Heat And Pressure Simultaneously To Effect Sintering Patents (Class 419/48)
  • Patent number: 5447801
    Abstract: A target for magneto-optical recording media having a microstructure having a matrix phase of a eutectic structure of a rare earth metal and an iron-group metal, particles I made of a pure iron-group metal or an alloy thereof and having an average diameter of 200 .mu.m or less and particles II made of a corrosion resistance-improving metal and an iron-group metal and having an average diameter of 200 .mu.m or less is produced by mixing rapidly-quenched powder A made of the rare earth metal and the iron-group metal and having a eutectic structure with powder B made of a pure iron-group metal or an alloy thereof and having an average diameter of 200 .mu.m or less, and powder C made of the corrosion resistance-improving metal and the iron-group metal and having an average diameter of 200 .mu.m or less, and pressure-sintering the resulting mixed powder at a temperature lower than a liquid phase-appearing temperature.
    Type: Grant
    Filed: December 9, 1993
    Date of Patent: September 5, 1995
    Assignee: Hitachi Metals, Ltd.
    Inventors: Kaoru Masuda, Shunichiro Matsumoto
  • Patent number: 5445789
    Abstract: A plunger charged as an electrode is received in a trough charged as a counter-electrode in order to heat material in the trough above the annealing temperature of metal material or the sintering temperature of ceramic-material. The trough and plunger are situated in a vacuum chamber separated from a condenser and pump stand by a valve. The plunger can be retracted into a cover of the chamber by a hydraulic drive on the cover. The cover, drive, and plunger are removable from the lower part of the chamber as a unit.
    Type: Grant
    Filed: March 16, 1994
    Date of Patent: August 29, 1995
    Assignee: Leybold Durferrit GmbH
    Inventors: Erwin Wanetzky, Franz Hugo
  • Patent number: 5439500
    Abstract: A magneto-optical sputter target having a composition comprising at least one rare earth element and at least one transition metal, with a structure which includes a transition metal constituent and a finely mixed alloy constituent of a rare earth phase and a rare earth/transition metal intermetallic compound. The structure of the present target contains a minimum of the intermetallic compound. A method of producing the present sputter target includes mixing particles of the transition metal constituent (preferably only alloyed transition metals) with particles of the finely mixed alloy to produce a powder blend and subjecting the powder blend to a pressing operation in an oxidizing inhibiting environment for a time and at a temperature and pressure which minimizes the rare earth/transition metal intermetallic compound content of the target.
    Type: Grant
    Filed: December 2, 1993
    Date of Patent: August 8, 1995
    Assignee: Materials Research Corporation
    Inventor: Daniel R. Marx
  • Patent number: 5427736
    Abstract: A method for making metal alloy foils directly from metal alloy powder is described. The metal alloy foils are formed by the use of a combination of a means for heating and a means for pressing, such as a hot isostatic press, to densify a metal alloy powder so as to directly form a metal alloy foil. The metal alloy powder is contained within an apparatus which has a near-net shape of a foil, such that the application of heat and pressure will consolidate the metal powder and form the metal alloy foil. This method may be used to make metal foils out of a wide variety of metal alloys, particularly high temperature alloys, such as Ti-base, Ni-base, and B-base and Al-Si alloys. After the step with heating and pressing, the metal alloy foil is removed from the apparatus which is used to contain it, such as by the use of chemical etching or milling.
    Type: Grant
    Filed: April 5, 1994
    Date of Patent: June 27, 1995
    Assignee: General Electric Company
    Inventors: Ann M. Ritter, Paul L. Dupree, Donald N. Wemple, Jr.
  • Patent number: 5418071
    Abstract: In the present invention, metal silicide grains form an interlinked structure of a metal silicide phase, and Si grains which form a Si phase are discontinuously dispersed between the metal silicide phase to provide a sputtering target having a high density two-phased structure and having an aluminum content of 1 ppm or less. Because of the high density and high strength of the target, the generation of particles from the target during sputtering is reduced, and due to the reduced carbon content of the target, the mixing of carbon into the thin film during sputtering can be prevented.
    Type: Grant
    Filed: February 4, 1993
    Date of Patent: May 23, 1995
    Assignee: Kabushiki Kaisha Toshiba
    Inventors: Michio Satou, Takashi Yamanobe, Takashi Ishigami, Mituo Kawai, Noriaki Yagi, Toshihiro Maki, Minoru Obata, Shigeru Ando
  • Patent number: 5415831
    Abstract: The method serves to produce a material based on a doped intermetallic compound. In carrying out the method, at least two differently doped powders each based on the intermetallic compound are selected. One of the two powders predominantly has coarse-grained particles. On the other hand, another powder is formed from comparatively fine-grained particles composed of a material having a lower creep strength but a higher ductility than the material of the coarse-grained powder. The at least two powders are mixed with one another in a ratio serving to establish a desired mixed microstructure and then hot-compacted and heat-treated to form the material.Material produced by this method is suitable for components which are exposed to high mechanical loads at high temperatures, such as, in particular, gas-turbine blades or turbine wheels of turbo chargers.
