Silica Patents (Class 423/335)
  • Patent number: 8211193
    Abstract: A method of chemical mechanical polishing a surface of a substrate including the step of: contacting the substrate and a composition including a plurality of colloidal silica particles having less than 200 ppb of each trace metal impurity, excluding potassium and sodium, have less than 2 ppm residual alcohol and wherein the cumulative concentration of the trace metal, excluding potassium and sodium, is in the range from about 0.5 to about 5 ppm; and a medium for suspending the particles; wherein the composition is an ultrapure colloidal silica dispersion; and wherein the contacting is carried out at a temperature and for a period of time sufficient to planarize the substrate.
    Type: Grant
    Filed: September 22, 2006
    Date of Patent: July 3, 2012
    Assignee: Fujifilm Planar Solutions, LLC
    Inventors: Deepak Mahulikar, Yuhu Wang, Ken A. Delbridge, Gert R. M. Moyaerts, Saeed H. Mohseni, Nichole R. Koontz, Bin Hu, Liqing Wen
  • Publication number: 20120164052
    Abstract: The present invention is to provide hollow particles with a low degree of agglomeration and having a high roundness, and a process for producing them. Hollow particles comprising a silicon compound, having an average particle size of from 5 to 65 nm and an average roundness of at least 0.90, and having a shell comprising the silicon compound and having a thickness of from 1 to 20 nm. Further, a method for producing hollow particles, which comprises adding sulfuric acid to a liquid containing spherical organic polymer-silicon compound composite particles having a core comprising an organic polymer and a shell comprising a silicon compound in a medium containing at least 95 mass % of water, followed by heating to carbonize the organic polymer thereby to convert it to a carbide, and subjecting the carbide to decomposition using a liquid oxidizing agent other than sulfuric acid.
    Type: Application
    Filed: March 6, 2012
    Publication date: June 28, 2012
    Applicant: Denki Kagaku Kogyo Kabushiki Kaisha
    Inventors: Takashi Kawasaki, Motoharu Fukazawa, Isao Sugimoto
  • Publication number: 20120156121
    Abstract: A coating for spark plugs and engine parts is resistant to fouling. The coating may be applied to the spark plug or engine part by dipping the part in a sol gel solution, ensuring it wets the part, and extracting it at a slow, controlled rate. As the part is allowed to dry, the sol gel reacts with moisture in the air to form a thin oxide film. Unlike conventional sol gel applications, which apply the oxide directly to the part, the present invention may form an oxide coating, in situ, while drying in place on the part.
    Type: Application
    Filed: December 15, 2010
    Publication date: June 21, 2012
    Applicant: HONEYWELL INTERNATIONAL INC.
    Inventors: DEREK RAYBOULD, CHRISTIAN DELACRUZ, CARL KISER
  • Patent number: 8202502
    Abstract: The invention provides hydrophobic surface-treated silica particles having (1) a ratio T2:T3 of about 0.4 or more, wherein T2 is the intensity of a peak having a chemical shift in the CP/MAS 29Si NMR spectrum centered within the range of ?56 ppm to ?59 ppm, and wherein T3 is the intensity of a peak having a chemical shift in the CP/MAS 29Si NMR spectrum centered within the range of ?65 ppm to ?69 ppm, and (2) a ratio (T2+T3)/(T2+T3+M) of greater than about 0.05, wherein M is the intensity of a peak having a chemical shift in the CP/MAS 29Si NMR spectrum centered within the range of +7 ppm to +18 ppm. The invention also provides a method of preparing hydrophobic surface-treated silica particles.
    Type: Grant
    Filed: July 6, 2007
    Date of Patent: June 19, 2012
    Assignee: Cabot Corporation
    Inventors: Joachim K. Floess, William R. Williams, Dmitry Fomitchev
  • Publication number: 20120148470
    Abstract: A method for producing silica particles, includes preparing a silica particle dispersion containing silica particles, and a solvent containing an alcohol and water, and bringing supercritical carbon dioxide into contact with the silica particle dispersion to remove the solvent.
    Type: Application
    Filed: November 3, 2011
    Publication date: June 14, 2012
    Applicant: FUJI XEROX CO., LTD.
    Inventors: Sakae TAKEUCHI, Shinichiro KAWASHIMA, Hiroyoshi OKUNO, Hideaki YOSHIKAWA, Yuji MASUDA, Shunsuke NOZAKI, Yuka ZENITANI
  • Patent number: 8197782
    Abstract: The present invention is directed to a method of making metal oxide and mixed metal oxide particles. The method includes treating a mixture formed from a metal source, such as metal alkoxide, a surfactant, and a first alcohol in an aqueous media at a very high metal oxide yield. The mixture is reacted using a catalyst to form metal oxide particles having a desired particle size in said mixture. The method is particularly suitable for forming silica particles. The metal oxide particles can then be heat treated to form synthetic fused metal oxides such as, for example, synthetic fused silica.
