Titanium Base Patents (Class 420/417)
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Patent number: 11666993Abstract: A brazing process using Nickel(Ni)-Carbon as graphite(Cg) alloys, Ni-Cg-Molybdenum(Mo) alloys, and Ni-Cobalt(Co)-Cg-Mo alloys for brazing together ceramics, ceramics to metals, metals to metals. Semiconductor processing equipment made with the use of Ni-Cg alloys, such as heaters and chucks. Semiconductor processing equipment components and industrial equipment components using a highly wear resistant surface layer, such as sapphire, joined to a substrate such as a ceramic, with a Ni-Cg alloy braze.Type: GrantFiled: May 28, 2019Date of Patent: June 6, 2023Assignee: WATLOW ELECTRIC MANUFACTURING COMPANYInventors: Alfred Grant Elliot, Brent Elliot
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Patent number: 11586146Abstract: The present invention relates to a spiral spring for a balance wheel made of an alloy of niobium and titanium with an essentially single-phase structure, and the method of manufacture thereof which comprises: a step of producing a blank in a niobium-based alloy consisting of: niobium: balance to 100 wt %, titanium: between 40 and 49 wt %, traces of elements selected from the group consisting of O, H, C, Fe, Ta, N, Ni, Si, Cu, Al, between 0 and 1600 ppm by weight individually, and cumulatively less than 0.Type: GrantFiled: September 27, 2018Date of Patent: February 21, 2023Assignee: Nivarox-FAR S.A.Inventor: Christian Charbon
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Patent number: 11390935Abstract: A titanium alloy material contains: in mass %, Cu: 0.7% to 1.4%; Sn: 0.5% to 1.5%; Si: 0.10% to 0.45%; Nb: 0.05% to 0.50%; Fe: 0.00% to 0.08%; O: 0.00% to 0.08%; and the balance composed of Ti and impurities, in which in a structure, an area fraction of an ? phase is 96.0% or more and an area fraction of an intermetallic compound is 1.0% or more, and an average crystal grain size of the ? phase is 10 ?m or more and 100 ?m or less and an average grain size of the intermetallic compound is 0.1 to 3.0 ?m.Type: GrantFiled: February 7, 2018Date of Patent: July 19, 2022Assignee: NIPPON STEEL CORPORATIONInventors: Hidenori Takebe, Sosuke Nishiwaki, Tomonori Kunieda
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Patent number: 11136650Abstract: A titanium alloy melt includes about 7.0 to about 9.0 percent by weight vanadium (V), about 3.0 to about 4.5 percent by weight aluminum (Al), about 0.8 to about 1.5 percent by weight iron (Fe), at most about 0.15 percent by weight oxygen (O), and titanium (Ti) and a titanium alloy powder, formed from the titanium alloy melt, includes about 7.0 to about 9.0 percent by weight vanadium (V), about 3.0 to about 4.5 percent by weight aluminum (Al), about 0.8 to about 1.5 percent by weight iron (Fe), at most about 0.18 percent by weight oxygen (O), and titanium (Ti).Type: GrantFiled: March 14, 2017Date of Patent: October 5, 2021Assignee: The Boeing CompanyInventors: Joe Pecina, Robert Burkett, Gary M. Backhaus
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Patent number: 11008639Abstract: A sintered Ti alloy comprising: 4 to 6 wt. % iron; 1 to 4 wt. % aluminium or 1 to 3 wt. % copper; >0 to 0.5 wt. % silicon; >0 to 0.3 wt. % boron; >0 to 1 wt. % lanthanum, and the balance being titanium with incidental impurities. In the associated powder metallurgy formation process, the boron and lanthanum content is preferably introduced into a blended powder mixture in the form of lanthanum boride (LaB6).Type: GrantFiled: September 16, 2015Date of Patent: May 18, 2021Assignee: Baoshan Iron & Steel Co., Ltd.Inventors: Yafeng Yang, Ma Qian, Shudong Luo, Jifeng Sun, Aijun Huang
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Patent number: 10947162Abstract: A braze alloy for joining or repairing ceramic matrix composite (CMC) components comprises a braze composition including silicon at a concentration from about 48 at. % to about 66 at. %, titanium at a concentration from about 1 at. % to about 35 at. %, and an additional element selected from aluminum, cobalt, vanadium, nickel, and chromium. The braze composition comprises a melting temperature of less than 1300° C.Type: GrantFiled: April 12, 2018Date of Patent: March 16, 2021Assignees: ROLLS-ROYCE CORPORATION, TRUSTEES OF THE COLORADO SCHOOL OF MINESInventors: Scott Nelson, Raymond Xu, Sean Landwehr, Juan Wei, Stephen Liu, Juan Carlos Madeni
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Patent number: 10934607Abstract: A titanium sintered body is composed of a material containing titanium, and has an oxygen content of 2500 ppm by mass or more and 5500 ppm by mass or less and a surface Vickers hardness of 250 or more and 500 or less. It is preferred that an ?-phase and a ?-phase are contained as crystal structures, and an area ratio occupied by the ?-phase in a cross section is 70% or more and 99.8% or less. It is also preferred that in an X-ray diffraction spectrum obtained by X-ray diffractometry, the value of a peak reflection intensity by the plane orientation (110) of the ?-phase is 5% or more and 60% or less of the value of a peak reflection intensity by the plane orientation (100) of the ?-phase. It is also preferred that particles composed mainly of titanium oxide are included.Type: GrantFiled: March 28, 2017Date of Patent: March 2, 2021Inventors: Hidefumi Nakamura, Taku Kawasaki
