Abstract: The present invention relates to an electrode composed of an Al-M-Cu based alloy, to a process for preparing the Al-M-Cu based alloy, to an electrolytic cell comprising the electrode the use of an Al-M-Cu based alloy as an anode and to a method for extracting a reactive metal from a reactive metal-containing source using an Al-M-Cu based alloy as an anode.

Abstract: Medical devices, such as stents, and methods of the devices are described.

Abstract: Medical devices and methods for making and using the same are disclosed. An example medical device may include a guidewire. The guidewire may include an elongate shaft. The shaft may include a porous metal alloy. The porous metal alloy may be arranged so that the porous metal alloy has a first pore distribution along a first portion of the shaft and a second pore distribution different from the first pore distribution along a second portion of the shaft.

Abstract: The invention relates to an assembly (1, 35, 71) of metal elements constituting a precursor for a superconductor. The assembly comprises at least one conductor element (5, 41, 73) adapted to provide a superconducting filament in the finished superconductor, and at least one doping element (7, 43, 75) providing a doping source for doping the conductor element. The invention also relates to a method suitable for producing a superconductor.

Abstract: A metallic article is prepared by first furnishing at least one nonmetallic precursor compound, wherein all of the nonmetallic precursor compounds collectively containing the constituent elements of the metallic article in their respective constituent-element proportions. The constituent elements together form a titanium-base alloy having a stable-oxide-forming additive element therein, such as magnesium, calcium, scandium, yttrium, lanthanum, cerium, praseodymium, neodymium, promethium, samarium, europium, gadolinium, terbium, dysprosium, holmium, erbium, thulium, ytterbium, and lutetium, and mixtures thereof. The stable-oxide-forming additive element forms a stable oxide in a titanium-based alloy. At least one additive element is present at a level greater than its room-temperature solid solubility limit in the titanium-base alloy. The precursor compounds are chemically reduced to produce an alloy material, without melting the alloy material. The alloy material may be consolidated.

Abstract: The presence of mycotoxins in agricultural products necessitates large scale testing of a wide range of sample material to ensure the safety of food and feed. The mycotoxin ochratoxin A represents an enablement for all mycotoxins as the level of sensitivity necessary for regulatory requirements for this compound at the part per billion level are as low or lower than any other mycotoxin. This invention describes the identification of a set of DNA ligands with sufficiently high binding affinity and specificity for ochratoxin A to enable an improvement over existing methods for the separation, concentration and quantitative determination of ochratoxin A in sample material.

Abstract: A method of forming an article from an ??? titanium including, in weight percentages, from about 2.9 to about 5.0 aluminum, from about 2.0 to about 3.0 vanadium, from about 0.4 to about 2.0 iron, from about 0.2 to about 0.3 oxygen, from about 0.005 to about 0.3 carbon, from about 0.001 to about 0.02 nitrogen, and less than about 0.5 of other elements. The method comprises cold working the ??? titanium alloy.

Abstract: The present disclosure is related to homogeneous alloys comprising titanium and 9% to less than 20% by weight of tungsten, wherein the alloy has a yield strength of at least 120,000 psi and ductility of least 20% elongation; and with further alloying an ultimate tensile strength of at least 200,000 psi and useful ductility of at least 2% elongation; and with the addition of ceramic particulate reinforcements can exhibit an ultimate tensile strength of at least 180,000 psi. Products and metal matrix composites comprising such homogeneous alloys are also disclosed. The metal matrix composites further comprise a discontinuous reinforcement chosen from TiC, TiB2, or TiB, particles or combinations of such particles. Method of making such alloys and composites as well as products made from such alloys and composites are also disclosed.

Abstract: A titanium alloy containing carbon with and without addition of silicon exhibiting improved corrosion resistance and mechanical strength as compared to commercially pure ASTM grade 2 titanium or PGM-alloyed ASTM grade 7 titanium.

