Subsequent Working Patents (Class 419/28)
  • Patent number: 5403372
    Abstract: Vane material, vane and method of producing a vane to be used in a compressor using a substitute freon, improving the wear resistance thereof. The vane material has a composition consisting of by weight: 1.0-2.5% of C; not more than 1.5% of Si; not more than 1.0% of Mn; 3-6% of Cr; one or two of not more than 20% W and not more than 12% Mo where "W+2Mo" being 15-28%; 3.5-10% of one or two of V and Nb; and the balance of Fe and incidental impurities. Carbides are uniformly dispersed in the matrix thereof where their average diameter does not exceed 1.5 .mu.m and the maximum diameter thereof does not exceed 6 .mu.m. A method of producing a vane is also disclosed, in which an atomized powder having the composition as described is compacted and it is then subjected to hot working, or to hot working and cold working.
    Type: Grant
    Filed: June 18, 1992
    Date of Patent: April 4, 1995
    Assignee: Hitachi Metals, Ltd.
    Inventor: Norimasa Uchida
  • Patent number: 5403670
    Abstract: The crack-resistant compound sleeve roll having a shell portion made of a sintered alloy and a core portion made of steel is produced by (a) charging an alloy powder consisting essentially, by weight, of 1.0-3.5% of C, 2% or less of Si, 2% or less of Mn, 10% or less of Cr, 3.0-15.0% of W, 2.0-10.0% of Mo and 1.0-15.0% of V, the balance being substantially Fe and inevitable impurities, into a metal capsule disposed around a roll core; (b) after evacuation and sealing, subjecting the alloy powder to a HIP (hot isostatic pressing) treatment at 1100.degree.-1300.degree. C. to form a shell portion; (c) after removing the metal capsule, subjecting the sintered shell portion to a heat treatment having hardening at 1140.degree.-1220.degree. C. and annealing at 540.degree.-620.degree. C.; and (d) chamfering edge portions of the roll on both axial ends thereof such that a boundary of the shell portion and the core portion exists in a chamfered surface.
    Type: Grant
    Filed: December 21, 1993
    Date of Patent: April 4, 1995
    Assignee: Hitachi Metals, Ltd.
    Inventors: Takuya Ohsue, Akira Noda, Hiroshi Fukuzawa, Itsuo Korenaga
  • Patent number: 5399311
    Abstract: A magnet is formed as a ring magnet and magnetized by radial application of a magnetic field while the intensity of the magnetic field is changed periodically along the circumference of the ring magnet to give a circumferentially sinusoidal waveform distribution of magnetic flux density to the ring magnet in the magnetized state of the magnet.
    Type: Grant
    Filed: November 12, 1992
    Date of Patent: March 21, 1995
    Assignee: Daido Tokushuko Kabushiki Kaisha
    Inventors: Yasuaki Kasai, Hiyoshi Yamada, Norio Yoshikawa
  • Patent number: 5387272
    Abstract: The present invention provides an Al-Si based sintered alloy of high strength and high ductility, a method for production thereof and use thereof. The alloy comprises 1-45% of Si, 0.1-20% of an element of Group IIIa, 0.01-5% of at least one element of Groups IVa and Va, the balance of substantially Al. This alloy can further contain at least one of 0.01-5% of Cu, 0.01-5% of Mg, 2.0% or less of Fe, 1.5% or less of Mn and 1.5% or less of Co and the oxygen content is reduced to 0.15% or less by sintering under vacuum. The present invention is applied to automobile parts such as a piston and scroll compressors. The alloy has a tensile strength of about 40 kg/mm.sup.2 or higher and an elongation of 1.5% or more at 150.degree. C.
    Type: Grant
    Filed: April 8, 1992
    Date of Patent: February 7, 1995
    Assignees: Hitachi, Ltd., Hitachi Powdered Metals Company, Limited
    Inventors: Yasuo Kamitsuma, Yusaku Nakagawa, Mitsuo Chigasaki, Tadashi Iizuka, Kooichi Inaba, Keiichi Nakamura, Masaki Minabe, Tsuyoshi Kagaya
  • Patent number: 5376329
    Abstract: A method of making a composite orifice having a tungsten core which is diffusion bonded to a molybdenum shell. Tungsten and molybdenum powders in contact with each other in a mold are isostatically pressed to form a pressed bonded composite part. The pressed, unsintered tungsten core portion of the part is then machined to the desired dimensions. The pressed composite part is then sintered to form a diffusion bonded composite orifice. The pressed and sintered molybdenum shell portion of the orifice may then be machined to the desired dimensions.
    Type: Grant
    Filed: November 16, 1992
    Date of Patent: December 27, 1994
    Assignee: GTE Products Corporation
    Inventors: Ricky D. Morgan, James A. Giffen, Jr.