    Type: Grant
    Filed: February 8, 2010
    Date of Patent: June 12, 2012
    Assignee: Momentive Performance Materials
    Inventor: Antonio L. DeVera
  • Patent number: 8192522
    Abstract: A process for generating energy comprises process comprises exothermically reacting Mg with SiO2 to yield at least Mg2Si and Si; b)reacting the Mg2Si to yield at least lower silanes, and at least one magnesium product; c) generating at least higher silanes from at least a portion of the lower silanes; d) combusting the higher silanes and the Si to yield at least one silicon product.
    Type: Grant
    Filed: March 26, 2009
    Date of Patent: June 5, 2012
    Assignee: ET-Energy Corp.
    Inventor: Petr Gladkov
  • Publication number: 20120127633
    Abstract: A metal electrolytic capacitor capable of quickly absorbing and immobilizing a belching vapor of a driving electrolyte and widely reducing leakage when an explosion-proof valve operates. An aluminum electrolytic capacitor body is configured by housing a capacitor element in a cylindrical aluminum case, a pair of leads extend from the capacitor body, an explosion-proof valve is formed on a top panel portion of the metal case, a cylindrical cap as a casing is attached from above to the capacitor body, a plurality of small openings are formed on a top panel portion (bottom portion) of the cap, and an absorbent or a mixture of an absorbent and a water molecular compound wrapped in a permeable fiber material, such as unwoven fabric and filter paper, is placed in a space between the cap and the top panel portion of the capacitor body.
    Type: Application
    Filed: June 2, 2010
    Publication date: May 24, 2012
    Inventors: Koichi Mori, Mitsuru Nozue, Minoru Yagi
  • Publication number: 20120130482
    Abstract: The disclosure describes a coating for medical implants, in particular, vascular stents, said coating comprising silicon dioxide, towards medical implants with a coating containing silicon dioxide and towards a method for their production. The coating can contain additional admixtures and have functionalization coats. The substrate of the coating is produced from a durable material, preferably from a stainless steel.
    Type: Application
    Filed: January 31, 2012
    Publication date: May 24, 2012
    Applicant: AXETIS AG
    Inventor: Carlo Civelli
  • Publication number: 20120128958
    Abstract: Silica aerogels with improved properties are disclosed together with methods for synthesizing such aerogels. The improved properties include lower thermal conductivity (better insulating capacity), lower acoustic velocity, lower dielectric constant and improved ductility. Greater tunability of the refractive index can also be achieved. The silica aerogels are prepared by a sol-gel processing method that provides better control of the formation of aerogel structures. Generally speaking, the improvements arise from control of the synthesis to create a morphology of primary clusters and diverse-sized secondary clusters of dense silica aerogels separated by less densely packed regions. By providing a broader range of secondary clusters and/or pore sizes and loose connectivity between clusters, reductions can be achieved in thermal conductivity and flexural modulus.
    Type: Application
    Filed: August 9, 2011
    Publication date: May 24, 2012
    Applicant: MASSACHUSETTS INSTITUTE OF TECHNOLOGY
    Inventors: Taofang Zeng, Yanjia Zuo, Gang Chen
  • Publication number: 20120121494
    Abstract: The present invention relates to a process for increasing the binding capacity, in particular reactivation, of silica surfaces, in particular silica matrices, by treatment with water or an aqueous solution and also the use of water for reactivating silica membranes.
    Type: Application
    Filed: May 20, 2010
    Publication date: May 17, 2012
    Inventor: Markus Sprenger-Haus-Sels
  • Patent number: 8178067
    Abstract: A production method of amorphous silicon oxide powder comprises a step of preparing a wood, agricultural crop or plant containing hexose and/or pentose and silicon oxide as a starting raw material, a step of hydrolyzing the starting raw material with nitric acid, hydrochloric acid, sulfuric acid, phosphoric acid or organic acid to reduce a content of the hexose to 10% by weight or less and/or a content of the pentose to 20% by weight or less, and a step of burning residue yielded in the hydrolyzing step at a temperature of 400° C. to 1200° C.
    Type: Grant
    Filed: August 29, 2006
    Date of Patent: May 15, 2012
    Assignee: Kurimoto, Ltd.
    Inventors: Katsuyoshi Kondoh, Yoshisada Michiura
  • Publication number: 20120115967
    Abstract: The invention relates to the preparation of a Fischer-Tropsch catalyst support and of a Fischer-Tropsch catalyst. A silica comprising support is subjected to hydrothermal treatment. The hydrothermal treatment results in catalysts having improved C5+ selectivity as compared with catalysts prepared with a non-treated silica comprising support.
