Subsequent Working Patents (Class 419/28)
  • Patent number: 5008071
    Abstract: A consolidated tungsten alloy body consisting essentially of from about 70% to about 98% by weight of tungsten, balance nickel and iron in essentially an 8:2 weight ratio. A process for producing the consolidated bodies where the tungsten content is greater than about 88% by weight comprises forming a relative uniform blend of the described metal powders, compacting the powders to form a green body then liquid phase sintering the green body to full density. For alloys containing less than about 90% tungsten solid state sintering can be used.
    Type: Grant
    Filed: November 25, 1988
    Date of Patent: April 16, 1991
    Assignee: GTE Products Corporation
    Inventors: James R. Spencer, James A. Mullendore
  • Patent number: 5006289
    Abstract: Method for producing an elongated sintered article, characterized by the steps including filling powder material in a pipe, carrying out plastic deformation of the pipe filled with the powder material, and heating the pipe filled with the powder material to burn and/or sinter the powder material.The method of the present invention is advantageously applicable to production of wire or rod of ceramics, particularly so called new ceramics or fine ceramics, sintered alloys or their combination, which are difficult of shaping or moulding by conventional process such as wire-drawing, rolling or extrusion or powder material and are difficult of machining or processing after the powder material is sintered.
    Type: Grant
    Filed: June 17, 1987
    Date of Patent: April 9, 1991
    Assignee: Sumitomo Electric Industries, Ltd.
    Inventors: Susumu Yamamoto, Teruyuki Murai, Nozomu Kawabe, Masaaki Tobioka
  • Patent number: 4992236
    Abstract: A method of making a golf club head and golf club heads produced by said method which involves filling a mold with material selected from the group consisting of metal powders, castings, wrought metal, and green compact metal powders and combinations thereof so as to achieve the desired properties in the particular areas of the club head, compressing the material in the mold to form a green compact of the material, removing the green compact of the material from the mold land then heating the green compact to an elevated temperature to form a sintered product. Thereafter, the sintered product may be further heated under pressure to improve its density.
    Type: Grant
    Filed: January 16, 1990
    Date of Patent: February 12, 1991
    Inventor: Chester S. Shira
  • Patent number: 4990306
    Abstract: The invention relates to a method of producing a sintered Nd-Fe-B magnet which has a cylindrical or annular shape and is magnetized in radial directions with polar anisotropic orientation. In a cylindrical mold cavity filled with a Nd-Fe-B magnetic alloy powder a pulse of magnetic field is produced so as to cause polar anisotropic orientation of the magnetic powder with at least six poles distributed around the circumference, and a pulse-like pressure is applied to the powder in the mold cavity to compact the powder into a cylindrically shaped body while the pulse of magnetic field is lasting. The shaped body is sintered, and subsequently the side surface of the sintered body is abraded to remove projecting regions, which are attributed to anisotropic shrinkage during sintering, until the surface becomes accurately cylindrical.
    Type: Grant
    Filed: November 17, 1989
    Date of Patent: February 5, 1991
    Assignee: Shin-Etsu Chemical Co., Ltd.
    Inventor: Ken Ohashi
  • Patent number: 4988480
    Abstract: The proposed invention is used for the manufacture from the obtained composite of cutting tools, hard alloy tooling, dies and other products. A method according to the invention involves preparing a mixture, compacting it, placing the mixture into a synthesis zone, igniting the mixture, with subsequent reaction of components of the mixture under combustion conditions. Then cure is carried out during a period ranging from about 0.1 seconds to about 0.5 hours, and the hot combustion products are compacted under pressure at an average pressure rise rate ranging from about 10 to about 2000 kgf/cm.sup.2.s, with subsequent cure of the compacted product under isobaric conditions to complete homogenization of the composite, with subsequent cooling thereof to obtain an end composite.
    Type: Grant
    Filed: August 23, 1990
    Date of Patent: January 29, 1991
    Inventors: Alexandr G. Merzhanov, Inna P. Borovinskaya, Alexandr N. Pitjulin, Viktor I. Ratnikov, Konstantin L. Epishin, Vadim L. Kvanin
  • Patent number: 4983355
    Abstract: A seal elements of hard material for use, for instance, as a pair of small plates which form the parts to control the fluid flow through a faucet. The seal is constructed of a hard material--a metal, a metallic oxide, a metallic carbide, a metallic nitride, a ceramic or glassy material--which is sintered from a semi-finished product obtained by mixing a powder of fine particle size of the aforementioned hard materials with an organic binder--a plastic material, a wax, or a combination of these substances. This mixture is formed under compression in a mold and, eventually, at least some of the binder is eliminated.