  • Patent number: 5368629
    Abstract: The rapidly solidified aluminum alloy powder is preformed in a cold or warm environment to form a powder compact having a relative density of 75-93%. Then, the preformed compact is heated and degassed in the atmosphere of an inert gas at temperature of 300.degree. C. to 560.degree. C. for 0.25-3 hours. Immediately thereafter, the compact is subjected to hot coining at 300.degree.-560.degree. C. to obtain a solidified compact having pores at a rate of 2-5%. The solidified compact is then subjected to sizing. Since the inorganic gas prevents reaction between the evaporated water and aluminum while preheating the compact, the hot coining can be carried out in a state where solid state diffusion easily occurs. Thus, the powder particles can be bonded together strongly with a single forging. Also, at the end of hot coining, pores remain in the solidified compact at the rate of 2-5%. Utilizing these pores, the compact can be subjected to sizing to improve its dimensional accuracy.
    Type: Grant
    Filed: December 3, 1992
    Date of Patent: November 29, 1994
    Assignee: Sumitomo Electric Industries, Ltd.
    Inventors: Katsuyoshi Kondo, Yoshinobu Takeda
  • Patent number: 5366138
    Abstract: A method to form a composite wear resistant die face of titanium carbide, tungsten carbide/cobalt alloy or similar material having a metal backing which is readily bondable to a substrate. Since sintered powdered metallurgy wear resistant materials are difficult to solder or braze directly to a die by conventional methods, a steel backed composite is formed by hot isostatic pressing of the wear resistant material to both sides of a steel substrate and this composite is cut through the middle of the steel blank to formed separate steel backed wear resistant die facing plates, especially useful for pelletizers.
    Type: Grant
    Filed: May 5, 1993
    Date of Patent: November 22, 1994
    Assignee: Alloy Technology International Inc.
    Inventors: Timothy M. Vela, David H. Atkinson
  • Patent number: 5362438
    Abstract: This invention relates to a powder substantially of dental metal, which powder is suitable for the manufacture of a dental restoration such as a crown or a bridge, comprising a substructure of dental metal and a fired on coating of a dental ceramic material. The powder comprises a core substantially of a dental metal, which core is coated with one or more layers substantially of metal which protect the dental metal of the core during sintering against oxidation and/or reduce the temperature at which the powder is sintered.The invention also relates to a process for the manufacture of a dental restoration such as a crown or a bridge, comprising a substructure of a dental metal and a fired on coating of a dental ceramic material.
    Type: Grant
    Filed: June 10, 1993
    Date of Patent: November 8, 1994
    Assignee: Elephant Edelmetaal B.V.
    Inventor: Joseph M. van der Zel
  • Patent number: 5358684
    Abstract: The friction lining for disk brakes comprises a carrier plate (10) and a block (16) of a compressed friction material secured to the latter, wherein the carrier plate, on the side bearing the block of friction material, is provided with a sinter-fused mounting bed (12) for the block of friction material of individual shaped members (13) forming frictional and positive connections with the block of friction material, in which, prior to the block of friction material is pressed onto the carrier plate (10) with the mounting bed sinter-fused thereupon, a galvanically, thermally or in some other suitable way produced metallic coating (50) is applied to the carrier plate as a corrosion protection.
    Type: Grant
    Filed: August 19, 1992
    Date of Patent: October 25, 1994
    Assignee: Jurid Werke GmbH
    Inventor: Wolfgang Valentin
  • Patent number: 5358685
    Abstract: A new silicon carbide material is made following a procedure including hot pressing to provide a finished product having a microstructure with an optimal grain size of less than 7 micrometers. The material exhibits a dominant failure mode of intergranular fracture requiring significant energy for crack propagation. The method of manufacturing is cost-effective by allowing the use of "dirty" raw materials since the process causes impurities to segregate at multi-grain boundary junctions to form isolated pockets of impurities which do not affect the structural integrity of the material. End uses include use as optical and electronic substrate materials.
    Type: Grant
    Filed: September 3, 1993
    Date of Patent: October 25, 1994
    Assignee: Cercom Inc.
    Inventor: Andre Ezis
  • Patent number: 5344507
    Abstract: An aluminum-alloy, which is wear-resistant and does not wear greatly the opposed cast iron or steel, and which can be warm worked. The alloyings the following composition and structure. Composition: Al.sub.a Si.sub.b M.sub.c X.sub.d T.sub.e (where M is at least one element selected from the group consisting of Fe, Co and. Ni; X is at least one element selected from the group consisting of Y, Ce, La and Mm (misch metal); Y is at least one element selected from the group consisting of Mn, Cr, V, Ti, Mo, Zr, W, Ta and Hf; a=50-85 atomic %, b=10-49 atomic %, c=0.5-10 atomic %, d=0.5-10 atomic %, e=0-10 atomic %, and a+b+c+d+e=100 atomic %. Structure: super-saturated face-centered cubic crystals and fine Si precipitates.
    Type: Grant
    Filed: March 16, 1992
    Date of Patent: September 6, 1994
    Assignees: Tsuyoshi Masumoto, Yoshida Kogyo KK, Teikoku Piston Ring Co., Ltd.
    Inventors: Tsuyoshi Masumoto, Akihisa Inoue, Kazuhiko Kita, Hitoshi Yamaguchi
  • Patent number: 5342571
    Abstract: Dual phase sputter targets consisting essentially of TiN and Al, methods of manufacture thereof, and cathodic sputtering methods using such targets are disclosed. The targets are prepared by blending TiN and Al powders followed by compaction to full density. The thus compacted materials are optionally sintered and are then formed into the desired target shape. The targets are used in cathodic sputtering processes to form opaque, dark colored decorative and wear resistant coatings.
