Abstract: A vessel (1) contains a rotor disc (23) mounted for rotation around a vertical axis (17) and arranged to bound a processing space (31) disposed above it. The agglomeration and/or the coating of particles are accomplished by moving the particles by the rotation of the rotor disc (23) and by means of a gas, in particular air, passed upwardly through the processing space (31) and by spraying them with a liquid. The torque required for the rotation of the rotor disc (23) is continuously measured by means of a torque measuring member (75) disposed between the rotor disc (23) and the drive device (77) arranged to drive the same. The agglomeration and/or the coating operation is controlled on the basis of the time-dependent variation of the torque and/or of the first derivative of the same, and/or of a variable having relation to the torque and/or its derivative.

Abstract: A tangled fibrous material from cut glass fibre bundles, with the cut glass fiber bundler being fed into a compressed air flow and a glass fibre-laden air being deflected into a turbulent eddy flow of varying direction, so that a tangled fibrous material of wadding-like consistency is formed. Through the simultaneous addition of dry polymer-based binder powder, it is possible to obtain a tangled fibrous material as a starting product for a production of glass fibre-reinforced plastic moundings, which can be compressed to a felt. This can be packed as an intermediate or further processed in a heated belt press to glass fibre-reinforced plastic plates.

Abstract: Silicon of high purity is made by decomposing silane in a fluidized bed reactor. To obtain good process economics, two modes of operation are used. In a first mode, the reactor is operated under high productivity conditions which also result in co-production of silicon dust or fines. The dust on the particles can cause problems in handling. For example, in bagging the particles, or removing the particles from a bag, the dust can become airborne from the larger particle surfaces and form an objectionable cloud of silicon dust. The invention provides a method for uniting dust to the larger silicon particles. In a second process mode, a thin (0.1-5.0 micron) layer of high purity silicon is deposited on the dust laden particles. This second mode is most preferably carried out by (a) treating the dust-laden particles with a deposition gas comprising 1 to 5 mole % silicon admixed with an inert carrier gas such as hydrogen, (b) in a fluidized bed reactor, and (c) at a process temperature of 620.degree.-650.degree.

Abstract: The present invention includes:(i) a method for making a coated particulate comprising the steps ofheating until liquid a polyolefin wax;fluidizing with a hot gas, additive particles selected from the group comprising an antioxidant, a processing stabilizer, an acid acceptor, and mixtures thereof;spraying the liquid polyolefin wax on the heated fluidized additive particles; andmaintaining the fluidized additive particles at a temperature which is sufficient to prevent the formation of fibers and adequate to form discrete substantially coated additive particles;(ii) a coated particulate made by the above process; and(iii) a process for providing in-reactor stabilization of a polyolefin during a polymerization reaction, using the coated additives prepared by the above described method.

Abstract: Hydrogen-containing effluent gas can be treated with activated carbon to remove boron or phosphorus impurity prior to recycle to a fluidized bed reactor. The process is conducted at cryogenic temperatures.

Abstract: Undesirable conversion of a silicon source, such as silane, in the freeboard above a fluidized bed of silicon particles in a fluidized bed reactor, can be reduced by cooling the gas within the freeboard. Preferably, the reduction in temperature is achieved by introducing into the freeboard, a stream of relatively cool quench gas such as hydrogen, which also reduces the concentration of silane in the freeboard. As a result of these two factors, the invention improves the service factor of the fluidized bed apparatus, and reduces the amount of silane conversion to undesired by-products.

Abstract: A method of producing a calcium carbonate, magnesium carbonate or calcium-magnesium carbonate which is surface modified with an organic material wherein the carbonate in substantially dry, particulate form is contacted with an organic monomer, copolymers or a prepolymer, and surface polymerization or reaction in situ on the carbonate in the presence of a gaseous hydrogen atmosphere is effected. In the case where the carbonate has been wet processed and residues of a dispersing agent employed remain as a coating on the carbonate particles after drying, a minor amount of a calcined kaolin or TiO.sub.2 is used as a polymerization catalyst. When the carbonate has been dry ground so that the particles are free from processing chemicals, no catalyst is needed to initiate the polymerization.