    Type: Application
    Filed: November 8, 2011
    Publication date: May 10, 2012
    Applicant: SHELL OIL COMPANY
    Inventors: Gerrit Leendert BEZEMER, Peter GEERINCK
  • Patent number: 8173092
    Abstract: A novel silica which is in the form of ultrafine particles having mesopores and has a regular structure; and a process for producing the silica. The silica is a self-organized nanoparticulate silica characterized in that the average particle diameter is 4 to 30 nm, preferably 6 to 20 nm, and these particles are regularly arranged so as to form a primitive cubic lattice. The self-organized nanoparticulate silica is produced by mixing an alkoxysilane with an aqueous solution of a basic amino acid, reacting the mixture at 40 to 100° C., and subjecting the reaction mixture to drying and preferably to subsequent burning. Also provided is a process for producing fine silica particles having a particle diameter of 4 to 30 nm, which comprises mixing a solution of an alkoxysilane compound having 1 to 4 alkoxy groups with a solution of a basic amino acid and reacting the mixture at 20 to 100° C. to cause hydrolysis and condensation polymerization.
    Type: Grant
    Filed: March 10, 2006
    Date of Patent: May 8, 2012
    Assignee: Japan Science and Technology Agency
    Inventors: Takashi Tatsumi, Toshiyuki Yokoi
  • Patent number: 8163260
    Abstract: The present invention relates to processes for the production of monodisperse SiO2 particles by hydrolytic polycondensation of tetraalkoxysilanes and/or organotrialkoxysilanes, in which the hydrolytic polycondensation is carried out in a medium comprising water, one or more solubilizers and one or more amines, and in which highly monodisperse, non-porous particles are obtained. The present invention likewise relates to powders obtainable by the processes, and to the use thereof.
    Type: Grant
    Filed: February 10, 2005
    Date of Patent: April 24, 2012
    Assignee: Merck Patent GmbH
    Inventor: Armin Kuebelbeck
  • Publication number: 20120094125
    Abstract: A method for preparing precipitated silica includes the reaction of sodium metabisulfite or sodium sulfite with sand, wherein a) sand is mixed with sodium metabisulfite or sodium sulfite; b) the mixture thus obtained is melted to produce solid sodium silicate and sulfurous anhydride; c) the solid sodium silicate is dissolved in water to provide a sodium silicate aqueous solution, d) the sulfurous anhydride is reacted with the sodium silicate aqueous solution to provide a mixture containing precipitated silica; and e) the precipitated silica is separated from said mixture.
    Type: Application
    Filed: July 3, 2009
    Publication date: April 19, 2012
    Applicant: Rhodia Operations
    Inventors: Anne-Laure Pinault, Joël Racinoux, Petro Pechkurov
  • Patent number: 8153107
    Abstract: The instant invention relates to a process for the preparation of an aqueous suspension of anionic colloidal silica having a neutral pH which is stable over time and comprises individualized particles of colloidal silica which are not bound to one another by siloxane bonds. The instant suspensions show high storage stability and are particularly useful for the clarification of beer, for the preparation of cosmetic formulations, for the production of ink for printers, for paints and for anticorrosive treatments.
    Type: Grant
    Filed: January 26, 2011
    Date of Patent: April 10, 2012
    Assignee: AZ Electronic Materials USA Corp.
    Inventors: Eric Jacquinot, Marie-Laure Perard, Uwe Falk, Torsten Henning
  • Patent number: 8142753
    Abstract: A large scale process for preparing fumed silica with consistent product parameters wherein a silica precursor compound is fed to a burner at ?100 Kg/h along with a combusting gas at ?300 m3/h and a combustible gas at ?100 m3/h, with a nozzle gas velocity between 10 and 200 m/s, and a radially symmetrical, homogenous gas velocity and gas temperature.
    Type: Grant
    Filed: November 8, 2007
    Date of Patent: March 27, 2012
    Assignee: Wacker Chemie AG
    Inventors: Herbert Barthel, Helmut Maginot
  • Patent number: 8118898
    Abstract: The present invention provides a sol of spinous silica-based particles in which silica-based particles having peculiar forms, spinous forms are dispersed in a solvent. The spinous silica-based particles have verrucous projections formed on surfaces of spherical silica-based particles. In the spinous particles, a value of the surface roughness (SA1/SA2, SA1 indicating a specific surface area measured by the BET method or the Sears method and SA2 indicating a specific surface area converted from an average particle diameter (D2) measured by the image analysis method) is in the range from 1.7 to 10. Furthermore the average diameter (D2) measured by the image analysis method is in the range from 7 to 150 nm.