    Type: Grant
    Filed: February 19, 1992
    Date of Patent: August 30, 1994
    Assignee: Tosoh SMD, Inc.
    Inventors: Mark B. Dittmar, Paul E. Scheiderer
  • Patent number: 5342573
    Abstract: A method of producing a tungsten heavy alloy product according to a powder metallurgical procedure utilizing the injection molding technique which enables production of tungsten heavy alloy products having high dimensional accuracy and complex configuration and yet having high physical strength and toughness in high productivity and at low cost. A powder mixture of tungsten powder and nickel powder, iron powder or copper powder is mixed with an organic binder and they are kneaded together. The kneaded mixture is injection molded into a predetermined shape, and thereafter the binder is removed from the molded product. Subsequently, the molded product is sintered in a temperature range of from the melting point of the bond phase of nickel, iron or copper to +50.degree. C. relative to the melting point.
    Type: Grant
    Filed: August 20, 1992
    Date of Patent: August 30, 1994
    Assignee: Sumitomo Electric Industries, Ltd.
    Inventors: Yoshinari Amano, Masahiro Omati, Junzo Matsumura
  • Patent number: 5330702
    Abstract: Purely powder-metallurgical processes or sinter-impregnation processes are often used to manufacture CuCr contact materials. Here the aim is to obtain the lowest possible residual porosity, which should be <1%. According to the invention, a powder moulding of the components is densified in two stages; the first stage is a sintering process with a densification of the sintered body to a closed porosity, and the second stage is a hot-isostatic pressing operation (HIP), in which the unencased workpieces are taken to a final density amounting to a space occupation of at least 99%. Thus, an economical method of manufacturing high grade material is obtained. It is possible to produce multi-layer contacts or self-adhesive bonds between the sintered body and a solid substrate, e.g. a copper contact bolt.
    Type: Grant
    Filed: December 2, 1991
    Date of Patent: July 19, 1994
    Assignee: Siemens Aktiengesellschaft
    Inventors: Horst Kippenberg, Franz Hauner
  • Patent number: 5328772
    Abstract: A multilayer sliding material for high-speed engine, comprising a steel back metal, a Cu or Cu-base alloy plating layer, a Cu-Pb bearing alloy layer, and an overlay, said steel back metal having 155 or more of Vickers hardness and 42 kgf/mm.sup.2 or more of 0.2% yield strength, a Cu-Pb bearing alloy layer containing 15-30 wt % of Pb and 0.5-2.0 wt % of Sn and having 0.25 cal/cm.s..degree. C. or more of thermal conductivity, 75 or more of Vickers hardness and 18 kgf/mm.sup.2 or more of tensile strength, said overlay of a lead base alloy containing 2-8 wt % of Sn and 3-11 wt % of In and having more than 250.degree. C. of melting start temperature. The material has a superior antiseizure property at high speed of engine. In particular, the rising of the melting start temperature of the metal of the overlay and the thermal conductivity of the bearing alloy provides a superior sliding property of plain bearing at high speed of engine.
    Type: Grant
    Filed: February 12, 1992
    Date of Patent: July 12, 1994
    Assignee: Daido Metal Company
    Inventors: Tadashi Tanaka, Masaaki Sakamoto, Motomu Wada, Koichi Yamamoto, Hideo Ishikawa, Youji Nagai, Kenji Sakai
  • Patent number: 5319851
    Abstract: A method for manufacturing a bearing for a wiper arm structure includes the steps of: a) forming the bearing by sintering so that the outer peripheral surface of the bearing includes rough sintered surfaces of protruding ridges and recessed portion; b) sizing only the sintered surfaces of the protruding ridges without processing the recessing portions to smooth only outer peripheral surfaces of the protruding ridges so that the outer peripheral surfaces define a circular cross-section for the bearing, the sintered surfaces of the recessed portions remaining in a rough sintered condition relative to the outer peripheral surfaces of the protruding ridges which are sizing-processed; and c) forming a resin material on the outer peripheral surface of the bearing by insert molding.
    Type: Grant
    Filed: January 12, 1993
    Date of Patent: June 14, 1994
    Assignee: Mitsuba Electric Manufacturing Co., Ltd.
    Inventors: Ryu Ikezawa, Hironobu Kishi
  • Patent number: 5309639
    Abstract: A machine component has a wear surface along which excessive friction will develop unless the surface receives adequate lubrication. To provide lubrication for the wear surface in the absence of any other lubricating medium, the component is formed from powdered metal compacted to less than theoretical density so as to contain pores, and the pores hold oil. Even though the component is mechanically machined along its wear surface, the pores are nevertheless open at the wear surface to enable the entrapped oil to exude from the ring and lubricate that surface. During manufacture of the ring, the mechanical machining creates a Bielby layer at the wear surface, that is it smears the metal and closes the pores at that surface, but the Bielby layer is removed by electro-discharge machining This procedure erodes the Bielby layer with electrical arcs so that the pores at the wear surface are again exposed and open.
