Subsequent Working Patents (Class 419/28)
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Patent number: 4817858Abstract: Method of manufacturing a workpiece of any given cross-sectional dimensions from an oxide-dispersion-hardened nickel-based superalloy available in the form of coarse-grained longitudinally directed columnar crystals by connecting previously very finely machined workpiece parts derived from a semi-finished product by diffusion-bonding using hot isostatic pressing, the workpiece parts being first heat-treated under a protective gas in the temperature range of 50.degree. to 100.degree. C. below the recrystallization temperature, under a pressure p.sub.k of not more than 5 MPa with the machined surfaces to be connected joined together, the workpiece then being heated at least to a critical temperature T.sub.K, above which no further cold working takes place, and the pressure then being gradually increased to the diffusion bonding pressure p.sub.max of 100 to 300 MPa with simultaneous increase in temperature are a heating rate of not more of 2.degree. C./min to the diffusion bonding temperature T.sub.D of 0 to 50.Type: GrantFiled: May 11, 1988Date of Patent: April 4, 1989Assignee: BBC Brown Boveri AGInventor: Clemens Verpoort
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Patent number: 4793967Abstract: The present invention is directed to a cermet material comprising a matrix of aluminum alloy with ceramic particles distributed therein. The cermet is adapted for use as a semiconductor substrate and is manufactured using powder technology procedures. The cermet comprises from about 40 to about 60 volume % of aluminum or aluminum alloy, from an effective amount up to about 10 volume % of binder for enhancing bonding between the aluminum alloy and ceramic particles, and the balance essentially ceramic particles.Type: GrantFiled: December 31, 1987Date of Patent: December 27, 1988Assignee: Olin CorporationInventors: Michael J. Pryor, Eugene Shapiro, Deepak Mahulikar
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Patent number: 4784690Abstract: A low density tungsten alloy article is disclosed and the method for producing the article. The method involves compacting a relatively uniform tungsten alloy powder with the tungsten content comprising no greater than about 90% by weight of the alloy and the balance a matrix phase to produce a preformed article which is then sintered in a reducing atmosphere at a temperature below the melting point of the matrix phase for a sufficient time to form a densified article which is mechanically worked to produce the final article.Type: GrantFiled: October 11, 1985Date of Patent: November 15, 1988Assignee: GTE Products CorporationInventor: James A. Mullendore
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Patent number: 4774749Abstract: A plain bearing comprises a metal cylinder as an external member and a resinous cylinder as an internal member, in which the outer surface of the resinous cylinder is firmly engaged and bitten with a concavo-convex portion formed on the inner surface of the metal cylinder. A process for manufacturing the plain bearing comprises producing the metal cylinder, forming the concavo-convex portion on the inner surface of the metal cylinder, combining the concavo-convex portion of the metal cylinder with the resinous cylinder, inserting a core pin into the interior of a combined cylinder of the metal cylinder and the resinous cylinder, squeezing the combined cylinder through a draw die and producing a finished plain bearing.Type: GrantFiled: November 3, 1986Date of Patent: October 4, 1988Assignee: Nippon Seiko Kabushiki KaishaInventor: Kyozaburo Furumura
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Patent number: 4770948Abstract: There is provided a high-purity molybdenum target or high-purity molybdenum silicide target for LSI electrodes which comprises a high-purity metallic molybdenum having an alkali metal content of not more than 100 ppb and a radioactive element content of not more than 10 ppb. Further, a process is provided for producing such target comprising a wet purification processing followed by a series of dry processings.Type: GrantFiled: June 23, 1986Date of Patent: September 13, 1988Assignees: Nihon Kogyo Kabushiki Kaisha, Nippon Telegraph and Telephone CorporationInventors: Hideo Oikawa, Takao Amazawa, Nakahachiro Honna, Hideo Miyazaki, Iwao Kyono, Nobuyuki Mori, Yoshiharu Katoh, Masami Kuroki
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Patent number: 4770283Abstract: A friction ring for clutches and brakes consists of an annular metal element having at least one cylindrical or conical friction surface comprising a spray-sintered friction lining. The friction linings are directly sintered onto the annular element itself, the intially planar friction surfaces being formed, after applying the spray-sintered friction linings, into cylindrical or conical shape by a non-cutting shaping process such as stamping, deepdrawing or the like. The method of producing the friction ring comprises producing an annular metal element, applying a spray-sintered friction lining on to one or both sides thereof and shaping the annular element together with the sintered linings applied thereto into a cylindrical or conical form. The shaping is performed by means of a shaping tool comprising a die and an associated plunger working on the annular element.Type: GrantFiled: July 23, 1986Date of Patent: September 13, 1988Assignee: Hoerbiger & Co.Inventors: Hermann Putz, Ulrich Wollenteit