Abstract: A titanium alloy which, even under the influence of high application temperatures, has a low tendency to becoming brittle as a result of coarse grain formation, comprises (in wt. %) Fe: ?2%, Si: 0.01 to 0.8%, 0: ?0.3%, C: ?0.1%, one or more elements of the Lanthanide group at total levels of 0.01-2% and, optionally, one or more elements of Al and O at total levels of a maximum of 1%, one or more elements of Mo, Ta, Nb, Zr, Mn, Cr, Co, Ni, Cu, V, Si, and H at total levels of a maximum of 3%, the remainder being titanium and unavoidable impurities.

Abstract: Commercially pure titanium having UFG structure and enhanced mechanical and biomedical characteristics has nanocrystalline alpha-phase grains with a hexagonal close-packed lattice, in which the share of grains with a size of 0.1 . . . 0.5 ?m and a grain shape coefficient of no more than 2 in the mutually perpendicular planes makes no less than 90%, over 60% of the grains having high-angle boundaries disoriented in relation to the adjacent grains by the angles from 15 to 90°. The method for making a rod of the material provides for equal-channel angular pressing of a billet at T?450° C. with the total accumulated true strain e?4 to effect severe plastic deformation of the billet and subsequent thermomechanical treatment with a gradual decrease of the temperature in the range of 450 . . . 350° C. and the strain rate of 10?2 . . . 10?4 s?1 with the strain degree from 40 to 80% to effect additional plastic deformation.

Abstract: A method of removing oxygen from a solid metal, metal compound or semi-metal M1O by electrolysis in a fused salt of M2Y or a mixture of salts, which comprises conducting electrolysis under conditions such that reaction of oxygen rather than M2 deposition occurs at an electrode surface and that oxygen dissolves in the electrolyte M2Y and wherein, M1O is in the form of (sintered) granules or is in the form of a powder which is continuously fed into the fused salt. Also disclosed is a method of producing a metal foam comprising the steps of fabricating a foam-like metal oxide perform, removing oxygen from said foam structured metal oxide preform by electrolysis in a fused salt of M2Y or a mixture of salts, which comprises conducting electrolysis under conditions such that reaction of oxygen rather than M2 deposition occurs at an electrode surface. The method is advantageously applied for the production of titanium from Ti-dioxide.

Abstract: An intracranial stent formed from Nitinol has variable flexibility. The stent (10) is formed from a plurality of stent rings (12) connected by tie bars (14). The tie bars (14) in a central soft zone (16) are heat treated so as to confer a higher transition temperature on the Nitinol. As a result, at body temperature, the soft zone (16) has reduced longitudinal stiffness as compared to the stiffer zones (18) found at the ends of the stent (10).

Abstract: A method of increasing the apparent density of agglomerated ligmental titanium or titanium alloy powder produced by the subsurface reduction of titanium tetrachloride vapor or a mixture of titanium tetrachloride and other halide vapors in a flowing stream of alkali or alkaline earth metal or mixtures thereof having a first apparent density after distillation is disclosed. The agglomerated ligmental titanium or titanium alloy powder is introduced into an attriting system wherein the agglomerated ligmental titanium or titanium alloy powder is attrited until the powder becomes more spherical than ligmental and the first apparent density is increased by a factor of from about 3 to about 8. Inert atmosphere may be used to prevent unwanted oxygen contamination.

Abstract: Provided is a beta-based titanium alloy with a low elastic modulus, including no elements harmful to the human body and having excellent biocompatibility. The beta-based titanium alloy includes titanium (Ti), niobium (Nb) and zirconium (Zr) as major alloying elements, and further includes tantalum (Ta), hafnium (Hf), molybdenum (Mo), tin (Sn), and the like. The beta-based titanium alloy has a much lower elastic modulus than the typical biomedical titanium alloys, and thus can resolve the problem of so-called “stress shield effect.” Therefore, the beta-based titanium alloy can be widely used as a material for general civilian goods such as eyewear frames and headsets and sports and leisure goods, as well as a biomedical material for artificial bones, artificial teeth and artificial hip joints.

Abstract: To provide a production process of an electrode catalyst for fuel cell whose initial voltage is high and whose endurance characteristics, especially, whose voltage drop being caused by high-potential application is less. A production process according to the present invention of an electrode catalyst for fuel cell is characterized in that: it includes: a dispersing step of dispersing a conductive support in a solution; a loading step of dropping a platinum-salt solution, a base-metal-salt solution and an iridium-salt solution to the resulting dispersion liquid, thereby loading respective metallic salts on the conductive support as hydroxides under an alkaline condition; and an alloying step of heating the conductive support with metallic hydroxides loaded in a reducing atmosphere to reduce them, thereby alloying them.