    Type: Grant
    Filed: November 23, 1992
    Date of Patent: May 10, 1994
    Assignee: The Timken Company
    Inventor: Peter W. Lee
  • Patent number: 5298336
    Abstract: The present invention provides a multilayer composite sliding material with excellent seizure resistance property having a steel plate or a steel plate having surfaces plated with copper or the like; a bond layer having a thickness of 0.05 to 0.5 mm, formed on the steel plate, and made of a sintered powder material consisting of 5 to 16% Sn, 0 to 15% Pb, 0 to 0.5% P and balance essentially Cu; and an alloy layer having a thickness of 0.1 to 1.0 mm, formed on the bond layer, and made of a sintered powder material consisting of 5 to 16% Sn, 1 to 12% MoS.sub.2 and balance essentially Cu. In a modified form of the alloy layer, not more than 20% Pb, not more than 1% P or not more than 12% Ni may be added. MoS.sub.2 powder may be coated with Cu or Ni.
    Type: Grant
    Filed: February 17, 1993
    Date of Patent: March 29, 1994
    Assignee: Daido Metal Company, Ltd.
    Inventors: Tadashi Tanaka, Masaaki Sakamoto, Koichi Yamamoto, Tsukimitsu Higuchi
  • Patent number: 5283031
    Abstract: A process for producing a precision metal part of a sintered body by powder molding comprises using a metal powder of which the oxygen content and the hydrogen reduction loss are controlled to 0.5-6 wt. % and 1-7 wt. %, respectively. The sintered body has a high density near the theoretical density and is excellent in dimensional accuracy. The molding is facilitated, and the process is simple.
    Type: Grant
    Filed: July 23, 1991
    Date of Patent: February 1, 1994
    Assignee: Citizen Watch Co., Ltd.
    Inventors: Naoto Ogasawara, Kenji Kurimura, Ken-ichi Yoshioka, Shigeru Saito, Takao Kasai, Masami Hoshi, Seiichi Nakamura
  • Patent number: 5252119
    Abstract: A high speed tool steel produced by sintering powder, consisting essentially, by weight, of more than 1.5% but not more than 2.2% C, not more than 1.0% Si, not more than 0.6% Mn, 3.0 to 6.0% Cr, an amount of W and Mo in which the content of W+2Mo is in the range of 20 to 30% and in which the ratio of W/2Mo is not less than 1, not more than 5.0% V, 2.0 to 7.0% Nb, the ratio of Nb/V being not less than 0.5, and the balance Fe and incidental impurities, the value of C-Ceq, which Ceq is defined by 0.24+0.033.times.W+0.063.times.Mo+0.2.times.V+0.1.times.Nb, being in a range of -0.20 to 0.05, the density of carbides in the sintered steel having grain size of 2 to 5 .mu.m being in a range of 10,000 to 30,000 pieces/mm.sup.2.
    Type: Grant
    Filed: October 29, 1991
    Date of Patent: October 12, 1993
    Assignee: Hitachi Metals, Ltd.
    Inventors: Junichi Nishida, Norimasa Uchida
  • Patent number: 5252288
    Abstract: Method for producing an elongated sintered article, characterized by the steps including filling powder material in a pipe, carrying out plastic deformation of the pipe filled with the powder material, and heating the pipe filled with the powder material to burn and/or sinter the powder material.The method of the present invention is advantageously applicable to production of wire or rod of ceramics, particularly so called new ceramics or fine ceramics, sintered alloys or their combination, which are difficult to shape or mold by conventional process such as wire-drawing, rolling or extrusion of powder material which is difficult to mold and machine after the powder material is sintered.
    Type: Grant
    Filed: May 15, 1992
    Date of Patent: October 12, 1993
    Assignee: Sumitomo Electric Industries, Inc.
    Inventors: Susumu Yamamoto, Teruyuki Murai, Nozomu Kawabe, Masaaki Tobioka
  • Patent number: 5248474
    Abstract: A method of making a threaded tungsten metal part having a diameter or thickness greater than two inches. Tungsten metal powder is hot isostatically pressed and sintered and then machined to the desired thread configuration using a single point tungsten carbide cutting tool.
    Type: Grant
    Filed: October 5, 1992
    Date of Patent: September 28, 1993
    Assignee: GTE Products Corporation
    Inventor: Ricky D. Morgan
  • Patent number: 5190102
    Abstract: A prepack well screen assembly has a resistance welded outer screen concentrically mounted in radially spaced relation on a perforated mandrel, thereby defining an annulus in which a sintered metal prepack sleeve is loaded. The longitudinal spacing distance between adjacent turns of the outer screen selectively exclude sand fines of a predetermined minimum size. The porosity of the sintered metal prepack sleeve is selected to pass sand fines in the size range of from about 20 microns to about 150 microns. The effective inlet flow area through the sintered metal prepack sleeve is substantially greater than the effective inlet flow area through the outer screen. The sintered metal prepack screen excludes sand fines from inflowing formation fluid during the initial production phase following a gravel pack operation, without limiting production of formation fluid.