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Patent number: 10640859Abstract: An aspect of the present invention is a production method of a rolled sheet for cold-rolling, the method being characterized by including: a hot-rolling step for forming a rolled sheet by hot-rolling a pure titanium material while coiling; and an annealing step for annealing the hot-rolled sheet after the hot-rolling step, the coiling temperature in the hot-rolling step being 500° C. or less, and the annealing step being controlled so that the percentage area of recrystallized grains in the microstructure of the hot-rolled sheet after annealing is at least 90% and the mean grain size of the recrystallized grains is 5 ?m to 10 ?m.Type: GrantFiled: March 16, 2016Date of Patent: May 5, 2020Assignee: Kobe Steel, Ltd.Inventors: Kazuya Kimijima, Masanori Kobayashi, Tohru Shiogama, Keitaro Tamura, Yasuyuki Fujii
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Patent number: 10589344Abstract: A method for forming a mold for casting a titanium-containing article, the method including combining calcium aluminate with a liquid to produce an initial slurry of calcium aluminate and adding oxide particles into the initial slurry to create a final slurry. The method further includes introducing the final slurry into a mold cavity that contains a fugitive pattern and allowing the final slurry to cure in the mold cavity to form a mold of a titanium-containing article.Type: GrantFiled: October 4, 2017Date of Patent: March 17, 2020Assignee: General Electric CompanyInventors: Bernard Patrick Bewlay, Stephen Bancheri, Michael Weimer, Joan McKiever, Brian Ellis
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Patent number: 10494698Abstract: Methods of preparing Zr based metallic using Zr sponge refined by a refining process are described. An exemplary method includes heating Zr sponge in a processing chamber with an electron-beam-heating apparatus or an arc-melting apparatus under a desired pressure condition to release volatile contaminants from the Zr sponge, introducing a purge gas into the processing chamber and permitting the purge gas to intermingle with at least some of the released volatile contaminants, evacuating the processing chamber to extract at least some of the purge gas and released volatile contaminants, repeating the heating of the Zr sponge, the introducing of the purge gas, and the evacuating of the processing chamber release and evacuate additional volatile contaminants from the Zr sponge to provide a processed Zr sponge with enhanced purity, and melting the processed Zr sponge with multiple other alloy constituents to provide a Zr-based metallic alloy.Type: GrantFiled: March 28, 2018Date of Patent: December 3, 2019Assignee: Materion CorporationInventor: James A. Yurko
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Patent number: 10227677Abstract: A titanium alloy including by mass %, a platinum group metal: 0.01 to 0.15% and a rare earth metal: 0.001 to 0.10%, with the balance being Ti and impurities. The titanium alloy preferably includes as a partial replacement for Ti, Co: 0.05 to 1.00% by mass, and the content of the platinum group metal is preferably in the range of 0.01 to 0.05% by mass. Furthermore, it is preferred that the platinum group metal be Pd and the rare earth metal be Y. Consequently, it is possible to provide a titanium alloy having corrosion resistance comparable to or better than that of the conventional art as well as good workability while offering an economic advantage with a lower content of platinum group metal or an advantage of less likelihood of corrosion growth originating at defects such as flaws that occurred in the surface.Type: GrantFiled: July 20, 2012Date of Patent: March 12, 2019Assignee: NIPPON STEEL & SUMITOMO METAL CORPORATIONInventors: Hideya Kaminaka, Yoshihisa Yonemitsu, Satoshi Matsumoto, Kouichi Takeuchi
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Patent number: 10167673Abstract: Binder compositions for use in forming a bit body of an earth-boring bit include at least one of cobalt, nickel, and iron, and at least one melting point-reducing constituent selected from at least one of a transition metal carbide up to 60 weight percent, a transition metal boride up to 60 weight percent, and a transition metal silicide up to 60 weight percent, wherein the weight percentages are based on the total weight of the binder. Earth-boring bit bodies include a cemented tungsten carbide material comprising tungsten carbide and a metallic binder, wherein the tungsten carbide comprises greater than 75 volume percent of the cemented tungsten carbide material.Type: GrantFiled: July 29, 2016Date of Patent: January 1, 2019Assignees: Baker Hughes Incorporated, TDY Industries, LLCInventors: Prakash K. Mirchandani, Jimmy W. Eason, James J. Oakes, James C. Westhoff, Gabriel B. Collins