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Patent number: 4770848Abstract: A rapidly-solidified aluminum alloy powder having a nominal composition of 7% Zn, 2.5% Mg, 2% Cu, 0.3% Zr, and 0.3% Cr is used to make a high forming-rate, superplastic, high-strength aluminum alloy. The powder is outgassed, consolidated, and extruded, thereby developing a wide range of particle size distribution of dispersoids in the process, containing respectively zirconium and chromium dispersoids, as well as age hardening precipitates. The consolidated powder is then rolled to 85% reduction to provide a sheet material which is superplastically formed at a temperature in the range of 450.degree. C. to 490.degree. C. and at a rate between 5.times.10.sup.-3 to 5.times.10.sup.-2 per second.Type: GrantFiled: August 17, 1987Date of Patent: September 13, 1988Assignee: Rockwell International CorporationInventors: Amit K. Ghosh, Chimata Gandhi
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Patent number: 4769212Abstract: Metallic sintered parts with hollow structure and high density and toughness can be produced easily by kneading a raw metallic powder with an aqueous solution of an organic binder, extruding the resulting kneaded mixture, removing the organic binder from the extruded product and sintering the binder removed extruded product.Type: GrantFiled: June 4, 1987Date of Patent: September 6, 1988Assignee: Hitachi Metals, LtdInventors: Hideki Nakamura, Takayuki Fukaya
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Patent number: 4769211Abstract: A process for the passivating, multistage compaction of hot iron particles supplied in the form of a packed bed from a reduction unit and for the subsequent breaking apart of the compacted iron band is described. Prior to the final compacting, the iron particles pass through a homogenizing and precompressing stage. Thus, the compacted iron has a pore volume of max. 40% and a density of at least 5.5 g/cm.sup.3. The iron compacted to a band is subsequently guided between the rollers (7,8,11) of a separating stage exposing it to bending stresses such that it breaks apart at the predetermined desired breaking points. The latter have a smaller density than the band regions between them. They can be produced in that in the precompression stage the feed speed is briefly decelerated compared with the feed speed in the compaction stage or in the compaction stage there is less marked compression at these points than in the intermediate regions.Type: GrantFiled: August 27, 1987Date of Patent: September 6, 1988Assignee: Korf Engineering GmbHInventor: Klaus Langner
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Patent number: 4762678Abstract: The present invention provides a method of producing a bulk amorphous metal alloy article. The method involves mechanically alloying a matrix metal and a fast diffuser element into a powder mixture consisting of particles having a modulated structure and whereby the powder is at least 50% but less than 100% amorphous. The resultant powder mixture is formed into a bulk amorphous metal alloy article by standard forming methods such as cold or hot-pressing. This bulk article can be further processed into a bulk crystalline metal alloy article by heating at a temperature above the glass transition temperature of the amorphous metal alloy article.Type: GrantFiled: November 3, 1987Date of Patent: August 9, 1988Assignee: Allied-Signal Inc.Inventor: Benjamin P. Dolgin
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Patent number: 4762559Abstract: A tungsten-nickel-iron-cobalt high density alloy having unexpected improved strength and hardness properties and the method of making such alloy are disclosed. The alloy has from about 85-98% by weight tungsten with the remainder being a nickel-iron-cobalt binder in which the cobalt is present in amounts of from at least about 5% up to 47.5% by weight of the binder and the amount of cobalt being equal to or less than the amount of nickel. After the powders of the elements in the indicated amounts are homogeneously blended, compacted into a shape and sintered, the sintered shape is subjected to a heat treatment in a flowing argon atmosphere for a period of time and at a temperature at least sufficiently high to solubilize the intermetallic or .mu. phase, Co.sub.7 W.sub.Type: GrantFiled: July 30, 1987Date of Patent: August 9, 1988Assignee: Teledyne Industries, IncorporatedInventors: Thomas W. Penrice, James Bost
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Patent number: 4762677Abstract: This invention deals with a method of producing a bulk amorphous metal alloy article. The method involves mechanically alloying an amorphous matrix material and a crystalline element which is a fast diffuser in the matrix material to give a powder mixture which is at least 50% but less than 100% amorphous. This powder mixture is then formed into a bulk amorphous metal alloy article by ordinary forming methods such as hot-pressing. The resultant bulk amorphous metal alloy article can be heated above its glass transition temperature to provide a bulk crystalline metal alloy article.Type: GrantFiled: November 3, 1987Date of Patent: August 9, 1988Assignee: Allied-Signal Inc.Inventor: Benjamin P. Dolgin
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Patent number: 4762679Abstract: A process for manufacturing powder metallurgy (P/M) preforms which are conditioned for optimum intrinsic workability is described which comprises steps of heating a quantity of P/M material in a can to a first preselected temperature under vacuum to degas the material, compacting the canned material at a second preselected temperature under pressure to provide a compact of the material; or cold compacting the powder to about 75% density and degassing it at suitable temperature and then vacuum hot pressing the powder at about 0.Type: GrantFiled: July 6, 1987Date of Patent: August 9, 1988Assignee: The United States of America as represented by the Secretary of the Air ForceInventors: Harold L. Gegel, Yellapregada V. R. K. Prasad, Sokka M. Doraivelu, Raghavan Srinivasan, J. S. Gunasekera, Douglas R. Barker, James T. Morgan, Jr., James C. Malas, Kristine A. Lark, Lawrence E. Matson