    Type: Grant
    Filed: December 13, 1993
    Date of Patent: May 16, 1995
    Assignee: ABB Research Ltd.
    Inventors: Robert Baumann, Joachim Rosler, Christoph Tonnes
  • Patent number: 5411700
    Abstract: Powder metallurgy techniques are disclosed for fabricating gamma titanium alloy articles (TiAl type alloys) from mixture of powder wherein one species is based on Al.sub.3 Ti and the other Ti.sub.3 Al. Mixtures of these powders in the proper ratio can be compacted, worked, and heat treated to form the desired gamma TiAl alloy.
    Type: Grant
    Filed: December 14, 1987
    Date of Patent: May 2, 1995
    Assignee: United Technologies Corporation
    Inventor: Ricky L. Martin
  • Patent number: 5407750
    Abstract: A high purity and high density silicon carbide sintered body is made by controlling an amount of aluminum in an aluminum compound as a sintering additive from more than the solid solution upper limit in silicon carbide, preferably, as aluminum from 0.4 to 0.7% by weight of the total silicon carbide and aluminum compound. The sintered body has a density of 99.9% or more and can have a smooth surface with an average surface roughness of 2 nm or less when polished. Thus, this sintered body is suitable for producing a precise, rigid and heat resistant mirror substrate.
    Type: Grant
    Filed: December 18, 1992
    Date of Patent: April 18, 1995
    Assignee: Nippon Steel Corporation
    Inventors: Toshiya Kinoshita, Hiroshi Kubo
  • Patent number: 5405571
    Abstract: A fiber reinforced composite tape is made by casting a mixture comprising high temperature metal or intermetallic particles, substantially continuous ceramic fibers and a polymeric binder. The particles are preferably titanium alloy or titanium aluminide particles having a top size of greater than about 50 microns and the binder is preferably a polyisobutylene. The cast composite tape is combined with other tapes, heated in a vacuum to remove the binder and pressed at an elevated temperature and pressure to form a composite structure suitable for high temperature applications.
    Type: Grant
    Filed: November 8, 1993
    Date of Patent: April 11, 1995
    Assignee: Aluminum Company of America
    Inventors: William G. Truckner, Jon F. Edd
  • Patent number: 5403540
    Abstract: A method is presented for uniformly heating plastically deformable material, which comprises particles of electrically conducting matter. This method comprises inducing an electric current, or causing hysteresis loss within such material, by using electromagnetic radiation with frequency between about 50 Hertz and about 10 MegaHertz, to cause heating of the material.
    Type: Grant
    Filed: October 29, 1990
    Date of Patent: April 4, 1995
    Assignee: Corning Incorporated
    Inventors: Kevin R. Brundage, David L. Hickman, David F. Thompson
  • Patent number: 5391347
    Abstract: Process for obtaining fritted oxide pellets of the MxOy type for nuclear fuels from solutions of soluble salts of the element or elements M, involving stage of precipitating the elements M by hydrogen peroxide in an acid medium. During this precipitation, there is an instantaneous dispersion of one of the reagents (solution of salts or peroxide) in the other, in order to obtain a homogenous mixture and an also instantaneous precipitation of the nuclei in a continuous liquid phase confined in an enclosure having minimum dimensions, the mother liquors being rapidly exhausted. The process makes it possible to obtain sintered pellets whose density exceeds 96% of the theoretical density.
    Type: Grant
    Filed: January 12, 1994
    Date of Patent: February 21, 1995
    Inventors: Bernard Bastide, Antoine Floreancig
  • Patent number: 5387272
    Abstract: The present invention provides an Al-Si based sintered alloy of high strength and high ductility, a method for production thereof and use thereof. The alloy comprises 1-45% of Si, 0.1-20% of an element of Group IIIa, 0.01-5% of at least one element of Groups IVa and Va, the balance of substantially Al. This alloy can further contain at least one of 0.01-5% of Cu, 0.01-5% of Mg, 2.0% or less of Fe, 1.5% or less of Mn and 1.5% or less of Co and the oxygen content is reduced to 0.15% or less by sintering under vacuum. The present invention is applied to automobile parts such as a piston and scroll compressors. The alloy has a tensile strength of about 40 kg/mm.sup.2 or higher and an elongation of 1.5% or more at 150.degree. C.
    Type: Grant
    Filed: April 8, 1992
    Date of Patent: February 7, 1995
    Assignees: Hitachi, Ltd., Hitachi Powdered Metals Company, Limited
    Inventors: Yasuo Kamitsuma, Yusaku Nakagawa, Mitsuo Chigasaki, Tadashi Iizuka, Kooichi Inaba, Keiichi Nakamura, Masaki Minabe, Tsuyoshi Kagaya
  • Patent number: 5382405
    Abstract: A method of manufacturing a shaped article from a powdered precursor, wherein the components of the powdered precursor are subjected to a self-propagating high-temperature synthesis (SHS) reaction and are consolidated essentially simultaneously. The shaped article requires essentially no machining after manufacture.