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Patent number: 10144992Abstract: An amorphous alloy and a method for preparing the amorphous alloy are provided. The amorphous alloy is represented by a formula of (Zr,Hf)aMbNcBed. M contains at least one element selected from transition group elements. N contains at least one selected from Al and Ti. And 40?a?70, 10?b?40, 5?c?20, 5?d?25, and a+b+c+d=100. The ratio of an atomic percentage of Hf to an atomic percentage of Zr is in a range of about 0.01 to about 5.Type: GrantFiled: December 24, 2013Date of Patent: December 4, 2018Assignee: BYD COMPANY LIMITEDInventors: Faliang Zhang, Qing Gong
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Patent number: 10124547Abstract: A method of identifying and/or tracking deformation of a mechanical part made of composite material for a turbine engine, in which the part includes a preform of fiber material and a resin, is provided. The method includes incorporating metal particles in the preform or the resin during fabrication of the part, and subjecting the mechanical part to two X-ray inspections on two different occasions so as to identify the part and/or so as to deduce deformation of its internal structure.Type: GrantFiled: September 26, 2013Date of Patent: November 13, 2018Assignee: SAFRAN AIRCRAFT ENGINESInventors: Julien Schneider, Ludovic Edmond Camille Molliex
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Patent number: 10090379Abstract: When hydrogen penetrates in to the semiconductor device, a gate voltage threshold of a gate structure (Vth) is shifted. Penetrating of hydrogen into the semiconductor device from the edge termination structure section which is positioned at an end portion of the semiconductor device is prevented. To provide a semiconductor device comprising a semiconductor substrate in which an active region and an edge termination structure section which is provided around the active region are provided, a first lower insulating film which is provided in the edge termination structure section on the semiconductor substrate, and a first protective film which is provided on the first lower insulating film, and is electrically insulated from the semiconductor substrate, and occludes hydrogen.Type: GrantFiled: March 31, 2017Date of Patent: October 2, 2018Assignee: FUJI ELECTRIC CO., LTD.Inventors: Yuichi Harada, Yasuyuki Hoshi
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Patent number: 10087506Abstract: A titanium alloy having ultrahigh strength and ultralow elastic modulus, and showing linear elastic deformation behavior is disclosed. The titanium alloy (Ti-20Nb-5Zr-1Fe-O) of the present invention consists of titanium, niobium, zirconium, iron and oxygen. More specifically, the amount of niobium is 18 to 22 at. %, the amount of zirconium is 3 to 7 at. %, the amount of iron is 0.5 to 3.0 at. %, the amount of oxygen is 0.1 to 1.0 wt. %, and the balance is titanium.Type: GrantFiled: March 28, 2013Date of Patent: October 2, 2018Assignee: Korea Institute of Machinery & MaterialsInventors: Chan Hee Park, Jong Taek Yeom, Seung Eon Kim, Seong Woong Kim, Jeoung Han Kim, Jae Keun Hong
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Patent number: 10023942Abstract: A titanium alloy, components formed thereof, and methods of use are provided. Embodiments of the alloy may be useful in the energy extraction environment. Components formed of the alloy may include subsea or land-based components associated with oil and gas production and drilling.Type: GrantFiled: April 28, 2015Date of Patent: July 17, 2018Assignee: Arconic Inc.Inventors: Ronald W. Schutz, Birendra C. Jena
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Patent number: 9947941Abstract: A titanium material for a polymer electrolyte fuel cell separator consists of, by mass %, a platinum group metal: 0.005% to 0.15% and a rare earth metal: 0.002% to 0.10%, with the balance being Ti and impurities. The titanium material of the present invention is provided with a film formed of a titanium oxide and a platinum group metal on the surface thereof. It is preferred that the film has a thickness of 50 nm or less, and that the concentration of the platinum group metal on the surface of the film is 1.5% by mass or more. With the thus formed film, the titanium material of the present invention is capable of achieving a reduction in initial contact resistance and ensuring good corrosion resistance. In the titanium material of the present invention, the rare earth metal is preferably Y, and the platinum group metal is preferably Pd.Type: GrantFiled: July 19, 2012Date of Patent: April 17, 2018Assignee: NIPPON STEEL & SUMITOMO METAL CORPORATIONInventors: Hideya Kaminaka, Kentarou Yoshida, Kouichi Takeuchi, Satoshi Matsumoto
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Patent number: 9913519Abstract: A hair iron has at least one heat transfer element that includes a substrate and a coating deposited on the substrate, the coating having a composition with at least 50 percent by mass of titanium and zirconium, a heating element, and an insulated grip region.Type: GrantFiled: June 9, 2015Date of Patent: March 13, 2018Assignee: Farouk Systems, Inc.Inventor: Farouk M. Shami