Abstract: Silicon nitride powder is prepared in a gas-phase reaction by reacting silicon tetrachloride with ammonia at above 500.degree. C. in a fluidized bed of silicon nitride particles. An amorphous silicon nitride having a BET specific surface area of greater than 50 m.sup.2 /g is used at the beginning of the reaction. The resulting silicon nitride is then separated from the ammonium chloride simultaneously formed.

Abstract: An apparatus and process for making pellets from a fluidizable material having a fluid bed chamber with a perforated base and an open upper end in which a rotatable means for shaping the pellets is located. Gas for the formation of a fluidized current is introduced through the perforated base. A fluid spray for the agglomeration and coating of the fluidizable material is introduced into the fluid bed chamber, preferably near the perforated base in the central area of the fluid bed chamber. Additionally, a device for channeling agglomerated material is preferably located at a distance above the perforated base and concentrically with the longitudinal axis of the sprayer. A fluidized current carries particles, while still plastic, upwardly through the channeling device causing them to impinge on the underside of the rotatable means.

Abstract: An apparatus and method for applying hard surface coatings to articles of manufacture such as particles, filaments, sphereoids, rollers, bearings, tools, and assemblies. In one form, coating of hard surface film, such as synthetic diamond, is effected while the objects fall freely through space in a coating chamber. In another form, coating is effected while particles are fluidized by gas containing molecules which are formed of matter to be deposited by gas or chemical vapor deposition employing high energy radiation, such as microwave energy and/or other form of radiation. In other forms, an ion beam or beams containing hot carbon ions is directed through a fluidized bed of particles to be coated or through a chamber in which small objects are made to continuously fall freely through space to coat same with carbon in the form of synthetic diamond.

Abstract: Particles of silicon and a p or n carrier substance which are in spherical or spheroidal form, and suitable for use in the preparation of doped semiconductor devices, can be prepared by a fluidized bed technique for chemical vapor deposition of a carrier substance (B, P, As or Sb). The prepared products have a kernel of high purity polysilicon and a layer of silicon/dopant alloy upon the kernel. Optionally, the particles have a thin outer layer of silicon.

Abstract: A fluidized granulating and coating apparatus having a cylindrical treating vessel provided with at least one spray nozzle, at least one air supply duct and one exhaust duct, and a downwardly converging frusto-conical portion. The spray nozzle is disposed at a position below the interface of the fluidized particles within the region of the frusto-conical portion. At least one compressed air nozzle is disposed at a level below the interface of the fluidized particles and within the range of the frusto-conical portion. Disclosed also is a fluidized granulating and coating method which makes use of this apparatus. With the apparatus and the method of the invention, it is possible to produce granular products such as a slow-effecting or long-lasting pharmaceutical product with a high quality and homogeneity at a high yield, by coating cores of spherical granules with a coating composition containing the medical component of the desired property.

Abstract: A method of forming a surface layer of carbide, nitride, carbonitride, or solid-solution on the surface of a material to be treated, which comprises disposing in a fluidized bed furnace a treating agent comprising a powder of a refractory material, and a powder of a metal for forming a carbide, nitride, carbonitride or solid-solution or a powder of an alloy thereof, introducing a fluidizing gas into the fluidized bed furnace to fluidize the treating agent and form a fluidized layer, disposing the material to be treated in the fluidized layer, and introducing a predetermined amount of halide into the fluidized layer, and an apparatus for forming the surface layer on the material to be treated, comprising a furnace body for forming the surface layer in the fluidized layer of the treating agent, a heating furnace for heating the fluidized layer, a halide supply pipe in communication with the outside of the furnace body, and a halide gas jetting pipe disposed within the furnace body, which is connected to the hal