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Patent number: 4759905Abstract: Apparatus is provided for the production of ultrafine powder. The powder is produced by spark erosion within an electric discharge cell. The starting material for production of the powder is a body in chunk form of the material to be pulverized. The material is contained in an electric discharge cell having a fine mesh screen bottom. The cell and its contents are immersed in a dielectric fluid such as water, liquified gas or an organic base liquid. The cell and its contents are vibrated to cause the chunks to separate repeatedly and momentarily. A sparking voltage is impressed repeatedly through the body to develop sparks between confronting portions of separated chunk surfaces. Small particles produced as a result of the sparking fall through the screen of the cell and are collected as product.Type: GrantFiled: April 3, 1987Date of Patent: July 26, 1988Assignee: General Electric CompanyInventors: John L. Walter, Ami E. Berkowitz
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Patent number: 4756677Abstract: The weapon barrel comprises a liner and at least one jacket tube. The liner is made of a highly wear-resistant material, like a cobalt or nickel base alloy, and the jacket tube is made of a tough alloy, like steel. In the manufacturing process the liner material is packed into the jacket tube in the form of a powdery material which may be pre-pressed or pre-sintered. The packing is arranged such as to leave a central free space in the jacket tube, and the jacket tube may be surrounded by an encapsulating tube. The jacket tube or the encapsulating tube is closed either before or after evacuation, and the closed tube arrangement is subjected to a combined heat and pressure treatment at temperatures of at least 900.degree. C., but below the melting point of the relevant materials and at pressures of at least 900 bar. The compound body thus obtained is formed with a full-area metallic bond between the liner and the jacket tube.Type: GrantFiled: October 7, 1986Date of Patent: July 12, 1988Assignee: Vereinigte Edelstahlwerke AktiengesellshaftInventors: Bruno Hribernik, Manfred Gstettner, Alexander Kohnhauser
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Patent number: 4756753Abstract: An aluminum matrix composite containing evenly dispersed reinforcement particles in the aluminum matrix wherein the contents of oxygen and carbon are controlled so that their volume percentage is not larger than 20% and wherein the contents of the reinforcement particles, oxygen and carbon are controlled so that their volume percentage is not larger than 40%. The control of oxygen and carbon is effected by carrying out the main process at a non-oxidizing atmosphere and minimizing the addition of an anti-seizure agent required to facilitate the mechanical alloying treatment.Type: GrantFiled: August 26, 1987Date of Patent: July 12, 1988Assignee: Showa Aluminum Kabushiki KaishaInventor: Tsunemasa Miura
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Patent number: 4753782Abstract: Cemented silver powder is thermal conditioned in order to preserve the cemented silver powder morphology through subsequent processing operations.Type: GrantFiled: April 27, 1987Date of Patent: June 28, 1988Assignee: GTE Products CorporationInventor: Larry J. Gaudino
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Patent number: 4752333Abstract: The invention concerns alloys comprising a matrix based on at least one conductor metal M, formed by a homogeneous dispersion in the matrix of stable coherent particles of one or more associations of ions of type M, M', O in which M represents the metal or metals of the matrix, M' represents a different metal from M, which is capable of undergoing internal oxidation, and O represents oxygen.It also concerns the process for the production of such alloys which comprises subjecting a starting alloy powder to the action of an oxidizing agent formed by a powder with a granulometry of the order of 1 .mu.m of a metal oxide capable by thermal decomposition of providing the oxygen necessary for the internal oxidization of M', the starting alloy being based on at least one metal M, if appropriate hardened by one or more elements R or A as defined hereinbefore.Use of such alloys for the electrical, electronic and connection arts.Type: GrantFiled: January 9, 1987Date of Patent: June 21, 1988Assignee: TrefimetauxInventors: Jules Caisso, Martine Cahoreau, Edmond Dedieu, Michel Grosbras
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Patent number: 4749410Abstract: An article of tungsten heavy alloy material is disclosed, the article having essentially elongated tungsten grains, the alloy material comprising tungsten, nickel, and iron, the elongated tungsten grains having a length to diameter ratio of at least about 2 to 1.A method is disclosed for producing the above article which involves rolling a pressed and sintered body of tungsten heavy alloy material comprising tungsten, iron, and nickel in a tandem rolling mill having a succession of roll stands, each stand consisting essentially of three rolls positioned at about 120.degree. to each other so that the gap between the rolls is a triangle, each stand being rotated about 180.degree. with respect to the adjacent roll stands, the rolling being done at a sufficient temperature to produce the article which has essentially elongated tungsten grains.Type: GrantFiled: February 17, 1987Date of Patent: June 7, 1988Assignee: GTE Products CorporationInventors: James A. Mullendore, James R. Spencer