    Type: Grant
    Filed: October 11, 2007
    Date of Patent: February 21, 2012
    Assignee: JGC Catalysts and Chemicals Ltd.
    Inventors: Yoshinori Wakamiya, Hiroyasu Nishida, Yuji Tawarazako, Kazuaki Inoue, Osamu Yoshida, Akira Nakashima
  • Publication number: 20120039782
    Abstract: A method for producing a densified fumed metal oxide having an increased bulk density and substantially the same surface area as an undensified fumed metal oxide with the same molecular composition is provided. The fumed metal oxide is wetted with a solvent to form a wetted fumed metal oxide. The wetted fumed metal oxide is dried to form a dried fumed metal oxide. The dried fumed metal oxide is calcined.
    Type: Application
    Filed: August 10, 2010
    Publication date: February 16, 2012
    Applicant: UOP LLC
    Inventor: Christopher P. Nicholas
  • Publication number: 20120041128
    Abstract: The present invention relates to a precipitated silica for elastomers and, more particularly, to a new highly dispersible and highly reinforcing precipitated silica for elastomers. The invention further provides the process for its production and rubber products made therefrom.
    Type: Application
    Filed: October 11, 2009
    Publication date: February 16, 2012
    Applicant: Dimona Silica Industries
    Inventor: Raisa Avgustovna Kosso
  • Patent number: 8114804
    Abstract: A process for making a self-deagglomerating suspension, in particular, a suspension which self-deagglomerates to form a substantially transparent suspension, of finely divided titanium (IV) oxide particles, comprising: vigorously mixing (a) a volume of a first component comprising a major proportion of an alcohol, a minor proportion of a titanium alkoxide and a minor proportion of a titanium alkoxide activator selected from the group consisting of water and a first aqueous base, and (b) a volume of a second component selected from the group consisting of water and a second aqueous base, at least one of the first component or the second component having a base therein, the second component being substantially free of alcohol, to form a mixture comprising a suspension of finely divided titanium (IV) oxide particles, the mixture having a water to titanium molar ratio ranging from about 40 to about 1 to about 5000 to about 1, wherein the proportion of the titanium alkoxide, the proportion of the activator, th
    Type: Grant
    Filed: December 20, 2007
    Date of Patent: February 14, 2012
    Assignee: E. I. du Pont de Nemours and Company
    Inventors: David M. Scott, Carmine Torardi, Vladimir Grushin
  • Patent number: 8114371
    Abstract: Process for the production of precipitated silica from olivine including the following steps: providing olivine particles with a particle size preferably below 1 mm in diameter, preferably mixing olivine and water to form an olivine/water slurry, mixing the olivine/water slurry with hydrochloric acid (HCl), preferably at a Concentration at 18 wt % or above, and at a temperature preferably between 50 -130° C., and reacting for a period of time, preferably between 20-360 minutes, removal of coarse mineral impurities (sand product), separation of precipitated silica from mother solution, mechanical treatment of the separated precipitated silica and optionally some water to obtain a slurry, preparation of a low viscosity slurry by adding sodium aluminate or another suitable aluminate, preferably to 100-6000 p.p.m., and adjusting the pH, preferably to values between 4-9 ageing at a temperature between 50-150° C.
    Type: Grant
    Filed: January 13, 2005
    Date of Patent: February 14, 2012
    Assignee: COD Technologies, a.s.
    Inventors: Gudmundur Gunnarsson, Oddmund Wallevik, Lars Øyvind Ekornrød, Birger Langseth, Per Bjøm Engseth
  • Patent number: 8110166
    Abstract: A process for producing from olivine precipitated silica with controlled specific surface area and high degree of purity. The process comprises adding olivine in a controlled manner to a heated mineral acid solution; after separating undissolved olivine and filtering the silica is slurried in aqueous solution to obtain a low viscosity high solid content silica slurry that can be efficiently degritted and dried with a relatively low energy consumption. The obtained silica can be in powder, bead or granule form and preferably has a specific surface area of at least about 100 m2/g.
    Type: Grant
    Filed: November 27, 2003
    Date of Patent: February 7, 2012
    Assignee: SilMag DA
    Inventor: Gudmundur Gunnarsson
  • Publication number: 20120014858
    Abstract: A method of preparing hydrophobic silica particles includes the step of reacting together in a single step a mixture of silane ether monomers and organically modified silane ether monomers with a hydrolyzing agent. The method also includes producing hydrophobic silica microparticles and nanoparticles that can include dyes and/or magnetizable components. The silica nanoparticles can be used in the detection, visualization and/or analysis of latent fingerprints.