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Patent number: 9885102Abstract: The present invention provides colored pure titanium or titanium alloy having low susceptibility to discoloration in an atmospheric environment exhibiting a superior resistance to discoloration even when the titanium is used in an environment of harsh acid rain such as a roof or wall material and free from deterioration of the aesthetic appearance over a long period of time, that is, colored pure titanium obtained by the anodic oxidation method, that is, colored pure titanium or titanium alloy having low susceptibility to discoloration in an atmospheric environment characterized by having an average phosphorus content in a range of 40 nm from a surface of a titanium oxide layer formed on the titanium surface of 5.5 atomic % or less and by having an average carbon concentration in a range of a depth of 100 nm from the titanium surface of 3 to 15 atomic %.Type: GrantFiled: May 25, 2006Date of Patent: February 6, 2018Assignee: NIPPON STEEL & SUMITOMO METAL CORPORATIONInventors: Michio Kaneko, Kiyonori Tokuno, Takao Wada, Mitsuyuki Hasegawa, Kazuo Yamagishi
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Patent number: 9675730Abstract: The invention relates to a joint prosthesis having a shaft made from a titanium alloy, in which at least the shaft is investment cast and has a body-centered cubic crystal structure. A titanium alloy having this crystal structure (known as ?-titanium alloy) has an advantageously low modulus of elasticity which is well matched to the physiological demands of joint prostheses. Furthermore, implementation as a shaped casting allows a complex shape to be achieved. It is particularly embodied as a femoral prosthesis for an artificial hip joint, which has an elongate shaft with grooves and sawtooth-like projections for bone anchoring.Type: GrantFiled: March 8, 2006Date of Patent: June 13, 2017Assignee: Waldemar Link GmbH & Co. KGInventors: Sevki Baliktay, Arnold Keller
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Patent number: 9428822Abstract: Binder compositions for use in forming a bit body of an earth-boring bit include at least one of cobalt, nickel, and iron, and at least one melting point-reducing constituent selected from at least one of a transition metal carbide up to 60 weight percent, a transition metal boride up to 60 weight percent, and a transition metal silicide up to 60 weight percent, wherein the weight percentages are based on the total weight of the binder. Earth-boring bit bodies include a cemented tungsten carbide material comprising tungsten carbide and a metallic binder, wherein the tungsten carbide comprises greater than 75 volume percent of the cemented tungsten carbide material.Type: GrantFiled: March 19, 2013Date of Patent: August 30, 2016Assignees: Baker Hughes Incorporated, TDY Industries, Inc.Inventors: Prakash K. Mirchandani, Jimmy W. Eason, James J. Oakes, James C. Westhoff, Gabriel B. Collins
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Patent number: 9399806Abstract: A titanium alloy having at least 4% by weight aluminum and at least 0.1% by weight oxygen, the alloy also including at least one element selected from vanadium, molybdenum, chromium, and iron. The titanium alloy also includes hafnium in a proportion by weight of at least 0.1%.Type: GrantFiled: June 8, 2010Date of Patent: July 26, 2016Assignee: MESSIER-BUGATTI-DOWTYInventors: Francis Soniak, Jean-Michel De Monicault
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Patent number: 9296036Abstract: Methods for producing forged products and other worked products are disclosed. In one embodiment, a method comprises using additive manufacturing to produce a metal shaped-preform and, after the using step, forging the metal shaped-preform into a final forged product. The final forged product may optionally be annealed.Type: GrantFiled: July 9, 2014Date of Patent: March 29, 2016Assignee: Alcoa Inc.Inventors: Dustin M. Bush, Eric V. Roegner, Edward L. Colvin, Larry N. Mueller, Roberto J. Rioja, Brandon Hendrickson Bodily
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Patent number: 9171497Abstract: The present invention provides a method for inspecting packaging effectiveness of an OLED panel, including: (1) in a manufacture process of an OLED component, forming a test block on a substrate, wherein the test block is made of an active metal, and then forming a plurality of test electrodes, wherein each of the test electrodes has an end connected to the test block and an opposite end extending to the outside for connection with a measurement device; (2) packaging an OLED panel so that said opposite ends of the test electrodes extend out of an enclosing frame; (3) electrically connecting the measurement device to the test electrodes to measure an actual conductivity of the test block; and (4) determining packaging effectiveness according to the actual conductivity.Type: GrantFiled: June 26, 2013Date of Patent: October 27, 2015Assignee: Shenzhen China Star Optoelectronics Technology Co., LtdInventor: Weijing Zeng