Abstract: A particulate, free-flowing and rapid dissolving polymer composition is prepared by comminuting a high molecular weight thermoplastic or viscoelastic polymer at a temperature below its glass transition temperature while maintaining the polymer in an inert environment. A finely divided, solid coating agent is mingled with the comminuted polymer while maintaining the polymer particles in a cold and inert atmosphere. The particles of coating agent form a protective shell around each polymer particle by tumble mixing the components while raising the temperature of the mixture. The polymer composition finds use as a drag reducing agent; as an anti-misting agent; to enhance the efficiency of oil skimming processes and devices; and for the preparation of polymer solutions for other uses.

Abstract: A fluidized-bed granulating apparatus which granulates powdered or granular raw materials by centrifugally tumbling and fluidizing them on a rotor rotating in a container and by supplying a gas from a lower portion of the container. The container and the rotor are supported by a horizontally movable wagon, are vertically and movably supported by a lift-up device, and can be attached to and separated from the lower portion of a body of the fluidized-bed granulating apparatus. The rotor is rotated by a motor provided outside the granulating apparatus, and the driving force of the motor is transmitted from the output shaft thereof to the rotor through a universal joint, a transmission shaft, and a reduction gear. When the container and the rotor are attached to and separated from the lower portion of the body of the graulating apparatus, the universal joint is similarly attached to and separated from the transmission shaft.

Abstract: A process whereby particulate materials with a polymeric coating of controlled thickness are obtained by passing gas at a pre-determined temperature and flow rate substantially symmetrically through a bed of particles to create a coherent symmetrical spouting zone of fully-spouted, suspended particles is disclosed. The suspended particles are contacted with an atomized spray of polymer solution. The spray has a controlled flow rate and is confined to the spouting zone. As the process proceeds, the solvent evaporates from the fine droplets of the polymer solvent solution on contact or very quickly after contact of the polymer solvent solution with the particles. Structurally sensitive particulate material such as biomass is therefore only fleetingly contacted with solvent, on its outer shell only, and no substantial damage to the material can be effected by the solvent. Also, the coating solidifies quickly so that the little or no particle agglomeration or attrition occurs.

Abstract: A particulate, free-flowing and rapid dissolving polymer composition is prepared by comminuting a high molecular weight thermoplastic or viscoelastic polymer at a temperature below its glass transition temperature while maintaining the polymer in an inert environment. A finely divided, solid coating agent is mingled with the comminuted polymer while maintaining the polymer particles in a cold and inert atmosphere. The particles of coating agent form a protective shell around each polymer particle by tumble mixing the components while raising the temperature of the mixture. The polymer composition finds use as a drag reducing agent; as an anti-misting agent; to enhance the efficiency of oil skimming processes and devices; and for the preparation of polymer solutions for other uses.

Abstract: Silicon of high purity is made by decomposing silane in a fluidized bed reactor. To obtain good process economics, two modes of operation are used. In a first mode, the reactor is operated under high productivity conditions which also result in co-production of silicon dust or fines. The dust on the particles can cause problems in handling. For example, in bagging the particles, or removing the particles from a bag, the dust can become airborne from the larger particle surfaces and form an objectionable cloud of silicon dust. The invention provides a method for uniting dust to the larger silicon particles. In a second process mode, a thin (0.1-5.0 micron) layer of high purity silicon is deposited on the dust laden particles. This second mode is most preferably carried out by (a) treating the dust-laden particles with a deposition gas comprising 1 to 5 mole % silicon admixed with an inert carrier gas such as hydrogen, (b) in a fluidized bed reactor, and (c) at a process temperature of 620.degree.650.degree. C.

Abstract: Foam control agents for inclusion in detergent compositions in powder form, are particulate and comprise a silicone antifoam compound and an organic material which is a fatty acid or a fatty alcohol, having 12 to 20 carbon atoms, or a mixture thereof and which has a melting point in the range 45.degree. to 80.degree. C. and is insoluble in water. The foam control agents are made by a process in which the antifoam and the organic material are contacted in their liquid phase. These foam control agents give a good storage stability in the detergent powders.

