Metal Oxide- Or Silicon-containing Coating (e.g., Glazed, Vitreous Enamel, Etc.) Patents (Class 427/376.2)
  • Publication number: 20030068437
    Abstract: A method of forming an insulating film containing silicon oxy-nitride first forms a silicon oxide film on the surface of a silicon wafer by oxidizing the water. In this oxidation, the atmosphere in a process chamber accommodating the silicon wafer is set at a first temperature of from 700 to 950° C. and a first pressure of from 0.7 to a value of [atmospheric pressure −0.375] Torr for a first processing time of from 0.5 to 30 min, and a first processing gas for oxidation is supplied into the process chamber. This first processing gas contains 1 to 5 vol % of water vapor and 95 to 99 vol % of nitrogen gas. After the silicon oxide film is formed, annealing is performed to convert at least a portion of the silicon oxide film into silicon oxy-nitride. In this annealing, the atmosphere in the process chamber is set at a second heating temperature of from 800 to 950° C. and a second pressure of from 0.
    Type: Application
    Filed: November 20, 2002
    Publication date: April 10, 2003
    Inventors: Genji Nakamura, Yoshihide Tada, Masayuki Imai, Asami Suemura, Shingo Hishiya
  • Patent number: 6544589
    Abstract: A method of controlling drying stresses through controlled shrinkage of a ceramic coating coated onto a substrate. The method first includes applying a non-cured ceramic coating onto the substrate and permitting the coating to dry until a mechanically stable outer surface layer of the coating is formed. Once this layer is formed, a drying control is applied in a quantity sufficient to penetrate into the surface layer, with the result of such application being the inhibition of formation of a dry outer skin as continued drying is permitted to occur. Once such drying is complete, the outer surface layer is subjected to an elevated temperature for curing and for evaporating therefrom the drying control agent to thereby produce a cured-ceramic coated substrate whose coating is void of large cracks and whose durability is beneficially opportune.
    Type: Grant
    Filed: August 20, 2001
    Date of Patent: April 8, 2003
    Assignee: Northrop Grumman Corporation
    Inventors: John Willis, Thomas A. Seitz, Steven J. Null, James W. Bohlen, Michael L. Peters, Blake T. Tatsuta
  • Patent number: 6541066
    Abstract: The invention relates to a method for applying a non-permeable, ceramic layer of a thickness of not more than about 100 &mgr;m to a ceramic or metallic body by applying a solution of one or more elastomers, which elastomers contain substantially not exclusively sulfur, carbon, hydrogen and oxygen, optionally drying, and pyrolyzing to form a porous layer and subsequently sintering at increased temperature to form a non-permeable ceramic layer.
    Type: Grant
    Filed: June 12, 2000
    Date of Patent: April 1, 2003
    Assignee: Universiteit Utrecht
    Inventor: John Wilhelm Geus
  • Publication number: 20030059633
    Abstract: An article protected by a thermal barrier coating system includes a substrate having a substrate surface, and a thermal barrier coating system overlying the substrate. The thermal barrier coating system has a thermal barrier coating formed of a thermal barrier coating material arranged as a plurality of columnar grains extending generally perpendicular to the substrate surface and having grain surfaces. A sintering inhibitor is within the columnar grains, either uniformly distributed or concentrated at the grain surfaces. The sintering inhibitor is lanthanum oxide, chromium oxide, and/or yttrium chromate, mixtures thereof, or mixtures thereof with aluminum oxide.
    Type: Application
    Filed: September 21, 2001
    Publication date: March 27, 2003
    Inventors: John Frederick Ackerman, Venkat Subramaniam Venkataramani, Irene Spitsberg, Ramgopal Darolia
  • Publication number: 20030059533
    Abstract: The object of the present invention is to provide a method for forming an interlayer coating film which is uniform even in a fine space of 0.13 &mgr;m or less between wiring layers by reducing an area of a rough portion and a dense portion, and reducing a roughness-density difference.
    Type: Application
    Filed: September 25, 2002
    Publication date: March 27, 2003
    Applicant: Tokyo Ohka Kogyo Co., Ltd.
    Inventor: Hiroki Endo
  • Patent number: 6537617
    Abstract: There is disclosed a method of mixing/dispersing solid phases of a carbon powder 4 and silicon powder 5, impregnating a woven fiber 2 with the powders, and subsequently exposing the woven fiber to a high temperature sufficient for reaction calcining to react/calcine the woven fiber, so that only small amounts of C and Si particles remain, a matrix forming speed is high, and CMC having high airtightness can be manufactured in a short time.
    Type: Grant
    Filed: May 8, 2001
    Date of Patent: March 25, 2003
    Assignee: Ishikawajima-Harima Heavy Industries Co., Ltd.