    Type: Grant
    Filed: December 16, 1991
    Date of Patent: March 2, 1993
    Assignee: Otis Engineering Corporation
    Inventors: Bryant A. Arterbury, James E. Spangler, Thomas V. Malorzo
  • Patent number: 5167728
    Abstract: The process of the invention relates to forming MA iron-base ODS alloys. A billet of iron-base ODS alloy is provided. The billet is consolidated at a temperature within a predetermined range of sufficient temperature for formation of coarse and/or fine grain sizes during a final heat treatment. The consolidated billet is worked into final form. The object is annealed to recrystallize grains to a size determined by the temperature of the consolidation and the working of the extruded billet.
    Type: Grant
    Filed: April 24, 1991
    Date of Patent: December 1, 1992
    Assignee: Inco Alloys International, Inc.
    Inventor: John H. Weber
  • Patent number: 5145512
    Abstract: A consolidated tungsten alloy body consisting essentially of from about 88% to about 98% by weight of tungsten, balance, nickel and iron, produced by liquid phase sintering, containing a continuous phase of a tungsten, nickel and iron alloy and a discontinuous phase of elongated grains of tungsten having an aspect ratio of at least 4:1 relatively uniformly distributed throughout the continuous phase and wherein said body has a recrystallization temperature of from about 1000.degree. C. to about 1200.degree. C. A process for producing the consolidated bodies comprises working and annealing at controlled temperatures to achieve the desired properties. The working temperatures are from about 700.degree. C. to about 900.degree. C. and the annealing temperature is preferably 1200.degree. C.
    Type: Grant
    Filed: January 3, 1989
    Date of Patent: September 8, 1992
    Assignee: GTE Products Corporation
    Inventors: James R. Spencer, James A. Mullendore
  • Patent number: 5145506
    Abstract: A non-magnetic, wear resistant composite of from 10 to 45 volume percent of titanium carbide or tungsten carbide particles bonded in a matrix of a nickel-titanium alloy wherein nickel comprises from 53 to 62 weight percent of the alloy with the remainder being essentially titanium.
    Type: Grant
    Filed: July 5, 1984
    Date of Patent: September 8, 1992
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: David Goldstein, Scott M. Hoover
  • Patent number: 5143192
    Abstract: A friction clutch or friction brake is provided having a basic body and a friction body portion. The friction body portion can be mass-produced separately from the basic body, using a planar metal sheet-like material which is treated leading to a sintered powder friction facing. The friction clutch has a non-planar friction surface, operating in a box filled with oil as a lubricant. The friction body is applied to the basis body by form-locking friction, friction-gripping and/or material-locking techiques. In a preferred embodiment, the friction clutch or brake is a synchronizing ring and/or a correcting ring for motor vehicle shift gears.The friction clutch or friction brake according to the invention has particularly favorable friction properties, a long service life and low manufacturing costs. In a great number of applications, the shaping of separte draining grooves for expelling the oil when the friction grip is produced between matching components can be omitted.
    Type: Grant
    Filed: April 25, 1991
    Date of Patent: September 1, 1992
    Assignee: Sinterstahl GmbH
    Inventors: Herbert Vojacek, Hermann Pflaum
  • Patent number: 5126102
    Abstract: The present invention is directed to a method of preparing a composite material excellent in joint strength and heat conductivity, and more specifically to a method of preparing a composite material composed of a high-melting material W and low-melting material Cu. The method comprising a first step of forming pores in the high-melting material W, to obtain a substrate material having a porosity distribution, with a high porosity at at least one region of the surface of the substrate material and the porosity gradually decreasing outward from the region; and a second step of impregnating the low melting material Cu to the substrate material obtained in the first step from the region of the highest porosity gradually downward. The substrate material being formed to have a gradient distribution of a composite ratio of the high-melting material and the low-melting material.
    Type: Grant
    Filed: March 12, 1991
    Date of Patent: June 30, 1992
    Assignee: Kabushiki Kaisha Toshiba
    Inventors: Masashi Takahashi, Yoshiyasu Itoh
  • Patent number: 5124119
    Abstract: A beryllium metal matrix phase includes up to 70% by volume of beryllium oxide single crystals dispersed therein. The composites are useful for electronics applications because of their light weight, high strength and effective thermal properties.
    Type: Grant
    Filed: February 12, 1991
    Date of Patent: June 23, 1992
    Assignee: Brush Wellman Inc.
    Inventor: Fritz C. Grensing
  • Patent number: 5124118
    Abstract: A method for manufacturing a brake fitting comprising a plurality of studs each surrounded by a less fragile belt, the studs being non-contiguously secured to a metal support. According to the method, the support is provided with a slip-resistant surface by coating with a braze welding suspension which is oxidized and reduced. Stud blanks then are molded and compacted from powdered friction products and belt blanks are molded and compacted from metal powders and given an internal diameter 1.005 to 1.05 times the external diameter of the stud blanks, and the belt blanks are disposed around the stud blanks and sintered, obtaining sheathed stud blanks which are placed on the slip resistant surface of the support, and welded thereto by heat treatment. Finally, the sheathed stud blanks are forged at over 400 degree C., shortening them by at least 15%.