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Patent number: 9039963Abstract: A titanium based, ceramic reinforced alloy ingot for use in producing medical implants. An ingot is formed from an alloy having comprising from about 5 to about 35 wt. % niobium, from about 0.5 to about 3.5 wt. % silicon, and from about 61.5 to about 94.5 wt. % of titanium. The alloy has a hexagonal crystal lattice ? phase of from about 20 vol % to about 70 vol %, and a cubic body centered ? crystal lattice phase of from about 30 vol. % to about 80 vol. %. The ingot has an ultimate tensile strength of about 940 MPa or more, and a Young's modulus of about 150 GPa or less. A molten substantially uniform admixture of a niobium, silicon, and titanium alloy is formed, cast into a shape, and cooled into an ingot. The ingot may then be formed into a medical implant and optionally annealed.Type: GrantFiled: October 12, 2012Date of Patent: May 26, 2015Assignee: Pulse Technologies, Inc.Inventors: Andrew E. Fisk, Anatolii Demchyshyn, Mykola Kuzmenko, Sergei Firstov, Leonid Kulak
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Publication number: 20150093287Abstract: A a titanium alloy can be applied on a substrate by one of melting, welding, and depositing said titanium alloy on said substrate and solidifying said deposited or molten titanium alloy. Further, 0.01-0.4 weight % Boron can be added to said titanium alloy before or during said melting, welding or depositing said titanium alloy on said substrate.Type: ApplicationFiled: May 16, 2012Publication date: April 2, 2015Applicant: GKN Aerospace Sweden ABInventors: Robert Pederson, Frank Skystedt
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Publication number: 20150075065Abstract: The invention provides a processing method for upgrading an organic phase substance by removing heavy element species from the organic phase substance originating from a resource substance in mild environmental conditions, and further provides a method for collecting removed heavy element species and a method for collecting other substances.Type: ApplicationFiled: October 24, 2014Publication date: March 19, 2015Applicant: NATIONAL INSTITUTE OF ADVANCED INDUSTRIAL SCIENCE AND TECHNOLOGYInventors: Tooru Nakamura, Yutaka Hayashi, Akira Suzuki, Richard Brommeland, Andrew Myles
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Publication number: 20150078958Abstract: The disclosure relates generally to core compositions and methods of molding and the articles so molded. More specifically, the disclosure relates to core compositions and methods for casting hollow titanium-containing articles, and the hollow titanium-containing articles so molded.Type: ApplicationFiled: September 18, 2013Publication date: March 19, 2015Applicant: GENERAL ELECTRIC COMPANYInventors: Bernard Patrick BEWLAY, Joan MCKIEVER, Brian Michael ELLIS, Nicholas Vincent MCLASKY
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Patent number: 8961816Abstract: Getter devices based on powders of alloys particularly suitable for hydrogen and nitrogen sorption are described. Such alloys have a composition including zirconium, vanadium, titanium and, optionally, one or more elements selected from iron, chromium, manganese, cobalt, nickel and aluminum.Type: GrantFiled: May 13, 2013Date of Patent: February 24, 2015Assignee: Saes Getters S.p.A.Inventors: Alberto Coda, Alessandro Gallitognotta, Antonio Bonucci, Andrea Conte
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Publication number: 20150021174Abstract: Provided is a high-purity titanium ingot having a purity, excluding an additive element and gas components, of 99.99 mass % or more, wherein at least one nonmetallic element selected from S, P, and B is contained in a total amount of 0.1 to 100 mass ppm as the additive component and the variation in the content of the nonmetallic element between the top, middle, and bottom portions of the ingot is within ±200%. Provided is a method of manufacturing a titanium ingot containing a nonmetallic element in an amount of 0.1 to 100 mass ppm, wherein S, P, or B, which is a nonmetallic element, is added to molten titanium as an intermetallic compound or a master alloy to produce a high-purity titanium ingot having a purity, excluding an additive element and gas components, of 99.99 mass % or more.Type: ApplicationFiled: February 13, 2013Publication date: January 22, 2015Inventors: Kazuto Yagi, Eiji Hino, Yuichiro Shindo
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Patent number: 8932518Abstract: The disclosure relates generally to mold compositions and methods of molding and the articles so molded. More specifically, the disclosure relates to mold compositions, intrinsic facecoat compositions, and methods for casting titanium-containing articles, and the titanium-containing articles so molded.Type: GrantFiled: February 29, 2012Date of Patent: January 13, 2015Assignee: General Electric CompanyInventors: Bernard Patrick Bewlay, Stephen Bancheri, Michael Weimer, Joan McKiever, Brian Ellis
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Publication number: 20150004337Abstract: The present invention provides a cold sprayed layer of tungsten, molybdenum, titanium, zirconium, or of mixtures of two or more of tungsten, molybdenum, titanium and zirconium, or of alloys of two or more of tungsten, molybdenum, titanium and zirconium, or of alloys of tungsten, molybdenum, titanium, zirconium with other metals, wherein the cold spayed layer has an oxygen content of below 1,000 ppm.Type: ApplicationFiled: July 4, 2014Publication date: January 1, 2015Inventors: STEFAN ZIMMERMANN, UWE PAPP, HEINRICH KREYE, TOBIAS SCHMIDT