    Inventors: Takeshi Nakamura, Shunsuke Satomi, Hiroshige Murata
  • Patent number: 6537388
    Abstract: Chromium, silicon, aluminum, and optionally manganese are diffused onto the surface of a high temperature alloy product, to provide a coating having improved resistance to carburization and catalytic coke formation and smoother surfaces for high temperature hydrocarbon environments. Preferably, a first layer of chromium or chromium and silicon is deposited and diffusion heat-treated and covered by the second layer of aluminum or aluminum-silicon. The inner layer contains a minimum of 8 weight percent chromium above that contained in the substrate alloy. The outer layer contains a minimum of 20 weight percent aluminum at the coating surface. The coating system is then aged to yield the improved coating that has 60 to 90 weight percent chromium at the surface. Each layer or the combination of layers is diffusion heat treated to cause a diffusion depth ranging from 0.006 inch (0.1524 millimeter) to 0.030 inch (0.762 millimeter) with targeted 0.012 inch (0.3048 millimeter) to 0.015 inch (0.3810 millimeter).
    Type: Grant
    Filed: October 27, 2000
    Date of Patent: March 25, 2003
    Assignee: Alon, Inc.
    Inventors: Kim A. Wynns, George T. Bayer
  • Publication number: 20030054108
    Abstract: A method of placing a ceramic coating on an article of manufacture comprising a substrate formed of a nickel or cobalt-based superalloy, which includes the steps of placing a bonding layer on the substrate and placing an anchoring layer, which is chemically different from the bonding layer and comprises a nitride compound, on the bonding layer. The method further includes the step of placing the ceramic coating on the anchoring layer.
    Type: Application
    Filed: October 25, 2002
    Publication date: March 20, 2003
    Applicant: Siemens Aktiengesellschaft
    Inventor: Wolfram Beele
  • Publication number: 20030054194
    Abstract: An environmentally resistant coating comprising silicon, titanium, chromium, and a balance of niobium and molybdenum for turbine components formed from molybdenum silicide-based composites. The turbine component may further include a thermal barrier coating disposed upon an outer surface of the environmentally resistant coating comprising zirconia, stabilized zirconia, zircon, mullite, and combinations thereof. The molybdenum silicide-based composite turbine component coated with the environmentally resistant coating and thermal barrier coating is resistant to oxidation at temperatures in the range from about 2000° F. to about 2600° F. and to pesting at temperatures in the range from about 1000° F. to about 1800° F.
    Type: Application
    Filed: September 24, 2002
    Publication date: March 20, 2003
    Inventors: Ji-Cheng Zhao, Bernard Patrick Bewlay, Melvin Robert Jackson
  • Publication number: 20030051341
    Abstract: A method for producing a spark plug, the spark plug comprising a center electrode, a metal shell and an alumina ceramic insulator disposed between the center electrode and the metal shell, wherein at least part of the surface of the insulator is covered with a glaze layer, the method comprising the steps of: preparing a plurality of kinds of element glaze powders wherein each kind of the element glaze powders has a different dilatometric softening point and a different linear expansion coefficient compared to other kinds of element glaze powders; coating a surface of the insulator with the plurality of kinds of element glaze powders so as to form a glaze powder layer; and baking the glaze powder layer to the surface of the insulator so as to form the glaze layer by heating the glaze powder layer.
    Type: Application
    Filed: June 26, 2002
    Publication date: March 20, 2003
    Applicant: NGK Spark Plug Co., Ltd.
    Inventors: Kenichi Nishikawa, Makoto Sugimoto
  • Patent number: 6531181
    Abstract: The invention relates to a process for producing a conductive coating on glass and enamelled steel using a screen-printable aluminum paste. The paste to be used contains: 40 to 80 wt. %, in particular, 50 to 75 wt. % aluminum powder; 5 to 40 wt. %, in particular, 9 to 25 wt. % glass frit having an initial softening temperature of 400 to 700° C., in particular, 420 to 580° C.; 10 to 35 wt. % of a liquid or thermoplastic medium; and 0 to 10 wt. % sintering aid. The substrate coated with the paste is heated at 500 to 750° C., in particular, 590 to 690° C. The coating on the substrate is characterized by having a low specific resistance of less than 100 &mgr;ohm·cm, in particular in the range of 10 to 70 &mgr;ohm·cm, and good adhesion.
