, SiB.sub.6, SiC, MgO, Al.sub.2 O.sub.3, ZrO.sub.2, CeO.sub.2, Y.sub.2 O.sub.3, La.sub.2 O.sub.3, MgAl.sub.2 O.sub.4, HfO.sub.2, ZrSiO.sub.4, Yb.sub.2 O.sub.3 and Mo.sub.2 B.sub.Type: GrantFiled: January 11, 1993Date of Patent: April 4, 1995Assignee: Lanxide Technology Company, LPInventors: Terry D. Claar, Gerhard H. Schiroky, Kevin P. Pochopien, Vilupanur A. Ravi, James C. Wang, Ratnesh K. Dwivedi
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Patent number: 5382405Abstract: A method of manufacturing a shaped article from a powdered precursor, wherein the components of the powdered precursor are subjected to a self-propagating high-temperature synthesis (SHS) reaction and are consolidated essentially simultaneously. The shaped article requires essentially no machining after manufacture.Type: GrantFiled: September 3, 1993Date of Patent: January 17, 1995Assignee: Inland Steel CompanyInventors: Kenneth F. Lowrance, II, Eric C. Knorr, William M. Goldberger, Daniel Boss, Doreen Edwards
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Patent number: 5372775Abstract: To prepare an aluminum matrix particle composite alloy, a molten metal, mainly composed of aluminum, containing ceramic particles is disintegrated by atomization, to prepare atomized powder. The atomized powder is mechanically ground/reflocculated with a ball mill or the like, to prepare mechanically ground/reflocculated powder containing ceramic particles of not more than 8 .mu.m in maximum diameter and not more than 3 .mu.m in mean particle diameter. The mechanically ground/reflocculated powder is then warm-formed/solidified. Alternatively, an aluminum alloy molten metal containing dispersed particles is disintegrated by atomization, and thereafter the powder containing the dispersed particles of not more than 20 .mu.m in mean particle diameter is warm-formed/solidified by powder forging. Thus, it is possible to obtain an aluminum matrix particle composite alloy in which extra-fine ceramic particles are homogeneously distributed without segregation.Type: GrantFiled: August 17, 1992Date of Patent: December 13, 1994Assignee: Sumitomo Electric Industries, Ltd.Inventors: Tetsuya Hayashi, Yoshinobu Takeda
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Patent number: 5366686Abstract: A method for producing an article including a refractory compound by infiltrating a preform with a liquid infiltrant and initiating a reaction between the preform and the liquid infiltrant to establish a reaction front which propagates in a direction opposite to the direction of flow of the liquid infiltrant is provided, as are articles prepared according to this method.Type: GrantFiled: March 19, 1993Date of Patent: November 22, 1994Assignee: Massachusetts Institute of Technology, a Massachusetts CorporationInventors: Andreas Mortensen, David C. Dunand
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Patent number: 5364586Abstract: A filter membrane and a process for making the filter membrane are provided. The filter membrane comprises a metal substrate having a filtering layer thereon comprising sintered ultra-fine particles of metal or ceramic compounds. The filtering layer preferably has an average pore size of from about 30 nanometers to about 200 nanometers. The filter membranes can withstand pressure drops of up to about 0.6 MPa and are useful for a variety of filtering applications.Type: GrantFiled: August 17, 1993Date of Patent: November 15, 1994Assignee: Ultram International L.L.C.Inventors: Lev I. Trusov, Vladimir N. Lapovok, Victor I. Novikov
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Patent number: 5364442Abstract: A composite electrode for electrochemical processing having improved high temperature properties, and a process for making the electrode by combustion synthesis. A composition from which the electrode is made by combustion synthesis comprises from about 4% to about 90% by weight of a particulate or fibrous combustible mixture which, when ignited, is capable of forming an interconnected network of a ceramic or metal-ceramic composite, and from about 10% to about 60% by weight of a particulate or fibrous filler material capable of providing the electrode with improved oxidation resistance and maintenance of adequate electrical conductivity at temperatures above 1000.degree. C. The filler material is molybdenum silicide, silicon carbide, titanium carbide, boron carbide, boron nitride, zirconium boride, cerium oxide, cerium oxyfluoride, or mixtures thereof.Type: GrantFiled: October 26, 1993Date of Patent: November 15, 1994Assignee: Moltech Invent S.A.Inventor: Jainagesh A. Sekhar
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Patent number: 5356721Abstract: It is the object of the invention to reduce the propagation of noises, in particular shifting noises, in mechanical transmissions. The invention consists in the use of a sintered shaped part formed in an individualized configuration as a noise-damped component, and in particular a gearwheel for a transmission. In the novel configuration, an axially symmetrical sintered shaped part has individual, approximately annular zones of material, for example, an inner rim zone close to the axis and an outer rim zone remote from the axis, the inner and outer rim zones having a high strength and being largely free from voids and a central region being highly porous and comparatively ductile.Type: GrantFiled: November 29, 1993Date of Patent: October 18, 1994Assignee: Sinterstahl Gesellschaft m.b.H.Inventor: Walter Knoess
