Boride Containing Patents (Class 419/12)
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Publication number: 20080145261Abstract: A method for forming a carbide composite that includes providing a mixture of carbide particles and a metallic binder in a container; sintering the container contents at a first processing condition having a pressure of less than about 45,000 psi; and sintering the container contents at a second processing condition having a pressure of greater than about 100,000 psi is disclosed.Type: ApplicationFiled: December 15, 2006Publication date: June 19, 2008Applicant: Smith International, Inc.Inventors: Zhou Yong, Sike Xia, Sharath Kolachalam
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Publication number: 20080113258Abstract: Provided is a reinforced matrix for molten carbonate fuel cell, wherein a mechanical strength of the matrix is increased by adding a reinforcing agent having a low melting point.Type: ApplicationFiled: November 28, 2006Publication date: May 15, 2008Inventors: Hyung C. Ham, Seong A. Hong, In-Hwan Oh, Tae-Hoon Lim, Suk-Woo Nam, Sung P. Yoon, Jonghee Han, Jaeyoung Lee, Hyoung-Juhn Kim, Eun A. Cho, Kwang S. Lee, Heung Y. Ha, Sang Y. Lee
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Patent number: 7344606Abstract: An anisotropic bonded magnet is produced at a low cost by avoiding various problems caused by remanence. Also, the unit weight and density of a compact is increased by filling even a cavity, having no easily feedable shape, with a magnet powder just as intended. An anisotropic bonded magnet is produced by feeding the cavity of a press machine with a magnetic powder (e.g., an HDDR powder) and compacting it. After the magnetic powder has been positioned outside of the cavity, an oscillating magnetic field (e.g., an alternating magnetic field) is created in a space including the cavity. The magnetic powder is transported into the cavity while being aligned parallel to the oscillating direction of the oscillating magnetic field. Thereafter, the magnetic powder is compressed within the cavity to make a compact for an anisotropic bonded magnet.Type: GrantFiled: October 18, 2002Date of Patent: March 18, 2008Assignee: Neomax Co., Ltd.Inventors: Shuji Mino, Noboru Nakamoto
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Publication number: 20070286761Abstract: A method of producing a high strength, high stiffness and high ductility titanium alloy, comprising combining the titanium alloy with boron so that the boron concentration in the boron-modified titanium alloy does not exceed the eutectic limit. The carbon concentration of the boron-modified titanium alloy is maintained below a predetermined limit to avoid embrittlement. The boron-modified alloy is heated to a temperature above the beta transus temperature to eliminate any supersaturated excess boron. The boron-modified titanium alloy is deformed at a speed slow enough to prevent microstructural damage and reduced ductility.Type: ApplicationFiled: June 7, 2006Publication date: December 13, 2007Inventors: Daniel B. Miracle, Seshacharyulu Tamirisakandala, Radhakrishna B. Bhat, Dale J. McEldowney, Jerry L. Fields, William M. Hanusiak, Rob L. Grabow, C. Fred Yolton, Eric S. Bono
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Patent number: 7255752Abstract: A method for manufacturing an R-T-B system rare earth permanent magnet that is a sintered body comprising a main phase consisting of an R2T14B phase (wherein R represents one or more rare earth elements (providing that the rare earth elements include Y), and T represents one or more transition metal elements essentially containing Fe, or Fe and Co), and a grain boundary phase containing a higher amount of R than the above main phase, wherein a product that is rich in Zr exists in the above R2T14B phase, the above manufacturing method comprising the steps of: preparing an R-T-B alloy containing as a main component the R2T14B phase and also containing Zr, and an R-T alloy containing R and T as main components, wherein the amount of R is higher than that of the above R-T-B alloy; obtaining a mixture of the R-T-B alloy powder and the R-T alloy powder; preparing a compacted body with a certain form from the above mixture; and sintering the above compacted body, wherein, in the above sintering step, the above produType: GrantFiled: March 11, 2004Date of Patent: August 14, 2007Assignee: TDK CorporationInventors: Chikara Ishizaka, Gouichi Nishizawa, Tetsuya Hidaka, Akira Fukuno, Nobuya Uchida
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Patent number: 7244318Abstract: A blended powder including a first powder containing an R2T14B phase as a main phase, and a second powder containing an R2T17 phase at 25 wt % or more of the whole is prepared. Herein, R is at least one element selected from the group consisting of all rare-earth elements and Y (yttrium), T is at least one element selected from the group consisting of all transition elements, and Q is at least one element selected from the group consisting of B (boron) and C (carbon). The blended powder is sintered, so as to manufacture a permanent magnet having a structure in which a rare-earth element included in the second powder is concentrated in a grain surgace region of a main phase.Type: GrantFiled: January 22, 2002Date of Patent: July 17, 2007Assignee: Neomax Co., Ltd.Inventors: Takao Sekino, Yuji Kaneko
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Patent number: 7214343Abstract: The method for producing a granulated powder of the present invention includes the steps of: preparing an R—Fe—B alloy powder; and granulating the alloy powder using at least one kind of granulating agent selected from normal paraffins, isoparaffins and depolymerized oligomers, to prepare a granulated powder. The produced R—Fe—B alloy granulated powder is excellent in flowability and compactibility as well as in binder removability.Type: GrantFiled: March 27, 2002Date of Patent: May 8, 2007Assignee: Neomax Co., Ltd.Inventors: Futoshi Kuniyoshi, Yuji Kaneko, Akihito Tsujimoto, Kazunari Shimauchi, Kazuo Tanaka, Shizuo Mori, Kiyofumi Suzuki