    Type: Grant
    Filed: September 22, 2000
    Date of Patent: March 11, 2003
    Assignee: DMC
    Inventors: Axel Niemann, Guy Roche
  • Patent number: 6528123
    Abstract: This invention relates to a method for preparing the surface of a ceramic component that enables direct brazing using a non-active braze alloy. The present invention also relates to a method for directly brazing a ceramic component to a ceramic or metal member using this method of surface preparation, and to articles produced by using this brazing method. The ceramic can be high purity alumina. The method comprises applying a first coating of a silicon-bearing oxide material (e.g. silicon dioxide or mullite (3Al2O3.2SiO2) to the ceramic. Next, a thin coating of active metal (e.g. Ti or V) is applied. Finally, a thicker coating of a non-active metal (e.g. Au or Cu) is applied. The coatings can be applied by physical vapor deposition (PVD). Alternatively, the active and non-active metals can be co-deposited (e.g. by sputtering a target made of mullite).
    Type: Grant
    Filed: June 28, 2000
    Date of Patent: March 4, 2003
    Assignee: Sandia Corporation
    Inventors: Charles H. Cadden, F. Michael Hosking
  • Publication number: 20030039744
    Abstract: The present invention provides a coating composition comprising: A coating composition comprising: TEOS; a surfactant; at least one organosilane; HCl; water; and ethanol. The present invention also provides films made from such a coating composition and a method for making such films.
    Type: Application
    Filed: June 7, 2002
    Publication date: February 27, 2003
    Inventors: Hongyou Fan, Gabriel P. Lopez, Charles Jeffrey Brinker, Yunfeng Lu
  • Publication number: 20030039841
    Abstract: An enhanced ceramic layer is produced for use in laminated ceramic devices. A layer of unfired ceramic material is provided and a coating of dielectric material (preferably alumina) is applied on at least one surface. The dielectric material forms a reaction barrier between excess glass forced to the surface during firing and metallization positioned on the coating. The coating can be applied by screen printing, spraying a slurry of dielectric material, or spraying a slurry of dielectric material and an adhesive allowing low pressure lamination.
    Type: Application
    Filed: August 27, 2001
    Publication date: February 27, 2003
    Applicant: Motorola, Inc.
    Inventors: Ross A. Miesem, Kristen June Law, Jeremy W. Burdon, Rickey G. Pastor
  • Publication number: 20030039756
    Abstract: The present invention provides a slurry for use in decorating a ceramic substrate. The slurry according to the invention includes solid particles of at least one color-contributing metal salt dispersed in a saturated solution of at least one color-contributing metal salt, and has a viscosity of from about 10 to about 20,000 centipoise. Preferably, the solid particles have a diameter of less than about 40 microns. The present invention also provides a method of decorating a surface of a ceramic substrate. The method according to the invention includes applying a slurry that includes solid particles of at least one color-contributing metal salt dispersed in a saturated solution of at least one color-contributing metal salt having a viscosity of from about 10 to about 20,000 centipoise to a ceramic substrate, applying a solvent to the ceramic substrate in amount sufficient to at least partially dissolve the solid particles, and firing the ceramic substrate.
    Type: Application
    Filed: September 18, 2002
    Publication date: February 27, 2003
    Applicant: Ferro Corporation
    Inventors: Carlos Benet Garcia, Javier Garcia Sainz, Juan Carlos Gallart
  • Patent number: 6524725
    Abstract: Enameled steel and process for enameling a zinc or zinc-alloy precoated steel surface includes providing steel having a surface to be precoated and enameled; applying a zinc or zinc-alloy coating having a thickness ranging from 1 to 30 &mgr;m to the surface of the steel to provide the zinc or zinc-alloy precoated steel surface; subjecting the zinc or zinc-alloy precoated steel surface to a heat pretreatment at a temperature of at least 500° C.; and enameling the zinc or zinc-alloy precoated steel surface with a vitreous enamel composition which has a content of adherence-providing oxides selected from the group consisting of Co, Ni, Cu, Sb and Mn of less than 0.1% by weight for a white enamel layer and less than 2.5% by weight for a colored enamel layer by firing the vitreous enamel composition to provide a vitreous enamel layer thereon.
    Type: Grant
    Filed: February 23, 2001
    Date of Patent: February 25, 2003
    Assignee: Enamels and Ceramic Coatings International C.V.
    Inventors: Koen Lips, Christian Schlegel
  • Publication number: 20030035901
    Abstract: The present invention provides a silicon carbide-based, porous, lightweight, heat-resistant material which can retain the shape of a porous structural body formed of, for example, corrugated cardboard and provides a manufacturing method therefor. The silicon carbide-based, porous, lightweight material is produced by a process including the steps of infiltrating a slurry composed of a resin and powdered silicon into a porous structural body having a framework formed of paper such as corrugated cardboard, wood, a woven cloth, a non-woven cloth, a plastic, or the like; carbonizing the infiltrated porous structural body at 900 to 1,350° C. in an evacuated or an inert atmosphere; and performing reaction-bonding for the obtained structural body at 1,350° C. or more in an evacuated or an inert atmosphere. By the reaction-bonding, silicon carbide having superior molten silicon wettability and open pores caused by the reaction during which the reaction volume decreases are simultaneously formed.