    Type: Application
    Filed: September 26, 2011
    Publication date: January 19, 2012
    Inventor: Frederick John Rowell
  • Patent number: 8097229
    Abstract: Inorganic oxide substrates are functionalized with silicon-free organic functionalizing agents. The organic functionalizing agent has a bonding functional group for bonding to the substrate and a functionalizing moiety that is not bonded to the substrate for imparting a desired functionality to the substrate. The functionalized inorganic oxide substrates are manufactured by selecting a functionalizing agent and reaction conditions that allows the bonding functional group to bond to the inorganic material while leaving the functionalizing moiety available for providing the desired functionality. The functionalized inorganic oxides can be used as filler materials in polymers or to manufacture a supported nanoparticle catalyst.
    Type: Grant
    Filed: January 17, 2006
    Date of Patent: January 17, 2012
    Assignee: Headwaters Technology Innovation, LLC
    Inventors: Bing Zhou, Changkun Liu, Clementine Reyes
  • Publication number: 20110315660
    Abstract: Disclosed are a method for recycling silica waste and a method for preparing nanoporous material and other valuable silica materials. More specifically, a method for preparing a nanoporous material by recycling silica-containing waste produced from a silica etching process in the synthesis of nanoporous carbon is provided. The present disclosure allows recycling of silica waste in an effective and environment-friendly manner, reduction of consumption of chemical materials, and reduction of chemical waste. Accordingly, the present disclosure enables effective preparation of various valuable nanoporous silica and other silica materials from silica waste released for production of various nanoporous materials.
    Type: Application
    Filed: April 29, 2011
    Publication date: December 29, 2011
    Inventor: Jong-Sung Yu
  • Publication number: 20110315912
    Abstract: A thermal insulation material comprising a precipitated silica having a modified tapped density of less than or equal to 70 g/l.
    Type: Application
    Filed: January 21, 2010
    Publication date: December 29, 2011
    Applicant: EVONIK DEGUSSA GmbH
    Inventors: Frank Menzel, Karl Meier, Christian Panz
  • Publication number: 20110319647
    Abstract: The invention provides a method of producing silica particles, the method including preparing an alkali catalyst solution containing an alkali catalyst in a solvent including an alcohol, at a concentration of from about 0.6 mol/L to about 0.85 mol/L; and supplying tetraalkoxysilane into the alkali catalyst solution, and concurrently supplying an alkali catalyst into the alkali catalyst solution at a rate of from about 0.1 mol to about 0.4 mol per mole of the total amount of supply of the tetraalkoxysilane supplied in one minute.
    Type: Application
    Filed: October 18, 2010
    Publication date: December 29, 2011
    Applicant: FUJI XEROX CO., LTD.
    Inventors: Hideaki YOSHIKAWA, Yuka ZENITANI, Hiroyoshi OKUNO, Shunsuke NOZAKI, Shinichiro KAWASHIMA, Sakae TAKEUCHI
  • Publication number: 20110318581
    Abstract: The invention provides silica particles including primary particles, the primary particles having a volume average particle diameter of from about 80 nm to about 300 nm, a particle size distribution index of from about 1.10 to about 1.40, an average circularity of from about 0.70 to about 0.92, and a circularity distribution index of from about 1.05 to about 1.50, the silica particles including primary particles having a circularity of about 0.95 or greater at a proportion of about 10% or less by number of particles.
    Type: Application
    Filed: October 26, 2010
    Publication date: December 29, 2011
    Applicant: FUJI XEROX CO., LTD.
    Inventors: Yuka ZENITANI, Hideaki YOSHIKAWA, Hiroyoshi OKUNO, Shunsuke NOZAKI, Shinichiro KAWASHIMA, Sakae TAKEUCHI
  • Patent number: 8084392
    Abstract: A method of producing a range of diatomaceous earth filter aids having selectable permeabilities and less than about 1 percent by weight total crystalline silica. The method includes milling diatomaceous earth ore to a size range of between about 100 micrometers and about 1400 micrometers; calcining the milled diatomaceous earth in a calciner; and milling the calcined diatomaceous earth in an adjustable milling and classification system to produce diatomaceous earth filter aids. Systems to implement such methods and compositions produced by such methods are also described.