    Type: Grant
    Filed: October 2, 1989
    Date of Patent: January 8, 1991
    Assignee: Masco Corporation of Indiana
    Inventor: R. Knapp Alfons
  • Patent number: 4981512
    Abstract: A composite material comprising a metal matrix containing tungsten grain is roduced from tungsten powders formed by plasma rapid solidification. The powders comprise tungsten and up to 20 weight percent of a metal selected from the group consisting of molybdenum, tantalum, niobium, rhenium, and chromium. The surfaces of the powders are cleaned to reduce the surface oxide thereon, and the powders are coated with at least one metal selected from the group consisting of copper, nickel, cobalt, hafnium and tantalum. The coated powders are formed into a sintered preform which is less than fully dense, and the sintered preform is further consolidated to full density by a technique selected from hot isostatic pressing, rapid omin-directional compaction, and hot extrusion.
    Type: Grant
    Filed: July 27, 1990
    Date of Patent: January 1, 1991
    Assignee: The United States of America as represented by the Secretary of the Army
    Inventor: Deepak Kapoor
  • Patent number: 4980122
    Abstract: A superplastic composite material is produced by thoroughly and homogeneously mixing particles or whiskers of silicon nitride and aluminum metal powder in a solvent, then removing the solvent from the resultant mixture, sintering the residual mixture at an elevated temperature, further compressing it at an elevated temperature, then hot extrusion-molding the compressed mixture thereby forming a shaped article, and heat-treating this shaped article.
    Type: Grant
    Filed: March 23, 1990
    Date of Patent: December 25, 1990
    Assignee: Agency of Industrial Science & Technology, Ministry of International Trade & Industry
    Inventors: Tsunemichi Imai, Mamoru Mabuchi
  • Patent number: 4971756
    Abstract: Producing a die for use in compacting permanent magnet alloy powder by placing a quantity of a magnetic or nonmagnetic alloy, which may be stainless steel, cobalt- or nickel-base, or a magnetic or nonmagnetic mixture of one of these alloys and carbide particles in a container, heating the particles to an elevated temperature and hot-isostatically compacting the particles at the elevated temperature to obtain a fully dense die blank and forming a die cavity in the die blank. Carbide particles may be mixed with the alloy particles. The die blank may have an exterior cladding of stainless steel.
    Type: Grant
    Filed: May 12, 1989
    Date of Patent: November 20, 1990
    Assignee: Crucible Materials Corporation
    Inventor: John J. DuPlessis
  • Patent number: 4971754
    Abstract: The method concerns preparing a contact material constituted by silver and tin oxide.According to the invention the method comprises the following steps:preparing an aqueous solution containing dissolved silver nitrate and tin oxide particles in suspension, with the size of said particles measured in terms of specific surface area using the BET method lying between about 2 m.sup.2 /g and 6 m.sup.2 /g;causing silver nitrate to precipitate in silver hydroxide by rapidly adding a strong base and stirring, with silver hydroxide being unstable and transforming progressively into silver oxide;eliminating the ions from the solution and then the water in order to obtain a dry product; andheating the dry product to a temperature of about 200.degree. C. to 500.degree. C. in order to reduce the silver oxide to metallic silver.The invention is applicable to manufacturing electrical contacts for opening and closing in electromechanical apparatuses.
    Type: Grant
    Filed: November 22, 1989
    Date of Patent: November 20, 1990
    Assignee: Telemecanique
    Inventors: Gerard Fontet, Michel Leclercq, Jacques Muniesa, Thierry Pagnier, Tretarre Rene
  • Patent number: 4966748
    Abstract: A clad metal is produced by forming a layer of a dissimilar metal powder on the surface of a base metal by cold fixing the powder to the surface under pressure, densing only the surface and a subsurface area of the layer of the dissimilar metal powder by melting and immediately solidifying in a vacuum, compressing the layer of the dissimilar metal powder together with the base metal at a temperature not higher than the solidus-line temperature of the two dissimilar metals under a pressure of not lower than 300 kgf/cm.sup.2 (or 29.4 MPa) using a hot isostatic press, and hot working the layer of the dissimilar metal powder together with the base metal.
    Type: Grant
    Filed: March 7, 1990
    Date of Patent: October 30, 1990
    Assignee: Nippon Steel Corporation
    Inventors: Akihiro Miyasaka, Hiroyuki Ogawa
  • Patent number: 4960563
    Abstract: The invention relates to a process for the production of a heavy tungsten-nickel-iron alloy with high mechanical characteristics comprising the steps of using powders of each of the elements of a FISHER diameter between 1 and 15 .mu.m, mixing the powders in proportions corresponding to the composition of the desired alloy, compressing the powders in the form of compacted items, sintering the compacted items at a temperature of between 1490 and 1650.degree. C. for 2 to 5 hours, treating the sintered compacted items under vacuum at between 1000.degree. and 1300.degree. C., and subjecting the compacted items after treatment under vacuum to at least three cycles of operation, each cycle comprising a working step followed by a heat treatment.
    Type: Grant
    Filed: March 7, 1990
    Date of Patent: October 2, 1990
    Assignee: Cime Bocuze
    Inventor: Guy Nicolas
  • Patent number: 4954314
    Abstract: A plural number of types of material powders are accommodated in an accommodation chamber in a mixed state and the material powders are continuously subjected to a self-exothermic reaction inducing chemical reactions between the material powders caused by heat of reaction released when the mixed material powders synthesize. The synthesized material of high temperature due to the self-exothermic reaction is pressed by utilizing an electromagnetic force just after the finish of the self-exothermic reaction. The exothermic reaction is caused by an ignition circuit including an ignition electrode and the electromagnetic force is generated by an electromagnetic force generation circuit including an electric current inducing means. These circuits are connected through and regulated by a relay circuit. Thus the synthetic products of fine structure are obtained.