    Type: Application
    Filed: August 17, 2001
    Publication date: February 20, 2003
    Applicant: Eiji TANI
    Inventor: Eiji Tani
  • Publication number: 20030035896
    Abstract: A method of controlling drying stresses through controlled shrinkage of a ceramic coating coated onto a substrate. The method first includes applying a non-cured ceramic coating onto the substrate and permitting the coating to dry until a mechanically stable outer surface layer of the coating is formed. Once this layer is formed, a drying control is applied in a quantity sufficient to penetrate into the surface layer, with the result of such application being the inhibition of formation of a dry outer skin as continued drying is permitted to occur. Once such drying is complete, the outer surface layer is subjected to an elevated temperature for curing and for evaporating therefrom the drying control agent to thereby produce a cured-ceramic coated substrate whose coating is void of large cracks and whose durability is beneficially opportune.
    Type: Application
    Filed: August 20, 2001
    Publication date: February 20, 2003
    Inventors: John Willis, Thomas A. Seitz, Steven J. Null, James W. Bohlen, Michael L. Peters, Blake T. Tatsuta
  • Publication number: 20030035937
    Abstract: This invention relates to the nature of thick film compositions that are specifically designed for the fabrication of circuit elements on diamond substrates, especially resistive elements. The nature of diamond sheet material requires special consideration because of its relatively low coefficient of thermal expansion and its sensitivity to oxygen at elevated processing temperatures. The general compositional requirements of thick film paste formulations are provided as a basis for accommodating the particular physical properties of diamond, and thereby establishing a method by which high performance microelectronic components can be fabricated economically. Thick film pastes containing certain borosilicate glasses, metal components, and optionally semiconducting materials are demonstrated to possess favorable behavior in terms of mechanical and electrical properties after sintering. Resistive elements on diamond can be fabricated by adding conductive components to a borosilicate glass.
    Type: Application
    Filed: April 9, 2002
    Publication date: February 20, 2003
    Inventor: Ronald R. Petkie
  • Patent number: 6521198
    Abstract: Metal surfaces are protected against corrosion by a coating of molecular sieve, notably a zeolite or a phosphate-containing molecular sieve, rendered substantially non-porous by the retention (or addition) of a pore-filling member inside the voids of the molecular sieve crystal structure. Pore-filling agents convenient for use include species typically used as structure-directing agents in the synthesis of zeolites and other molecular sieves. A further aspect of the invention is a method of protecting a metal surface from corrosion by crystallizing a molecular sieve in situ on the metal surface.
    Type: Grant
    Filed: December 20, 2000
    Date of Patent: February 18, 2003
    Assignee: The Regents of the University of California
    Inventors: Yushan Yan, Xiaoliang Cheng, Zhengbao Wang
  • Publication number: 20030031797
    Abstract: The invention concerns a method which consists in: providing a protective treatment against corrosion to the initial sheet metal using an aqueous emulsion containing colloids based on acrylic and/or methacrylic polymer; a step which consists in applying a coat of liquid enamelling composition comprising an enamel frit capable of being vitrified; a baking step adapted to vitrify said frit. The invention is characterised in that said method does not comprise a step for degreasing said surface subsequent to the protective treatment. The invention provides the advantages of improved adherence of the enamel and a simpler process.
    Type: Application
    Filed: August 16, 2002
    Publication date: February 13, 2003
    Inventors: Christophe Delmotte, Philippe Legros, Thierry Malot, Patrick Nicoletti
  • Patent number: 6517904
    Abstract: The present invention relates to a process for the enameling of aluminum or aluminum alloy surfaces, in particular containing a relatively high amount of Mg, Cu, or both, which is characterized by the use of a vitreous enamel containing CuO.
    Type: Grant
    Filed: November 22, 2000
    Date of Patent: February 11, 2003
    Assignee: Pemco Brugge N.V.
    Inventors: Marc Leveaux, Koen Lips, Nacy Crevits, Sebastien Humez
  • Patent number: 6518209
    Abstract: A chemical, thermal, and electrical corrosion resistant dry mix for use in fusing glass to metal motor vehicle and building industry articles. A chemical, thermal, and electrical corrosion resistant composition for fusing glass to metal motor vehicle and building industry articles. A method of glass fusing metal motor vehicle and building industry articles using a chemical, thermal, and electrical corrosion resistant dry mix. A method of glass fusing metal motor vehicle and building industry articles with a chemical, thermal, and electrical corrosion resistant composition. A method of fusing single or multiple layers of glass to metal motor vehicle and building industry articles.
