Abstract: An electrical contact formed of a mixture of finely divided electrically conductive metal doped with graphite or cadmium oxide. A thin coating of the electrically conductive metal is disposed upon the side of the contact which is adapted to be welded or brazed to an electrically conductive support. The electrical contact is made by mixing the finely divided cadmium oxide and pressing the mixture into a desired shape. A slurry of conductive metal is then sprayed on one side of the contact. After coating, the contact is sintered at a temperature less than the melting point of the electrically conductive material, whereby the contact is formed and the coating is firmly attached to it. The invention is particularly useful with silver or copper-based electrical contacts.

Abstract: A high-purity high-melting metal target or high-purity high-melting metal silicide target for LSI electrodes having an alkali metal content of not more than 100 ppb and a radioactive element content of not more than 10 ppb is provided by a wet purification process followed by a series of dry processings. Preferably the high-melting metal is molybdenum, tungsten, titanium, niobium or tantalum. More preferably, the high-melting metal is molybdenum.

Abstract: A camshaft is prepared from separately formed cams and a shaft. The cams may for example be formed by sintering. The cams are provided with holes which are under-sized and are provided with serrations. They are located on a correspondingly shaped dummy shaft in their required relative orientations and angular positions. Next, the cams are clamped in these positions and the dummy shaft removed. The cams are then heated to red heat and the serrated holes in them broached to bring them to their final size and to concentricity. Finally, a shaft having an exterior profile corresponding to the shape and size of the broached profile of the holes, at ambient temperature, is introduced into the holes and the cams are then cooled so that they shrink fit on to the shaft so ensuring that they are accurately positioned on the shaft. The cams are then released from the jig to give a finished camshaft.

Abstract: A process for producing strip from particulate metallic material in which a slurry comprising a suspension of particulate metallic material in a solution of water containing a film forming binder material is deposited as a coating onto a support surface and is heated to gel the binder and to dry the slurry coating, the dried strip subsequently being removed from the support surface and rolled to effect compaction thereof. The ratio of particulate metallic material to water content of the slurry lies within the range 3.4:1 and 4.2:1 to ensure good flowability of the slurry coating and to produce the required flat profile in the rolled strip.

Abstract: A hollow charge, or plate charge, lining, and a projectile charge coating, made from a composite material of tungsten and copper. Indicated are material proportions, grain sizes, and manufacturing methods.

Abstract: An improvement is disclosed in a method for producing a metal article of high density comprising pressing a metal powder at a sufficient pressure to form a green article and sintering said green article at a sufficient temperature for a sufficient time to form a sintered article, the improvement being pressing the sintered article at a sufficient temperature for a sufficient time at a sufficient pressure of a non-oxidizing atmosphere to produce the final high density article.

Abstract: The present invention concerns the manufacture of bars, wires or profiled elements by hot transformation which may be followed by cold transformation. The invention particularly concerns a new process for the manufacture of a composite billet for hot transformation as well as a method for the manufacture of products which are difficult to transform by making use of such a composite billet.

Abstract: A method of producing a high density tungsten alloy sheet product is disclosed which utilizes as a starting material a thin-gage sheet or foil substrate of a first alloy constituent, such as pure iron or an alloy thereof. A prescribed mixture of tungsten metal powder and a second metal alloy constitutent powder, such as nickel, is loaded on the substrate and partially consolidated in a protective atmosphere furnace to form a porous tungsten alloy skeleton which is also partially bonded to the substrate. The product is then preferably cooled in a protective atmosphere and sheared into desired lengths. The sized pieces are then further heated in a protective atmosphere at gradually increasing temperatures to a point above the melting point of the substrate, whereupon the substrate sheet or foil melts and infiltrates the porous tungsten alloy skeleton to complete the densification of the product.

Abstract: A copper-rich metal shape is produced by forming a coherent forerunner shape consisting essentially of cupreous powder, said powder containing a proportion of copper oxide sufficient for facilitating the obtaining of a high sinter density in sintered porous mass, and in a reducing atmosphere at temperature that will sinter copper present, converting said forerunner shape into a porous sintered mass virtually devoid of copper oxide. Said porous mass can be worked so virtually full density if desired.