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Publication number: 20140363330Abstract: Provided herein are methods of enhancing soft tissue integration with and seal around prosthetic devices.Type: ApplicationFiled: January 14, 2013Publication date: December 11, 2014Inventor: Takahiro Ogawa
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Publication number: 20140356221Abstract: Titanium alloy that is formed by subjecting titanium alloy to a treatment containing a hydrogen storing step for making the titanium alloy store hydrogen therein, a solution-treatment step for heating the titanium alloy having the hydrogen stored therein in the hydrogen storage step to apply a solution treatment to the hydrogen-stored titanium alloy, a cooling step for cooling the heated hydrogen-stored titanium alloy to develop martensitic transformation in the hydrogen-stored titanium alloy, a hot rolling step for heating the martensitic-transformed titanium alloy to a temperature which is not more than a predetermined transformation point and hot-rolling the martensitic-transformed titanium, and a dehydrogenation step for dehydrogenating the hot-rolled titanium alloy, thereby bringing the titanium alloy with the superplastic property.Type: ApplicationFiled: May 22, 2014Publication date: December 4, 2014Applicants: THE JAPAN RESEARCH INSTITUTE OF INDUSTRIAL SCIENCE, HONDA MOTOR CO., LTD.Inventors: Jun NAKAHIGASHI, Kyo TAKAHASHI
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Publication number: 20140348203Abstract: Provided in one embodiment is a method of identifying a stable phase of an ordering binary alloy system comprising a solute element and a solvent element, the method comprising: determining at least three thermodynamic parameters associated with grain boundary segregation, phase separation, and intermetallic compound formation of the ordering binary alloy system; and identifying the stable phase of the ordering binary alloy system based on the first thermodynamic parameter, the second thermodynamic parameter and the third thermodynamic parameter by comparing the first thermodynamic parameter, the second thermodynamic parameter and the third thermodynamic parameter with a predetermined set of respective thermodynamic parameters to identify the stable phase; wherein the stable phase is one of a stable nanocrystalline phase, a metastable nanocrystalline phase, and a non-nanocrystalline phase.Type: ApplicationFiled: May 20, 2014Publication date: November 27, 2014Applicant: Massachusetts Institute of TechnologyInventors: Heather A. Murdoch, Christopher A. Schuh
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Publication number: 20140348697Abstract: The present invention provides a heat resistant titanium alloy sheet excellent in cold workability having high temperature strength characteristics better than JIS Class 2 pure titanium and having a cold workability and high temperature oxidation resistance equal to or better than that of JIS Class 2 pure titanium and a method of production of the same, that is, a heat resistant titanium alloy sheet excellent in cold workability characterized by comprising, by mass %, 0.3 to 1.8% of Cu, 0.18% or less of oxygen, 0.30% or less of Fe, and, as needed, at least one of Sn, Zr, Mo, Nb, and Cr in a total of 0.3 to 1.5%, and the balance of Ti and less than 0.3% of impurity elements and by a ?-phase and Ti2Cu-phase being included in a volume percentage of 0 to 2% and, further, a method of production of that titanium alloy sheet characterized by performing the final annealing at 630 to 850° C. in temperature range or performing the hot-rolled sheet or coil annealing or intermediate annealing at 630 to 850° C.Type: ApplicationFiled: August 8, 2014Publication date: November 27, 2014Inventors: Hideki Fujii, Hiroaki Otsuka, Kazuhiro Takahashi
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Publication number: 20140322067Abstract: A titanium alloy having ultrahigh strength and ultralow elastic modulus, and showing linear elastic deformation behavior is disclosed. The titanium alloy (Ti-20Nb-5Zr-1Fe-O) of the present invention consists of titanium, niobium, zirconium, iron and oxygen. More specifically, the amount of niobium is 18 to 22 at. %, the amount of zirconium is 3 to 7 at. %, the amount of iron is 0.5 to 3.0 at. %, the amount of oxygen is 0.1 to 1.0 wt. %, and the balance is titanium.Type: ApplicationFiled: March 28, 2013Publication date: October 30, 2014Inventors: Chan Hee Park, Jong Taek Yeom, Seung Eon Kim, Seong Woong Kim, Jeoung Han Kim, Jae Keun Hong
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Publication number: 20140271336Abstract: A nanostructured titanium alloy article is provided. The nanostructured alloy includes a developed structure that has been processed from a combination of severe plastic deformation and non-severe plastic deformation type thermomechanical processing steps, with at least 80% of grains in the developed structure having a grain size?1.0 microns.Type: ApplicationFiled: March 15, 2013Publication date: September 18, 2014Applicant: CRS HOLDINGS INC.Inventors: Gian Colombo, Venkata N. Anumalasetty, Graham McIntosh