    Type: Grant
    Filed: February 7, 1990
    Date of Patent: September 4, 1990
    Assignee: Kawasaki Jukogyo Kabushiki Kaisha
    Inventors: Yukio Nishiyama, Junzo Fujioka, Haruki Hino, Yuji Matsuzaki, Masayuki Sakiyama, Minoru Yokoyama
  • Patent number: 4950327
    Abstract: A creep-resistant alloy having a tiered structural arrangement of one or several refractory metals Mo, W, Nb, Ta, V, Cr containing certain doping agents, as well as a process for producing the same. The special doping agents are compounds and/or mixed phases of such compounds selected from the group of oxides, nitrides, carbides, borides, silicates or aluminates having a melting point higher than 1500.degree. C. The size of their grains is .ltoreq.1.5 .mu.m, their proportion in the alloy is comprised between 0.005 and 10% by weight. Unlike in the known state of the art, the use of porassium as doping agent is avoided in this alloy. A good reproducible consolidation and in particular high densities during sintering can thus be obtained. Furthermore, this alloy has better ambient temperature, heat and creep resistance properties than known alloys of refractory metal with a tiered structual arrangement.
    Type: Grant
    Filed: September 27, 1988
    Date of Patent: August 21, 1990
    Assignee: Schwarzkopf Development Corporation
    Inventors: Ralf Eck, Gerhard Leichtfried
  • Patent number: 4941920
    Abstract: A sintered target member consisting essentially of 50-75 weight % of Co, 3-12 weight % of Cr and balance substantially Ni, which has a structure comprising dispersion phases consisting essentially of one or more elements constituting the target member and having a maximum permeability of 50 or less. This target member is produced by mixing metal or alloy powders corresponding to low-permeability dispersion phases, charging the resulting mixture into a metal container; sealing the metal container under reduced pressure; sintering it at a temperature of 900.degree.-1300.degree. C. and pressure of 500 atm or more; and removing the metal container from the resulting sintered body.
    Type: Grant
    Filed: November 23, 1988
    Date of Patent: July 17, 1990
    Assignee: Hitachi Metals, Ltd.
    Inventors: Tsutomu Inui, Shun-ichiro Matsumoto, Rokuo Ichiyasu, Takeo Mizuguchi
  • Patent number: 4940565
    Abstract: A method serves for manufacturing frictional locking rings, in particular for stepped motor vehicle transmission synchronizing mechanisms, in which a sintered frictional coating is applied on a surface of the element and the sintered frictional coating is compacted.For simplifying the method and improving the reproducibility of the dimensions of the surface of the sintered frictional coating one first applies a frictional coating of a sintering powder in a predetermined raw dimension regarding its thickness and compacts the frictional coating thereafter under pressure to a predetermined nominal dimension.
    Type: Grant
    Filed: July 24, 1989
    Date of Patent: July 10, 1990
    Assignee: Erich R. Mueller
    Inventor: Erich R. Muller
  • Patent number: 4940404
    Abstract: A method of making a tungsten tantalum material comprising generally 80 percent by weight tungsten and 20 percent by weight tantalum and forming the material into a high strength full density round bar, which can be utilized in a high velocity armor penetrator.
    Type: Grant
    Filed: April 13, 1989
    Date of Patent: July 10, 1990
    Assignee: Westinghouse Electric Corp.
    Inventors: Robert L. Ammon, Raymond W. Buckman, Jr., Ram Bajaj
  • Patent number: 4938799
    Abstract: The invention relates to heavy tungsten-nickel-iron alloys with high mechanical characteristics and a specific gravity between 15.6 and 18. The alloys include a tungsten .alpha.-phase in the shape of butterfly wings with dislocation cells of dimensions between 0.1 and 1 .mu.m, and a nickel-iron bonding .gamma.-phase having a mean free path of less than 15 .mu.m and an Ni/Fe ratio greater than or equal to 2.
    Type: Grant
    Filed: October 5, 1988
    Date of Patent: July 3, 1990
    Assignee: Cime Bocuze
    Inventor: Guy Nicolas
  • Patent number: 4929418
    Abstract: A cathode is made from tungsten powder using as an impregnant the product rmed from adding about 1 mole of a member selected from the group consisting of zirconium, zirconium dioxide, hafnium, hafnium dioxide, uranium, uranium dioxide, titanium, and titanium dioxide to about 50 to about 100 moles of a compound selected from the group consisting of Ba.sub.3 Al.sub.2 O.sub.6, Ba.sub.3 WO.sub.6, and Ba.sub.4 Al.sub.2 O.sub.7.