    Type: Grant
    Filed: July 12, 2001
    Date of Patent: February 11, 2003
    Inventor: Gary D. Wilson
  • Publication number: 20030027012
    Abstract: A coating system having a low thermal conductivity, and a method by which the low thermal conductivity of the coating system is maintained through the development of cracks within a thermal-insulating layer of the coating system. The thermal-insulating layer is a mixture of two or more materials with different coefficients of thermal expansion (CTE). The materials of the thermal-insulating layer are selected and combined so that a low thermal conductivity is maintained for the coating system as the result of cracks developing and propagating from interfaces between the materials when the coating system is subjected to heating and cooling cycles.
    Type: Application
    Filed: August 3, 2001
    Publication date: February 6, 2003
    Inventors: Irene Spitsberg, Hongyu Wang
  • Publication number: 20030022005
    Abstract: There is provided a non-chromium treated material in which peeling resistance between a metal plate and a rubber layer via a primer layer and a bond layer, which is decreased by fretting and antifreeze liquid, can be improved, the rubber layer is less liable to peel from the metal plate, and the material has little effect on the environment and human body. In a metal gasket raw material plate 1 of a laminated form in which a rubber layer 5 is provided on a stainless steel plate 2 via a bonding layer 4, a primer layer 3 of a silica-alumina condensate is formed on the surface of the stainless steel plate 2.
    Type: Application
    Filed: February 19, 2002
    Publication date: January 30, 2003
    Inventors: Masabumi Miyashita, Shingo Watanabe, Norifumi Misumi, Naomichi Mitsuyama
  • Publication number: 20030021900
    Abstract: The process described herein provides a simple and cost effective method for making crack free, high density thin ceramic film. The steps involve depositing a layer of a ceramic material on a porous or dense substrate. The deposited layer is compacted and then the resultant laminate is sintered to achieve a higher density than would have been possible without the pre-firing compaction step.
    Type: Application
    Filed: June 3, 2002
    Publication date: January 30, 2003
    Inventors: Craig P. Jacobson, Steven J. Visco, Lutgard C. De Jonghe
  • Publication number: 20030021901
    Abstract: A method for covering a part made of silicon carbide material, wherein a coating compound is applied to at least one surface of said part and the assembly formed by the part and the coating compound is heated to a temperature sufficient to cause the surface of the coating compound to melt in order to coat said piece with a deposit of silicon carbide material and, wherein the coating compound is a non-reactive composition comprised of, in atomic percentages, from 40 to 97% silicon and 60 to 3% of another element selected from among chrome, rhenium, titanium, vanadium, ruthenium, iridium, rhodium, palladium, cobalt, platinum, cerium and zirconium and, wherein prior to heating, a SiC and/or C reinforcement is added.
    Type: Application
    Filed: August 29, 2002
    Publication date: January 30, 2003
    Inventor: Adrien Gasse
  • Patent number: 6511718
    Abstract: A venturi mist generator creates a mist comprising droplets having a mean diameter less than one micron from liquid precursors containing multi-metal polyalkoxide compounds. The mist is mixed and then passed into a gasifier where the mist droplets are gasified at a temperature of between 100° C. and 250° C., which is lower than the temperature at which the precursor compounds decompose. The gasified precursor compounds are transported by carrier gas through insulated tubing at ambient temperature to prevent both condensation and premature decomposition. The gasified precursors are mixed with oxidant gas, and the gaseous reactant mixture is injected through a showerhead inlet into a deposition reactor in which a substrate is heated at a temperature of from 300° C. to 600 ° C. The gasified precursors decompose at the substrate and form a thin film of solid material on the substrate. The thin film is treated at elevated temperatures of from 500° C. to 900° C.
    Type: Grant
    Filed: December 17, 1999
    Date of Patent: January 28, 2003
    Assignee: Symetrix Corporation
    Inventors: Carlos A. Paz de Araujo, Larry D. McMillan, Narayan Solayappan, Jeffrey W. Bacon
  • Publication number: 20030017950
    Abstract: Manufacturing process of an electrically insulating and mechanically structuring sheath on an electric conductor.
    Type: Application
    Filed: July 19, 2002
    Publication date: January 23, 2003
    Applicant: COMMISSARIAT A L'ENERGIE ATOMIQUE
    Inventors: Jean-Michel Rey, Sandrine Marchant, Arnaud Devred, Eric Prouzet
  • Publication number: 20030012874
    Abstract: A process for producing crystalline III-V compound films, preferably thin films of gallium nitride and other III-V nitrides, on various single crystal substrates. The process enables the preparation of III-V compound films by the simple, direct deposition of an amorphous layer of a III-V compound precursor on a single crystal substrate (as a template). A chemical reaction followed by a single heat treatment leads to the crystallization and formation of films by pyrolysis. According to specific examples of the invention, the chemical precursors gallium dimethyl amide (Ga2[N(CH3)2]6), gallium nitrate (Ga(NO3)3, and gallium isopropoxide [Ga(OC3H7)3 are used to produce gallium nitride thin films.