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Patent number: 7208056Abstract: An R-T-B system rare earth sintered magnet having a high mechanical strength and excellent corrosion resistance is provided. The R-T-B system rare earth sintered magnet of the present invention comprises a sintered body comprising a main phase consisting of an R2T14B phase where R represents one or more rare earth elements and T represents one or more transition metal elements essentially containing Fe, or Fe and Co, and a grain boundary phase containing a higher amount of R than the above described main phase, wherein the surface of the above described sintered body is partially covered with a carbon compound layer. In the R-T-B system rare earth sintered magnet of the present invention, the area ratio of the partial surface of the above described sintered body covered with the above described carbon compound layer to the entire surface thereof is preferably between 10% and 90%.Type: GrantFiled: January 31, 2005Date of Patent: April 24, 2007Assignee: TDK CorporationInventors: Makoto Iwasaki, Chikara Ishizaka, Taku Takeishi
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Patent number: 7204891Abstract: Rare earth magnet scrap and/or sludge is remelted for reuse. Once a rare earth-free magnet-constituent metal feed is loaded in a melting furnace and heated into a melt, a rare earth-containing metal feed and the rare earth magnet scrap and/or sludge are added to the melt, a particulate flux of an alkali metal, alkaline earth metal or rare earth metal halide and having an average particle size of 1–50 ?m, preferably wrapped in a metal foil, is added to the melt, and the resulting mixture is melted, from which an alloy ingot is obtained. The valuable elements in the scrap and/or sludge can be recycled. Better separation between the slag and the molten metal ensures that the ingot is obtained from the melt in a high yield.Type: GrantFiled: August 31, 2005Date of Patent: April 17, 2007Assignee: Shin-Etsu Chemical Co., Ltd.Inventors: Koichi Hirota, Takehisa Minowa
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Patent number: 7201810Abstract: A rare earth alloy sintered compact includes a main phase represented by (LR1-xHRx)2T14A, where T is Fe with or without non-Fe transition metal element(s); A is boron with or without carbon; LR is a light rare earth element; HR is a heavy rare earth element; and 0<x<1. The sintered compact is produced by preparing multiple types of rare earth alloy materials including respective main phases having different HR mole fractions, mixing the alloy materials so that the sintered compact will include sintering a main phase having an average composition represented by (LR1-xHRx)2T14A, thereby obtaining a mixed powder, and the mixed powder. The alloy materials include first and second rare earth alloy materials represented by (LR1-uHRu)2T14A (where 0??&<x) and (LR1-vHRV)2T14A (where x<v?1) and including a rare earth element R(=LR+HR) at R1 and R2 (at%), respectively. ?=|R1?R2| is about 20% or less of (R1+R2)/2.Type: GrantFiled: March 29, 2002Date of Patent: April 10, 2007Assignee: Neomax Co., Ltd.Inventors: Hitoshi Morimoto, Yuji Kaneko
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Patent number: 7166171Abstract: Disclosed is a longitudinal magnetic field compacting method and device for manufacturing a neodymium (Nd) based rare earth magnet in the shape of a butterfly for use in VCM of HDD or DVD, a disk or coin for use in coreless motors, and a block for use in linear motors, characterized in that a longitudinal compacting process is performed under a pulse magnetic field for orientation of rare earth powders in the direction of an applied magnetic field. Further, a compacted body of the rare earth powders has the same shape as end products, thus no additional processing cost, thereby lowering manufacturing costs. In addition, the rare earth powders can be subjected to an aligning process and a longitudinal compacting process at the same time under the high pulse magnetic field of 50–70 kOe, whereby the resulting rare earth magnet can have excellent magnetic properties of 42–50 MGOe.Type: GrantFiled: July 16, 2003Date of Patent: January 23, 2007Assignee: Jahwa Electronics Co., Ltd.Inventor: Dong-Hwan Kim
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Patent number: 7163591Abstract: Disclosed is a method of preparing a micro-structured powder for bonded magnets having high coercivity, which is advantageous in terms of low preparation costs by recycling magnet scraps, simplified mass production, minimal environmental contamination by such a recycling process, and the preparation of stable anisotropic powders having high coercivity. Further, a magnet powder prepared by the above method is provided. The current method is characterized in that R—Fe—B type anisotropic sintered magnets or scraps thereof are crushed to prepare 50–500 ?m sized magnet powders, which are then mixed with 1–10 wt % of rare earth fluoride (RF3) powders and thermally treated at high temperatures (500–1100° C.) in a vacuum or an inert gas, to cause the change of matrix-near surface and grain boundary of the powders.Type: GrantFiled: December 12, 2003Date of Patent: January 16, 2007Assignee: Jahwa Electronics Co., Ltd.Inventors: Andrew S. Kim, Seok Namkung, Dong-Hwan Kim