Abstract: A method of fabricating a porous metal-based biomaterial, the method includes dispersing microwave susceptors into organic solvent to form a homogeneous suspension, dispersing bioactive fillers into organic solvent to form a homogeneous solution, mixing metal powder with the homogeneous solution and the homogeneous suspension to form a mixture, cold-pressing the mixture into a compact with predefined shape and size, placing the compact in a sintering container, and emitting microwave to heat the compact and remove the organic solvent resided in the compact at the same time.

Abstract: A titanium base alloy powder having lesser amounts of aluminum and vanadium with an alkali or alkaline earth metal being present in an amount of less than about 200 ppm. The alloy powder is neither spherical nor angular and flake shaped. 6/4 alloy is specifically disclosed having a packing fraction or tap density between 4 and 11%, as is a method for making the various alloys.

Abstract: There is provided a titanium alloy for corrosion-resistant materials, which contains 0.01-0.12% by mass in total of at least one of platinum group elements; at least Si and one of, or both of, Sn and Mn, selected from the group consisting of Al, Cr, Zr, Nb, Si, Sn and Mn, wherein the total content of Al, Cr, Zr, Nb, Si, Sn and Mn is 5% by mass or less; and the residue comprising Ti and impurities.

Abstract: A titanium alloy containing carbon with and without addition of silicon exhibiting improved corrosion resistance and mechanical strength as compared to commercially pure ASTM grade 2 titanium or PGM-alloyed ASTM grade 7 titanium.

Abstract: A method for the production of titanium trifluoride from a titanium-containing material, includes the steps of producing a fluoride solution of Ti(IV) from the titanium-containing material and reducing the Ti(IV) in the solution with a transition metal or an alloy of the transition metal. The transition metal is selected from manganese, iron, cobalt, nickel and zinc. An ammonium containing salt and either ammonia or ammonium fluoride are added to the resulting solution containing Ti(III) to produce a precipitate, and the precipitate is pyrolysed to produce titanium trifluoride.

Abstract: The present invention is directed to a process for the preparation of a metal powder having a purity at least as high as the starting powder and having an oxygen content of 10 ppm or less comprising heating said metal powder containing oxygen in the form of an oxide, with the total oxygen content being from 50 to 3000 ppmf in an inert atmosphere at a pressure of from 1 bar to 10?7 to a temperature at which the oxide of the metal powder becomes thermodynamically unstable and removing the resulting oxygen via volatilization. The metal powder is preferably selected from the group consisting of tantalum, niobium, molybdenum, hafnium, zirconium, titanium, vanadium, rhenium and tungsten. The invention also relates to the powders produced by the process and the use of such powders in a cold spray process.

Abstract: Particles and manufacturing methods thereof are provided. The manufacturing method of the particle includes providing a precursor solution containing a precursor dissolved in a solution, and irradiating the precursor solution with a high energy and high flux radiation beam to convert the precursor to nano-particles. Particles with desired dispersion, shape, and size are manufactured without adding a stabilizer or surfactant to the precursor solution.

Abstract: The invention provide for a method of improving bioactivity of a surface of an object. The invention further provides for a method of preparing an object for medical implantation. The invention even further provide for an article made by a method comprising the steps of forming a gas-cluster ion-beam in a reduced-pressure chamber, introducing the article into the reduced-pressure chamber, and irradiating at least a portion of the surface of the object with the gas-cluster ion-beam. The invention still further provides for an article for medical or surgical implantation made by a method comprising selecting at least a portion of a surface of the object for increased bioactivity, forming a gas-cluster ion-beam in a reduced-pressure chamber, introducing the object into the reduced-pressure chamber, and irradiating the selected at least a portion with the gas-cluster ion-beam to increase the bioactivity of the at least a portion.