    Type: Grant
    Filed: September 3, 1993
    Date of Patent: January 17, 1995
    Assignee: Inland Steel Company
    Inventors: Kenneth F. Lowrance, II, Eric C. Knorr, William M. Goldberger, Daniel Boss, Doreen Edwards
  • Patent number: 5380482
    Abstract: A method of manufacturing ingots for use in making objects having heat, thermal shock, corrosion and wear resistance by formulating a composition of about 17-80% TiB.sub.2 powder, about 0.0 to 4.0% Y.sub.2 O.sub.3 powder, and the balance of NiAl powder, the powders being thoroughly admixed, and placing the admixture into a mold in which it is subjected to a pressure of about 7000 psi and a temperature of about 1400.degree. C. for 20 to 140 minutes in an inert atmosphere, after which the mold is cooled and the ingot is removed and ready for use in manufacturing an object. In some applications the use of a ceramic filler material mixed with the powder is employed to improve the physical characteristics of the finished ingot.
    Type: Grant
    Filed: April 2, 1993
    Date of Patent: January 10, 1995
    Assignee: Aspen Research, Inc.
    Inventors: David B. Maginnis, Frank Maginnis
  • Patent number: 5374392
    Abstract: Densify powdered materials, either ceramic or metal or both, at temperatures of 1400.degree. C. or higher using a fluid die fabricated from a mixture of alumina and a calcium aluminate cement. The fluid die may be separated from a fluid pressure-transmitting medium by a barrier material such as graphite foil.
    Type: Grant
    Filed: December 4, 1991
    Date of Patent: December 20, 1994
    Assignee: The Dow Chemical Company
    Inventors: James S. Skelcey, Craig J. Bartkowiak
  • Patent number: 5371049
    Abstract: A ceramic composite is disclosed which may be used as lightweight armor or for other impact or wear resisting purposes. The ceramic composite may comprise distinct phases of AlN and SiC; may be a solid solution of SiC; or may contain AlN or SiC, or both AlN and SiC as residual phase(s) in a solid solution matrix of SiC and AlN.
    Type: Grant
    Filed: January 9, 1989
    Date of Patent: December 6, 1994
    Assignee: FMC Corporation
    Inventors: Keith R. Moffett, John D. Morrow
  • Patent number: 5368629
    Abstract: The rapidly solidified aluminum alloy powder is preformed in a cold or warm environment to form a powder compact having a relative density of 75-93%. Then, the preformed compact is heated and degassed in the atmosphere of an inert gas at temperature of 300.degree. C. to 560.degree. C. for 0.25-3 hours. Immediately thereafter, the compact is subjected to hot coining at 300.degree.-560.degree. C. to obtain a solidified compact having pores at a rate of 2-5%. The solidified compact is then subjected to sizing. Since the inorganic gas prevents reaction between the evaporated water and aluminum while preheating the compact, the hot coining can be carried out in a state where solid state diffusion easily occurs. Thus, the powder particles can be bonded together strongly with a single forging. Also, at the end of hot coining, pores remain in the solidified compact at the rate of 2-5%. Utilizing these pores, the compact can be subjected to sizing to improve its dimensional accuracy.
    Type: Grant
    Filed: December 3, 1992
    Date of Patent: November 29, 1994
    Assignee: Sumitomo Electric Industries, Ltd.
    Inventors: Katsuyoshi Kondo, Yoshinobu Takeda
  • Patent number: 5366688
    Abstract: A heat sink composed of metal particles dispersed in a binder or a sintered structure in which the binder is removed; and the method of forming a heat sink by molding the heat sink from a thermoplastic or epoxy material which has been filled with metal particles.
    Type: Grant
    Filed: March 10, 1994
    Date of Patent: November 22, 1994
    Assignee: Iowa State University Research Foundation, Inc.
    Inventors: Robert L. Terpstra, Barbara K. Lograsso, Iver E. Anderson, Jeffrey A. Moore
  • Patent number: 5358685
    Abstract: A new silicon carbide material is made following a procedure including hot pressing to provide a finished product having a microstructure with an optimal grain size of less than 7 micrometers. The material exhibits a dominant failure mode of intergranular fracture requiring significant energy for crack propagation. The method of manufacturing is cost-effective by allowing the use of "dirty" raw materials since the process causes impurities to segregate at multi-grain boundary junctions to form isolated pockets of impurities which do not affect the structural integrity of the material. End uses include use as optical and electronic substrate materials.
    Type: Grant
    Filed: September 3, 1993
    Date of Patent: October 25, 1994
    Assignee: Cercom Inc.