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Patent number: 7147686Abstract: A rare earth magnet comprises rare earth magnet particles and a rare earth oxide being present between the rare earth magnet particles. The rare earth oxide is represented by a following general formula (I): R2O3??(I) where R is any one of terbium, dysprosium, holmium, erbium, thulium, ytterbium, and lutetium.Type: GrantFiled: June 23, 2003Date of Patent: December 12, 2006Assignee: Nissan Motor Co., Ltd.Inventors: Tetsurou Tayu, Hideaki Ono, Munekatsu Shimada, Makoto Kano
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Patent number: 7141126Abstract: Rare earth alloy powder having an oxygen content of 50 to 4000 wt. ppm and a nitrogen content of 150 to 1500 wt. ppm is compacted by dry pressing to produce a compact. The compact is impregnated with an oil agent and then sintered. The sintering process includes a first step of retaining the compact at a temperature of 700° C. to less than 1000° C. for a period of time of 10 to 420 minutes and a second step of permitting proceeding of sintering at a temperature of 1000° C. to 1200° C. The average crystal grain size of the rare earth magnet after the sintering is controlled to be 3 ?m to 9 ?m.Type: GrantFiled: June 22, 2004Date of Patent: November 28, 2006Assignee: Neomax Co., Ltd.Inventors: Futoshi Kuniyoshi, Hitoshi Morimoto
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Patent number: 7056393Abstract: A method of making a sintered body for a rare earth magnet includes the steps of (a) preparing a first coarse powder by coarsely pulverizing a rare earth alloy sintered body by a hydrogen pulverization process, (b) preparing a first fine powder by finely pulverizing the first coarse powder, (c) preparing a second fine powder by pulverizing an alloy block of a rare earth alloy material, and (d) sintering a mixed powder including the first and second fine powders. The first and second fine powders each includes a main phase represented by (LR1-xHRx)2T14A, where T is Fe and/or at least one non-Fe transition metal element; A is boron and/or carbon; LR is at least one light rare earth element; HR is at least one heavy rare earth element; and 0?x<1.Type: GrantFiled: May 28, 2002Date of Patent: June 6, 2006Assignee: Neomax, Co., Ltd.Inventors: Koki Tokuhara, Hitoshi Morimoto
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Patent number: 7048808Abstract: The present invention provides a rare-earth sintered magnet exhibiting desirable magnetic properties in which the amount of Nd and/or Pr forming a non-magnetic phase in a grain boundary phase is reduced. Specifically, the present invention provides a rare-earth sintered magnet having a composition of (R1x+R2y)T100-x-y-zQz where R1 is at least one element selected from the group consisting of all rare-earth elements excluding La (lanthanum), Y (yttrium) and Sc (scandium); R2 is at least one element selected from the group consisting of La, Y and Sc; T is at least one element selected from the group consisting of all transition elements; Q is at least one element selected from the group consisting of B and C, and including, as a main phase, a crystal grain of an Nd2Fe14B crystalline structure, wherein: molar fractions x, y and z satisfy 8?x?18 at %, 0.1?y?3.Type: GrantFiled: October 1, 2001Date of Patent: May 23, 2006Assignee: Neomax Co., Ltd.Inventors: Yuji Kaneko, Katsuya Taniguchi, Takao Sekino
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Patent number: 7018485Abstract: An apparatus for subjecting a rare earth alloy block to a hydrogenation process includes a casing, gas inlet and outlet ports, a member arranged to produce a gaseous flow, and a windbreak plate. The casing defines an inner space for receiving a container. The container includes an upper opening and stores the rare earth alloy block therein. A hydrogen gas and an inert gas are introduced into the inner space through the gas inlet port, and are exhausted from the inner space through the gas outlet port. The gaseous flow is produced by a fan, for example, in the inner space. The windbreak plate is disposed upstream with respect to the gaseous flow that has been produced inside the inner space. Also, the windbreak plate reduces a flow rate of the gaseous flow that has been produced near the upper opening of the container.Type: GrantFiled: June 25, 2002Date of Patent: March 28, 2006Assignee: Neomax Co., Ltd.Inventors: Akihito Tsujimoto, Katsumi Okayama, Shinji Kidowaki, Tadayoshi Muneto
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Patent number: 7014811Abstract: A method for producing rare earth sintered magnets includes the steps of pressing and compacting an alloy powder for the rare earth sintered magnets, thereby preparing a plurality of green compacts, arranging the green compacts on a receiving plane in a direction in which a projection area of each of the green compacts onto the receiving plane is not maximized, and heating the green compacts, thereby sintering the green compacts and obtaining a plurality of sintered bodies.Type: GrantFiled: June 25, 2002Date of Patent: March 21, 2006Assignee: Neomax Co., Ltd.Inventors: Daisuke Harimoto, Yuji Kaneko, Akira Nakamura
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Patent number: 6994755Abstract: Disclosed are methods for producing compositionally modified sintered RE—Fe—B-based rare earth permanent magnets, by the addition of small amounts of Nd, Cu, Ti, Nb, or other transition metals, and mixtures thereof, to maximize fracture toughness with corresponding improved machinability, while maintaining maximum energy product, said method comprising the steps of: (a) prepare a magnetic composition; (b) melt the composition and form powders with an average particle size smaller than 5 microns from the same; (c) press the powder under a magnetic field to obtain green compacts, which are then sintered at from about 1030° C. to 1130° C., and heat treating the sintered material at from about 570° C. to 900° C.Type: GrantFiled: November 13, 2002Date of Patent: February 7, 2006Assignees: University of Dayton, Electron Energy CorporationInventors: Shiqiang Liu, Jinfang Liu