    Type: Grant
    Filed: January 22, 1990
    Date of Patent: May 29, 1990
    Assignee: The United States of America as represented by the Secretary of the Army
    Inventors: Louis E. Branovich, Bernard Smith, Gerard L. Freeman, Eckart Donald W.
  • Patent number: 4923674
    Abstract: A method of producing powder forged components produces parts which precisely fit together, the method including the steps of: forming a one-piece preform by pressing from powder; forming at least one tear notch in the preform at a selected location; sintering the preform; providing a protective layer on each tear notch; forging the preform into a component, including closing each tear notch during the forging to form a corresponding slit; cooling the component; and separating the component at the corresponding selected location into a plurality of individual parts by breaking.
    Type: Grant
    Filed: February 27, 1989
    Date of Patent: May 8, 1990
    Assignee: Sintermetallwerk Krebsoge GmbH
    Inventor: Manfred Weber
  • Patent number: 4923673
    Abstract: In a method for producing tungsten-alloyed rods, a particular tungsten electrodes for tungsten inert gas welding, tungsten plasma welding, tungsten plasma fusion cutting and the like, in which pulverulent tungsten with an admixed oxide additive is compacted, sintered, mechanically worked and submitted to a recrystallization treatment, to achieve a hitherto unobtained high lanthanum integration the pulverulent tungsten is alloyed with a highly pure relaxed lanthanum oxide additive of about 1.8 to 2.2% by weight with respect to the total weight the compacting is carried out with a multiphase pressure buildup and the sintering is carried out with a multiphase temperature buildup.
    Type: Grant
    Filed: August 28, 1989
    Date of Patent: May 8, 1990
    Assignee: Gesellschaft fur Wolfram-Industrie mbH
    Inventor: Richard Litty
  • Patent number: 4923512
    Abstract: Cobalt-bound tungsten carbide metal matrix composites having a unique microstructure are produced by consolidating partially sintered greenware under high pressures, e.g., 120,000 psi, at temperatures less than those used for conventional liquid phase sintering in a relatively short time, e.g., from less than one minute to less than about one hour. The composites have a binder phase which contains less than about 80 weight percent of the tungsten found in a composite prepared from the same or similar compositions via liquid phase sintering. These composites provide cutting tools with both toughness and wear resistance which exceed that of cutting tools made from the same or similar compositions via liquid phase sintering.
    Type: Grant
    Filed: April 7, 1989
    Date of Patent: May 8, 1990
    Assignee: The Dow Chemical Company
    Inventors: Ed E. Timm, Douglas B. Schwarz
  • Patent number: 4923671
    Abstract: Method of producing powder-metallurgical objects, specifically elongate objects such as rods, sections, tubes or the like, wherein a powder of metal and/or metal alloys of great hardness, particularly tool steel or high-speed steel powder, is charged into a thin-walled capsule, said capsule is then sealed so as to be airtight, is heated, and subjected to isostatic compression to produce a blank which will then undergo hot-working, specifically extrusion, for the production of the finished product. In a first alternative, the airtight and sealed capsule is initially heated to a temperature higher than 1,000.degree. C. Following through-heating of the capsule, the latter is maintained at an elevated temperature for a prolonged period. Then the capsule is slowly cooled and subjected to cold isostatic compression prior to final shaping. In a second alternative, the capsule is sealed so as to be airtight, and then subjected to an initial cold isostatic compression.
    Type: Grant
    Filed: February 6, 1989
    Date of Patent: May 8, 1990
    Inventor: Christer Aslund
  • Patent number: 4920009
    Abstract: Magnetically isotropic, fine grain, RE.sub.2 Fe.sub.4 B phase containing particulate material is hot pressed to full density and bonded to a metal backing layer of desired shape and composition. Additionally, if desired, the fully dense isotropic material can be further deformed in a direction lateral to the press direction so as to strain the particles to align the preferred magnetic axes of the crystal grains therein and thus form a laminate of a magnetically anisotropic magnet layer bonded to a metal backing layer.
    Type: Grant
    Filed: August 5, 1988
    Date of Patent: April 24, 1990
    Assignee: General Motors Corporation
    Inventors: Robert W. Lee, Earl G. Brewer
  • Patent number: 4917961
    Abstract: This invention relates to a method of producing a corrosion-, heat- and wear-resistant member which comprises packing an atomized powder of a high-carbon high-chromium steel into a capsule, heating the capsule packed with the powder, then extruding the capsule packed with the powder to obtain a stock not containing carbide grains greater than 3 .mu.m, working the stock, polishing a surface of the stock, and evaporating a film of TiC and/or TiN onto the polished surface, and further a corrosion-, heat- and wear-resistant member produced by the method. The corrosion-, heat- and wear-resistant member according to this invention is suitable for being members for tools used under extremely severe conditions, such as various tools for can manufacturing, molding tools for reinforced plastics, etc.
    Type: Grant
    Filed: August 14, 1989
    Date of Patent: April 17, 1990
    Assignees: Sanyo Special Steel Co., Ltd., Fuji Die Co., Ltd.