    Inventor: Andre Ezis
  • Patent number: 5354536
    Abstract: A silicon carbide material is made following a procedure including hot pressing to provide a finished product having a microstructure with an optimal grain size of less than 7 micrometers. The material exhibits a dominant failure mode of intergranular fracture requiring significant energy for crack propagation. The method of manufacturing is cost-effective by allowing the use of "dirty" raw materials since the process causes impurities to segregate at multi-grain boundary junctions to form isolated pockets of impurities which do not affect the structural integrity of the material. End uses include use as protective projectile-resistant armor.
    Type: Grant
    Filed: September 3, 1993
    Date of Patent: October 11, 1994
    Assignee: Cercom Inc.
    Inventor: Andre Ezis
  • Patent number: 5342572
    Abstract: In accordance with this invention, there is provided a process for producing a shaped article in which a reaction mixture containing at least two elemental materials is first charged into a die to form a shaped green body. A uniaxial pressure of from about 500 to about 5,000 pounds per square inch of cross-sectional area of the green body is then uniaxially applied to the green body, and the green body is then ignited; during ignition, the uniaxial pressure of from about 500 to about 5,000 pounds per square inch is maintained at a substantially constant level and continually applied to the reaction mixture.
    Type: Grant
    Filed: September 27, 1993
    Date of Patent: August 30, 1994
    Assignee: Alfred University
    Inventors: Gregory C. Stangle, William C. Williams
  • Patent number: 5340533
    Abstract: A process for producing a dense composite material by combustion synthesis. In the first step of the process, a reaction mixture comprised of an elemental material is provided. The elemental material is charged to a die, a uniaxial pressure of from about 500 to about 5,000 pounds per square inch is applied to the elemental material within the die, and the elemental material within the die is ignited. Prior to, during, and subsequent to the time said elemental material is been ignited, the uniaxial pressure of from about 500 to about 5,000 pounds per square inch is applied to the elemental material within said die.
    Type: Grant
    Filed: April 27, 1993
    Date of Patent: August 23, 1994
    Assignee: Alfred University
    Inventors: Gregory C. Stangle, Scott E. Niedzialek, William C. Williams
  • Patent number: 5326525
    Abstract: A process is disclosed for fabricating a metal aluminide composite which comprises providing a metal aluminide, such as titanium aluminide, or a titanium aluminide alloy, and a reinforcing fiber material, such as silicon carbide fiber, and placing an interlayer or diffusion barrier layer in the form of a metal selected from the group consisting of silver, copper and gold, and alloys thereof, between the metal aluminide and the reinforcing fiber material. The interlayer metal can be a foil of the metal or in the form of a coating, such as a silver coating, on the reinforcing fiber material. The metal aluminide, the reinforcing fiber material, and the metal interlayer, e.g., in the form of a packet of a plurality of alternate layers of metal aluminide alloy and reinforcing fiber material, each layer being separated by the metal interlayer, is pressed and heated at an elevated temperature, e.g., ranging from about 900.degree. to about 1200.degree. C., at which diffusion bonding occurs.
    Type: Grant
    Filed: July 11, 1988
    Date of Patent: July 5, 1994
    Assignee: Rockwell International Corporation
    Inventor: Amit K. Ghosh
  • Patent number: 5316720
    Abstract: The present invention describes a process for the compaction and densification of discrete powder materials utilizing a high amplitude stress wave which produces a high pressure condition at a surface of the particles thereby driving said stress wave into and through the particles.
    Type: Grant
    Filed: November 20, 1992
    Date of Patent: May 31, 1994
    Assignee: Rockwell International Corporation
    Inventors: Lyle B. Spiegel, William E. McDermott
  • Patent number: 5312650
    Abstract: The method of making a composite article of different metal portions by spraying molten metal on the surface of a solid metal member that has been cleaned and preheated in a controlled atmosphere at low pressure. The molten metal is sprayed on the surface of the solid metal member, preferably by plasma jet spraying. It is rapidly solidified to be adherent to the surface of the solid metal member to form a composite preform. The composite preform is cooled at a rate sufficiently low to reduce residual stresses and then hot pressed to eliminate voids in the sprayed metal portion and metallurgically bonded to the surface of the solid member.
    Type: Grant
    Filed: January 12, 1988
    Date of Patent: May 17, 1994
    Assignee: Howmet Corporation
    Inventors: Ranes P. Dalal, John M. McFadden, Mark J. Straszheim, Louis E. Dardi
  • Patent number: 5310520
    Abstract: Discrete powder particles of copper 14 and INVAR 12 are mixed together in a container 16 and packed into a powder metal article. This article is hot vacuum degassed and vacuum sealed and then heated to temperature well below the sintering temperature of copper or INVAR. Immediately after heating the article, it is subjected to a high pressure, high strain force such as extrusion through a die thereby yielding a fully dense, strong composite material 10 with excellent combined thermal expansion and conductivity properties.