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Patent number: 6984271Abstract: A rare earth magnet to be used in a motor. The rare earth magnet comprises rare earth magnet particles. Additionally, a rare earth oxide is present among the rare earth magnet particles, the rare earth oxide being represented by the following general formula (I): R2xR?2(1?x)O3??(I) where each of R and R? is one element selected from the group consisting of yttrium (Y), lanthanum (La), cerium (Ce), praseodymium (Pr), neodymium (Nd), samarium (Sm), europium (Eu), gadolinium (Gd), terbium (Tb), dysprosium (Dy), holmium (Ho), erbium (Er), thulium (Tm), ytterbium (Yb) and lutetium (Lu), and 0<x<1.Type: GrantFiled: March 26, 2004Date of Patent: January 10, 2006Assignee: Nissan Motor Co., Ltd.Inventors: Tetsurou Tayu, Takae Ono, legal representative, Makoto Kano, Munekatsu Shimada, Yoshio Kawashita, Takeshi Yamauchi, Hideaki Ono, deceased
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Patent number: 6960319Abstract: Disclosed is a flow-softening tungsten alloy having the general formula: W100-pAiBjCkDe wherein W is tungsten; A is one or more elements selected from the group consisting of nickel, iron, chromium and cobalt; B is in or more elements selected from the group consisting of molybdenum, niobium and tantalum; C is one or more of the elements selected from the groups consisting of titanium and aluminum; D is one or more elements selected from the group consisting of boron, carbon, and silicon; i is from about 5 to about 8 weight percent; j is from 0 to about 4 weight percent; k is from about 0.1 to about 4 weight percent; 1 is from 0 to about 0.1 weight percent; and p is greater than or equal to about 7 weight percent and less than or equal to about 20 weight percent. In this alloy p is approximately equal to the sum of i, j, k and 1. A method of preparing this alloy and a kinetic energy penetrator manufactured from it are also disclosed.Type: GrantFiled: October 27, 1995Date of Patent: November 1, 2005Assignee: The United States of America as represented by the Secretary of the ArmyInventor: Deepak Kapoor
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Patent number: 6926777Abstract: The invention relates to a method for producing rod-shaped permanent magnets according to which pressed parts (2) are produced that are then assembled to a rod-shaped green product. Said green product is subsequently sintered, whereby a rod-shaped single-piece permanent magnet (1) is produced.Type: GrantFiled: December 19, 2000Date of Patent: August 9, 2005Assignee: Vacuumschmelze GmbH & Co. KGInventors: Georg Werner Reppel, Volker Zellmann
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Patent number: 6921422Abstract: This invention relates to a ductile binder phase for use with AlMgB14 and other hard materials. The ductile binder phase, a cobalt-manganese alloy, is used in appropriate quantities to tailor good hardness and reasonable fracture toughness for hard materials so they can be used suitably in industrial machining and grinding applications.Type: GrantFiled: September 23, 2003Date of Patent: July 26, 2005Assignee: Iowa State University Research Foundation, Inc.Inventors: Bruce A. Cook, Alan Russell, Joel Harringa
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Patent number: 6835349Abstract: A boron containing ceramic-aluminum metal composite is formed by mixing a boron containing ceramic with a metal powder comprised of aluminum or alloy thereof, shaping the mixture into a porous preform, contacting the preform with an infiltrating metal comprised of aluminum or alloy thereof that melts at a lower temperature than the metal powder and heating to a temperature sufficient to melt the infiltrating metal, but insufficient to melt the metal powder, such that the infiltrating metal infiltrates the porous preform to form the composite. The composite that is formed may be used for vehicular parts.Type: GrantFiled: August 22, 2002Date of Patent: December 28, 2004Assignee: The Dow Chemical CompanyInventors: Aleksander J. Pyzik, Uday V. Deshmukh, Nicholas M. Shinkel, Tim L. Allen
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Patent number: 6814775Abstract: A sintered cubic boron nitride (cBN) compact for use in a tool is composed of between about 60 and 80 vol-% cBN having a volumetric mean particle size of between about 3 to 6 &mgr;m and between about 40 and 20 vol-% of a ceramic binder phase. The ceramic binder is composed of between about 20 and 60 vol-% of one or more of a carbide, nitride, or boride of a Group IVB or VIB metal, and between about 40 and 80 vol-% of one or more of carbides, nitrides, borides, or oxides of aluminum. The cBN compact additionally contains between about 3 and 15 wt-% tungsten. The cBN compacts are especially useful in machining iron and like chemically reactive parts, especially where such parts are powder metal parts.Type: GrantFiled: May 14, 2003Date of Patent: November 9, 2004Assignee: Diamond Innovations, Inc.Inventors: Robert Dean Scurlock, Stephen Lee Dole
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Patent number: 6802883Abstract: An iron-based sintered alloy, which consists of from 0.5 to 5% of Ni, from 0.5 to 4% of Cr, from 0.5 to 2% of C, the balance being Fe and unavoidable impurities, and which has a micro-structure comprising an iron-based matrix containing Ni and a part of Cr as solutes and carbides containing the other part of Cr and dispersed in the matrix. The iron-based sintered alloy is appropriate for use as a valve seat of an internal combustion engine. Wear resistance is maintained at a moderate level while the additive amount of alloying elements is decreased to attain low cost.Type: GrantFiled: March 10, 2003Date of Patent: October 12, 2004Assignee: Kabushiki Kaisha RikenInventors: Hiroji Henmi, Akiyoshi Ishibashi