Abstract: Provided herein are materials that can achieve up to 14% hydrogen absorption by weight in ambient conditions, which is a marked improvement over the hydrogen absorption values found in the prior art. Further provided are experimental conditions necessary to produce these materials. In order to produce the hydrogen storage material, a transition metal (or Lithium) is vaporized in a pi bond gas in conditions that permit only a few bonding collisions to occur between the vaporized transition metal atoms and pi bond gas molecules before the resulting bonded material is collected.

Abstract: A titanium alloy containing carbon with and without addition of silicon exhibiting improved corrosion resistance and mechanical strength as compared to commercially pure ASTM grade 2 titanium or PGM-alloyed ASTM grade 7 titanium.

Abstract: An oxidation resistant, high strength titanium alloy, particularly adapted for use in the manufacture of automotive exhaust system components and other applications requiring oxidation resistance and strength at elevated temperatures. The alloy comprises, in weight percent, iron less than 0.5, or 0.2 to less than 0.5%, oxygen 0.02 to less than 0.15%, silicon 0.15 to 0.6%, and balance titanium. Optional alloying elements are Al, Nb, V, Mo, Sn, Zr, Ni, Cr and Ta, with a total content of less than 1.5.

Abstract: The use of Titanium metal fine-particles for increasing of effect of the germicidal medicines used for human skin, skin infection and traumatism, is provided. The application of the Titanium metal fine-particles layer being laid on or close to skin, in combination with a medicine, functions to restrain bacteria breeding and multiplying, accelerate skin and dermic-organism metabolism, and promoting capillary purification. By these functions, an environment which is harmful and fatal for bacteria breeding/multiplying will be developed on the human body skin and dermic-organism. These functions are demonstrated by the increased effects of the germicidal medicines which are used for human skin dermatosis, skin infection and traumatism.

Abstract: A method of producing titanium metal from a titanium-containing material includes the steps of producing a solution of M?TiF6 from the titanium-containing material, selectively precipitating M?2TiF6 from the solution by the addition of (M?)aXb and using the selectively precipitated M?2TiF6 to produce titanium. M? is a cation of the type which forms a hexafluorotitanate, M? is selected from ammonium and the alkali metal cations, X is an anion selected from halide, sulphate, nitrite, acetate and nitrate and a and b are 1 or 2.

Abstract: A mechanical structure is provided with a crystalline superelastic alloy that is characterized by an average grain size and that is characterized by a martensitic phase transformation resulting from a mechanical stress input greater than a characteristic first critical stress. A configuration of the superelastic alloy is provided with a geometric structural feature of the alloy that has an extent that is no greater than about 200 micrometers and that is no larger than the average grain size of the alloy. This geometric feature is configured to accept a mechanical stress input.

Abstract: The patent provides the titanium alloy with extra-low modulus and superelasticity containing 20˜35 wt. % niobium, 2˜15 wt. % zirconium, balanced titanium and other unavoidable impurity elements. The advantages of the invention alloy are shown as follows: The invention titanium alloy has superior cold processing capacity and low work hardening rate; It can be severely deformed by cold rolling and cold drawing; It has superelasticity, shape memory effect, damping capacity, low modulus, high strength, good corrosion resistance and high biocompatibility; The invention titanium alloy can be made into nano-size materials by cold deformation and extra high strength can be achieved by heat treatment.

Abstract: A hydrogen-permeable Nb—Ti—Ni alloy having a composition represented by Nb100-x-yTixNiy, wherein 10?x?60, and 10?y?50 by atomic %, with an oxygen content of 1000 ppm or less in an as-cast state, which comprises (a) a hydrogen-permeable primary phase containing 70 atomic % or more of Nb and 10 atomic % or less of Ni, and (b) a eutectic phase having a particle phase comprising Nb and Ti as main components with a small Ni content and having an average particle size of about 5 ?m or less, which is dispersed in a matrix phase comprising 60 atomic % or more in total of Ni and Ti and having hydrogen embrittlement resistance, the alloy having a structure substantially free from an intermetallic compound phase.

Abstract: An alloy having from about 5 to about 15 wt % Ta, from 0 to about 5 wt % Nb, from about 0.5 to about 15 wt % Zr, and the balance Ti is disclosed. The alloy is particularly intended for medical devices, such as implants for the body.