    Type: Grant
    Filed: May 17, 1991
    Date of Patent: June 23, 1992
    Assignee: Le Carbone Lorraine
    Inventors: Hassan Youssef, Yves Bigay
  • Patent number: 5118341
    Abstract: The invention provides a sinterable brass powder blend, comprising about 90% to about 99% by weight of brass powder, about 0.2% to about 6.0% by weight manganese sulfide, and 0% to about 5.0% by weight of lubricants, binders, graphite, sintering enhancing additives and mixtures thereof.The invention also provides methods for making lead-free but machinable sintered brass powder metal parts.
    Type: Grant
    Filed: March 28, 1991
    Date of Patent: June 2, 1992
    Assignee: Alcan Aluminum Corporation
    Inventors: Edul M. Daver, Krishnakant B. Patel
  • Patent number: 5110688
    Abstract: The present invention relates to a method of fabricating various types of bearing materials and the bearing materials produced thereby. The processes of the invention may be used to produce porous self-lubricating bearings, laminated composite bearings (babbitt bearings) and bearings for high temperature application. The processes of the invention involve the use of micro-pyretic synthesis to achieve bearing materials with improved bearing properties, including higher bearing capacity and toughness.
    Type: Grant
    Filed: December 3, 1990
    Date of Patent: May 5, 1992
    Assignee: University of Cincinnati
    Inventors: Jainagesh A. Sehkar, A. K. Bhattacharya, Hung P. Li
  • Patent number: 5088554
    Abstract: A tubular sand screen is made in one piece entirely of powdered metal slivers which are molded and sintered to form a metallurgically integral rigid tubular structure. Aggregate metal particles, for example, stainless steel slivers, are bonded together by interatomic diffusion as a result of sintering the compacted slivers under high temperature and pressure conditions. The sintered metal sand screen performs the function of the conventional prepack assembly as well as the screen function. In one aspect of the invention, the sintered metal screen is subjected to electropolishing to yield an effective porosity of 40-60 mesh, with an average pore size of 150 microns. Most of the surface irregularities are removed by electropolishing, and very few nucleation sites remain where particles in the size range of 74 microns-100 microns can become captured or otherwise lodged to cause plugging of the screen.
    Type: Grant
    Filed: October 22, 1990
    Date of Patent: February 18, 1992
    Assignee: Otis Engineering Corporation
    Inventors: Bryant A. Arterbury, James E. Spangler
  • Patent number: 5085679
    Abstract: Oxide dispersion strengthened metals are ring rolled into a profiled member which can be employed as a spinner in the manufacture of fibrous glass. Sufficient hot working and annealing are provided to develop the desired coarse grain structure.
    Type: Grant
    Filed: November 23, 1990
    Date of Patent: February 4, 1992
    Assignee: Owens-Corning Fiberglas Corporation
    Inventors: Jay W. Hinze, Richard D. Lawson, Mott J. Blake
  • Patent number: 5074907
    Abstract: Enhanced crystallographic texture is developed in an alpha or alpha-beta titanium alloy having a dispersion of particles therein, by heating the alloy to essentially the all beta phase range and mechanically hot working the alloy in this range. The mechanical working is preferably accomplished by extrusion, rolling, or forging. The particles are stable during working, and prevent the formation of random texture in recrystallized beta phase grains at the working temperature. The particles are preferably oxides formed from rare earth elements such as erbium or yttrium, that are introduced into the alloy during manufacture. The alloys processed according to the invention are preferably prepared by powder metallurgy to achieve a uniform microstructure prior to working. A particularly suitable alpha-beta (but near alpha) titanium alloy contains aluminum, zirconium, hafnium, tin, columbium, molybdenum, tungsten, ruthenium, germanium, silicon, and erbium.
    Type: Grant
    Filed: August 16, 1989
    Date of Patent: December 24, 1991
    Assignee: General Electric Company
    Inventors: Richard A. Amato, Andrew P. Woodfield, Michael F. X. Gigliotti, Jr., John R. Hughes, Lee C. Perocchi
  • Patent number: 5071474
    Abstract: A magnesium base metal component is forged from a billet by subjecting the billet to a forging process using multiple steps in a closed-die or an open-die forging and a forging temperature ranging from 200.degree. C. to 300.degree. C. The billet is compacted from a rapidly solidified magnesium based alloy defined by the formula Mg.sub.bal Al.sub.a Zn.sub.b X.sub.c, wherein X is at least one element selected from the group consisting of manganese, cerium, neodymium, praseodymium, and yttrium, "a" ranges from about 0 to 15 atom percent, "b" ranges from about 0 to 4 atom percent, "c" ranges from about 0.2 to 3 atom percent, the balance being magnesium and incidental impurities, with the proviso that the sum of aluminum and zinc present ranges from about 2 to 15 atom percent. The alloy has a uniform microstructure comprised of a fine grain size ranging from 0.2-1.0 .mu.m together with precipitates of magnesium and aluminum containing intermetallic phases of a size less than 0.1 .mu.m.
    Type: Grant
    Filed: June 15, 1990
    Date of Patent: December 10, 1991
    Assignee: Allied-Signal Inc.