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Publication number: 20140271335Abstract: Provided is a super elastic alloy for biological use having a high biocompatibility, good processability and super elasticity, said super elastic alloy being a super elastic zirconium alloy for biological use comprising 27-54 mol % inclusive of titanium, 5-9 mol % inclusive of niobium which is a ? phase-stabilizing element capable of stabilizing the ? phase of zirconium, and 1-4 mol % inclusive in total of tin and/or aluminum which are ? phase-suppressing elements capable of suppressing the ? phase of zirconium, with the balance consisting of zirconium and inevitable impurities.Type: ApplicationFiled: August 28, 2012Publication date: September 18, 2014Applicant: UNIVERSITY OF TSUKUBAInventors: Shuichi Miyazaki, Heeyoung Kim, Yosuke Sato
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Publication number: 20140255816Abstract: A titanium material for a polymer electrolyte fuel cell separator consists of, by mass %, a platinum group metal: 0.005% to 0.15% and a rare earth metal: 0.002% to 0.10%, with the balance being Ti and impurities. The titanium material of the present invention is provided with a film formed of a titanium oxide and a platinum group metal on the surface thereof. It is preferred that the film has a thickness of 50 nm or less, and that the concentration of the platinum group metal on the surface of the film is 1.5% by mass or more. With the thus formed film, the titanium material of the present invention is capable of achieving a reduction in initial contact resistance and ensuring good corrosion resistance. In the titanium material of the present invention, the rare earth metal is preferably Y, and the platinum group metal is preferably Pd.Type: ApplicationFiled: July 19, 2012Publication date: September 11, 2014Applicant: NIPPON STEEL & SUMITOMO METAL CORPORATIONInventors: Hideya Kaminaka, Kentarou Yoshida, Kouichi Takeuchi, Satoshi Matsumoto
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Patent number: 8821610Abstract: A method and a device are described for the production of metal powder or alloy powder of a moderate grain sizes less than 10 ?m, comprising or containing at least one of the reactive metals zirconium, titanium, or hafnium, by metallothermic reduction of oxides or halogenides of the cited reactive metals with the aid of a reducing metal, wherein said metal powder or alloy powder is phlegmatized by adding a passivating gas or gas mixture during and/or after the reduction of the oxides or halogenides and/or is phlegmatized by adding a passivating solid before the reduction of the oxides or halogenides, wherein both said reduction and also said phlegmatization are performed in a single gas-tight reaction vessel which can be evacuated.Type: GrantFiled: January 8, 2009Date of Patent: September 2, 2014Assignee: Tradium GmbHInventor: Ulrich Gerhard Baudis
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Patent number: 8801875Abstract: A radiopaque alloy based on titanium nickelide and having shape memory and superelastic properties includes, according to one embodiment, at least one radiopaque alloying element selected from among gold, platinum, and palladium at a concentration of from about 10 at. % to about 20 at. %, and at least one additional alloying element selected from among aluminum, chromium, cobalt, iron, and zirconium, where the additional alloying element has a concentration of from about 0.5 at. % to about 4 at. %. The alloy includes titanium at a concentration of from about 48 at. % to about 52 at. %, and the balance of the alloy is nickel. The radiopaque alloy preferably exhibits superelastic behavior suitable for medical device applications in the human body.Type: GrantFiled: December 16, 2008Date of Patent: August 12, 2014Assignees: Cook Medical Technologies LLC, Lithotech Medical Ltd.Inventors: Valery Diamant, Dan Koren, Alexander I. Lotkov, Vladimir P. Sivokha, Liydmila L. Meysner, Viktor N. Grishkov, Vladimir P. Voronin
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Patent number: 8802151Abstract: The instant invention relates to shaped transition metal particles, in particular in the form of a dispersion in an aqueous and/or organic medium, the manufacture thereof and their use as an infrared (IR) absorbing agent, an IR curing agent for coatings, an additive in conductive formulations, an antimicrobial agent or for sensoring organic and/or inorganic compounds. Further, the invention relates to dispersions comprising said shaped particles and an aqueous and/or organic medium, such as a thermoplastic or crosslinkable polymer, as well as to antimicrobial compositions and products.Type: GrantFiled: March 17, 2010Date of Patent: August 12, 2014Assignee: BASF SEInventors: Nikolay A. Grigorenko, Michael Muehlebach, Florian Muehlebach