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Publication number: 20040166013Abstract: When an R-T-B system rare earth permanent magnet is obtained by a mixing method to obtain a sintered body with a composition consisting essentially of 25% to 35% by weight of R (wherein R represents one or more rare earth elements, providing that the rare earth elements include Y), 0.5% to 4.5% by weight of B, 0.02% to 0.6% by weight of Al and/or Cu, 0.03% to 0.25% by weight of Zr, 4% or less by weight (excluding 0) of Co, and the balance substantially being Fe, wherein a coefficient of variation (CV) showing the dispersion of Zr is 130 or lower, Zr is contained in a low R alloy. This sintered body enables to inhibit the grain growth, while keeping the decrease of magnetic properties to a minimum, and to improve the suitable sintering temperature range.Type: ApplicationFiled: September 29, 2003Publication date: August 26, 2004Applicant: TDK CORPORATIONInventors: Gouichi Nishizawa, Chikara Ishizaka, Tetsuya Hidaka, Akira Fukuno
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Patent number: 6759005Abstract: The present invention relates to a method of manufacturing sputtering targets doped with non-metal components including boron, carbon, nitrogen, oxygen and silicon. A powder process is utilized whereby alloyed powders, which contain non-metal elements of B/C/N/O/Si and non-metal containing phases of less than ten microns in microstructure, are blended, canned and subjected to hot isostatic press consolidation. The sputtering targets of the present invention avoid spitting problems during sputtering of the target material on a substrate.Type: GrantFiled: July 23, 2002Date of Patent: July 6, 2004Assignee: Heraeus, Inc.Inventor: Wenjun Zhang
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Patent number: 6746545Abstract: An R—Fe—B permanent magnet wherein R is Nd or a combination of Nd with a rare earth element is prepared by casting an R—Fe—B alloy, crushing the alloy in an oxygen-free atmosphere of argon, nitrogen or vacuum, effecting comminution, compaction, sintering, aging, and cutting and/or polishing the magnet to give a finished surface. The magnet is then heat treated in an argon, nitrogen or low-pressure vacuum atmosphere having a limited oxygen partial pressure, obtaining a highly oil resistant sintered permanent magnet having corrosion resistance and hydrogen barrier property even in a high pressure hot environment of refrigerant and/or lubricant as encountered in compressors.Type: GrantFiled: May 30, 2001Date of Patent: June 8, 2004Assignee: Shin-Etsu Chemical Co., Ltd.Inventors: Kazuo Tamura, Masanobu Shimao, Ryuji Hamada, Takehisa Minowa
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Patent number: 6723279Abstract: Golf club structures, including club heads and shafts, composed of composites comprised of a matrix of metal, such as an aluminum alloy, or a plastic material and a fiber such as graphite or a ceramic, which may be whiskerized, and which may also be selectively weighted as in the toe and heel of a club head, with heavy particles such as tungsten metal. The club structure may also be surface hardened by applying a coating of fullerenes to a metal club structure and heat treating it to produce a hard coating of metal carbide, preferably by coating a titanium golf club structure with fullerenes and heat treating the coated structure to produce a titanium carbide surface.Type: GrantFiled: March 15, 1999Date of Patent: April 20, 2004Assignee: Materials and Electrochemical Research (MER) CorporationInventors: James C. Withers, Raouf O. Loutfy, Sion M. Pickard, Kenneth J. Newell, William B. Kelly
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Patent number: 6723387Abstract: A thermal spray method for the fabrication of ceramic/metal and ceramic/ceramic hardcoating for wear applications. The method makes use of feedstock powder, composed of micron-scale aggregates of hard phase material particles that are either mixed or coated with a readily fusible nano-scale binder phase material. Thus, during thermal spraying, the nanostructured material undergoes rapid melting while the aggregated material is heated but not necessarily melted. A dense coating is formed when the molten nano-material fills the available pore spaces between the heated and softened aggregates, providing a strong and tough matrix for the consolidated material. Optimal wear properties are achieved when the volume fraction of aggregated particles is high, typically in the range of 0.5-0.9. Aggregated material may be composed of one, two or more particles of difference sizes and/or compositions, with particle size distribution that gives high packing density for the hard phase.Type: GrantFiled: September 19, 2002Date of Patent: April 20, 2004Assignee: Rutgers UniversityInventors: Bernard H. Kear, Ganesh Skandan
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Publication number: 20040067154Abstract: A melt of an alloy, represented (Fe1-mTm)100-x-y-zQxRyMz, where T is Co and/or Ni, Q is B and/or C, R is at least one rare-earth element, M is selected from Al, Si, Ti, V, Cr, Mn, Cu, Zn, Ga, Zr, Nb, Mo, Ag, Hf, Ta, W, Pt, Au and Pb; 10 at %≦x≦35 at %; 2 at %≦y≦10 at %; 0 at %≦z≦10 at %; and 0≦m≦0.5, is prepared. Next, the melt is brought into contact with, and rapidly cooled and solidified by, the surface of a rotating chill roller. The melt is teemed onto a guide member, of which the guide surface defines a tilt angle with a horizontal plane, runs down on the guide surface, and then is fed through at least one tubular hole onto a contact area on the surface of the chill roller.Type: ApplicationFiled: June 27, 2003Publication date: April 8, 2004Applicant: Sumitomo Special Metals Co., LtdInventor: Hirokazu Kanekiyo