    Type: Grant
    Filed: July 3, 2008
    Date of Patent: December 27, 2011
    Assignee: EP Minerals, LLC
    Inventors: Peter E. Lenz, Michael J Nannini, James S Shui
  • Publication number: 20110312055
    Abstract: The invention provides a process for producing alcohol from a cellulosic material, said process comprising: hydrolyzing said cellulosic material with an aqueous acid to produce a hydrolysate; extracting acid and water from said hydrolysate with a water-miscible organic extraction solvent to yield (a) a first aqueous acidic solution containing said extraction solvent and (b) a residue containing sugars; subjecting said residue to an oligosaccharide cleavage reaction to yield an aqueous solution of fermentable sugars; fermenting said fermentable sugars and distilling alcohol from the resulting fermented mixture; contacting said first aqueous acidic solution with a pressurized fluid lipophilic solvent in non-gaseous form, which fluid solvent is substantially water-immiscible and is gaseous at ambient conditions, to yield a second aqueous acid solution and a solvent mixture of said extraction solvent and said fluid solvent; depressurizing said solvent mixture to release said extraction solvent for recycling; and,
    Type: Application
    Filed: October 1, 2009
    Publication date: December 22, 2011
    Applicant: Weyland AS
    Inventor: Karl Ragnar Weydahl
  • Publication number: 20110302849
    Abstract: The present invention relates to suspensions which have a very low salt content and contain at least one precipitated silica, a process for producing them and also their use.
    Type: Application
    Filed: March 11, 2010
    Publication date: December 15, 2011
    Applicant: EVONIK DEGUSSA GmbH
    Inventors: Patrik Stenner, Florian Zschunke, Juergen Behnisch, Markus Ruf, Manfred Dannehl, Silke Suhr
  • Patent number: 8075862
    Abstract: The present invention relates to a hydrophobic, fumed silica which is obtained by milling a fumed silica which has fixed dimethylsilyl and/or monomethylsilyl groups on the surface due to silanization; and to a process for the preparation of the silica according to the invention, and to silicone rubber materials containing the silica according to the invention.
    Type: Grant
    Filed: May 6, 2008
    Date of Patent: December 13, 2011
    Assignee: Evonik Degussa GmbH
    Inventors: Juergen Meyer, Horst Zeizinger, Mario Scholz, Uwe Ellenbrand
  • Patent number: 8076425
    Abstract: Disclosed is a carbamate functional silica, comprising repeating units: wherein R is H or an alkyl group of from 1 to 50 carbon atoms and n is a number from 1 to 100. Also disclosed is a functional silica comprising repeating units: wherein R is an alkyl group of from 1 to 50 carbon atoms, n is from 1 to 100, R1 and R2 may be the same or different and are at least one of a hydrocarbon group comprising from 1 to 100 carbon atoms with the proviso that at least one of R1 and R2 is not hydrogen. In one embodiment, R1 and R2 are hydrogen or the residual of an aminoplast polymer, an alkylating alcohol, or the like. Methods for making the disclosed functional silicas and coating compositions comprising the same are also provided.
    Type: Grant
    Filed: September 29, 2005
    Date of Patent: December 13, 2011
    Assignee: BASF Coatings GmbH
    Inventors: Gregory G. Menovcik, Walter H. Ohrbom
  • Publication number: 20110300047
    Abstract: A method for recycling silicon, comprises a filtrating step, providing a siliceous mortar containing silicon carbide, silicon and a buffer, and further filtering out the buffer form the siliceous mortar to obtain a siliceous slurry; a removing step, heating the siliceous slurry till the buffer has evaporated to obtain a mixture of silicon and silicon carbide; a stirring step, placing the mixture of silicon and silicon carbide in a liquid-substrate followed by stirring and incubating for a while to obtain a sedimentation of the mixture of silicon and silicon carbide and a suspension containing the liquid-substrate and silicon; and a purifying step, filter off the liquid-substrate in the suspension, and silicon powders are obtained.
    Type: Application
    Filed: July 9, 2010
    Publication date: December 8, 2011
    Inventors: Yu-Lung Sun, Yung-Hao Liu
  • Publication number: 20110300222
    Abstract: The disclosure relates to imaging agents and drug delivery systems.
    Type: Application
    Filed: February 20, 2010
    Publication date: December 8, 2011
    Applicant: THE REGENTS OF THE UNIVERSITY OF CALIFORNIA
    Inventors: Michael J. Sailor, Luo Gu, Ji-Ho Park
  • Patent number: 8066806
    Abstract: A sintered silicon oxide for film vapor deposition having a density of 1.0 to 2.0 g/cm3, three-point flexural strength of at least 50 g/mm2, and a BET specific surface area of 0.1 to 20 m2/g is provided. When this sintered silicon oxide is used for evaporation source of a film, pin holes and other defects of the film caused by the problematic splash phenomenon can be reliably prevented and stable production of a reliable package material having excellent gas barrier property is been enabled. This invention also provides a method for producing such sintered silicon oxide, and this method can be used in a large scale production without requiring any special technology, and therefore, this method is capable of supplying the market with the sintered silicon oxide at reduced cost.