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Patent number: 4748088Abstract: The invention relates to a blank for a tool die, made of compound steel with a core of high speed steel and a surrounding ring of a different steel, said ring bringing about a prestress in the core. According to the invention, the prestress is due to the fact that the core consists of a high speed steel powder which has been compacted to full density, that the ring consists of a steel alloy, the residual austenite transformation to martensite and consequent volume increase of which is zero or considerably less than the residual austenite transformation to martensite of the high speed steel after the same heat treatment, and that the blank has been hardened and tempered to create in the core a compression stress as a result of the obstruction by the surrounding ring of the volume increase of the core.The invention relates also to a method for manufacturing such blanks. A high speed steel powder is filled into a thick-walled pipe, said pipe consisting of a steel different from high speed steel.Type: GrantFiled: June 19, 1985Date of Patent: May 31, 1988Assignee: Kloster Speedsteel AktiebolagInventor: Per Billgren
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Patent number: 4732625Abstract: An age hardened spinodally decomposed alloy prepared by powder metallurgy consisting essentially of from about 5 to about 30 percent by weight nickel, from about 4 to about 13 percent by weight tin, from about 0.5 to about 3.5 percent by weight cobalt and the balance copper exhibits an excellent combination of strength, ductility, formability and electrical conductivity characteristics.Type: GrantFiled: July 29, 1985Date of Patent: March 22, 1988Assignee: Pfizer Inc.Inventor: Ronald J. Livak
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Patent number: 4731115Abstract: A microcomposite material having a matrix of a titanium-base alloy, the material further including about 10-80% by weight TiC substantially uniformly dispersed in the matrix. Several methods of cladding a macrocomposite structure including pressing quantities of a matrix material and a microcomposite material composed of the matrix material and a compatible stiffener material into layers to form a multi-layered compact and sintering the multi-layered compact to form an integral metallurgical bond between the layers of the compact with diffusion but essentially no composition gradient between the layers. A multi-layered macrocomposite article composed of an alloy layer of a matrix material and a layer of a microcomposite material composed of the matrix material and a compatible stiffener material bonded together at the interface region between the layers, the interface region being essentially free of a composition gradient.Type: GrantFiled: February 22, 1985Date of Patent: March 15, 1988Assignee: Dynamet Technology Inc.Inventors: Stanley Abkowitz, Harold L. Heussi, Harold P. Ludwig
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Patent number: 4731116Abstract: Sputter targets and a process for producing sputter targets are provided, comprised of carbides and/or nitrides and/or borides of refractory metals. In a first step, a dense composite body is produced comprised of one or more carbides and/or nitrides and/or borides of the metals of Groups IV A-VI A of the periodic table and a metallic binding agent comprised of one or more metals of the iron group of the periodic table. This composite body in the form of a shaped blank is machined, if necessary, and the binding agent is removed by chemical or electrochemical treatment. The sputter target as so produced has excellent mechanical strength and high thermal shock resistance. Levels of contaminating elements and the residual metallic binding agent are extremely low, meeting the requirements typically placed on sputter targets.Type: GrantFiled: December 18, 1986Date of Patent: March 15, 1988Assignee: Schwarzkopf Development CorporationInventor: Erich Kny
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Patent number: 4726927Abstract: A method and apparatus are disclosed for producing a powder metal part having a plurality of cavities. The method involves introducing a metal powder and an apparatus into a mold, the apparatus being made of a plurality of solid pieces which are in the shape of the cavities to be formed. The pieces are joined together by joining means and are positioned relative to each other by adjusting means so that the cavities formed therefrom are equally spaced about the center of the part. The apparatus is then removed from the mold, and the powder is then isostatically pressed in the mold to produce a green part which is then sintered to form the final part having the cavities.Type: GrantFiled: February 25, 1987Date of Patent: February 23, 1988Assignee: GTE Products CorporationInventors: Ricky D. Morgan, Vito P. Sylvester
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Patent number: 4722825Abstract: A method of producing a metal/ceramic composite structure in which an uncolidated metal or metal alloy powder is loaded into a sealable glass mold comprising a hollow ceramic sleeve and a sealable outer glass envelope surrounding the ceramic sleeve and forming with the outer wall of the ceramic sleeve a sealable chamber for the metal or metal alloy powder, wherein the glass is a type which becomes plastic when heated. The air in the mold is removed under vacuum and the mold is sealed and placed into a free flowing refractory powder in a crucible and consolidated by sintering under atmospheric pressure (CAP.RTM. process). Removal of the glass envelope leaves a composite article having a consolidated metal or metal alloy layer surrounding and placing a hollow ceramic liner (sleeve) under both radial and axial compression. A ceramic-line metal gun barrel insert can be produced by using a ceramic sleeve with rifling on its inner surface.Type: GrantFiled: July 1, 1987Date of Patent: February 2, 1988Assignee: The United States of America as represented by the Secretary of the NavyInventor: David Goldstein