Abstract: A process for the production of valve seat rings by powder metallurgy wherein molybdenum disulfide in the range of about 0.5% to 1.5% by weight is added to a powder mixture containing 0.8% to 1.5% by weight graphite, 1.0% to 4% by weight lead, 0.5% to 5% by weight nickel, 1.2% to 1.8% by weight molybdenum, 9.6% to 14.4% by weight cobalt, and the remainder iron. The resulting powder mixture is pressed into valve seat rings at a pressing force between 40 and 60 and preferably 50 KN/cm.sup.2. The rings are then sintered in a neutral atmosphere at a temperature of 1100.degree. C. to 1200.degree. C., finally compressed at a pressing force above 120 KN/cm.sup.2 and heat-treated if required. The resulting valve seat rings have greatly improved wear properties when used in internal combustion engines using lead-free gasoline.

Abstract: A process for making a strip or sheet comprising dispersion strengthened metal or dispersion strengthened metal alloy which comprises rolling directly from dispersion strengthened metal powder to a green strip or sheet density of from at least 90% to 95% of theoretical density, sintering the green strip or sheet in an inert atmosphere at a temperature and for a period of time sufficient to form a rigid body; reducing the thickness of the strip or sheet by at least 25% by cold rolling or hot rolling and resintering at sintering temperature of at least about 1800.degree. F. for 40 to 75 or more minutes.

Abstract: The present invention discloses a method for densifying previously sintered parts constructed of powdered metals, ceramics or the like to nearly 100% theoretical density. The method of the present invention comprises heating the parts containing binder and hard phase above their liquid phase temperature and then applying a pressure in a predetermined range to the parts for a predetermined period of time and simultaneously maintaining the parts at or above their liquid phase temperature. This pressure range is set so that the pressure is below the pressure necessary to overcome the capillary force acting on the binder to keep the binder from entering the voids but above the pressure necessary to physically move or collapse the microstructure inwardly, thus filling the voids with a homogenous mixture of binder and hard phase. The method of the present invention achieves complete closure of even large voids and the elimination of substantially all porosity within the part.

Abstract: The invention relates to a multi-lobe composite casing, the inner wall of said casing being constituted by several adjacent cylindrical sectors, each enveloping a screw over the portion of the latter outside the penetration zone. According to the invention the hardest metal layer deposited on the inner wall of the body is applied in the form of a powder containing the desired constituents. This powder is welded to the metallic inner base wall by means of a plasma torch operating on the principle of a transferred arc or a semi-transferred arc. The invention is applied to machines with several overlapping screws of the extruder type.

Abstract: An article comprising a first portion which is formed porously by sintering of an alloy or cermet material and a second portion which is formed of a metal and intimately bonds to the first portion. For example, the article is a rocker arm for an automotive internal combustion engine, in which first portion is the wear-resistant tip portion and the second portion the body portion. The second portion is formed by molten metal forging, with the sintered first portion set in the mould as an insert, such that the molten metal under pressure is forced to infiltrate into the pores of the sintered first portion at least in a region contiguous to the interface between the first and second portions. This article features very high strength of the bond at the interface between the first and second portions.

Abstract: A dual alloy cooled turbine is manufactured by casting a hollow cylinder of first nickel-base alloy material with high creep resistance to produce directionally oriented grain boundaries. A preform of a second nickel-base alloy material with high tensile strength and high low-cycle-fatigue strength is diffusion bonded into the bore of the hollow cylinder by subjecting the cylinder and preform to hot isostatic pressing. The resulting cylindrical block is cut into thin precisely flat wafers. A plurality of alignable holes for forming fluid cooling passages are photochemically etched into the individual wafers. The wafers then are laminated by vacuum diffusion bonding techniques, with the holes aligned to form fluid cooling passages. The resulting laminated block is machined to produce the turbine wheel with turbine blades through which the cooling passages extend.