    Type: Grant
    Filed: January 29, 1993
    Date of Patent: May 10, 1994
    Assignee: Texas Instruments Incorporated
    Inventors: Sunil C. Jha, James A. Forster, Henry F. Breit
  • Patent number: 5302340
    Abstract: A method of forming a ceramic layer, which is compact and rich in adhesion to a metallic body, on the metallic body without adding binders even though said ceramics is hard to be sintered ceramics such as various kinds of non oxide ceramics. Said method comprises a step of placing ceramic powders and/or a mixture of ceramic powders and metallic powders or a mixture of metallic powders and non metallic powders on the metallic body and a step of forming the ceramic layer on the metallic body in a moment by a reaction heat of the Thermit.RTM. reaction under the pressurized condition. In addition, a metallic insert member can be disposed between said metallic body and various kinds of powder placed on said metallic body. Furthermore, the resulting ceramic/metal composite member is subjected to a hot hydrostatic pressing or a hot pressing under high temperatures and high pressures.
    Type: Grant
    Filed: May 5, 1992
    Date of Patent: April 12, 1994
    Assignee: Kabushiki Kaisha Komatsu Seisakusho
    Inventor: Shuichi Takeda
  • Patent number: 5298338
    Abstract: A titanium-tungsten target material used to form, by sputtering, a barrier metal or the like for use in semiconductor devices. The titanium-tungsten target material is substantially composed of tungsten particles and a titanium-tungsten alloy phase surrounding the tungsten particles. The area ratio at which tungsten grains occupy in a cross section of the titanium-tungsten target material is, preferably, not more than 15%, more preferably, not more than 10%. If the average crystal grain size of the target material is not more greater 15 .mu.m, a uniform thin film can be obtained by sputtering. The target material can be obtained by sintering a titanium powder and a tungsten powder.
    Type: Grant
    Filed: July 16, 1992
    Date of Patent: March 29, 1994
    Assignee: Hitachi Metals, Ltd.
    Inventor: Akitoshi Hiraki
  • Patent number: 5256368
    Abstract: A pressure-reaction synthesis process for producing increased stiffness and improved strength-to-weight ratio titanium metal matrix composite materials comprising exothermically reacting a titanium powder or titanium powder alloys with non-metal powders or gas selected from the group consisting of C, B, N, BN, B.sub.4 C, SiC and Si.sub.3 N.sub.4 at temperatures from about 900.degree. to about 1300.degree. C., for about 5 to about 30 minutes in a forming die under pressures of from about 1000 to 5000 psi.
    Type: Grant
    Filed: July 31, 1992
    Date of Patent: October 26, 1993
    Assignee: The United States of America as represented by the Secretary of the Interior
    Inventors: Laurance L. Oden, Thomas L. Ochs, Paul C. Turner
  • Patent number: 5250130
    Abstract: A green body to be hot pressed by heating the body and applying pressure in a uniaxial direction to the body for an amount of time wherein the body has at least one non-uniform composition cross section relative to the uniaxial direction which cross section has regions which require differing amounts of shrinkage in the uniaxial direction to achieve maximum density under the pressure and heating for the amount of time, may be hot pressed according to a method including:a) laminating auxiliary material with the green body in the uniaxial direction wherein the auxiliary material includes at least one non-uniform composition cross section relative to the uniaxial direction which cross section has regions which require differing amounts of shrinkage in the uniaxial direction to achieve maximum density under the pressure and heating for the amount of time, whereby the net uniaxial shrinkage required by the laminate to achieve maximum density under the heating and pressure for the amount of time is substantially eq
    Type: Grant
    Filed: May 20, 1991
    Date of Patent: October 5, 1993
    Assignee: W. R. Grace & Co.-Conn.
    Inventors: Jack H. Enloe, John W. Lau
  • Patent number: 5183632
    Abstract: A method of manufacturing an aluminum-base composite disc rotor comprising the steps of preparing a rough-shaped disc rotor made of a mixture of aluminum powder or aluminum alloy powder with reinforcing particles or aluminum alloy, placing a mixture of aluminum powder or aluminum alloy powder with reinforcing particles or a preform made thereof on each of fixed positions of the rough-shaped disc rotor, and heating the mixture or the preform to at least a region of mashy state temperature to mold under pressure. Thereby the heat resistance and the wear resistance of the aluminum-base composite disc rotor for light-duty cars and industrial machinery are improved.
    Type: Grant
    Filed: March 3, 1992
    Date of Patent: February 2, 1993
    Assignees: Akebono Brake Industry Co., Ltd., Akebono Research and Development Centre Ltd.