    Inventors: Nobuhiro Tsujii, Genryu Abe, Akira Yamaguchi, Minoru Mishuku, Nobujiro Tsuchiya
  • Patent number: 4917858
    Abstract: A method for producing foil of titanium aluminide is described which comprises providing a preselected quantity of blended powder of chloride free commercially pure elemental titanium, aluminum and other alloying metal(s) in preselected proportions, rolling the blended powder into a green foil, sintering the green foil, and thereafter pressing the sintered foil to full density.
    Type: Grant
    Filed: August 1, 1989
    Date of Patent: April 17, 1990
    Assignee: The United States of America as represented by the Secretary of the Air Force
    Inventors: Daniel Eylon, Francis H. Froes
  • Patent number: 4917722
    Abstract: A method for producing a single crystal of chromium is disclosed, comprising sintering a chromium molding to thereby apply thereto a thermal strain and heat treating the resulting thermally strained chromium molding. The method achieves high efficiency of crystal growth and produces a single-crystal chromium molding of complicated shape.
    Type: Grant
    Filed: May 18, 1989
    Date of Patent: April 17, 1990
    Assignee: Tosoh Corporation
    Inventors: Tsutomu Kuniya, Koichi Hanawa, Tomoyuki Oikawa
  • Patent number: 4914080
    Abstract: A method for fabricating a superconductive film composed of a RE.sub.1 Ba.sub.2 Cu.sub.3 O.sub.x compound, or a (Bi.Sr.Ca.Cu.O) compound. In a first embodiment, oxides or carbonates of the component materials, namely Y.sub.2 O.sub.3, BaCO.sub.3, and CuO are mixed in atomic ratios of 1:2:3, according to the chemical formula of RE.sub.1 Ba.sub.2 Cu.sub.3 O.sub.x, and sintered to create a rhombic perovskite structure. The sintered mixture is powdered again, with added powdered amounts of Y.sub.2 O.sub.3 and powdered metallic Cu, and sintered. The sintered product is used as the source for an electron beam evaporator. In a second embodiment the (Bi.Sr.Ca.Cu.O) compound is formed into a sintered pellet which is composed of a mixture of one part of BiO, 3-15 parts of SrCO.sub.3, 4-30 parts of CaCO.sub.3, and 2-5 parts of CuO, in atomic ratios of Bi, Sr, Ca and Cu.
    Type: Grant
    Filed: January 24, 1989
    Date of Patent: April 3, 1990
    Assignee: Fujitsu Limited
    Inventors: Kohta Yoshikawa, Naoki Awaji, Kyung-ho Park, Nagisa Ohsako, Seigen Ri
  • Patent number: 4911990
    Abstract: A microstructurally toughened metallic article is disclosed. The article includes discrete metal regions which are enclosed within and separated from each other by a network of metal. The regions are bonded to the network to form stable interfacial boundaries. The article exhibits high impact resistance. The process for making the article is also disclosed. The process includes positioning a plurality of structural elements within a container to define one or more void spaces within the container, introducing a quantity of metallic particles into the void spaces, and then consolidating the container, structural elements, and particles to form the microstructurally toughened article.
    Type: Grant
    Filed: February 5, 1988
    Date of Patent: March 27, 1990
    Assignee: United Technologies Corporation
    Inventors: Karl M. Prewo, Vincent C. Nardone, James R. Strife
  • Patent number: 4911626
    Abstract: A long life high current density cathode is made from a mixture of tungsten nd iridium powders by processing the mixture of powders with an activator into a porus billet, and then impregnating the billet with a mixture of barium peroxide and a coated emitter by firing the billet in a dry hydrogen furnace at a temperature at which the impregnant melts.
    Type: Grant
    Filed: November 20, 1989
    Date of Patent: March 27, 1990
    Assignee: The United States of America as represented by the Secretary of the Army
    Inventors: Louis E. Branovich, Bernard Smith, Gerard L. Freeman, Donald W. Eckart
  • Patent number: 4904537
    Abstract: An improved process and an improved composite bearing material produced thereby comprising a hard metal backing strip having leaded-bronze bearing lining tenaciously bonded to at least one face surface thereof and wherein the bearing lining is characterized by having the lead constituent thereof substantially uniformly distributed throughout the lining matrix in the form of extremely fine-sized particles providing improved operating characteristics to the bearing materials fabricated therefrom.
    Type: Grant
    Filed: October 14, 1987
    Date of Patent: February 27, 1990
    Assignee: Federal-Mogul Corporation
    Inventor: Michael D. Lytwynec
  • Patent number: 4902357
    Abstract: This invention concerns a heat treatment method for rare earth type permanent magnets which are primarily of the Nd-Fe-B type. With regard to these permanent magnets, which oxidize rather easily in the air, the alloy is crushed, and either compression formed in a magnetic a non-magnetic field, sintered at 900.degree. to 1,200.degree. C., and then machined into the shape desired, and then solution treated in an atmosphere of oxygen and/or nitrogen at a temperature of 900.degree. to 1,200.degree. C., and then aged at 300.degree. to 900.degree. C. in order that an oxide and/or nitride protective layer of 0.001 to 10 .mu. be formed on the surface of the permanent magnet to prevent corrosion and in order to relieve machining strain.