    Type: Application
    Filed: November 20, 2001
    Publication date: January 16, 2003
    Inventors: Frederick F. Lange, David Kisailus
  • Patent number: 6506452
    Abstract: A process for producing a honeycomb structure, comprising the steps of: providing a substrate having cell walls in a honeycomb form and comprising SiO2, Al2O3 and MgO as the main chemical components, applying to said substrate a mixture of a component for lowering the cordierite crystal phase crystallization temperature of said substrate with a liquid medium, and firing said substrate with said mixture applied to form a honeycomb structure comprising a crystalline cordierite phase, said crystalline cordierite phase comprising 42-56% by mass of SiO2 30-42% by mass of Al2O3 and 12-18% by mass of MgO as the main chemical components.
    Type: Grant
    Filed: December 6, 2000
    Date of Patent: January 14, 2003
    Assignee: Denso Corporation
    Inventor: Masakazu Murata
  • Publication number: 20030008067
    Abstract: A method for fabricating a CMC (Ceramic Matrix Composite) article, comprising: performing a CVI (Chemical Vapor Infiltration) treatment for forming a SiC matrix layer on the surface of a woven fabric; performing a machining process, after the CVI treatment, for machining the woven fabric; and performing a PIP (Polymer Impregnation and Pyrolysis) treatment, after the machining process, for impregnating an organic silicon polymer as a base material into voids in the matrix layer and pyrolyzing the organic silicon polymer. By this method, the throughput of CMC articles can be preferably increased. The throughput may be further increased by performing a slurry impregnation treatment before or after the PIP treatment, in which slurried SiC is impregnated into the voids in the matrix layer.
    Type: Application
    Filed: April 8, 2002
    Publication date: January 9, 2003
    Inventors: Hirohide Yamaguchi, Takeshi Nakamura, Hiroshige Murata
  • Publication number: 20030008077
    Abstract: The present invention provides a process for imparting colours to colourless gemstone/minerals and enhancing properties of gemstone/minerals by coating a thin/thick film of a particular material or multiple films of different materials on polished gemstones/minerals to impart colour in colourless stones and to enhance the colour in paler stones, and to such gemstones/mineral obtained by the process.
    Type: Application
    Filed: January 25, 2002
    Publication date: January 9, 2003
    Inventors: Samir Gupta, Manuj Goyal
  • Patent number: 6503849
    Abstract: A method for forming an insulating film, wherein a precursor film of a coating type insulating film having Si—H bonding is coated, the precursor film is calcined in an atmosphere containing at least one of an inert gas and oxygen gas for converting it into a ceramic film as the insulating film, and then the ceramic film is cooled under reduced pressure lower than that for the calcination.
    Type: Grant
    Filed: October 10, 2000
    Date of Patent: January 7, 2003
    Assignee: Sharp Kabushiki Kaisha
    Inventors: Yoshihiro Ooishi, Yushi Inoue
  • Patent number: 6503573
    Abstract: A multicomponent film on a substrate can be annealed at higher temperatures in oxygen by using a specifically designed annealing vessel. The vessel is formed of a multicomponent material which has at least all of the components of the first multicomponent material of the film or, in the case where there are nonvolatile components, then the vessel is formed of a second multicomponent material which has at least the same composition of relatively volatile components as the first multicomponent film. As the multicomponent film is annealed for a sufficient time within the vessel the multicomponent film remains in contact with a vapor of the first multicomponent material and the vessel material. This process called bomb annealing prevents loss of volatile components from the film and roughening of the film surface and leads to films with lower dielectric loss. Preferred thin film materials are ferroelectric materials although any material could be used.
    Type: Grant
    Filed: September 23, 1999
    Date of Patent: January 7, 2003
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: James Horwitz, Douglas B. Chrisey, Adriaan Carter, Manfred Kahn, Jeffrey M. Pond, Steven W. Kirchoefer, Wontae Chang
  • Publication number: 20030003235
    Abstract: A composition for forming a high-quality tantalum film which is advantageously used as an capacitor insulating film and a process for forming the high-quality tantalum film. The composition for forming a tantalum oxide film, which comprises at least one tantalum compound selected from the group consisting of a reaction product of a compound capable of reacting with a tantalum alkoxide and a tantalum alkoxide and a hydrolyzate of the reaction product, and a solvent, and the process for forming the tantalum oxide film by applying this composition to a substrate and heating it.