Abstract: A method for forming a finished implant prosthesis which comprises: (a) providing an unforged alloy consisting essentially of Ti(x %)Al(y %)Nb wherein x is between about 45 to 54% by atoms, y is between about 15 to 25% by atoms and the balance is niobium; (b) forging the alloy at an elevated temperature below a melting point of the alloy in a shape which is an implant preform; and (c) machining the implant preform to provide a machined implant; and (d) finishing the exposed surfaces of the implant so as to provide the exposed surfaces with a finish which provides biocompatibility, to thereby form the implant prosthesis.

Abstract: The invention relates to a process for the production of metal alloy powders, in particular the invention relates to a process for producing titanium metal alloys from titanium dioxide and aluminium. Optionally the process can also include the use of one or more other oxides (metal or non-metal). The result is at least a Ti—Al alloy powder. If another metal oxide is used the result is a Ti-ternary alloy powder. If SiO2 is used the result is a Ti—Al—Si alloy.

Abstract: Composite structures having a reinforced material interjoined with a substrate and methods of creating a composite material interjoined with a substrate. In some embodiments the composite structure may be a line or a spot or formed by reinforced material interjoined with the substrate. The methods typically include disposing a precursor material comprising titanium diboride and/or titanium monoboride on at least a portion of the substrate and heating the precursor material and the at least a portion of the substrate in the presence of an oxidation preventative until at least a portion of the precursor material forms reinforced material interjoined with the substrate. The precursor material may be disposed on the substrate as a sheet or a tape or a slurry or a paste. Localized surface heating may be used to heat the precursor material. The reinforced material typically comprises a titanium boron compound, such as titanium monoboride, and preferably comprises ?-titanium.

Abstract: A fuel cell catalyst comprising platinum, titanium and tungsten. In one or more embodiments, the concentration of platinum is less than 60 atomic percent, and/or the concentration of titanium is at least 20 atomic percent, and/or the concentration of tungsten is at least 25 atomic percent.

Abstract: A method and apparatus for making alloys or ceramics by the subsurface injection of an equilibrium vapor of a boiling liquid of the ceramic or alloys constituents is disclosed. Various powders and products are disclosed.

Abstract: The object of the present invention is to provide a mold which has low reactivity with molten alloys and which is inexpensive, a method for manufacturing the same and a molded article using the mold. A mold 40 in accordance with the present invention serves for manufacturing a molded article 60 of a titanium-aluminum alloy or a titanium alloy. At least an initial layer 44a of a cavity surface 43 of a mold body 41 constituting the mold 40 is formed of a calcined product of a slurry comprising a filler having cerium oxide as a main component and a binder having silica sol as a main component.

Abstract: An oxidation resistant, high strength titanium alloy, particularly adapted for use in the manufacture of automotive exhaust system components and other applications requiring oxidation resistance and strength at elevated temperatures. The alloy comprises, in weight percent, iron less than 0.5, or 0.2 to less than 0.5%, oxygen 0.02 to less than 0.15%, silicon 0.15 to 0.6%, and balance titanium. Optional alloying elements are Al, Nb, V, Mo, Sn, Zr, Ni, Cr and Ta, with a total content of less than 1.5.

Abstract: A titanium alloy containing carbon with and without addition of silicon exhibiting improved corrosion resistance and mechanical strength as compared to commercially pure ASTM grade 2 titanium or PGM-alloyed ASTM grade 7 titanium.

Abstract: A radiopaque nitinol medical device such as a stent for use with or implantation in a body lumen is disclosed. The stent is made from a superelastic alloy such as nickel-titanium or nitinol, and includes a ternary element selected from the group of chemical elements consisting of iridium, platinum, gold, rhenium, tungsten, palladium, rhodium, tantalum, silver, ruthenium, or hafnium. The added ternary element improves the radiopacity of the nitinol stent comparable to that of a stainless steel stent of the same size and strut pattern coated with a thin layer of gold. The nitinol stent has improved radiopacity yet retains its superelastic and shape memory behavior and further maintains a thin strut/wall thickness for high flexibility.