    Type: Grant
    Filed: March 4, 2011
    Date of Patent: November 29, 2011
    Assignee: Shin-Etsu Chemical Co., Ltd.
    Inventors: Hirofumi Fukuoka, Meguru Kashida, Toshio Ohba
  • Publication number: 20110287215
    Abstract: A process of producing a structure for molecular separations includes providing a plurality of template materials. The template materials are selected from biomolecules, biopolymers, polymers, or combinations thereof. A sieve material, suitable for producing a structure for molecular separations, is provided around the template materials. The template materials are positioned in an arrangement for leaving pores suitable for molecular separations. The template materials are removed to leave pores in the sieve material and produce the structure suitable for molecular separations.
    Type: Application
    Filed: April 30, 2011
    Publication date: November 24, 2011
    Applicant: CERAHELIX
    Inventors: Karl D. Bishop, Tyler J. Kirkmann, Susan G. MacKay
  • Publication number: 20110284801
    Abstract: The invention relates to a process of preparing functional layers, like protection, encapsulation and alignment layers, on an electronic device by a low energy particle beam deposition process, to functional layers obtainable by said process, and to electronic devices comprising such functional layers.
    Type: Application
    Filed: November 18, 2009
    Publication date: November 24, 2011
    Applicant: Merck Patent Gesellschaft Mit Beschrankter Haftung
    Inventors: Michael Coelle, Owain Llyr Parri, David Sparrowe, Oleg Yaroshchuk, Eugene Telesh
  • Patent number: 8057771
    Abstract: In the process disclosed herein, siliceous plant matter is steeped in water, soaked in an aqueous solution containing a solute which solubilizes inorganic oxides, soaked in an aqueous solution containing an oxidizing solute, rinsed, dried and thermally pyrolyzed to produce amorphous silica with of low carbon content, low water content, low inorganic impurity content and is of high porosity. Practice of the invention yields usable energy, does not produce carbonization of the atmosphere and is of lower nitrogen oxide and sulphur emission than currently used processes. By varying steps of the process herein disclosed, the carbon content, inorganic impurities and porosity of the resulting amorphous silica may be selectively controlled.
    Type: Grant
    Filed: May 10, 2007
    Date of Patent: November 15, 2011
    Inventor: Larry W. Shipley
  • Patent number: 8057772
    Abstract: Disclosed are mesoporous silica particles and a preparation method thereof, particularly, a method of preparing mesoporous silica particles, including mixing a silica precursor, an alkylamine-based surfactant, and a phosphoric acid-based cosurfactant, thus preparing a mixture solution (a mother liquor); adding or not adding the mixture solution with an acid solution, and conducting stirring, thus providing mesoporous silica particles; and thermally treating the mesoporous silica particles. These mesoporous silica particles are prepared using a phosphoric acid-based cosurfactant for stabilizing the surface of the particles to prevent the aggregation thereof, thereby uniformly distributing the particles.
    Type: Grant
    Filed: October 23, 2007
    Date of Patent: November 15, 2011
    Assignee: Korea Atomic Energy Research Institute
    Inventors: Jong-Yun Kim, Suk Bon Yoon, Yong-Joon Park, Myung Ho Lee, Kwang-Yong Jee
  • Publication number: 20110274594
    Abstract: An object is to provide a material capable of removing A? from a body fluid efficiently and use of the material, which are developed for the purpose of establishing a therapeutic or preventive method for Alzheimer's disease. Provided is an amyloid ? protein remover, containing a carrier made of any one material selected from the group consisting of cellulose, silica, polyvinyl alcohol, and activated carbon, wherein the carrier does not have an alkyl chain on the surface thereof or has an alkyl chain having 1 to 18 carbon atoms on the surface thereof.
    Type: Application
    Filed: June 22, 2011
    Publication date: November 10, 2011
    Applicants: KANEKA CORPORATION, FUJITA HEALTH UNIVERSITY
    Inventors: Nobuya Kitaguchi, Kazunori Kawaguchi
  • Patent number: 8053495
    Abstract: The present invention provides ceramic powder capable of being incorporated into rubber or a resin for the preparation of a composition, which shows excellent heat resistance and flame retardancy and which is used, for instance, as a semiconductor-sealing material. The ceramic powder has a multi-peak frequency distribution pattern having at least two peaks as a particle size distribution as determined using a laser diffraction-scattering type particle size-analyzer, wherein the maximum particle size for the first peak ranges from 40 to 80 ?m and that for the second peak ranges from 3 to 8 ?m and wherein the rate of the particles having a particle size of not less than 20 ?m and less than 40 ?m is not more than 20% by mass (inclusive of 0% by mass).