    Type: Application
    Filed: July 22, 2002
    Publication date: January 2, 2003
    Inventors: Hiroshi Shiho, Hitoshi Kato, Sachiko Okada, Isamu Yonekura, Yasuo Matsuki
  • Publication number: 20030003237
    Abstract: Processes for preparing aqueous suspensions of a nanoscale ceramic electrolyte material such as yttrium-stabilized zirconia. The invention also includes a process for preparing an aqueous coating slurry of a nanoscale ceramic electrolyte material. The invention further includes a process for depositing an aqueous spray coating slurry including a ceramic electrolyte material on pre-sintered, partially sintered, and unsintered ceramic substrates and products made by this process.
    Type: Application
    Filed: July 2, 2001
    Publication date: January 2, 2003
    Inventors: Matthew M. Seabaugh, Scott L. Swartz, William J. Dawson, Buddy E. McCormick
  • Patent number: 6501014
    Abstract: An object of the invention is to provide a coated article having a protective member which is improved in light transparency, heat resistance, and weather resistance, and easy to manufacture, as typified by a solar battery module which experience no deterioration of performance during long-term outdoor installation; and to provide a coated article capable of protecting a functional film or device from water vapor and gases for dramatically improve the life of the functional film or device. These objects are achieved by a coated article having as a protective member a silica coating which is obtained by applying a polysilazane-containing coating solution on at least one surface of a resinous substrate having light transparency and heat resistance under atmospheric pressure, followed by steam oxidation and heat treatment.
    Type: Grant
    Filed: October 6, 2000
    Date of Patent: December 31, 2002
    Assignee: TDK Corporation
    Inventors: Yuichi Kubota, Michio Arai
  • Patent number: 6500490
    Abstract: A hydrophilic coating can be optionally corrosion resistant and/or microbial resistant for a substrate such as a heat exchanger. The coating is provided by a zeolite layer that can be formed from a synthesis solution comprising a structure directing agent, a base, a silicon source, an aluminum source, and a solvent. In one preferred embodiment, the synthesis solution comprises tetrapropylammonium hydroxide, sodium hydroxide, aluminum oxide, tetraethylorthosilicate, and water. The layer is characterized by a zeolite MFI structure and by a composition having the formula of Mn/m[AlnSi(96−n)O192], or [AlnSi(96−n)O192]·4[(CH3CH2CH2)4N—OH] wherein M is a metal ion of valence m+ (e.g., Na+) and 27>n>=0. After formation of the coating, the organic structure directing agent can be left intact inside the zeolite coating to make the coating corrosion resistant.
    Type: Grant
    Filed: March 23, 2000
    Date of Patent: December 31, 2002
    Assignee: Honeywell International Inc.
    Inventor: Yushan Yan
  • Publication number: 20020197408
    Abstract: The present invention relates to a process for manufacturing recyclable black enamels that contain at least zinc, in which process glass forming materials comprising at least bismuth, silicon, boron and manganese are melted, at temperatures greater than about 900° C., and then a glass frit comprising at least zinc is added to the mixture obtained after this direct melting. The invention also relates to zinc-based recyclable black enamel compositions.
    Type: Application
    Filed: August 13, 2002
    Publication date: December 26, 2002
    Applicant: Saint-Gobain Vitrage
    Inventors: Andre Beyrle, Daniel Dages
  • Publication number: 20020197409
    Abstract: A transparent substrate having a glare reducing diffuser surface coating in which the coating has a thickness of less than about 3 microns. The diffuser surface coated substrate is bendable, overcoatable with functional coatings such as transparent conductor coatings, abrasion resistant, and generally serviceable for its intended use.
    Type: Application
    Filed: August 23, 2002
    Publication date: December 26, 2002
    Applicant: Donnelly Corporation, a Michigan corporation
    Inventors: Desaraju V. Varaprasad, Craig A. Dornan, Catherine A. Getz
  • Publication number: 20020197455
    Abstract: A method of manufacturing a touch screen panel, the method including applying a resistive coating to one surface of an insulative substrate, applying an insulative protective coating to the resistive coating, depositing a conductive edge electrode pattern including a plurality of edge electrodes on the protective coating, and firing the panel until the edge electrodes etch through the protective coating and make electrical contact with the resistive coating.
    Type: Application
    Filed: June 20, 2001
    Publication date: December 26, 2002
    Inventors: Paul J. Richter, Michael J. Kardauskas, Frank J. Bottari
  • Publication number: 20020192365
    Abstract: The present invention relates to a method for imparting hydrophilicity to a substrate whereby high hydrophilic properties and water-holding properties can be maintained for a long period of time. According to the present invention, an SiO2 film is formed directly or through an undercoat layer on a substrate under a reduced pressure of 100 Pa or less and immediately after the SiO2 film is formed, the SiO2 film is treated with water. Before forming the SiO2 film, it is also desirable that an undercoat layer consisting of a TiO2 film, Al2O3 film, Nb2O5 film, a laminated film prepared by laminating the TiO2 film on the Al2O3 film, a laminated film prepared by laminating the TiO2 film on the Nb2O5 film, or a low emissivity film be formed on a substrate and the SiO2 film be then formed on the undercoat film to serve as an SiO2 composite film.