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Patent number: 6669788Abstract: A Fe—B—R type permanent magnetic, consisting of: 13-19 atomic % R, where R consists essentially of a mixture of rare earth elements Nd and/or Pr, and Ce, where Ce is between 0.2 and 5.0 wt. % of R; 4-20 atomic % B, and the balance comprising Fe. In a preferred aspect, R comprises 15-16 atomic % B; of which Ce is approximately 0.5% and the remaining rare earths Pr and Nd are in a ratio of 3:1. A process of producing a Fe—B—R permanent magnet as described above, and a Fe—B—R magnetic material made by such process.Type: GrantFiled: May 21, 2001Date of Patent: December 30, 2003Assignees: General Electric Company, Batou Iron and Steel (Group) Co. LTDInventors: Chen Pei Xin, Wang Biao, Ni De Zhen, Mark Gilbert Benz, Juliana C. Shei
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Patent number: 6648984Abstract: A compact is produced from an alloy powder for R—Fe—B type rare earth magnets including particles having a size in a range of about 2.0 &mgr;m to about 5.0 &mgr;m as measured by a light scattering method using a Fraunhofer forward scattering in a proportion of approximately 45 vol. % or more and particles having a size larger than about 10 &mgr;m in a proportion of less than about 1 vol. %. The compact is then sintered to obtain a R—Fe—B type rare earth magnet having an average crystal grain size in a range of about 5 &mgr;m to about 7.5 &mgr;m, and an oxygen concentration in a range of about 2.2 at. % to about 3.0 at. %.Type: GrantFiled: September 24, 2001Date of Patent: November 18, 2003Assignee: Sumitomo Special Metals Co., Ltd.Inventors: Shigeru Takaki, Ken Makita
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Patent number: 6641776Abstract: X-ray imageable articles, for instance surgical implements or parts therefore which are used in minimally invasive surgical procedures, may be prepared by a process including the steps of: (a) preparing a mixture composition comprising: i) radiolucent particulate material selected from ceramic materials, metallurgic materials, and combinations thereof and having a particulate size of no more than 40 microns, ii) radiopaque particulate material selected from ceramic materials, metallurgic materials, and combinations thereof and having a particulate size of no more than 40 microns, and (iii) at least one polymeric binder material; (b) injection molding the mixture composition into a preform; (c) optionally removing the binder material from the preform; and (d) sintering the preform.Type: GrantFiled: November 15, 2000Date of Patent: November 4, 2003Assignee: SciMed Life Systems, Inc.Inventors: Timothy J. Weaver, Dion Mraz
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Patent number: 6635098Abstract: A low cost titanium, titanium alloy material, or Ti matrix composite comprising clean and divided titanium turnings that are blended with titanium, titanium alloy powder, and/or ceramic powder and consolidated is provided. A method of making the material is also provided. The low cost material is formed into preshapes, such as a billet, which is subsequently used as feedstock for extrusion, forging, casting, or rolling.Type: GrantFiled: February 12, 2002Date of Patent: October 21, 2003Assignee: Dynamet Technology, Inc.Inventors: Stanley Abkowitz, Susan M. Abkowitz, Harold L. Heussi, Kevin M. McCarthy
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Patent number: 6630100Abstract: A rectangular pipe is molded by mixing aluminum powder with powder of a neutron absorbing material, molding a premolded body by means of cold isostatic pressing (CIP), canning the premolded body, sintering the premolded body by means of hot isostatic pressing (HIP), performing outer cutting and end face cutting on the can after the sintering, taking a billet out of the can, and extruding this billet.Type: GrantFiled: April 9, 2001Date of Patent: October 7, 2003Assignee: Mitsubishi Heavy Industries, Ltd.Inventors: Kazuo Murakami, Yasuhiro Sakaguchi, Toshiro Kobayashi, Toyoaki Yasui
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Patent number: 6616829Abstract: A method of preparing carbonaceous blocks or bodies for use in a cathode in an electrolytic cell for producing aluminum wherein the cell contains an electrolyte and has molten aluminum contacting the cathode, the cathode having improved wettability with molten aluminum. The method comprises the steps of providing a carbonaceous block and a boron oxide containing melt. The carbonaceous block is immersed in the melt and pressure is applied to the melt to impregnate the melt into pores in the block. Thereafter, the carbonaceous block is withdrawn from the melt, the block having boron oxide containing melt intruded into pores therein, the boron oxide capable of reacting with a source of titanium or zirconium or like metal to form titanium or zirconium diboride during heatup or operation of said cell.Type: GrantFiled: April 13, 2001Date of Patent: September 9, 2003Assignee: EMEC ConsultantsInventors: Rudolf Keller, David G. Gatty, Brian J. Barca
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Patent number: 6572671Abstract: In the invention, a stainless steel powder of the desired composition is either directly mixed with a h-BN powder, compressed and sintered or the stainless steel powder is compressed, impregnated with a solution containing h-BN and then sintered or compressed, sintered and then impregnated with a solution containing h-BN. The sintered bodies in all the aforementioned cases may be resin impregnated. Steel body formation may be done by traditional press compacting or, alternatively, by injection molding steel powder in molds (metal injection molding, MIM).Type: GrantFiled: August 9, 2000Date of Patent: June 3, 2003Assignee: Maxtech Manufacturing IncInventors: Tandjaoui Baazi, Roch Angers, Danielle Lacombe