Abstract: Manufacture of a workpiece from a creep-resistant nickel superalloy which is hardened by means of an oxide dispersion, by a powder-metallurgical process in which the mechanically alloyed powder is subjected to an isothermal or quasi-isothermal hot-rolling operation, in the course of which the powder particles are converted into a flake-shaped form with a pronounced longitudinal axes, and the rolled powder is introduced into a steel container and is compressed by isostatic hot-pressing. The workpiece is afterwards subjected to an annealing treatment which is designed to develop a coarse grain size. A preferred embodiment comprises the introduction of the powder into the mold or container in an oriented manner, in order to obtain a stratified packing of the powder, and an annealing treatment which is designed to develop a coarse grain size and is performed as a zone-annealing treatment.

Abstract: A composite material containing dispersed particles is manufactured by disposing within a mold a porous shaped article of ceramic particles, then pouring a molten metal into the mold, compressing the contents of the mold, subsequently allowing the molten metal to solidify, and subjecting the resultant solidified composite to a plasticizing treatment.

Abstract: A canless method for hot working a nickel-base gas atomized alloy powder. The powder is blended with nickel powder, consolidated and sintered to a sufficient green strength. The surface of the resultant form is sealed to create an oxygen impervious layer so as to prevent oxidation therein. The sealed surface, in a sense, acts as a can. The form is then reheated and hot worked.

Abstract: The invention relates to a powder metallurgical method for producing high speed steel products, the shape of which is close to the desired final shape of the product, i.e. according to the so called near net shape technique.

Abstract: A method of producing rocket combustors wherein in forming an outer cylin by a powder metallurgical method on the outer side of a cylinder provided on its outer periphery with a cooling wall of channel construction having a plurality of grooves (14), an Ni electroforming layer is formed on the outer side of the outer cylinder, and also a method of producing rocket combustors wherein an outer cylinder is of multilayer construction having two or more layers.

Abstract: The present invention provides a method for consolidating rapidly solidified, transition metal alloys which includes the step of compacting a plurality of alloy bodies at a temperature ranging from about 0.90-0.99 Tm (melting temperature in .degree.C.) for a time period ranging from about 1 min to 24 hours. The alloy bodies contain at least two transition metal elements and consist essentially of the formula (Fe,Co and/or Ni).sub.bal (W, Mo, Nb and/or Ta).sub.a (Al and/or Ti).sub.b (Cr).sub.c (B and/or C).sub.d (Si and/or P).sub.e, wherein "a" ranges from about 0-40 at. %, "b" ranges from about 0-40 at. %, "c" ranges from about 0-40 at. %, "d" ranges from about 5-25 at. %, and "e" ranges from about 0-15 at. %. The alloy bodies also have a substantially homogeneous and optically featureless structure.

Abstract: To increase the creep strength of a titanium-containing alloy which also contains chromium, the alloy powder is heated in the presence of ammonia at a temperature of the order of 700.degree. C. so as to form a layer of chromium nitride(s) on the particles and is then heated further in an inert atmosphere at a temperature between 1000.degree. C. and 1150.degree. C. to dissociate the chromium nitride(s) thereby effecting nitriding of the titanium to titanium nitride which affords dispersion-strengthening of the alloy.

Abstract: A composite material for a sliding member has a back metal layer and a graphite-containing phosphor bronze sintered layer bonded to the back metal layer. The graphite-containing phosphor bronze sintered layer consists essentially of 0.03 to 1 wt % phosphorus, 7.5 to 16 wt % tin, 1 to 8 wt % graphite and the balance copper, and is constituted by phosphor bronze powder passing through a 200-mesh screen and a graphite powder passing through a 350-mesh screen. Also disclosed is a method of manufacturing the above-mentioned composite material for a sliding member.

Abstract: The present invention discloses a method for densifying previously sintered parts constructed of powdered metals, ceramics or the like to nearly 100% theoretical density. The method of the present invention comprises heating the parts containing binder and hard phase above their liquid phase temperature and then applying a pressure in a predetermined range to the parts for a predetermined period of time and simultaneously maintaining the parts at or above their liquid phase temperature. This pressure range is set so that the pressure is below the pressure necessary to overcome the capillary force acting on the binder to keep the binder from entering the voids but above the pressure necessary to physically move or collapse themicrostructure inwardly, thus filling the voids with a homogeneous mixture of binder and hard phase. The method of the present invention achieves complete closure of even large voids and the elimination of substantially all porosity within the part.