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Patent number: 4714468Abstract: A dispersion strengthened cobalt-chromium-molybdenum alloy produced by gas atomization containing a fine oxide dispersion, and characterized, after fabrication by gas atomization, thermomechanical processing and further high temperature exposure, by excellent corrosion resistance, high fatigue strength, high ductility and high temperature stability; a process for producing said alloy and prostheses formed from said alloy.Type: GrantFiled: January 27, 1987Date of Patent: December 22, 1987Assignee: Pfizer Hospital Products Group Inc.Inventors: Kathy K. Wang, Larry J. Gustavson, John H. Dumbleton
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Patent number: 4712411Abstract: The present invention provides an apparatus for producing in a single stroke a forged metal article with a helical contoured surface. The apparatus uses an upper punch with a generally smooth surface which is telescopically received in a punch housing and a lower punch of generally smooth surface which is mounted for free rotation with respect to the axis of the die assembly. This design allows for the use of a die of the general configuration and length of the finished article which is economical and efficient to operate.Type: GrantFiled: May 15, 1986Date of Patent: December 15, 1987Assignee: Clevite Industries Inc.Inventor: Roy S. Goodwin
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Patent number: 4710345Abstract: A manufacturing method of super-heat-resisting alloy material characterized in comprising the steps of: (1) filling and sealing the powder of Ni-based super-heat-resisting alloy in a rubber mold; (2) subjecting the powder in the rubber mold to cold isostatic pressing; (3) sintering the compact in vacuum or in gas atmosphere at a temperature of 1000.degree. C. or more so that the sintered density increases to 95% or more than the theoretical density; and (4) next, subjecting the sintered compact to hot isostatic pressing.Type: GrantFiled: April 22, 1986Date of Patent: December 1, 1987Assignee: Japan as represented by Director-General, Agency of Industrial Science & TechnologyInventors: Yoshihiko Doi, Nobuhito Kuroishi, Shigeki Ochi, Noboru Uenishi
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Patent number: 4708912Abstract: A sintered metal body with at least one toothing thereon and a method of forming the same. The toothing is formed in a sintered metal blank with or without pre-toothing by metal forming. The final toothing is cold rolled into the sintered metal blank. The thus formed sintered metal body with at least one toothing can be used for highly stressed toothed gears, such as involutes, cycloids, and epicycloids, as used, for example, on bevel gears, and particularly curved-toothed bevel gears.Type: GrantFiled: May 27, 1986Date of Patent: November 24, 1987Assignee: Sintermetallwerk Krebsoege GmgHInventor: Winfried Huppmann
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Patent number: 4707332Abstract: A process for manufacturing structural parts of complicated shape from intermetallic phases capable of sintering by means of special additives which serve at the same time as sintering assist and increase the ductility of the finished structural part. The process includes the steps of making by melting a pre-alloy of the intermetallic phase, comminuting the pre-alloy into fine powder and mixing the fine powder with one or more additives into a mass which can then be shaped and subsequently sintered at a temperature of 70 to 95% of the absolute melting point of the intermetallic phases into a structural part of increased ductility and a density greater than 95% of the theoretical density which might possibly be subjected to subsequent pressing operations.Type: GrantFiled: October 16, 1986Date of Patent: November 17, 1987Assignee: MTU Moroten-und Turbinen-Union Muenchen GmbHInventor: Werner Huether
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Patent number: 4704249Abstract: The invention relates to a process for producing a superconducting wire, using, e.g., Chevrel phases as superconductors, in particular PbMo.sub.6 S.sub.8. Until now, it was not possible to produce superconducting wires from such materials in a technically usable quality. According to the process of the invention, the superconducting Chevrel phase is loaded vacuum-tight into a molybdenum shell and the unit is advantageously sealed in another jacket made of steel. The powdery superconducting phase has an average grain size of less than 1 .mu.m. For shaping the superconducting wire, the unit is extruded in a first process step at temperatures between 1000.degree. and 1600.degree. C. and reduced in cross section in excess of 1:10, and subsequently further treated in a plurality of process steps by additional extruding and/or hot drawing.Type: GrantFiled: November 13, 1985Date of Patent: November 3, 1987Assignee: Schwarzkopf Development CorporationInventor: Wolfgang Glatzle