    Type: Grant
    Filed: April 26, 1988
    Date of Patent: February 20, 1990
    Assignee: Namiki Precision Jewel Co., Ltd.
    Inventor: Nobuo Imaizumi
  • Patent number: 4898711
    Abstract: A mirror having optical quality reflective faces is prepared by pressing of metallurgical powders. An optical quality surface, free of scratches and irregularities, is formed by pressing the faces with an optical quality tool face, applied to the face at an acute angle to achieve a degree of metal flow. The mirror is progressively formed, by first pressing an assembly of powder to a "green" powder mirror, sintering the pressed powder, and then repressing the sintered mirror using a tool having optical quality surfaces on the faces contacting the mirror faces. The mirror is annealed, repressed with the tool having optical quality surfaces, and coated on the reflective surfaces with a thin metallic coating. This technique is particularly effective for preparing large numbers of mirrors with multiple facets requiring precise facet intersections, as the pressing tool can be adjusted to produce highly exact facet intersections which are then reproduced exactly in subsequent mirrors.
    Type: Grant
    Filed: July 25, 1988
    Date of Patent: February 6, 1990
    Assignee: Hughes Aircraft Company
    Inventors: Donald W. Burt, Gerald A. Hans
  • Patent number: 4891080
    Abstract: A workable, boron-containing, stainless steel alloy and an article formed therefrom are disclosed together with a process for manufacturing same. The alloy consists essentially of, in weight percent, about______________________________________ w/o ______________________________________ Carbon 0.10 max. Manganese 2.00 max. Silicon 1.00 max. Phosphorus 0.045 max. Sulfur 0.010 max. Chromium 16.00-22.00 Nickel 10.00-15.00 Molybdenum 0-3.0 Boron 0.2-2.0 Nitrogen 0.075 max. ______________________________________and the balance consisting essentially of iron. The as-worked alloy in accordance with the invention is characterized by having a boride particle areal density per weight percent boron (A.sub.N) defined by the relationshipA.sub.N .gtoreq.58,080-18,130 (%B).The as-worked alloy of the invention is further characterized by having a Charpy V-notch impact strength (CVN) defined by the relationshipCVN.gtoreq.85.917 x e.sup.-1.20297(%B).
    Type: Grant
    Filed: June 6, 1988
    Date of Patent: January 2, 1990
    Assignee: Carpenter Technology Corporation
    Inventors: Gregory J. Del Corso, James W. Martin, David L. Strobel
  • Patent number: 4886639
    Abstract: Structural component made of powder metallurgical materials, particularly temperature resistant alloys, nickel base alloys, are produced by injection molding or pressing. The sintering is divided into individual work steps for producing dense and smooth structural components which are true to shape.
    Type: Grant
    Filed: April 30, 1987
    Date of Patent: December 12, 1989
    Assignee: MTU Motoren- und Turbinen-Union Muenchen GmbH
    Inventors: Gerhard Andrees, Josef Kranzeder, Wilhelm Vogel
  • Patent number: 4880599
    Abstract: A composite comprised of a sintered matrix of spinel ferrite and an electrically conductive phase of elemental silver is produced by co-firing a laminated structure of ferrite powder-containing tapes containing a silver metallization-forming material having two end portions wherein only the end portions are exposed.
    Type: Grant
    Filed: March 25, 1988
    Date of Patent: November 14, 1989
    Assignee: General Electric Company
    Inventors: Richard J. Charles, Achuta R. Gaddipati
  • Patent number: 4879091
    Abstract: This invention relates to substantially full-dense, near-net shape bodies made of dispersion strengthened copper (D.S.C.) powder and products which are cold formed and/or machined from these bodies, such as resistance welding electrodes. The invention includes processes for manufacturing substantially full-dense, near-net shape, substantially equiaxed bodies from D.S.C. powder.
    Type: Grant
    Filed: December 14, 1987
    Date of Patent: November 7, 1989
    Assignee: SCM Metal Products, Inc.
    Inventors: Prasan K. Samal, Anil V. Nadkarni
  • Patent number: 4878967
    Abstract: A rapidly solidified aluminum-base alloy consists essentially of the formula Al.sub.bal Fe.sub.a Si.sub.b X.sub.c wherein X is at least one element selected from the group consisting of Mn,V,Cr,Mo,W,Nb,Ta, "a" ranges from 2.0 to 7.5 atom percent, "b" ranges from 0.5 to 3.0 atom percent, "c" ranges from 0.05 to 3.5 atom percent and the balance is aluminum plus incidental impurities, with the proviso that the ratio {Fe+X}:Si ranges from about 2.0:1 to 5.0:1. The alloy exhibits high strength, ductility and fracture toughness and is especially suited for use in high temperature structural applications such as gas turbine engines, missiles, airframes and landing wheels.
    Type: Grant
    Filed: September 8, 1987
    Date of Patent: November 7, 1989
    Assignee: Allied-Signal Inc.