    Inventors: Manabu Kiuchi, Masao Arai
  • Patent number: 5152829
    Abstract: A rapidly solidified aluminum base alloy consists essentially of the formula Al.sub.bal Fe.sub.a Si.sub.b X.sub.c, wherein X is at least one element selected from the group consisting of W,Ta,Nb, "a" ranges from 3.0 to 7.1 at %, "b" ranges from 1.0 to 3.0 at %, "c" ranges from 0.25 to 1.25 at % and the balance is aluminum plus incidental impurities, with the provisos that the ratio [Fe+X]:Si ranges from about 2.33:1 to 3.33:1 and that the ratio Fe:X ranges from about 16:1 to 5:1. The alloy exhibits high strength, ductility and fracture toughness and is especially suited for use in high temperature structural applications such as gas turbine engines, missiles, airframes and landing wheels.
    Type: Grant
    Filed: June 3, 1991
    Date of Patent: October 6, 1992
    Assignee: Allied-Signal Inc.
    Inventors: David J. Skinner, Michael S. Zedalis
  • Patent number: 5149496
    Abstract: A magnesium based metal matrix composite is made from rapidly solidified magnesium alloy powder and SiC particulate using liquid suspension coprocessing or mechanical alloying. The composite is suitable for consolidation into bulk shapes having, in combination, high strength, high stiffness, low density, low coefficient of thermal expansion, and high hardness. The composite is suited for uses in such applications as space and missile guidance and navigation and control system precision components where low density, very high specific stiffness and long term dimensional and environmental stability are principal performance criteria.
    Type: Grant
    Filed: January 27, 1992
    Date of Patent: September 22, 1992
    Assignee: Allied-Signal Inc.
    Inventors: Santosh K. Das, Chin-Fong Chang, Derek Raybould
  • Patent number: 5147446
    Abstract: A method of producing a dense compact of ultra-fine powder employs low temperatures and high pressures to produce a very dense, nearly ideally packed compact from a starting nano-sized powder. The final product is capable of being easily hot-pressed or sintered to full density.
    Type: Grant
    Filed: August 6, 1991
    Date of Patent: September 15, 1992
    Assignee: The United States of America as represented by the Secretary of the Commerce
    Inventors: Alexander Pechenik, Gasper J. Piermarini
  • Patent number: 5145503
    Abstract: In a process for producing a high strength structural member by sintering a starting powder material, a powder mixture of a basic powder and an additional powder is used as the starting powder material. The basic powder is comprised of at least one of an amorphous single-phase alloy powder and at least one kind of a mixed-phase alloy powder which contains a crystalline phase and an amorphous phase and has a crystalline phase volume fraction C (Vf) less than 30%, and the additional powder is comprised of a mixed-phase alloy powder containing a crystalline phase and an amorphous phase and having a crystalline phase volume fraction C (Vf) of at least 30% to less than 80%. The relationship between the minimum volume fraction Pm (Vf) of the additional powder in the starting powder material and the crystalline phase volume fraction C (Vf) in the additional powder is established such that Pm (Vf)=-0.7 C (Vf)+61. This ensures that a structural member having a high strength and a high toughness can be produced.
    Type: Grant
    Filed: May 31, 1991
    Date of Patent: September 8, 1992
    Assignee: Honda Giken Kogyo Kabushiki Kaisha
    Inventor: Hiroyuki Horimura
  • Patent number: 5139720
    Abstract: In a method of manufacturing a sintered ceramic material using the heat generated in a thermit reaction as a heating source, a pre-heating is applied preceding to the sintering step or a mixture comprising: (A) at least one ceramic powder, (B) at least one non-metallic powder selected from the group consisting of carbon, boron and silicon, and (C) a metal powder and/or a non-metallic powder other than the above-mentioned (B) is used. Homogeneous and dense sintered ceramic material or sintered composite ceramic material can be obtained by this method, and the fine texture thereof, and the phase constitution, the phase distribution and the like of the composite ceramic phase can be controlled sufficiently.
    Type: Grant
    Filed: February 12, 1991
    Date of Patent: August 18, 1992
    Assignee: Kabushiki Kaisha Komatsu Seisakusho
    Inventors: Shuichi Takeda, Hideki Shishiba
  • Patent number: 5120350
    Abstract: A reinforced metal composite comprised of a mixture of fused yttria and a metal matrix selected from the group consisting of Ti, Nb, Fe, Co, Ni, Ti alloy, Co based alloys aluminides of Ti, aluminides of Ni, aluminides of Nb and their mixtures. Preferably, the metal matrix is Ti or a Ti alloy which has a low Cl content (e.g. less than 0.15 wt. % Cl).
    Type: Grant
    Filed: July 3, 1990
    Date of Patent: June 9, 1992
    Assignee: The Standard Oil Company
    Inventors: Edward C. Supan, Joseph F. Dolowy, Jr., Bradley A. Webb
  • Patent number: 5110542
    Abstract: The present invention describes a process for the compaction and densification of materials using heat and high pressure in which pressure is applied isostatically to the workpiece to be compacted, heat is applied to the pressurized workpiece as rapidly as feasible, effecting thereby full compaction and densification. Heating is terminated and the workpiece cooled while the workpiece is still pressurized. This process effects hot-isostatic-processing of workpieces while reducing the time such workpieces spend at elevated temperatures. The resulting parts can have novel structures, properties or compositions not obtained with other processing procedures.