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Patent number: 4702885Abstract: A process for producing an aluminum alloy comprises: producing an aluminum alloy powder, consisting of (A) 10 to 36 wt % of Si, 1 to 12 wt % of Fe, 2 to 10 wt % of at least one of metal selected from the group consisting of Ni, Co, Cr and Mn, reminder of the alloy powder consisting of aluminum, or consisting of (B) 10 to 36 wt % of Si, 2 to 10 wt % of Ni, 2 to 10 wt % of at least one of metal selected from the group consisting of Fe, Co, Cr, and Mn, and remainder of the alloy powder consisting of aluminum; compressing a mass of the powder by either compacting the power or accumulating the powder in a can where in case of compacting the powders are so as to have its actual density ratio of 65% to 90%, and in case of the accumulation the powders are compressed so as to have its actual density ratio of not more than 90%; heating the thus compressed mass of powder in convection type heating furnace at a temperature of 250.degree. C. to 550.degree. C.Type: GrantFiled: June 27, 1986Date of Patent: October 27, 1987Assignee: Sumitomo Electric Industries, LTD.Inventors: Yusuke Odani, Kiyoaki Akechi, Nobuhito Kuroishi
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Patent number: 4699657Abstract: Very fine grain metal billets are produced by loading alloy metal powder of desired composition into a metal extrusion container in successive layers of two or four inches deep. Each layer after loading is compacted by a high energy rate forming ram so as to introduce energy on the order of 3.times.10.sup.6 psi per layer and at least 18.times.10.sup.6 psi total. An inner plate is then loosely placed on the compacted powder. On top of the inner plate is placed a cover plate which is welded to the container. The filled container is then heated in a furnace to an extrusion temperature below the melting point of the alloy and is extruded in an extrusion press having a ratio of about 3:1 with a force of about 3,000 tons. The inner plate does not move at the same rate as the container and in effect is partially extruded against the powder so as to raise the density of the extruded billet to substantially 100% of its theoretical density.Type: GrantFiled: November 3, 1986Date of Patent: October 13, 1987Assignee: Worl-Tech LimitedInventor: Vincent N. DiGiambattista
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Patent number: 4699763Abstract: An electrical contact material characterized by a pressed and sintered powder of silver composite with about 5 weight percent of graphite fibers.Type: GrantFiled: June 25, 1986Date of Patent: October 13, 1987Assignee: Westinghouse Electric Corp.Inventors: Semahat D. Sinharoy, Jere L. McKee, Norman S. Hoyer
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Patent number: 4693864Abstract: Mill scale, iron ore, or taconite is utilized in a powder metallurgy process to form steel articles having approximately the same density as that of conventional rolled steel. Particulate iron is mixed with manganese, carbon, additional alloying ingredients, and a binder to form a particulate admixture. The particulate admixture is then compressed, preferably under extreme pressure until the density of the compressed particulate admixture is from about 0.2408 lbs/in.sup.3 (6.67 g/cm.sup.3) to about 0.2833 lbs/in.sup.3 (7.83 g/cm.sup.3), which corresponds to a density of from about 85% to about 100% of the density of conventional rolled steel. The resultant coherent mass is subjected to sintering and below fusion heating to form an alloyed article which can be swaged, rolled, drawn, or worked at elevated temperature to decrease the grain size of the alloyed article. The resultant end-product will preferably have a density of from about 0.2408 lbs/in.sup.3 (6.67 g/cm.sup.3) to about 0.2833 lbs/in.sup.3 (7.Type: GrantFiled: December 5, 1985Date of Patent: September 15, 1987Assignee: Donald W. Lloyd Realty, Inc.Inventor: Donald W. Lloyd
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Patent number: 4693863Abstract: A powder metallurgy consolidation process and apparatus for carrying out said process produces integral metal bodies by heating metal powder of a predetermined composition to a temperature sufficient to cause solid state interparticle bonding, while simultaneously maintaining a reactive fluid in contact with the metal powder. The metal powder is compacted to a density greater than 90% of the full theoretical density of the composition after the reactive fluid has been removed. The reactive fluid is selected to modify the powder particle surface chemistry in order to improve bondability and to obtain other properties as desired. Metal bodies which have been consolidated by the process are sufficiently dense to be mechanically hot worked and exhibit exceptionally low retained gas content.Type: GrantFiled: April 9, 1986Date of Patent: September 15, 1987Assignee: Carpenter Technology CorporationInventors: Gregory J. Del Corso, Robert E. Carnes, David Esposito
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Patent number: 4689077Abstract: A method is disclosed for manufacturing a reaction sintered composite article which comprises at least one ceramic component. The method comprises preparing a particulate mixture of precursor powders leading to the formation of said composite material upon reaction sintering, pressing said particulate mixture to a self-sustaining body, heating said body up to a temperature below the temperature at which the reaction sintering is initiated, comminuting the heat treating body, selecting particles of a suitable grain size distribution, pressing said particles into shapes of desired size and configuration, and heating said shapes up to a temperature at which the reaction sintering is initiated. The reaction sintered body comprises borides, carbides, nitrides or silicides of a transition metal of the groups IVb, Vb or VIb of the periodic table (comprising titanium, hafnium, zirconium, vanadium, niobium, tantalum, chromium, molybdenum and tungsten), and a metal oxide.Type: GrantFiled: May 19, 1986Date of Patent: August 25, 1987Assignee: ELTECH Systems CorporationInventors: Michel Chevigne, Dominique Darracq, Jean-Pol Wiaux