Abstract: An apparatus for maintaining the purity of solid/granular product and dispensing high purity granular product from a vessel. A noncontaminating surface is provided by a cup, cylinder, or other structure having a surface of silicon, silicon carbide, silicon nitride, sialon, or similar materials and preferably operates as an angle of repose valve in a pressurized system to prevent contamination by undue contact of the high purity product with conventional gastight valves such as ball valves, butterfly valves, pinch valves, etc.

Abstract: The invention concerns a method for the continuous production of a solid granulate by drying and simultaneous granulation in a flow bed. In this connection, the solid to be granulated, in the form of a solution or suspension, is sprayed into or onto the bed of material consisting of pregranulated solid and fluidized by an injected drying gas of suitable temperature, a corresponding quantity of granulate is discharged from the bed of material and separately therefrom the drying gas is drawn off together with the water vapor produced. In order to obtain a mode of operation independent of the flow velocity of the drying gas, the granules of the fluidized bed of material are continuously subjected to a centrifugal force classification, the mixture of drying gas and water vapor serving as carrier gas for classification.

Abstract: A continuous granulator includes a granulator body for continuously processing powdered materials into granules, and a screw conveyor for discharging the produced granules from the granulator body, the screw conveyor including a pneumatic classifier for separating or classifying the produced granules while they are being conveyed. The pneumatic classifier includes a porous lower portion of the screw conveyor which permits passage of streams of pressurized air therethough into the interior of the screw conveyor. With this construction, discharging conveyance of the produced granules and classification of the produced granules can be carried out concurrently at the same station and hence the granules of a uniform grain size can be produced at an increased rate.

Abstract: There is disclosed a process for coating particles, such as ceramic, metallic and organic cores, with fine powder, such as ceramic, metal, organic or carbon powder. The process comprises providing a mixture comprising the particles and a binder which is capable of slowly melting to viscous state. Then the mixture is tumbled while slowly heating it to enable the binder to reach the viscous state while allowing the particles to be substantially covered with the binder. The next step includes cooling the mixture to about room temperature and thereafter breaking up the particles that may have agglomerated during the tumbling and heating to give individual particles covered with the binder. As a final step, the fine powder is added to the individual binder covered particles and the mixture is tumbled and heated again to the viscous state under conditions effective to provide a coating of the fine powder on the particles.

Abstract: A battery element useful as at least a portion of the positive plates of a lead-acid battery comprises an acid resistant substrate coated with electrically conductive doped tin oxide. This battery element may also be used in the bipolar plates of a lead-acid battery.

Abstract: An apparatus for preparing high-purity polycrystalline silicon is constructed with a heating applicator, a vertical fluidized bed quartz reactor within the applicator, a microwave generator, microwave guide tubes for conveying microwaves from the microwave generator to the applicator, a reacting gas inlet and outlet, a gas distribution device for distributing reacting gas within the reactor, a silicon seed inlet for introducing silicon seed into the reactor, and an outlet for withdrawing polycrystalline silicon from the reactor. The microwaves provide the heat for the fluidized bed reaction.

Abstract: A method and apparatus for forming a layer of a carbide or nitride of, for example, titanium or vanadium on the surface of material to be treated in a fluidized bed furnace. A refractory powder for forming a fluidized bed, a vessel or vessels filed with powder of a treating agent, and the material to be treated are placed in the furnace. The treating agent includes powder of at least one carbide or nitride forming metal or alloy and powder of at least one compound selected from the group consisting of chlorides, fluorides, bromides, iodides and boro-fluorides of alkali and alkaline earth metals and/or at least one of an ammonium halide and a metal halide. A fluidizing gas is introduced into the furnace under heat to form a fluidized bed in which the surface of the material to be treated is treated. The vessel or vessels are placed in the furnace in a spaced-apart relation from the material to be treated, so that no powder of the treating agent may adhere to the surface of the material to be treated.