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Patent number: 5352301Abstract: A method is provided for forming a high energy product, anisotropic, hot pressed iron-rare earth metal permanent magnet without the requirement for magnetic alignment during pressing or additional hot working steps. The method of this invention includes providing a quantity of anisotropic iron-rare earth metal particles and hot pressing the particles so as to form a substantially anisotropic permanent magnet. The pressed permanent magnet of this invention permits a greater variety of shapes as compared to conventional hot worked anisotropic permanent magnets. As a result, the magnetic properties and shape of the permanent magnet of this invention can be tailored to meet the particular needs of a given application.Type: GrantFiled: November 20, 1992Date of Patent: October 4, 1994Assignee: General Motors CorporationInventors: Viswanathan Panchanathan, John J. Croat
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Patent number: 5342574Abstract: A method for producing an anisotropic rare earth magnet is improved by extruding using a compacted material formed in a shape having difference in level between the center part to be in contact with the end face of a punch and the outer peripheral part to be faced with a molding cavity formed between the punch and a cylindrical die of a mold.Type: GrantFiled: April 6, 1993Date of Patent: August 30, 1994Assignee: Daido Tokushuko Kabushiki KaishaInventors: Yasuaki Kasai, Hiyoshi Yamada, Norio Yoshikawa
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Patent number: 5326525Abstract: A process is disclosed for fabricating a metal aluminide composite which comprises providing a metal aluminide, such as titanium aluminide, or a titanium aluminide alloy, and a reinforcing fiber material, such as silicon carbide fiber, and placing an interlayer or diffusion barrier layer in the form of a metal selected from the group consisting of silver, copper and gold, and alloys thereof, between the metal aluminide and the reinforcing fiber material. The interlayer metal can be a foil of the metal or in the form of a coating, such as a silver coating, on the reinforcing fiber material. The metal aluminide, the reinforcing fiber material, and the metal interlayer, e.g., in the form of a packet of a plurality of alternate layers of metal aluminide alloy and reinforcing fiber material, each layer being separated by the metal interlayer, is pressed and heated at an elevated temperature, e.g., ranging from about 900.degree. to about 1200.degree. C., at which diffusion bonding occurs.Type: GrantFiled: July 11, 1988Date of Patent: July 5, 1994Assignee: Rockwell International CorporationInventor: Amit K. Ghosh
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Patent number: 5298052Abstract: An Ni-based bearing alloy consisting, by weight, of 9-30% Cr, 5-19% Fe, 0.1-1.5% Si, 2-22% Co, 1.4-11.0% Mo, and the balance Ni and incidental impurities, said alloy having a matrix in which hard particles of a Co-Mo-Cr-Si alloy and/or BN are uniformly dispersed in weight ratios of 5 to 35% and not more than 5.0, respectively. The Ni-based alloy matrix provides superior heat resistance. Hard particles of Co-Mo-Cr-Si alloy uniformly dispersed in the matrix improve sliding characteristic with or without uniform dispersion of Bn as a solid lubricant, whereby the bearing alloy exhibits superior heat resistance and sliding characteristic when used in high temperature oxidizing atmosphere.Type: GrantFiled: June 11, 1992Date of Patent: March 29, 1994Assignee: Daido Metal Company, Ltd.Inventors: Tadashi Tanaka, Masaaki Sakamoto, Koichi Yamamoto, Kenji Sakai
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Patent number: 5288670Abstract: This invention relates generally to a novel method of preparing self-supporting bodies, and to novel products made thereby. In its more specific aspects, this invention relates to a method of producing self-supporting bodies comprising one or more boron-containing compounds, e.g., a boride or a boride and a carbide, by reactive infiltration of a molten parent metal actinide into (1) a bed or mass containing boron carbide and, optionally, (2) at least one of a boron donor material (i.e., a boron-containing material) and a carbon donor material (i.e., a carbon-containing material), (3) a bed or mass comprising a mixture of a boron donor material and a carbon donor material and, optionally, (4) one or more inert fillers in any of the above masses, to form the body.Type: GrantFiled: November 23, 1992Date of Patent: February 22, 1994Assignee: Lanxide Technology Company, LPInventor: Paul V. Kelsey
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Patent number: 5282904Abstract: A permanent magnet of the neodymium-iron-boron type having improved corrosion resistance imparted by a combination of oxygen, carbon and nitrogen. Oxygen is provided in an amount equal to or greater than 0.6 weight percent in combination with carbon of 0.05-0.15 weight percent and nitrogen 0.15 weight percent maximum. Preferably, oxygen is within the range of 0.6-1.2% with carbon of 0.05-0.1% and nitrogen 0.02-0.15 weight percent or more preferably 0.04-0.08 weight percent. The magnet may be heated in an argon atmosphere and thereafter quenched in an atmosphere of either argon or nitrogen to further improve the corrosion resistance of the magnet.Type: GrantFiled: October 27, 1992Date of Patent: February 1, 1994Assignee: Crucible Materials CorporationInventors: Andrew S. Kim, Floyd E. Camp, Edward J. Dulis