    Type: Application
    Filed: April 12, 2002
    Publication date: December 19, 2002
    Inventors: Toshiaki Kitazoe, Keisuke Tanaka, Kenji Murata
  • Publication number: 20020192511
    Abstract: A functional coating on a substrate, including an inorganic matrix phase composed as far as possible of a phosphate and a functional material embedded in it. In addition, a method of producing this functional coating whereby first at least one functional material is dispersed in a matrix solution including a liquid component and a phosphate, and the gelatinous dispersion thus produced is applied to the substrate in the form of a coating. Then this coating is converted by a heat treatment to the functional coating including the inorganic matrix phase and the functional material integrated into it. The functional coating described here is suitable e.g., for protection against wear or corrosion or for thermal insulation, e.g., in automotive engineering or in heating technology.
    Type: Application
    Filed: May 20, 2002
    Publication date: December 19, 2002
    Inventors: Martin Hruschka, Ulrich Hasenkox, Guido Klamt
  • Publication number: 20020192361
    Abstract: The present invention uses an ultraviolet sensitive semiconductor ceramics to fabricate an ultraviolet sensor. For example, adding Sb5+ to tin dioxide containing Sn4+ to form SnO2:Sb. When exposing SnO2:Sb to ultraviolet rays, the electron Sb5+ exists in Energy Gap or Forbidden Band being excited, and jumps to Conductive Band, causing the conductivity of SnO2:Sb to be increased. More electrons are moved to Conductive Band following increasing of ultraviolet intensity, thereby causing the electric resistance value of SnO2:Sb to be reduced. A film of photosensitive semiconductor ceramics is connected and arranged with driving power, amplifier and control circuit, alarm system, etc., forming a miniature sensor.
    Type: Application
    Filed: May 28, 2002
    Publication date: December 19, 2002
    Applicant: AUDEN TECHNO CORP.
    Inventors: Daniel Chang, Ming-Tarng Yeh
  • Patent number: 6492029
    Abstract: The invention relates to a novel method of enameling substrates comprised of glass or vitroceramic material, according to which method the enamel composition contains graphite as a component, with the aim of improving the mechanical properties of the enameled substrate and/or conferring anti-adhesive properties on the composition. The invention also relates to the composition, and the enameled substrates obtained.
    Type: Grant
    Filed: July 12, 1995
    Date of Patent: December 10, 2002
    Assignee: Saint-Gobain Glass France
    Inventor: Andre Beyrlé
  • Publication number: 20020182341
    Abstract: An amorphous silicon deposition method includes the step of forming a buffer layer on a transparent substrate; depositing amorphous silicon on the buffer layer by a thickness ranging from 600 to 2,000 angstroms; repeatedly irradiating the amorphous silicon layer to completely melt using a laser beam that has a complete melting energy density; and moving the laser beam by a transaction distance for the next laser beam irradiation.
    Type: Application
    Filed: May 30, 2002
    Publication date: December 5, 2002
    Inventor: Yun-Ho Jung
  • Publication number: 20020182310
    Abstract: Improved photovoltaic cells utilizing for a semiconductor layer, titanium dioxide powders, consisting of porous particles, ranging in size from 0.1 to 10 microns (10-6 meters), and possess relatively high bulk density combined with high surface area.
    Type: Application
    Filed: July 17, 2002
    Publication date: December 5, 2002
    Inventor: Ying Wang
  • Publication number: 20020182342
    Abstract: A method of depositing an optical quality silica film on a substrate is described wherein the film is formed on the substrate by plasma enhanced chemical vapor deposition (PECVD) in the presence of reactive gases while controlling the total pressure of the gases. The as-deposited film is then subjected to a low temperature treatment between 400° to 1200° C. to minimize the presence of contaminant compounds in the film.
    Type: Application
    Filed: April 13, 2001
    Publication date: December 5, 2002
    Inventors: Luc Ouellet, Manuel Grondin, Jonathan Lachance, Stephane Blain
  • Patent number: 6488981
    Abstract: A method of manufacturing a touch screen panel, the method including applying a resistive coating to one surface of an insulative substrate, applying an insulative protective coating to the resistive coating, depositing a conductive edge electrode pattern including a plurality of edge electrodes on the protective coating, and firing the panel until the edge electrodes etch through the protective coating and make electrical contact with the resistive coating.
    Type: Grant
    Filed: June 20, 2001
    Date of Patent: December 3, 2002
    Assignee: 3M Innovative Properties Company
    Inventors: Paul J. Richter, Michael J. Kardauskas, Frank J. Bottari