Abstract: Silicon of high purity is used in making semiconductor devices. Silicon for this purpose is made by decomposing silane in a fluidized bed reactor. This process entails thermal decomposition of silane to deposit additional metallic silicon on particles of high purity silicon. To obtain good process economics, two modes of operation are used. In a first mode, the reactor is operated under high productivity conditions which also result in co-production of silicon dust or fines. Some of the dust is deposited on the product silicon particles and some of it is elutriated by gas flow in the reactor and removed through an exit point near the top of the reactor apparatus. The dust on the particles can cause problems in handling. For example, in bagging the particles, or removing the particles from a bag, the dust can become airborne from the larger particle surfaces and form an objectionable cloud of silicon dust.

Abstract: This invention relates to an enzyme and peroxyacid bleach granular composition comprising (1) a homogeneously mixed granulate of enzymes and alkaline buffer salt to protect the enzymes from deactivation when mixed with (2) a strong peroxyacid bleach granulate. This composition can also contain detergent surface-active agents, water-soluble builder salts, and other ingredients commonly used in detergents and laundry additive products.

Abstract: A particle for releasing bleach is provided combining from 50 to 99.5% of a core consisting essentially of an oxidizing material and from 0.5 to 20% of a polycarboxylate coating surrounding the core. These particles are particularly useful in automatic dishwasher powder detergent compositions.

Abstract: A process is disclosed for coating particles comprising suspending the particles in a fluidized bed and introducing therein an encapsulating latex. During introduction of the latex, the fluid bed must be maintained at a temperature which is within 10.degree. C. lower to 20.degree. C. higher than the glass transition temperature of the polymer. Typical core materials include halogen and peroxygen bleaches, bleach precursors, enzymes, colorants and fabric softeners. Preferably, the latex comprises water as a carrier and a polymer with carboxyl functionality, the polymer being insoluble in water.

Abstract: The invention relates to a fluidized-bed method for simultaneously obtaining the dry matter from aqueous solutions of extract substances from deproteinized calves blood and producing granules which can be compressed to give solid medicament forms and contain at least 50% by weight of extract substances, relative to the total dry weight of the granules, a binder and pharmaceutically acceptable fillers and carriers, by spraying an aqueous solution of the extract substances and of the binder on to the fillers and carriers and granulating the mixed material at a defined water content in the fluidized bed. After drying, granules ready for compression are obtained, and they are used for producing solid medicament forms of high stability and constant quality.

Abstract: Granules are processed with a liquid coating material in a vessel having a fluidizing bed on a horizontal or slightly inclined perforated plate and spouting beds, the fluidizing bed having a depth of 0.10 to 1.00 m in the static state and 0.30 to 1.50 m in the fluidizing state, the coating material being sprayed upwardly in a conical form with a spray angle of 30 to 80 degree from spray nozzles disposed in the spouting beds, a gas strean being fed at a spouting velocity of 5 to 50 m/sec. and a flow rate of 250 to 10,000 Nm.sup.3 /hour, each spouting bed unit being disposed in a density of 0.5 to 5 units/m.sup.2 on the fluidizing bed.

Abstract: Atmospheric contamination by residual hazardous particles remaining on a substrate following removal from the substrate of a layer of material containing such particles is substantially reduced by coating the substrate with certain aqueous coating compositions which produce tacky films on drying. For example, the health hazard from airborne asbestos fibers remaining attached to a substrate from which a layer of asbestos-containing material has been removed is substantially reduced by coating the substrate with an aqueous latex composition containing certain carboxylated butadiene styrene polymers.

Abstract: Undesirable conversion of a silicon source, such as silane, in the freeboard above a fluidized bed of silicon particles in a fluidized bed reactor, can be reduced by cooling the gas within the freeboard. Preferably, the reduction in temperature is achieved by introducing into the freeboard, a stream of relatively cool quench gas such as hydrogen, which also reduces the concentration of silane in the freeboard. As a result of these two factors, the invention improves the service factor of the fluidized bed apparatus, and reduces the amount of silane conversion to undesired by-products.