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Patent number: 4680161Abstract: A method of producing a sliding composite material. The method comprises the step of: forming an adhesive layer bonded to the surface of a metal strip by sintering a powder for the adhesive layer which contains no solid lubricant and which is disposed onto the surface of the metal strip; forming a surface layer by sintering another powder for the surface layer which contains a solid lubricant and which is disposed onto the sintered adhesive layer; and rolling the resulting layers and the metal strip to obtain the composite material.Type: GrantFiled: August 13, 1986Date of Patent: July 14, 1987Assignee: Daido Metal Company Ltd.Inventor: Takashi Muto
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Patent number: 4678717Abstract: Coatings of a powdered protective metallic material or refractory material and mixtures thereof are formed on a ferrous metal strip as a wet film dispersion in a resin binder composition of a synthetic organic resin and a volatile organic solvent compatible with said resin, and the coated strip is heated to effect curing said resin binder and forming a flexible non-tacky dry film. The metal strip having the cured dry film containing powdered protective metallic material can be subjected to varying heat treatments to provide a wide range of protective coatings having improved surface properties, including iron-protective metal diffusion alloy coatings, such as iron-aluminum diffusion alloy coatings having a surface concentration of aluminum between about 8 and 10 wt. percent aluminum, which have improved high temperature oxidation resistance after being severely strained during fabrication at room temperature.Type: GrantFiled: September 17, 1985Date of Patent: July 7, 1987Assignee: Inland Steel CompanyInventors: Richard A. Nickola, Brian A. Sok, Shashi B. Agarwal
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Patent number: 4673550Abstract: There is disclosed a process for synthesizing TiB.sub.2 composite materials containing a metallic phase. The preparation of these composites comprises providing mixtures of titanium alloys which in addition to at least 30 wt. % titanium also contain F, Ni, Al, Mo, Cr, Co, Cu or mixtures thereof, and boron or ferroboron, reacting these mixtures by local igniting and exothermic reaction or by heating or melting, resulting in the synthesis of composite material containing fine TiB.sub.2 crystals dispersed in a fine metallic phase which is derived from the metallic element previously alloyed or combined with the titanium of the titanium alloys or the metallic element or elements contained in the ferroboron. By leaching out the metallic phase, fine TiB.sub.2 powders may be obtained. Parts and coatings can also be obtained. The parts are normally obtained by treating the TiB.sub.2 material by powder metallurgic techniques. Coatings may be obtained by thermo or plasma spray depositing on a substrate.Type: GrantFiled: September 24, 1986Date of Patent: June 16, 1987Inventors: Serge Dallaire, Blaise Champagne
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Patent number: 4670214Abstract: A method and apparatus for making electrode material from high hardness active electrode alloy powder are disclosed. In one embodiment, the method involves feeding the powder onto a carrier web, aligning a mesh or screen substrate with the carrier web, and compacting the powder and mesh in a series of roller mills. The carrier is removed after it has passed through the first roller mill, and the remaining green electrode web is passed through the second roller mill and into a sintering furnace. After sintering and cooling, the web is calendared, and then is wound on a take-up reel. The furnace provides a substantially water and oxygen-free argon-hydrogen atmosphere for sintering which discourages web oxidization at the elevated sintering temperature. A loss-in-weight feeder can be used to accurately deposit the desired amount of active material on the carrier web.Type: GrantFiled: May 12, 1986Date of Patent: June 2, 1987Assignee: Energy Conversion Devices, Inc.Inventors: Douglas Magnuson, Merle Wolff, Sam Lev, Kenneth Jeffries, Scott D. Mapes
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Patent number: 4665828Abstract: The invention relates to a penetrator (1, 11) made of heavy metal, such as, for instance, tungsten heavy metal or depleted uranium, for driving-cage projectiles which have the penetrator led by the driving cage in the gun barrel. The driving cage (6, 12) detaches itself from the penetrator after the launch. The penetrator (1, 11) shows lower strength and higher ductility in the middle portion (d) of its length than in its head portion (c) and, in its tail portion, it shows higher strength and lower ductility than in its middle portion (d) and lower strength and higher ductility than in its head portion (c). This shall decrease the risk of fracture when striking an armour.Type: GrantFiled: November 23, 1984Date of Patent: May 19, 1987Assignee: Voest-Alpine AktiengesellschaftInventor: Ekkehard Auer
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Patent number: 4666665Abstract: An apparatus and method of hot-forging in a forging press a cylindrical powdered metal preform to substantially full theoretical density to thereby produce a powdered metal part having a small inner bore wherein the core rod defining such bore is constructed so as to allow a continuous flow of a highly vaporizable liquid coolant such as nitrogen to the metal forming portion of the core rod and to thermally insulate the incoming coolant to assure its being maintained substantially unvaporized until being expelled to the core rod cooling chamber.Type: GrantFiled: January 30, 1986Date of Patent: May 19, 1987Assignee: Federal-Mogul CorporationInventors: William S. Hornsby, Joseph C. Skurka, Hayward P. Summers