    Inventors: Derek Raybould, Chin-Fong Chang, Santosh K. Das
  • Patent number: 5070591
    Abstract: Metal and ceramic particles of various morphologies are clad with a coating from the transition metal group consisting of silver, gold, copper, nickel, iron, cobalt, aluminum etc., or combinations thereof, to provide improved coated particles for microelectronics or metal matrix composites or other uses. Refractory metal precursor core particles, such as tungsten, molybdenum, niobium and zirconium, as examples, are provided from a composite of tungsten and copper, for example, made by pressurizing and infiltrating or liquid phase sintering of molten copper into a porous tungsten skeleton. Precursor chip particles derived from a tungsten impregnated billet are used as starter particles which may be further enhanced by cogrinding in an attritor ball mill with smaller copper particles to thereby produce an enhanced copper clad-coating of tungsten particles with predetermined percent by weight of copper and tungsten content.
    Type: Grant
    Filed: January 22, 1990
    Date of Patent: December 10, 1991
    Inventors: Nathaniel R. Quick, James C. Kenney
  • Patent number: 5069869
    Abstract: A process for shaping penetrating projectiles useful in the manufacture of military ammunition, comprising: preparing an alloy of tungsten, nickel, iron and copper by powder metallurgy, compacting the alloy mass into a rough shaped blank having an axis of revolution, sintering the rough shaped blanks thereby producing a blank having a density of at least 17,000 kg/m.sup.3, and work-hardening the sintered blank at a temperature ranging from ambient temperature to 500.degree. C., thereby producing a blank having a variable degree of reduction in section in a direction parallel to the axis of the blank.
    Type: Grant
    Filed: May 3, 1991
    Date of Patent: December 3, 1991
    Assignee: Cime Bocuze
    Inventors: Jean-Claude Nicolas, Raymond Saulnier
  • Patent number: 5069866
    Abstract: A method of preparing a compound pipe, the wall of which comprises an inner layer of a first material and an outer layer of a second material. Powders of the two materials are isostatically hot pressed to form a cylindrical tubular blank in which the first material forms an inner layer and the second material forms an outer layer, the blank after heating to a suitable temperature being extruded over a mandrel.
    Type: Grant
    Filed: May 31, 1990
    Date of Patent: December 3, 1991
    Assignee: ABB Stal AB
    Inventor: Ragnar Ekbom
  • Patent number: 5064608
    Abstract: A method for producing a camshaft having a tubular steel shaft and a sintered cam piece joined to the shaft. The sintered cam piece has iron tetroxide film at its surface. The camshaft is produced by assembling a powder compact to the steel shaft to provide a camshaft assembly, sintering the assembly to provide an integral assembly, correcting bending to the assembly, annealing the assembly, grinding the cam piece and effecting vaporization treatment to the assembly at a temperature lower than the annealing temperature.
    Type: Grant
    Filed: February 5, 1991
    Date of Patent: November 12, 1991
    Assignee: Nippon Piston Ring Co., Ltd.
    Inventors: Yasuo Suzuki, Shunsuke Takeguchi
  • Patent number: 5053192
    Abstract: The invention relates to the powder metallurgy. The invention involves deforming combustion products by extrusion at an extrusion temperature chosen in the range from 0.3T.sub.1 to T.sub.2, wherein T.sub.1 is the melting point of a hard phase of the combustion products and T.sub.2 is the melting point of a binder material in a container (5) made up of vertically extending segments (12) defining spaces (13) with one another and having a die (14) and a heat insulated sizing member (17) the temperature conditions of extrusion being controlled by means of a unit (21) having a temperature pick-up (22) and a member (23) receiving information from the pick-up (22) and sending a command for moving the punch (10).
    Type: Grant
    Filed: August 23, 1990
    Date of Patent: October 1, 1991
    Inventors: Alexandr G. Merzhanov, Alexandr M. Stolin, Vadim V. Podlesov, Leonid M. Buchatsky, Tatyana N. Shishkina
  • Patent number: 5051231
    Abstract: A method for the fabrication of a superplastic composite material having metallic aluminum reinforced with silicon nitride includes thoroughly mixing silicon nitride with metallic aluminum, pressure-sintering the resultant mixture, further heating and pressing the sintered mixture, hot extrusion-molding the resultant sintered article, subjecting the molded article, when necessary, to a heat treatment such as the T6 treatment thereby forming a superplastic composite material, and deforming the composite material in a temperature region in which the material exhibits superplasticity.
    Type: Grant
    Filed: September 14, 1990
    Date of Patent: September 24, 1991
    Assignees: Agency of Industrial Science & Technology, Ministry of International Trade & Industry
    Inventors: Tsunemichi Imai, Mamoru Mabuchi
  • Patent number: 5051232
    Abstract: The separation of two or more forged powder metal components is facilitated by forming a compacted and sintered powder metal preform with at least one slit that separates the component pieces. An anti-bonding agent such as graphite is introduced into the slit and the preform is then forged to final shape. The anti-bonding agent prevents the complete bonding of the powder metal pieces to each other thereby facilitating separation of the pieces at the slit. This method is particularly suited for the manufacture of piston connecting rod assemblies of the type including a connecting rod and cap.