Abstract: To provide a Ti—Ni—Nb alloy device which is a shape memory device excellent in response characteristics. The Ti—Ni—Nb alloy device is made of a Ti—Ni—Nb alloy which finishes transformation at a temperature lower than 10° C. after start of reverse transformation.

Abstract: Disclosed are a Ti alloy having an excellent hydrogen absorption inhibition effect, a Ti alloy member using the Ti alloy, and a manufacturing thereof. A Ti alloy is characterized in that it contains 0.1 to 5.0% by mass in total of at least one of Zr and Hf, and a residue comprising Ti and impurities.

Abstract: A Ti-precursor for forming a Ti-containing thin layer represented by the formula I below, a method of preparing the same, a method of preparing a Ti-containing thin layer by employing the Ti-precursor and the Ti-containing thin layer are provided: wherein X1 and X2 are independently F, Cl, Br or I; n is 0, 1, 2, 3, 4 or 5; m is 0, 1, 2, 3, 4, 5, 6 or 7; and R1 and R2 are independently a linear or branched C1-10 alkyl group. The Ti precursor for forming the Ti-containing thin layer can be deposited at a deposition temperature of approximately 150° C.˜200° C., and a Ti-containing thin layer with a high performance character can be prepared.

Abstract: The invention relates to a titanium alloy which, even under the influence of high application temperatures, has a low tendency to becoming brittle as a result of coarse grain formation. The titanium alloy thus comprises (in wt. %) Fe:=2%, Si:0.1=0.8%, O:=0.3%, C:=0.1%, one or more elements of the Lanthanide group at total levels of 0.01-2% and, optionally, one or more elements from the group Al, O at total levels of a maximum of 1%, one or more elements from the group Mo, Ta, Nb, Zr, Mn, Cr, Co, Ni, Cu, V, Si, or H at total levels of a maximum of 3%, the remainder being titanium and unavoidable impurities.

Abstract: An object is to provide a titanium alloy for corrosion-resistant materials that is capable of being produced at low cost while maintaining the capability to suppress the deterioration of corrosion resistance. According to the present invention, there is provided a titanium alloy for corrosion-resistant materials, which contains 0.01-0.12% by mass in total of at least one of platinum group elements, at least one of Al, Cr, Zr, Nb, Si, Sn and Mn, and the residue comprising Ti and impurities, in which the total content of Al, Cr, Zr, Nb, Si, Sn and Mn is 5% by mass or less.

Abstract: A braze material and method of brazing titanium metals. The material may consist of Ti, Ni, Cu Zr, PM and M where PM is a precious metal and M may be Fe, V, Cr, Co, Mo, Nb, Mn, Si, Sn, Al, B, Gd, Ge or combinations thereof, with the (Cu+PM)/Ni ratio around 0.9. Optionally, a second brazing may be performed to rebraze any braze joint that did not braze successfully. The second brazing material has a lower braze temperature than the first and may consist of a mixture of Ti, Ni, Cu, Zr PM and M with from 1-20 wt % more Zr, PM, M or combinations thereof than the first braze. The braze material may be placed on a base material, in a vacuum furnace, and heated to form a braze joint between the braze and base material. The heating step may occur from about 800-975° C. and over 3 to 15 minutes.

Abstract: A method of producing a non-metal element or a metal or an alloy thereof from a halide or mixtures thereof. The halide or mixtures thereof are contacted with a stream of liquid alkali metal or alkaline earth metal or mixtures thereof in sufficient quantity to convert the halide to the non-metal or the metal or alloy and to maintain the temperature of the reactants at a temperature lower than the lesser of the boiling point of the alkali or alkaline earth metal at atmospheric pressure or the sintering temperature of the produced non-metal or metal or alloy. A continuous method is disclosed, particularly applicable to titanium.

Abstract: A high-strength titanium alloy of the present invention includes Ti as a major component, 15 to 30 at % Va group element, and 1.5 to 7 at % oxygen (O) when the entirety is taken as 100 atomic % (at %), and its tensile strength is 1,000 MPa or more. Overturning the conventional concept, regardless of being high oxygen contents, it has been possible to achieve the compatibility between the high strength and high ductility on a higher level.