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Patent number: 6551371Abstract: A titanium-based composite material according to the present invention is characterized in that it comprises: a matrix containing a titanium (Ti) alloy as a major component, and titanium compound particles and/or rare-earth element compound particles dispersed in the matrix, wherein the matrix contains 3.0-7.0% by weight of aluminum (Al), 2.0-6.0% by weight of tin (Sn), 2.0-6.0% by weight of zirconium (Zr), 0.1-0.4% by weight of silicon (Si) and 0.1-0.5% by weight of oxygen (O), the titanium compound particles occupy 1-10% by volume, and the rare-earth element compound particles occupy 3% by volume or less. With this arrangement, it is possible to obtain a titanium material, which is good in terms of the heat resistance, hot working property, specific strength, and so on.Type: GrantFiled: January 22, 2001Date of Patent: April 22, 2003Assignees: Kabushiki Kaisha Toyota Chuo Kenkyusho, Toyota Jidosha Kabushiki KaishaInventors: Tadahiko Furuta, Takashi Saito, Hiroyuki Takamiya, Toshiya Yamaguchi
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Patent number: 6521013Abstract: A niobium sintered body for a capacitor, which exhibits an LC value of not larger than 300 &mgr;A/g as measured after an electrolytic oxide film is formed thereon. The sintered body preferably exhibits a product (CV) [i.e., a product of capacity (C) with electrolysis voltage (V)] of at least 40,000 &mgr;F·V/g. The sintered body is produced by sintering a niobium powder containing at least one niobium compound selected from niobium nitride, niobium carbide and niobium boride. A capacitor manufactured from the sintered body has a large capacity per unit weight and good leak current characteristics. Especially, a sintered body made of a niobium powder having a large average degree of roundness has a relatively large porosity and a good packed density, and a capacitor manufactured from this sintered body has a large capacity and good withstand voltage characteristics.Type: GrantFiled: February 5, 2001Date of Patent: February 18, 2003Assignee: Showa Denko Kabushiki KaishaInventors: Kazumi Naito, Atsushi Shimojima
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Publication number: 20020144754Abstract: An R—T—B rare earth sintered magnet containing an R2T14B-type intermetallic compound as a main phase and thus having improved squareness ratio is produced by carrying out a reduction and diffusion method comprising the steps of (a) mixing oxide powder of at least one rare earth element R, T-containing powder, wherein T is Fe or Fe and Co, B-containing powder, and a reducing agent such as Ca, (b) heating the resultant mixture at 900-1350° C. in a non-oxidizing atmosphere, (c) removing reaction by-products from the resultant reaction product by washing, and (d) carrying out a heat treatment for Ca removal by heating the resultant R—T—B rare earth alloy powder at 900-1200° C. in vacuum at 1 Torr or less, followed by pulverization of the resultant alloy powder bulk, molding, sintering in vacuum, heat treatment, and surface treatment. The alloy powder bulk obtained by the heat treatment for Ca removal is preferably pulverized after removal of its surface layer.Type: ApplicationFiled: November 24, 1999Publication date: October 10, 2002Applicant: HITACHI METALS, LTD.Inventors: HISATO TOKORO, NOBUHIKO FUJIMORI
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Patent number: 6444048Abstract: Processes for the preparation of a sintered alloy comprising R2Fe14B as a magnetic phase constituting a main phase include a binary alloy process wherein a main phase alloy having a lower R content than the above phase is mixed with a grain boundary phase alloy rich in R component and serving as a liquid phase in the sintering in order to prepare a mixture to be used as the starting material. The conventional main phase alloy has a structure comprising the R2Fe14B phase and, in addition, a large amount of an easily oxidizable lamella R-rich phase and a harmful dendrite &agr; phase. On the other hand, the main phase alloy of the invention has a low dendrite a phase content and a low lamella R-rich phase and contains a lamella &agr; Fe phase. This contributes to excellent oxidation resistance and improved properties of the magnet. The preparation of a sintered magnet by mixing the main phase alloy with the grain boundary phase alloy by the binary alloy method can reduce abnormal growth of crystal grains.Type: GrantFiled: June 19, 2000Date of Patent: September 3, 2002Assignee: Showa Denko K.K.Inventors: Hiroshi Hasegawa, Yoichi Hirose
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Publication number: 20020117237Abstract: A compact is produced from an alloy powder for R—Fe—B type rare earth magnets including particles having a size in a range of about 2.0 &mgr;m to about 5.0 &mgr;m as measured by a light scattering method using a Fraunhofer forward scattering in a proportion of approximately 45 vol. % or more and particles having a size larger than about 10 &mgr;m in a proportion of less than about 1 vol. %. The compact is then sintered to obtain a R—Fe—B type rare earth magnet having an average crystal grain size in a range of about 5 &mgr;m to about 7.5 &mgr;m, and an oxygen concentration in a range of about 2.2 at. % to about 3.0 at. %.Type: ApplicationFiled: September 24, 2001Publication date: August 29, 2002Applicant: Sumitomo Special Metals Co., Ltd.Inventors: Shigeru Takaki, Ken Makita