    Type: Grant
    Filed: January 16, 1990
    Date of Patent: September 24, 1991
    Assignee: Federal-Mogul Corporation
    Inventor: Hayward P. Summers
  • Patent number: 5045276
    Abstract: An injection molded powder metallurgy product of highly satisfactory quality is obtained by a method which comprises injection molding mixture obtained by kneading a metal powder with a binder, depriving the molded mass of the binder while keeping the molded mass at least in contact with ceramic powder, projecting beads on the molded mass free from the binder, and thereafter sintering the molded mass studded with the beads.
    Type: Grant
    Filed: October 11, 1990
    Date of Patent: September 3, 1991
    Assignee: Sumitomo Metal Mining Company Limited
    Inventor: Yoshio Kijima
  • Patent number: 5043025
    Abstract: A particulate mixture of Cu and Fe is compacted and mechanically reduced to form an "in-situ" Cu-Fe composite having high strength and high conductivity. Compaction and mechanical reduction of the particulate mixture are carried out at a temperature and time at temperature selected to avoid dissolution of Fe into the Cu matrix particulates to a harmful extent that substantially degrades the conductivity of the Cu-Fe composite.
    Type: Grant
    Filed: June 12, 1990
    Date of Patent: August 27, 1991
    Assignee: Iowa State University Research Foundation, Inc.
    Inventors: John D. Verhoeven, William A. Spitzig, Edwin D. Gibson, Iver E. Anderson
  • Patent number: 5032353
    Abstract: Structural components of at least one intermetallc compound and having complicated contours, are made by the steps of preparing a powder mixture of elemental metal powders including at least one powder of a low melting metal element or component and one powder of a high melting metal element or component that subsequently are to form the intermetallic compound. The powder mixture is then sintered to form a sintered body which is machined to a contour close to the finished contour and to dimensions close to the final dimensions. The so machined and shaped part is enveloped with an envelope of the high melting metal element or component. The enveloped part is subjected to a hot isostatic reaction pressing whereby the intermetallic compound is formed.
    Type: Grant
    Filed: October 26, 1990
    Date of Patent: July 16, 1991
    Assignee: MTU Motoren-und Turbinen-Union Muenchen GmbH
    Inventors: Wilfried Smarsly, Raimund Lackermeier
  • Patent number: 5028386
    Abstract: In a process for making tools from medium and high alloy steels or stellites by superplastic precision forming a powder metallurgically produced starting material with an equiaxed structure and more than 30% by volume of carbidic and/or boridic precipitated phase of particle size 1 to 0.2 .mu.m is given a matrix grain size of 1 to 3 .mu.m by thermomechanical processing (hot forming) and formed in the superplastic state.
    Type: Grant
    Filed: October 17, 1990
    Date of Patent: July 2, 1991
    Assignee: Robert Zapp Werkstofftechnik GmbH & Co. KG
    Inventor: Georg Frommeyer
  • Patent number: 5015440
    Abstract: Light weight refractory aluminides, such as Al.sub.3 Nb and related aluminides may be produced from metallic powders by a high temperature exothermic reaction of refractory metals with molten aluminum. Mixtures of refractory metals and aluminum may be prepared and densified by powder metalurgy techniques. Applicant's process permits near net formations of stock shapes and parts by conducting the reaction in situ in a die.
    Type: Grant
    Filed: September 1, 1989
    Date of Patent: May 14, 1991
    Assignee: McDonnell Douglas Corporation
    Inventor: David M. Bowden
  • Patent number: 5009842
    Abstract: High strength steel parts or articles are made from a powder alloy by compacting the powder into a preform, sintering the preform in a sintering furnace or the like under a highly-reducing atmosphere and at a temperature of at least 1150.degree. C., cooling the preform, preheating the sintered preform in a highly-reducing atmosphere, such as an inert gas-based atmosphere containing hydrogen or pure hydrogen, to a temperature of at least 1000.degree. C. and transferring the preheated preform to an impact forging device and impacting the preform at a peak averaging forging pressure of at least about 1000 MPa to obtain a forged part or article. The time period between removal of the preheated preform from the preheater and the first forging impact is no more than about 8 seconds. The sintering and preheating steps can be combined with the sintered preform being cooled to the preheating temperature in the sintering furnace and transferred directly from the sintering furnace to the impact forging device.
    Type: Grant
    Filed: June 8, 1990
    Date of Patent: April 23, 1991
    Assignee: Board of Control of Michigan Technological University
    Inventors: Alfred A. Hendrickson, Darrell W. Smith
  • Patent number: 5009704
    Abstract: A nickel-based superalloy article formed from particles of the superalloy is processed to have a microstructure which is resistant to failure when processed using high strain thermomechanical processes. Articles having the desired microstrucuture are produced by hot isostatically pressing powder of the superalloy in a specified temperature range bounded by the incipient melting temperature as a minimum and the solvus temperature of stable high temperature phases. The compact is held under pressure in the specified temperature range to diffuse deleterious phases which exist as a result of the initial powder atomization operation. The powder compact thus formed can be processed using conventional processes to produce material for subsequent thermomechanical processing using high strain rate forging equipment and retain the benefits of chemical uniformity and cleanliness associated with traditional powder metal processes.
    Type: Grant
    Filed: June 28, 1989
    Date of Patent: April 23, 1991
    Assignee: Allied-Signal Inc.
    Inventor: Anthony Banik