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Patent number: 8795445Abstract: There is provided a titanium plate having both high strength and good workability. The titanium plate is made of a titanium material in a plate shape, the titanium material consisting of by mass: more than 0.10% and less than 0.60% iron; more than 0.005% and less than 0.20% oxygen; less than 0.015% carbon; less than 0.015% nitrogen; less than 0.015% hydrogen; and balance titanium and unavoidable impurities, provided that the iron content is greater than the oxygen content, wherein the titanium plate has a two-phase structure of an ? phase and a ? phase and the circle-equivalent mean diameter of ? phase grains is 10 ?m or less.Type: GrantFiled: December 17, 2008Date of Patent: August 5, 2014Assignee: Nippon Steel & Sumitomo Metal CorporationInventors: Yoshihisa Shirai, Satoshi Matsumoto
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Publication number: 20140208968Abstract: One object is to provide a structure including a thin primer film formed by a dry process and tightly bound to a fluorine-containing silane coupling agent. In accordance with one aspect, a structure according to an embodiment of the present disclosure includes: a substrate; and a thin primer film containing at least one substance selected from the group consisting of silicon, titanium, aluminum, aluminum oxide, and zirconium and formed on a surface of the substrate by a dry process.Type: ApplicationFiled: August 10, 2012Publication date: July 31, 2014Applicant: Taiyo Chemical Industry Co., Ltd.Inventor: Kunihiko Shibusawa
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Publication number: 20140212324Abstract: Provided by the present invention are a fine crystallite high-function metal alloy member, a method for manufacturing the same, and a business development method thereof, in which a crystallite of a metal alloy including a high-purity metal alloy whose crystal lattice is a face-centered cubic lattice, a body-centered cubic lattice, or a close-packed hexagonal lattice is made fine with the size in the level of nanometers (10?9 m to 10?6 m) and micrometers (10?6 m to 10?3 m), and the form thereof is adjusted, thereby remedying drawbacks thereof and enhancing various characteristics without losing superior characteristics owned by the alloy.Type: ApplicationFiled: April 10, 2012Publication date: July 31, 2014Applicant: THREE-O CO., LTD.Inventor: Kazuo Ogasa
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Publication number: 20140193289Abstract: A one-dimensional titanium nanostructure and a method for fabricating the same are provided. A titanium metal reacts with titanium tetrachloride to form the one-dimensional titanium nanostructure on a heat-resistant substrate in a CVD method and under a reaction condition of a reaction temperature of 300-900° C., a deposition temperature of 200-850° C., a flow rate of the carrier gas of 0.1-50 sccm and a reaction time of 5-60 hours. The titanium nanostructure includes titanium nanowires, titanium nanobelts, flower-shaped titanium nanowires, titanium nanorods, titanium nanotubes, and titanium-titanium dioxide core-shell structures. The titanium nanostructure can be densely and uniformly grown on the heat-resistant substrate. The present invention neither uses a template nor uses the complicated photolithographic process, solution preparation process, and mixing-coating process. Therefore, the process scale-up, cost down, and the simplified production process are achieved.Type: ApplicationFiled: March 18, 2013Publication date: July 10, 2014Applicant: NATIONAL CHIAO TUNG UNIVERSITYInventors: Tze-Lung CHEN, Hsin-Tien CHIU, Chi-Young LEE
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Patent number: 8771439Abstract: The invention is directed to a method for producing a titanium aluminide intermetallic alloy composition having an improved wear resistance, the method comprising heating a titanium aluminide intermetallic alloy material in an oxygen-containing environment at a temperature and for a time sufficient to produce a top oxide layer and underlying oxygen-diffused layer, followed by removal of the top oxide layer such that the oxygen-diffused layer is exposed. The invention is also directed to the resulting oxygen-diffused titanium aluminide intermetallic alloy, as well as mechanical components or devices containing the improved alloy composition.Type: GrantFiled: April 1, 2009Date of Patent: July 8, 2014Assignee: UT-Battelle, LLCInventors: Jun Qu, Hua-Tay Lin, Peter J. Blau, Vinod K. Sikka
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Publication number: 20140161660Abstract: A titanium alloy including by mass %, a platinum group metal: 0.01 to 0.15% and a rare earth metal: 0.001 to 0.10%, with the balance being Ti and impurities. The titanium alloy preferably includes as a partial replacement for Ti, Co: 0.05 to 1.00% by mass, and the content of the platinum group metal is preferably in the range of 0.01 to 0.05% by mass. Furthermore, it is preferred that the platinum group metal be Pd and the rare earth metal be Y. Consequently, it is possible to provide a titanium alloy having corrosion resistance comparable to or better than that of the conventional art as well as good workability while offering an economic advantage with a lower content of platinum group metal or an advantage of less likelihood of corrosion growth originating at defects such as flaws that occurred in the surface.Type: ApplicationFiled: July 20, 2012Publication date: June 12, 2014Applicant: NIPPON STEEL & SUMITOMO METAL CORPORATIONInventors: Hideya Kaminaka, Yoshihisa Yonemitsu, Satoshi Matsumoto, Kouichi Takeuchi