Abstract: A valve seat for ball valves comprises a ring-shaped or annular body fabricated of sintered metal particles having interparticulate spaces which are substantially completely filled with graphite. The seat is fabricated by pumping a dispersion of colloidal graphite in a liquid carrier through the matrix of a preformed ring-shaped sintered metal body, thereafter heating the body to drive off any portion of the liquid carrier which remains in the interparticulate spaces of the body, and then coining the body to collapse any voids which remain in the body and to mechanically bind into the body the graphite which has been trapped in said interparticulate spaces during the pumping step.

Abstract: The ductility and electrical conductivity of an age hardened spinodally decomposed copper-nickel-tin alloy can be improved, without detracting from the alloy's strength properties, by reducing the nickel content of the alloy and adding from about 3.5 to about 7 weight percent, based upon the weight of the alloy, of cobalt.

Abstract: A method of consolidating a metallic or ceramic body is disclosed. The method comprises the steps of forming an article of manufacture from powdered metal or ceramic; sintering the article of manufacture so as to increase the strength thereof; providing a bed of heated, generally spheroidal ceramic particles; and compacting the article of manufacture embedded in the heated bed under pressure to thereby consolidate the article into a dense, desired shape.

Abstract: A method of consolidating a metallic body is disclosed. The method comprises the steps of forming an article of manufacture from powdered metal; sintering the article of manufacture so as to increase the strength thereof; coating the article with a sacrificial layer of ceramic; providing a bed of heated, generally spheroidal ceramic particles; compacting the coated article of manufacture embedded in the heated bed under pressure to thereby consolidate the article into a dense, desired shape; and, removing said sacrificial coating such that the surface of the article remains substantially free of process-related imperfections.

Abstract: The invention is concerned with the problem of joining ceramic components to metal components.A composite ceramic-metal component is proposed, e.g. a rotor disc for a gas turbine engine (see FIG. 2), in which the main body of the component is made from a ceramic, e.g. Silicon Nitride, but the areas at which attachment is to be made to a metal component is formed from metal compacted onto the ceramic by a hot isostatic pressing process.The method of manufacture described is to form a ceramic core with holes appropriately positioned in it where a connection is to be made to another component, surround the core with a powdered metal, e.g. a Nickel-based superalloy, ensuring that the holes also fill with powder, compacting the powder by hot isostatic pressing, and then machining away unwanted metal.

Abstract: A process for making sintered metal articles of high strength in which a flowable mass of metallic particles is initially formed into a green compact having shape stability in a forming machine of the type used in the fabrication of sand cores in the metal casting field. The green compact is then subjected to sintering and the sintered body may be pressed, forged or mechanically shaped in other ways. The core blowing or core-sand slinging machine used to produce the green metal compact is surprisingly effective in producing a dense, reproducible structure in light of the fact that sand cores for casting purposes are intentionally made frangible to enable them to be removed effectively from the casting.

Abstract: A process and a product produced thereby, for forming rod or bar or tube stock or strip, comprising a sheath and a densified dispersion strengthened metal core. Powdered dispersion strengthened copper is put into a metal can and compressively reduced to size and density. The relationship between the tensile strength of the core when fully densified and the cold worked tensile strength of the can is important to the nature of the product.

Abstract: There is described a new material for jewelry and commodities which has a relatively low density and also is low carat but resistant to oxidation and corrosion. It consists of a noble metal or alloy and 1 to 70 volume % glass, whereby as glass there is used a glass frit having a transformation temperature of 300.degree. to 500.degree. C. and a softening interval of over 80.degree. C. There is also described a process for its production.