    Type: Grant
    Filed: March 4, 1991
    Date of Patent: May 5, 1992
    Assignee: Vital Force, Inc.
    Inventor: Robert M. Conaway
  • Patent number: 5100736
    Abstract: A polymer-reinforced metal matrix composite is disclosed which is formed by lending metal particles and polymer particles to form a homogeneous powder blend, and consolidating the powder blend to form a unitary mass. The unitary mass is then plastically deformed such as by extrusion in the presence of heat so as to cause an elongation thereof, whereby the metal particles form a matrix and the polymer particles form elongated filaments uniformly dispersed throughout the matrix and aligned in the direction of elongation of the unitary mass. An aluminum matrix reinforced with polyether-etherketone is shown to have enhanced specific strength and modulus over those of the aluminum alone.
    Type: Grant
    Filed: February 19, 1991
    Date of Patent: March 31, 1992
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: Gilbert J. London, William E. Frazier, John G. Williams
  • Patent number: 5098649
    Abstract: A rare earth metal-iron group metal target for a magneto-optical disk is produced by mixing power (a) produced by the rapid quenching treatment of an alloy composed of at least one rare earth metal and at least one iron group metal in a composition range which permits the formation of an eutectic structure, with powder (b) from at least one iron group metal in an amount necessary for meeting the composition requirements of the target; and subjecting the resulting mixture to pressure sintering in vacuum or in an inert gas atmosphere at a temperature lower than a liquid phase-appearing temperature of the mixture to produce a rare earth metal-iron group metal intermetallic bonding layer betwen the particles.
    Type: Grant
    Filed: June 26, 1990
    Date of Patent: March 24, 1992
    Assignee: Hitachi Metals, Ltd.
    Inventors: Shunichiro Matsumoto, Tsutomu Inui, Rokuo Ichiyasu, Yoshitaka Chiba
  • Patent number: 5098650
    Abstract: A method for producing titamium alloy articles having a desired microstructure which comprises the steps of:(a) providing a prealloyed gamma titanium aluminide alloy powder;(b) filling a suitable die or mold with the powder;(c) consolidating the powder in the filled mold at a pressure of 30 Ksi or greater and at a temperature of about 70 to 95 percent of the alpha-2+gamma eutectoid temperature of the alloy, in degrees C.
    Type: Grant
    Filed: August 16, 1991
    Date of Patent: March 24, 1992
    Assignee: The United States of America as represented by the Secretary of the Air Force
    Inventors: Daniel Eylon, Karen R. Teal
  • Patent number: 5093039
    Abstract: Disclosed is an electrically conductive sintered silicon carbide body having an electric resistivity of not higher than 1 .OMEGA..multidot.cm, which is produced by(a) mixing(1) a first silicon carbide powder having a mean grain size of from 0.1 to 10 .mu.m with(2) a second silicon carbide powder having a mean grain size of not greater than 0.1 .mu.m prepared by(2-1) introducing a starting gas composed of a silane compound of silicon halide and a hydrocarbon into a plasma of a non-oxidative atmosphere, and(2-2) conducting gas phase reaction between the silane compound or silicon halide and the hydrocarbon while controlling the pressure of the reaction system within the range of from less than 1 atom to 0.1 torr, and(3) optionally, a carbon powder which is required for reducing oxides contained in both the first and second silicon carbide powders,(b) optionally reducing the oxides with the carbon, and(c) heating the resulting mixture for sintering. Also, processes of producing the same are disclosed.
    Type: Grant
    Filed: November 6, 1989
    Date of Patent: March 3, 1992
    Assignees: Kazunori Kijima, Sumitomo Cement Co., Ltd.
    Inventors: Kazunori Kijima, Eiki Arai, Youichi Miyazawa, Mikio Konishi, Ken Kato
  • Patent number: 5093076
    Abstract: This invention describes a practice for the hot pressing and/or hot working of rare earth element-containing alloy powders using open-to-the-air presses. The rare earth-containing powder is pressed into a compact at ambient temperatures using a solid lubricant only on the die wall. This compact is then hot pressed in an open air press utilizing a heated die flooded with argon.
    Type: Grant
    Filed: May 15, 1991
    Date of Patent: March 3, 1992
    Assignee: General Motors Corporation
    Inventors: Kevin A. Young, Joseph J. Worden, Donald S. Kirk, Larry J. Eshelman
  • Patent number: 5089354
    Abstract: A copper alloy composite material which comprises a copper alloy matrix and at least one additive selected from solid materials having self-lubricity and wear-resistant materials and uniformly dispersed in the alloy matrix is described. The composite material has improved wear resistance and anti-seizing properties.
    Type: Grant
    Filed: December 11, 1990
    Date of Patent: February 18, 1992
    Assignee: Chuetsu Metal Works, Co., Ltd.