    Type: Grant
    Filed: May 11, 2007
    Date of Patent: November 8, 2011
    Assignee: Denki Kagaku Kogyo Kabushiki Kaisha
    Inventors: Yasuhisa Nishi, Mitsuyoshi Iwasa
  • Patent number: 8052788
    Abstract: Colloidal silica having a controllable broad particle size distribution and a controllable minimum particle size is disclosed and claimed. Particles below a predetermined size are excluded from the product colloidal silica of the invention. A method for continuously producing the desired colloidal composition is disclosed comprising the steps of providing preformed silica particles having a surface area which controls the particle size of the colloidal silica product, adding a feed silica comprising an alkaline solution and silicate at a feed rate which is less than a nucleation rate.
    Type: Grant
    Filed: September 24, 2008
    Date of Patent: November 8, 2011
    Assignee: Nalco Company
    Inventor: Dennis L. MacDonald
  • Publication number: 20110268956
    Abstract: The invention relates to a process for obtaining ceramic coatings and ceramic coatings obtained. This process allows obtaining coatings of ceramic oxides, such as ZrO2, Al2O3, TiO2, Cr2O3, Y2O3, SiO2, CaO, MgO, CeO2, Sc2O3, MnO, and/or complex mixtures thereof, by means of a high frequency pulse detonation technique in which the relative movement between the combustion stream and the substrate or piece to be coated takes place at a speed that produces an overlap between the successive coating areas exceeding 60% of the surface of a coating area. The allows producing ceramic coatings with a thickness greater than 30 microns in a single pass.
    Type: Application
    Filed: May 12, 2006
    Publication date: November 3, 2011
    Applicant: FUNDACION INASMET
    Inventors: Inaki Fagoaga Altuna, Maria Parco Camacaro, Georgiy Barikyn, Carlos Vaquero Gonzalez
  • Publication number: 20110265662
    Abstract: A method for replenishing carbon dioxide gas in a carbonated beverage container where a carbon dioxide regulator releases carbon dioxide at a rate approximately equal to the rate of carbon dioxide loss from said container. Also disclosed is packaging system for maintaining a consistent pressure of a carbonated beverage comprising a closure, a plastic container, and a carbon dioxide regulator. Also disclosed is a method for making a packaging system for maintaining a consistent pressure in a carbonated beverage comprising overmolding a perform around an assembly for a carbon dioxide regulator, or blending a carbon dioxide regulator into the plastic material used to form the body of a container for said carbonated beverage. Also, disclosed is carbon dioxide regulator composition for replenishing carbon dioxide gas in a carbonated beverage container comprising polymeric carbonates, organic carbonates, or materials that absorb and subsequently release carbon dioxide.
    Type: Application
    Filed: November 22, 2010
    Publication date: November 3, 2011
    Applicant: BP Corporation North America Inc.
    Inventors: John M. Forgac, Francis M. Schloss, Matthew A. Kulzick
  • Publication number: 20110268970
    Abstract: The present invention provides a process for making mesoporous nanoparticles. The process comprises providing an acidic mixture comprising a fluorocarbon surfactant, a second surfactant and a silica precursor. The silica precursor is then reacted to form the mesoporous nanoparticles.
    Type: Application
    Filed: July 7, 2011
    Publication date: November 3, 2011
    Applicant: AGENCY FOR SCIENCE, TECHNOLOGY AND RESEARCH
    Inventors: Jackie Y. YING, Yu HAN
  • Patent number: 8048394
    Abstract: The present invention relates to (1) hollow silica particles including an outer shell portion having a mesoporous structure with an average pore size of from 1 to 10 nm, wherein the silica particles have an average particle diameter of from 0.05 to 10 ?m, and 80% or more of the whole silica particles have a particle diameter falling within the range of ±30% of the average particle diameter; (2) composite silica particles including silica particles which include an outer shell portion having a mesoporous structure with an average pore size of from 1 to 10 nm, and have a BET specific surface area of 100 m2/g or more, and a hydrophobic organic compound or a polymeric organic compound incorporated inside of the silica particles; and a process for producing the hollow silica particles.
    Type: Grant
    Filed: October 15, 2007
    Date of Patent: November 1, 2011
    Assignee: Kao Corporation
    Inventors: Toshihiro Yano, Takuya Sawada
  • Patent number: 8048195
    Abstract: The present invention relates to the use of liquid-crystal displays (LCDs), and to processes for the recycling thereof. The processes according to the invention are characterised in that the LCDs are employed at least partly as replacement for other raw materials. In general, the LCDs are thermally treated here at a temperature in the range from 900 to 1700° C.
    Type: Grant
    Filed: February 25, 2005
    Date of Patent: November 1, 2011
    Assignee: Merck Patent GmbH
    Inventor: Roland Martin