Abstract: This invention relates to particle coaters and in particular to a method and apparatus for a circulating bed particle coater which is particularly adapted for coating small diameter particles.

Abstract: The interior of a rotary-disk apparatus is divided by a generally cylindrical wall into an inner processing zone and an outer processing zone. The inner processing zone can be connected to an disconnected from the outer processing zone by moving the wall into and out of sealing engagement with an underlying rotary disk. When the wall and the disk are not in sealing engagement with each other, a gap is formed which permits the transfer of granules from the inner processing zone to the outer processing zone as a result of the rotation of the disk.

Abstract: A free-flowing granulate of a powder-form or fine-grained component and a liquid component; the granulate containing at least 20% by weight of the liquid component, is prepared by moving the powder-form or fine-grained component in a mixer-granulator, adding the liquid component while mixing until a moist granulate having a particle size of at most 1.5 mm is obtained, subsequently coarsening the granulate thus obtained with an increase in temperature to a particle size of from 0.4 to 4 mm and optionally coating this coarse granulate with another powder-form and/or fine-grained component at 60.degree. to 90.degree. C. The optionally coated granulate is converted by lowering the treatment temperature into a dry-looking, free-flowing, coarse-grained product, which if desired, may be coated with another powder-form and/or fine-grained material. Despite the high percentage of a liquid component, the granulate thus obtained appears as a dry granulate and is free-flowing.

Abstract: A solid substrate, which contains or consists of a biologically or chemically active substance, is coated with coating material containing at least one polymerizable crosslinkable polyfunctional acrylic or methacrylic compound whereafter the coating material is subjected to polymerization substantially in the absence of non-polymerizable components to form a network coating of polymer on the surface of the solid substrate. This coating permits either the controlled release of active substance from the coated substrate or the controlled access of material reacting with said active substance into the coated substrate and the controlled release of the resulting reaction products from the coated substrate.

Abstract: This invention relates to an improved granulate enzyme composition comprising a core of enzyme material and a protective coating comprising alkaline buffer salt. The improved granulate enzyme composition has improved stability when mixed with a dry peroxyacid bleach granulate.

Abstract: A particulated thermoplastic polymer having a uniform surface coating of zinc stearate is prepared by contacting the polymer particles with atomized droplets of molten zinc stearate while supporting and conveying the polymer by a moving stream of a gas. Reduced frictional forces allow increased volumes of coated particles to be transported by pneumatic conveyance. Substantially reduced fine particulate generation or "dusting" is observed for the composition.

Abstract: Preparation of granules by making nuclei grow, in a fluidized bed, by causing a liquid material to solidify thereon. The liquid material is sprayed in the bed upwards, with the aid of a spraying device provided with a central channel through which the liquid material is supplied, and a channel concentric therewith carrying a powerful gas stream, with the liquid material contacting the gas stream and being carried with the gas stream to a dilute zone where the growth of the nuclei takes place, which zone is created by the gas stream and is completely within the fluidized bed. The liquid material is made to come out of the central channel as a virtually closed, conical film, with a thrust exceeding the thrust of the gas stream, and this film is nebulized to very fine droplets with the aid of the gas stream.In this process a very small amount of high-energetic gas is needed, while no agglomeration occurs in the bed.

Abstract: Gel inserts comprising a solidified liquid such as agarose suitable for use in an electrophoretic method, lysed cells entrapped within a matrix formed by the solidified liquid and macromolecules such as DNA or intact chromosomes derived from the lysed cells may be advantageously used in electrophoretic separations. The gel inserts are placed directly in a suitable support medium and subjected to one or more electric fields to separate the macromolecules.