    Inventors: Colin M. Adam, Richard L. Bye, Santosh K. Das, David J. Skinner
  • Patent number: 4855104
    Abstract: Contact materials based on AgSnO.sub.2 and having Bi.sub.2 O.sub.3 and CuO as further metal oxide additives were previously disclosed. In these materials the total content of all metal oxides was supposed to be between 10 and 25% by volume with the SnO.sub.2 share equal to or greater than 70% by volume of the total amount of oxide.According to this invention the quantity of SnO.sub.2 is kept smaller than 70% by volume; specifically at about 65%, but in any case equal to or greater than 50%. The SnO.sub.2 weight content is to be in the 4% to 8% range and the weight percentage ratio of SnO.sub.2 to CuO is to be between 8:1 and 12:1.In the associated production process, either Bi.sub.2 O.sub.3 powder is purposely admixed to an internally oxidized alloy powder (IOAP) in an additional operation, a grain restructuring with locally different Bi.sub.2 O.sub.3 concentrations occurring in the structure after sintering and compacting.
    Type: Grant
    Filed: May 6, 1988
    Date of Patent: August 8, 1989
    Assignee: Siemens Aktiengesellschaft
    Inventors: Bernhard Rothkegel, Wolfgang Haufe
  • Patent number: 4853179
    Abstract: This invention relates to a method of manufacturing a structural member made of a sintered Al alloy having heat resistance and high strength. A powder is used having a composition which makes it difficult to perform hot forging, i.e. 8.0 to 30.0 wt. % of Si, 0.8 to 7.5 wt. % of Cu, 0.3 to 3.5 wt. % of Mg, 2.0 to 10.0 wt. % of Fe, 0.5 to 5.0 wt. % of Mn, and a balance of Al. After being subjected to press-forming, this Al alloy powder is subjected to hot extrusion at a temperature of 300.degree. to 450.degree. C., the extruded product is heated with electric resistance heating by electric current which is passed therethrough and subjected to forging at a temperature of 300.degree. to 495.degree. C. According to this method, a structural member made of a sintered Al alloy having heat resistance and high strength and having the aforementioned powder composition can be easily obtained without cracking.
    Type: Grant
    Filed: October 22, 1986
    Date of Patent: August 1, 1989
    Assignee: Honda Giken Kogyo Kabushiki Kaisha
    Inventor: Haruo Shiina
  • Patent number: 4851189
    Abstract: Method of manufacturing cams for camsshafts by powder metallurgy, wherein the formed cams have constant properties over the volume thereof and are well polishable, includes molding into a cam blank a powder mixture made up of iron powder alloyed with carbide-forming elements of the fifth and sixth secondary groups of the periodic table, and graphite powder in a quantity necessary for carbide formation; sintering the blank at a temperature of at most 50 K above a solidus temperature of the blank; and compacting the blank by hot-isostatic compression at a temperature below the solidus temperature to at least 99% of a theoretical density.
    Type: Grant
    Filed: August 17, 1988
    Date of Patent: July 25, 1989
    Assignee: Ringsdorff-Werke GmbH
    Inventors: Jurgen Donch, Bernhard Schelb, Wolfgang Zimmermann
  • Patent number: 4849163
    Abstract: A process for producing flat products from gas atomised particulate material comprises the steps of forming a relatively smooth castable slurry comprising a suspension of such particulate material in a solution of film-forming binder material, depositing a coating of the slurry onto a substrate or support surface and drying the coating to form a flexible flat product. The dried flat product may be bonded onto the substrate or support surface by the drying process or, alternatively, may be removed therefrom and roll-bonded to a suitable substrate for subsequent compaction and sintering.
    Type: Grant
    Filed: September 8, 1987
    Date of Patent: July 18, 1989
    Assignee: Mixalloy Limited
    Inventors: John Bellis, Nigel J. Brooks
  • Patent number: 4844863
    Abstract: A method of producing clad metal comprises the steps of forming a cladding on the surface of a metal substrate by subjecting powder of a metal which is of a different type from that of the metal substrate and is selected from among Ni-base alloys, Co-base alloys, Ti-base alloys, Fe-base superalloys and stainless steels to hot isostatic pressing under a gas pressure load of not less than 300 Kg/cm.sup.2 at a temperature not higher than the solidus thereof, thereby to obtain a composite material, and elongating the composite material by hot working. Optionally the composite material is subjected to soaking or solution treatment before being subjected to hot working.
    Type: Grant
    Filed: March 24, 1988
    Date of Patent: July 4, 1989
    Assignee: Nippon Steel Corporation
    Inventors: Akihiro Miyasaka, Hiroyuki Ogawa, Hiroyuki Homma, Saburo Kitaguchi, Hiroshi Morimoto, Satoshi Araki
  • Patent number: 4840767
    Abstract: A cathode is made from a mixture of tungsten and iridium powders using a ium iridiate formed from barium peroxide and iridium oxide as the impregnant.