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Patent number: 4666787Abstract: A material which is intended for use in sliding surface bearings comprises a metallic backing, a porous metallic substrate layer applied to said backing, and a PTFE-filler mixture, which completely fills the pores of the substrate layer and constitutes an antifriction layer. The bond strength between the antifriction layer and the substrate layer is improved by coating that surface of the substrate layer which faces the antifriction layer with a primer.Type: GrantFiled: February 14, 1986Date of Patent: May 19, 1987Assignee: Kolbenschmidt AktiengesellschaftInventors: Wolfgang Bickle, Jurgen Braus, Hans-Paul Baureis
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Patent number: 4661155Abstract: A molded, boron carbide-containing, sintered article which includes at least 65 percent by volume boron carbide; and from 5 to 35 percent by volume of at least one binder metal selected from the group consisting of molybdenum, molybdenum alloys, tungsten and tungsten alloys, having a melting point above 1,800.degree. C., and forming no molten borides or carbides within a temperature range of from 1,800.degree. to 1,950.degree. C. A method for producing the article includes the steps of mixing to obtain a homogeneous mixture from 20 to 80 percent by weight boron carbide particles having a particle size ranging from 1 to 1,650 microns with up to 80 percent by weight of particles of the at least one binder metal having a particle size ranging from 35 to 100 microns; introducing the homogeneous mixture into a graphite matrix mold; heating to sinter the homogeneous mixture at a temperature ranging from 1,800.degree. to 2,000.degree. C.Type: GrantFiled: May 21, 1986Date of Patent: April 28, 1987Assignee: Kernforschungszentrum Karlsruhe GmbHInventors: Volker Heinzel, Hossein-Ali Keschtkar, Ingeborg Schub
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Patent number: 4657822Abstract: Alloy powder is packed into a mold which comprises a complex-shaped solid aphite inner core and a similarly complex-shaped thin glass outer wall. The mold is evacuated, sealed, and then heated to the alloy sintering temperature, the glass softens and applies an isostatic pressure on the alloy as the alloy particles consolidate. After the consolidation step, the mold and its contents are cooled and the glass and graphite materials are removed from the alloy object. This method is particularly useful for preparing complex fittings of Nitinol shape memory alloys.Type: GrantFiled: July 2, 1986Date of Patent: April 14, 1987Assignee: The United States of America as represented by the Secretary of the NavyInventor: David Goldstein
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Patent number: 4636251Abstract: A new alloy material for use in electrical contacts is disclosed, comprising by weight______________________________________ Beryllium 1-2% Palladium 2-20%; and ______________________________________the balance of nickel.Type: GrantFiled: April 17, 1986Date of Patent: January 13, 1987Assignee: International Business Machines CorporationInventor: Issa S. Mahmoud
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Patent number: 4632702Abstract: Metal powder of the desired composition having a particle size of -80 mesh is charged into an extrusion container, preferably a piece of carbon steel pipe, in successive layers about two inches thick. Each layer is compacted after deposition by a high energy rate forming ram so as to raise the tap density of the powder to about 80% of theoretical. An inner cover plate is then placed loosely on the compacted powder in the extrusion container, and is not attached to the container shell. On top of this inner plate is placed an outer cover plate which is welded to the container shell. Both plates are also of carbon steel, but are much thicker than the container wall. The container so prepared is heated in a heating furnace to a temperature below the melting temperature of the container and the powder alloy thus raising the density of the powder to about 90-93% of theoretical.Type: GrantFiled: April 9, 1986Date of Patent: December 30, 1986Assignee: Worl-Tech LimitedInventor: Vincent N. DiGiambattista
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Patent number: 4629505Abstract: A metallurgical method including cooling molten aluminum particles and consolidating resulting solidified particles into a multiparticle body, wherein the improvement comprises the provision of greater than 0.15% of a metal which diffuses in the aluminum solid state at a rate less than that of Mn.Aluminum containing greater than 0.15% of a metal which diffuses in the aluminum solid state at a rate less than that of Mn.Type: GrantFiled: April 2, 1985Date of Patent: December 16, 1986Assignee: Aluminum Company of AmericaInventor: Henry G. Paris
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Patent number: 4624705Abstract: Aluminum-base alloys and a method of preparing aluminum-base alloys by mechanical alloying in the presence of a carbidiferous processing aid wherein a strong carbide former such as titanium is included so as to produce carbides in the final alloy more thermally stable at temperatures in excess of 100.degree. C. than Al.sub.4 C.sub.3.Type: GrantFiled: April 4, 1986Date of Patent: November 25, 1986Assignee: Inco Alloys International, Inc.Inventors: Arun D. Jatkar, Paul S. Gilman, Raymond C. Benn