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Publication number: 20020106297Abstract: The invention relates to a Co-base target made of a sintered powder, having a restrained amount of oxygen, and a producing method thereof. The target contains from more than 10 to not more than 25 at % of B and not more than 100 ppm of oxygen. It may contain 30≧Pt≧5 at%, 30≧Cr≧10 at%, 10≧Ta>0 at% and/or 30≧Ni>0 at%. It may contain also from more than 0 (zero) to not more than 15 at% in total of one or more elements selected from the group consisting of Ti, Zr, Hf, V, Nb, Mo, W, Cu, Ag, Au, Ru, Rh, Pd, Os, Ir and rare earth elements. The target is produced by melting a Co-base alloy together with an additive B in an amount of from more than 10 to not more than 25 at% whereby deoxidizing, rapidly cooling the molten metal to produce an alloy powder and sintering the alloy powder.Type: ApplicationFiled: November 29, 2001Publication date: August 8, 2002Applicant: HITACHI METALS, LTD.Inventors: Tomonori Ueno, Hideo Murata, Shigeru Taniguchi, Hide Ueno
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Publication number: 20020057982Abstract: Rare earth alloy powder having an oxygen content of 50 to 4000 wt. ppm and a nitrogen content of 150 to 1500 wt. ppm is compacted by dry pressing to produce a compact. The compact is impregnated with an oil agent and then sintered. The sintering process includes a first step of retaining the compact at a temperature of 700° C. to less than 1000° C. for a period of time of 10 to 420 minutes and a second step of permitting proceeding of sintering at a temperature of 1000° C. to 1200° C. The average crystal grain size of the rare earth magnet after the sintering is controlled to be 3 &mgr;m to 9 &mgr;m.Type: ApplicationFiled: September 19, 2001Publication date: May 16, 2002Inventors: Futoshi Kuniyoshi, Hitoshi Morimoto
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Patent number: 6387196Abstract: A process for producing a particle-reinforced titanium alloy includes the steps of: heating a titanium alloy in which ceramic particles having a thermodynamically stable property are dispersed in a temperature range of not less than &bgr;-transus temperature; and cooling the titanium alloy to pass through the &bgr;-transus temperature at a cooling rate of 0.1-30° C./second. The process can further include, before the heating step, the step of compressing the titanium alloy in a two phase temperature range of &agr;+&bgr; thereof or in a temperature range of not less than &bgr;-transus temperature.Type: GrantFiled: October 18, 1999Date of Patent: May 14, 2002Assignees: Toyota Jidosha Kabushiki Kaisha, Kabushiki Kaisha Chuo Kenkyusho, Aisan Kogyo Kabushiki KaishaInventors: Toshiya Yamaguchi, Tadahiko Furuta, Takashi Saito, Kouji Sakurai
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Patent number: 6368551Abstract: The method for preparation of sintered permanent magnets according to the present invention comprises the steps of: mixing fully fine powder of a crystalline mother alloy for permanent magnet containing a rare-earth element, Fe and B as the essential components with fine powder of zinc oxide, compaction molding the resulted mixture in the presence of a magnetic field, sintering the compacted mixture in vacuum to cause generation of oxygen and metallic zinc by thermal decomposition of the zinc oxide; segregation of a part of metallic component in the mother alloy at the boundary and inside of the mother alloy crystal; formation of amorphous metallic oxide by forced oxidation of the segregated metal with the generated oxygen; crystallization of the amorphous metallic oxide; formation of an epitaxial junction between the crystallized metallic oxide and the mother alloy crystal; and evaporation of the metallic zinc into the vacuum, and quenching the sintered compact.Type: GrantFiled: August 16, 2000Date of Patent: April 9, 2002Assignee: Sanei Kasei Co., Ltd.Inventors: Shigenobu Sekine, Yuko Kawasaki, Yoshiki Kuwabara, Hiroji Sato, Minoru Narita, Kazushi Suzuki, Koichi Tono, Keiji Okada, Kenji Sakaguchi, Mitsuhisa Hirata
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Patent number: 6350294Abstract: The present invention relates to powder-metallurgically produced composite material comprising a matrix of a metal with a melting point of at most 1,200° C. and a granular additive which consists of at least two refractory components embedded in said matrix, characterized in that the refractory components are present as mixed crystals or intermetallic phases. In one embodiment of the invention one or a first group of refractory component(s) has a melting point in the range of 1,500 to 2,400° C. and the second or the second group of refractory component(s) has a melting point above 2,400° C. The composite material is produced by heating a pulverized mixture of the refractory components, thus converting it into a mixed crystal or an intermetallic phase, and then combining the powder obtained by cooling and pulverizing with a metal matrix having a melting point of at most 1,200° C. by means of powder-metallurgy.Type: GrantFiled: January 25, 2000Date of Patent: February 26, 2002Assignee: Louis Renner GmbHInventors: Gerd Renner, Udo Siefken
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Patent number: 6338907Abstract: The invention relates to an abrasive tool comprising a support body and at least one abrasive element connected thereto. Said abrasive element has an abrasive grain which is joined by a sintered metal. The sintered metal used for joining is copper-coated iron and is alloyed with metal borides, metal carbides and/or metal silicides and also with tin.Type: GrantFiled: April 3, 2000Date of Patent: January 15, 2002Assignee: Tyrolit Schleifmittelwerke Swarovski K.G.Inventor: Wolfgang Strelsky