    Type: Grant
    Filed: October 3, 1988
    Date of Patent: June 20, 1989
    Assignee: The United States of America as represented by the Secretary of the Army
    Inventors: Louis E. Branovich, Gerard L. Freeman, Bernard Smith, Donald W. Eckart
  • Patent number: 4839139
    Abstract: A powder metallurgy produced high speed tool steel article comprising a mixture of prealloyed high speed tool steel particles coated with a hard, wear resistant material, such as a carbide or nitride, mixed with prealloyed high speed tool steel uncoated particles; the particles are compacted to essentially full density and the hard, wear resistant material is at the boundaries of the coated particles and contained in a continuous matrix of the high speed tool steel. The article is produced by hot compacting a particle charge to essentially full density of a mixture of the coated and uncoated particles.
    Type: Grant
    Filed: February 25, 1986
    Date of Patent: June 13, 1989
    Assignee: Crucible Materials Corporation
    Inventors: Edward J. Dulis, Carl J. Dorsch, William Stasko
  • Patent number: 4836979
    Abstract: A method of producing a composite material from a mixture of copper and a low coefficient of thermal expansion nickel-iron alloy (Invar) powder is disclosed wherein advantageously at least part of the copper is deposited on the Invar powder prior to processing. Processing includes cold compacting to a green strip or other configuration, annealing in the temperature range of 550.degree.-750.degree. C. and working the annealed material at a temperature in that range to high density.
    Type: Grant
    Filed: June 14, 1988
    Date of Patent: June 6, 1989
    Assignee: Inco Limited
    Inventors: James A. E. Bell, Thijs Eerkes, Carlos M. Diaz, William L. Mankins
  • Patent number: 4836978
    Abstract: A production method of a vacuum circuit breaker electrode comprises the steps of mixing conductive metal powder, and refractory material powder with a higher melting point than said conductive metal powder, compacting the resultant mixture to form a compact, presintering the compact in a atmosphere of high purity hydrogen, sealing a presintered body in a capsule while exhausting, heating and degassing, and subjecting the sealed capsule to hot isostatic pressing treatment. The conductive metal powder is one or both of Cu and Ag. The hot isostatic pressing treatment is effected at a temperature higher than a melting point of the conductive metal so that the presintered body is sintered under liquid phase, and a part of molten conductive metal component is seeped out on a sintered body surface.
    Type: Grant
    Filed: September 2, 1987
    Date of Patent: June 6, 1989
    Assignee: Hitachi, Ltd.
    Inventors: Ryuji Watanabe, Hisashi Andoh, Kiyoji Iwashita, Kinko Shimizu
  • Patent number: 4832893
    Abstract: A method for producing PLZT generally expressed as (Pb.sub.1-x La.sub.x) (Zr.sub.1-y Ti.sub.y).sub.1-x/4 O.sub.3 (0<x.ltoreq.0.3, 0.ltoreq.y.ltoreq.1.0) comprises the steps of forming a coprecipitated body by reacting solution containing at least one of Pb, La and Ti with a zirconium-containing solution and a precipitation-forming solution, or (a) forming a solution containing at least one of Pb, La and Ti forming PLZT generally expressed as (Pb.sub.1-x La.sub.x) (Zr.sub.1-y Ti.sub.y).sub.1-x/4 O.sub.3 (0<x.ltoreq.0.3, 0.ltoreq.y.ltoreq.1.0) and a zirconium-containing solution and carrying out a hydrolysis reaction to produce a sol body, (b) drying and then presintering the coprecipitated body at a temperature of from 700.degree. to 1300.degree. C. to form a modified zirconia powder, (c) mixing the presintered body with a compound having a remaining component composition of a required PLZT composition, (d) presintering the mixture at a temperature of from 500.degree. to 1000.degree. C.
    Type: Grant
    Filed: December 16, 1987
    Date of Patent: May 23, 1989
    Assignees: Nippondenso Co., Ltd., Science and Technology Agency National Institute
    Inventors: Michio Hisanaga, Kazunori Suzuki, Masataka Naito, Shinichi Shirasaki
  • Patent number: 4818628
    Abstract: A process for making a composite bearing material comprising a steel backed, prealloyed, lead-bronze sintered powder metal matrix whereby the first sinter step includes induction heating the prealloyed powder and steel backing to above 650.degree. C. and thereafter sintering the same at temperatures of about 850.degree. C. in a second sintering furnace. A composite bearing material made by the same process and comprising a lead particle size averaging less than about 8 microns and having no lead islands larger than about 44 microns.
    Type: Grant
    Filed: August 31, 1987
    Date of Patent: April 4, 1989
    Assignee: Federal-Mogul Corporation
    Inventors: Robert G. Alexander, George C. Pratt
  • Patent number: 4818480
    Abstract: A cathode is made from a mixture of tungsten and iridium powders using a ium peroxide containing material as the impregnant.
    Type: Grant
    Filed: June 9, 1988
    Date of Patent: April 4, 1989
    Assignee: The United States of America as represented by the Secretary of the Army
    Inventors: Louis E. Branovich, Gerard L. Freeman, Bernard Smith, Donald W. Eckart