Abstract: A process for producing a wrought product of improved ductility from substantially noncompactible prealloyed metal powder. The process comprises the steps of: comminuting substantially noncompactible prealloyed metal powder so as to flatten the particles thereof; heating the comminuted particles of metal powder at an elevated temperature, the particles adhering and forming a mass during heating; crushing the mass of metal powder; compacting the crushed mass of metal powder; sintering the metal powder; and hot working the metal powder into a wrought product. The wrought product has a chemistry which is substantially the same, with the exception of carbon and certain residuals, as the chemistry of the prealloyed powder.

Abstract: Aluminum alloy atomized powder containing 4 to 15% iron and 1 to 12% cerium or other rare earth metal, when properly compacted and shaped into a useful article, exhibits very high strength at relatively high temperatures. The iron content exceeds the cerium or rare earth metal content, and the powder may contain refractory elements such as W, Mo and others. The powder is produced by atomizing alloyed molten aluminum, preferably in a nonoxidizing atmosphere, and is compacted to a density approaching 100% under controlled conditions including controlled temperature conditions. The alloy may be subsequently shaped by conventional forging, extruding or rolling processes.

Abstract: A powder metallurgical process for producing a wrought product characterized by a low level of residual impurities. The process comprises the steps of: comminuting metal powder to effect a reduction in particle size, at least 60% of the comminuted particles being capable of passing through a -270 mesh Tyler screen; blending the metal powder with a softer metal-bearing powder; heating the blended powder particles at an elevated temperature, the particles adhering and forming a mass during heating; crushing the mass of powder particles; cold-isostatically pressing the crushed mass of powder; sintering the powder in the absence of an encapsulating member under conditions which effect a reduction in the nitrogen, oxygen and carbon levels of the powder; and hot working the sintered powder into a wrought product. The wrought product has less than 0.015% carbon.

Abstract: The invention features a method and resultant article of the method, wherein deagglomerated silicon carbide whiskers are uniformly dispersed and/or distributed in a matrix material, generally a metal. The uniform distribution achieved by the invention greatly enhances the mechanical properties of the composite, such as the ultimate strength. The method comprises the deagglomeration of silicon carbide whiskers prior to mixing with matrix materials.

Abstract: A lens block used to secure an opthalmic lens during its formation by conventional forming equipment wherein the lens block comprises an integrally formed single piece structure of hardened metal material having centering means including a plurality of linearally aligned apertures each having a substantially conical configuration formed directly in the surface of the lens block oppositely disposed to the surface which is interconnected to the lens itself. The lens block is formed from a powdered metal material comprised of hard metal alloys which is sintered and heat treated to attain a desired condition of particle hardness in the upper range of the Rockwell C Scale.

Abstract: A material consisting essentially of tungsten having from 5 to about 20 grains per square millimeter and a hardness on the Rockwell C scale from about 31 to about 35 is suited for armor penetration.

Abstract: A method is described for producing articles having a metal core, an intermediate powder metallurgy layer, and an exterior wear- and chip-resistant layer on the portions thereof requiring the same, which comprises:applying to a bearing metal core, powdered steel alloy containing about 3.5% nickel by weight by cold isostatic compaction in a compressible mold under a pressure of about 6000 atmospheres to provide an intermediate powder metallurgical layer having a density of about 90%;sintering said intermediate layer on said core in an atmosphere of hydrogen at about 1200.degree. C. for about one hour;applying a wear- and chip-resistant layer to selected portions of said sintered intermediate powder metallurgical layer by plasma spraying; andhot isostatically compacting the sprayed article in a thin-walled deep-drawn vessel of low carbon steel having a wall thickness of about 0.

Abstract: A powder metallurgical alloy which comprises a solid solution of molybdenum and from about 10 to about 98 percent by weight tungsten has a dispersed phase of hafnium carbide. The alloy is prepared by mixing powders of hafnium carbide, carbon, molybdenum and tungsten, and subsequently pressing, sintering, and age- or work-hardening.