    Inventors: Kunio Nakashima, Ryouichi Ishigane, Takayuki Tanaka, Ken-ichi Ichida
  • Patent number: 5082540
    Abstract: A fluoride ion sensitive material suitable for use as the active component in a fluoride ion sensitive electrode comprises a sintered mixture comprising of up to 99.9 molar % of Lanthanum trifluoride and from 0.1 to 20 molar % Calcium difluoride formed from a body that has been pressed at 10.sup.7 Pa or more and then sintered in a inert atmosphere at 900.degree. C. or more.
    Type: Grant
    Filed: May 7, 1990
    Date of Patent: January 21, 1992
    Assignee: The Secretary of State for Defence in Her Britannic Majesty's Government of the United Kingdom of Great Britain and Northern Ireland
    Inventors: Jeffrey D. Newman, Ramin Pirzad, David C. Cowell, Antony A. Dowman
  • Patent number: 5073302
    Abstract: A varistor material comprising two crystalline phases of ZnO and ZnMn.sub.2 O.sub.4, wherein Zn and Mn are present at such a ratio that 3 to 7% by mol of ZnO is contained per 100% by mol of ZnO+MnO and the nonlinear index (.alpha.) of the varistor properties is at least 10; and a process for the production of the same, which comprises adding a manganese compound to ZnO at such a ratio as to give a content of MnO, sintering the mixture at 1100.degree. to 1350.degree. C., and further annealing the obtained sintered material at a temperature lower than the sintering temperature by at least 50.degree. C. and higher than 1000.degree. C. are disclosed.
    Type: Grant
    Filed: June 14, 1989
    Date of Patent: December 17, 1991
    Assignee: Somar Corporation
    Inventors: Akihide Igari, Zenbee Nakagawa
  • Patent number: 5053192
    Abstract: The invention relates to the powder metallurgy. The invention involves deforming combustion products by extrusion at an extrusion temperature chosen in the range from 0.3T.sub.1 to T.sub.2, wherein T.sub.1 is the melting point of a hard phase of the combustion products and T.sub.2 is the melting point of a binder material in a container (5) made up of vertically extending segments (12) defining spaces (13) with one another and having a die (14) and a heat insulated sizing member (17) the temperature conditions of extrusion being controlled by means of a unit (21) having a temperature pick-up (22) and a member (23) receiving information from the pick-up (22) and sending a command for moving the punch (10).
    Type: Grant
    Filed: August 23, 1990
    Date of Patent: October 1, 1991
    Inventors: Alexandr G. Merzhanov, Alexandr M. Stolin, Vadim V. Podlesov, Leonid M. Buchatsky, Tatyana N. Shishkina
  • Patent number: 5047205
    Abstract: A method for producing a compacted fully dense permanent magnet by providing a particle charge of a permanent magnet alloy composition from which the article is to be made and placing the charge in a cylindrical container having a generally axially positioned core with the charge surrounding the core within the container. The container and charge are heated to an elevated temperature and extruded to compact the charge to a substantially fully dense permanent magnet article.
    Type: Grant
    Filed: April 14, 1989
    Date of Patent: September 10, 1991
    Assignee: Crucible Materials Corporation
    Inventors: Vijay K. Chandhok, Robert F. Krause, Bao-Min Ma, John J. DuPlessis
  • Patent number: 5045278
    Abstract: An aluminum based metal matrix composite is produced from a charge containing a rapidly solidified aluminum alloy, a carbidiferous agent and particles of a reinforcing material present in an amount ranging from about 0.1 to 50% by volume of the charge. The charge is ball milled energetically to uniformly mix the carbidiferous agent within the aluminum matrix, and to enfold metal matrix material around each of the particles while maintaining the charge in a pulverulent state. Upon completion of the ball milling step, the charge is hot consolidated at suitable temperatures to decompose the carbidiferous agent and result in the formation of carbide and oxide particles, and to provide a powder compact having a formable, substantially void-free mass. The compact is especially suited for use in aerospace, automotive, electronic, wear resistance critical components, and the like, which often encounter service temperatures approaching 500.degree. C.
    Type: Grant
    Filed: November 9, 1989
    Date of Patent: September 3, 1991
    Assignee: Allied-Signal Inc.
    Inventors: Sontosh K. Das, Michael S. Zedalis, Paul S. Gilman
  • Patent number: 5045972
    Abstract: A thermally conductive diamond metal composite consisting essentially of 5 to 80 volume percent diamond particles having a particle size ranging from about 1 to 50 .mu.m and a metal matrix comprising a thermally conductive metal. Preferably, a fine metal powder having particle size below 53 microns is utilized as the source for the metal matrix.
    Type: Grant
    Filed: August 27, 1990
    Date of Patent: September 3, 1991
    Assignee: The Standard Oil Company
    Inventors: Edward C. Supan, Joseph F. Dolowy, Jr., Bradley A. Webb