Abstract: An improved heated fluidized bed reactor and method for the production of high purity polycrystalline silicon by silane pyrolysis wherein silicon seed particles are heated in an upper heating zone of the reactor and admixed with particles in a lower reaction zone, in which zone a silane-containing gas stream, having passed through a lower cooled gas distribution zone not conducive to silane pyrolysis, contacts the heated seed particles whereon the silane is heterogeneously reduced to silicon.

Abstract: Disclosed is a resin composition for sealing electronic parts, which comprises a thermosetting resin and, incorporated therein, high-purity magnesium oxide. A hydration-resistant magnesia powder having the particle surfaces covered with a continuous and uniform coating of silica is advantageously used as the magnesium oxide. This hydration-resistant magnesia powder is prepared by introducing a heated vapor of an organic silicate compound into a reactor of a fluidized bed of magnesia powder heated at 100.degree. to 600.degree. C. so that the concentration of the organic silicate compound is 1 to 20 mole %, and precipitating a coating of silica on the surfaces of magnesia particles by thermal decomposition and/or hydrolysis of the organic silicate compound on the surfaces of magnesia particles.

Abstract: A denture cleansing composition of the hypochlorite type is rendered substantially free of hypochlorite chlorine odor by incorporating into the composition a hypochlorite deactivator. The deactivator is released into the cleansing solution at a controlled rate to optimize cleansing efficacy at a reduced hypochlorite/chlorine odor. The deactivators suitable for use in this invention include sodium perborate monohydrate and sodium nitrite. The preferred method of controlling deactivator release rate is by encapsulating the deactivator.

Abstract: An improved deposition method for producing silicon carbide high-temperature semiconductor material comprising placing a semiconductor substrate composed of silicon carbide in a fluidized bed silicon carbide deposition reactor, fluidizing the bed particles by hydrogen gas in a mildly bubbling mode through a gas distributor and heating the substrate at temperatures around 1200.degree.-1500.degree. C. thereby depositing a layer of silicon carbide on the semiconductor substrate.

Abstract: High efficiency encapsulation of core particles, particularly halogen bleaches, by (i) encapsulating the core particle in at least two separate coats wherein the melting point of the inner or first coating material is below the melting point of the outer or second coating material, (ii) heating the thus encapsulated particle to a temperature between the melting points of the inner and outer coating materials in order to liquefy the inner coat, and (iii) allowing the liquid inner coat to solidify and form a continuous, nonporous encapsulating coating.

Abstract: Hard spherical bleaching particles are disclosed whose composition is an intimately dispersed agglomerated core mixture of an active halogen oxidizing material, an inorganic diluent salt and a binder. The cores are coated with a mixture of from about 70-85% of a C.sub.16 -C.sub.18 fatty acid soap and from about 15-30% of a C.sub.12 -C.sub.14 fatty acid soap. A method for bleaching substrates as well as a process for preparing the bleach particles are disclosed.

Abstract: A particulate material containing particles to be agglomerated and/or provided with a coating is introduced in batches into a space bounded by a container, in which a gas, in particular air, is passed through the particles. The particles are set in motion, for instance by the gas, such as in whirling motion, to form a whirling, layer. The particles are wetted by means of a mixture consisting of a gas and the vapor of a wetting agent. This mixture is introduced into the space containing the particles, and cold gas and a mixture of warm gas and wetting agent are supplied for example, alternately. In this manner, the particles may be wetted uniformly and relatively fast, and held at a relatively low temperature. This is of considerable advantage when processing thermolabile materials.

Abstract: What is disclosed is a method of forming a high-strength proppant that resists the deleterious effects of high temperature saline environments characterized by the steps of forming a plurality of particles of propping agent; and coating particles with a thin high-strength covering in a fluidized bed employing chemical vapor deposition to deposit a coating substantially uniformly over all the exposed surfaces of the particles to increase durability of the particles, as well as their strength and resistance to the deleterious effects of hot saline environment. Preferably, each particle has at least one passageway formed directly therethrough for increased permeability once deposited.