Abstract: Ductility is controlled by controlling the size of the particles of particulate material and/or the degree of sphericity of the particles, the smaller and/or more spherical the particles, the greater the ductility of the material. The material has preferably spherical pores, preferably hermetic, with a controlled ratio of pore volume to material volume to provide the property of compressibility. The particulate material itself must have the capability of becoming ductile. The ratio of pore volume to total volume of the material is controlled by particle size, sintering profile the property of the material and the initial volume loading of the pre-sintered part (i.e. the ratio of binder to particulate material). Some materials which are not ductile in and of themselves can be formed into ductile and/or compressible materials in accordance with the system of the present invention.

Abstract: The present invention discloses a method for densifying previously sintered parts constructed of powdered metals, ceramics or the like to nearly 100% theoretical density. The method of the present invention comprises heating the parts above their liquid phase temperature and then applying a pressure in the range of 50-2,000 psi to the parts for a predetermined period of time and simultaneously maintaining the parts at or above their liquid phase temperature. The method of the present invention achieves complete closure of even large voids and the elimination of substantially all porosity within the part.

Abstract: In production of so-called anisotropic fine grain type hard magnetic material, particles of highly magnetic substance powder are each plated with nonmagnetic substance before compaction, sintering and plastic deformation in order to provide the product with stable magnetic characteristics for reduced production cost.

Abstract: A method for making a powdered metal ferrule by compacting and sintering powdered metal to have a density of at least 80 percent of the theoretical maximum compacted density and an elongation of at least 2.9 percent; and powdered metal ferrule having a density of at least 80 percent of theoretical maximum compacted density and an elongation of at least 2.9 percent.

Abstract: The method of the invention relates to powder metallurgy and is intended to be used for making cutting tools, dies as well as vital structural members.The method comprises charging a powder into a capsule, sealing the capsule, heating and then extruding the capsule containing the powder. The sealed capsule is heated up to a temperature of 700.degree. to 1000.degree. C., whereupon the capsule is depressurized and heated up to a temperature of 1050.degree. to 1200.degree. C.

Abstract: A method of making a bonding tool from two different materials is provided. A bonding nib partially made from hard jewel-like material and a bonding nib holder is partially made from a larger and tougher material. The two partially made elements are joined by shrink fitting the nib holder onto the bonding nib to provide an unfinished bonding tool. The unfinished composite bonding tool is finished by grinding and polishing exterior surfaces of the bonding nib.

Abstract: The present invention provides a method for manufacturing complex metallic plates. A hollow metal piece, which will form the outer layer, is first made. A powder which will form the inner layer is then filled within the hollow metal piece. The multi-layer plate is then manufactured by hot-rolling the metal piece.

Abstract: Powder metal first pressed into a green briquette having an inner cavity is then sintered to form a rigid part. The inner cavity of the part is next sized in a lap-like operation by a spherical-shaped tool. The tool is rotated in an orbital pattern comprising a series of elliptically-shaped cycles. As the tool rotates, small successive portions of a surface of the cavity are contacted by the tool. This lap-like interaction between the tool and cavity surface not only sizes the cavity to an exact dimension but improves the wear quality of the cavity surface by increasing the density of a wall of the cavity as well as providing an improved surface finish.

Abstract: A method and material for the manufacture of improved bearing elements such as annular inner and outer bearing ring blanks for ball, roller and needle bearing assemblies comprising the steps of mixing a powder consisting substantially of iron with ferro-alloy powders of substantially smaller size, each ferro-alloy containing at least 80% iron and the balance being an alloying element, together with graphite powder and a lubricant, compacting the resulting mixture to form a preform, pre-sintering the preform, and then coating the sintered preform with a stop-off and lubricant. The preform is subjected to a plastic deformation of at least 50% in a cold (room temperature) forging operation to produce an article which is at least 98% dense and has approximately the shape of the finished article. This cold forged shape is resintered and annealed, after which the annealed and resintered shape is roll formed into substantially final dimensions.

Abstract: Process for manufacturing a forged article in which a preform is generated by filling a semi-rigid liner with powdered metal, providing the liner with a sealing element, and isostactically compressing the liner and its contents. The liner is then removed from the green preform, the preform is sintered, and the resulting sintered preform is forged.