Abstract: A structural design method of a product is provided. The method includes obtaining a preliminary design of a subsurface mesh structure by filling a body model of the product with spherical cells at preset positions of the body model and performing an finite element analysis and optimization; and optimizing, through a design method for optimizing functions, filling features of the spherical cells based on a simulation analysis so that the structure of the product satisfies a preset target.

Abstract: The present disclosure provides an interconnect structure, including a substrate, a first conductive feature over the substrate, a second conductive feature over the first conductive feature, and a dielectric layer surrounding the first conductive feature and the second conductive feature. A width of the first conductive feature and a width of the second conductive feature are between 10 nm and 50 nm. The present disclosure also provides a method for manufacturing an interconnect structure, including (1) forming a via opening and a line trench in a dielectric layer, (2) forming a 1-dimensional conductive feature in the via opening, (3) forming a conformal catalyst layer over a sidewall of the line trench, a bottom of the line trench, and a top of the 1-dimensional conductive feature, and (4) removing the conformal catalyst layer from the bottom of the line trench and the top of the 1-dimensional conductive feature.

Abstract: The invention relates to a mounted optical component and also a method for the production of mounted optical components. Furthermore, the invention relates to the use of mounted optical components.

Abstract: A method for applying a graphene coating to a substrate comprising iron or aluminium, the method comprising: providing a metallic layer on a surface of the substrate; and contacting said metallic layer with a source of carbon atoms to provide a graphene coating on the metallic layer. There is also described an iron- or aluminium-containing substrate, for example a component of a chain, with a metallic layer on a surface of the substrate and a graphene coating disposed on said metallic layer.

Abstract: Disclosed is an aluminum-diamond composite having both high thermal conductivity and thermal expansion coefficient close to those of semiconductor elements, which is improved in platability in the surface and surface roughness so that the composite becomes suitable for use as a heat sink of a semiconductor element of the like. Specifically disclosed is a plate-like aluminum-diamond composite containing diamond particles and a metal mainly composed of aluminum. The aluminum-diamond composite is composed of a composite part and surface layers formed on both sides of the composite part, and the surface layers are composed of a material containing a metal mainly composed of aluminum. The diamond particle content is 40-70% by volume of the entire aluminum-diamond composite.

Abstract: Technologies are generally described for methods, systems, and structures that include patterns formed by optical lithography. In some example methods, a photoresist layer is applied to a substrate, and a grapheme layer can be applied to the photoresist layer. Light can be applied through a mask to the graphene layer, where the mask includes a pattern. The light can form the pattern on the graphene layer such that the pattern forms on the photoresist layer.

Abstract: A black-coated steel sheet exhibits good bendability and a good appearance after press working is provided. Zinc based plating layers, a chromium-free chemical conversion coating disposed on the zinc based plating layer, and a colored single organic coating which is disposed on the chemical conversion coating and which contains a polyester resin having a hydroxyl value of 10 KOHmg/g or more, an imino-containing melamine resin, and 5 to 15 percent by mass of carbon black are included, wherein the glass transition temperature (Tg) of the organic coating is 40° C. or higher, the film thickness is 10 ?m or less, and the hardness is 200 N/mm2 or more.

Abstract: A method of assembling a metallic-graphite structure includes forming a wetted graphite subassembly by arranging one or more layers of graphite fiber material including a plurality of graphite fibers and applying a layer of metallization material to ends of the plurality of graphite fibers. At least one metallic substrate is secured to the wetted graphite subassembly via the layer of metallization material.

Abstract: A piston ring includes: a refined steel including: carbon C in a range of 0.20% mass to 0.90% mass, silicon Si in a range of 0.10% mass to less than 0.60% mass, manganese Mn in a range of 0.20% mass to 1.50% mass, chromium Cr in a range of 0.30% mass to 2.00% mass, and a remnant including: iron Fe, and an unavoidable impurity. A parameter A calculated from the following expression (1) based on contents of the Si, Mn and Cr is 9.0 or less: parameter A=8.8 Si+1.6 Mn+1.7 Cr—expression (1). A parameter B calculated from the following expression (2) based on contents of the C, Si, Mn and Cr is 10.8 or more: parameter B=36 C+4.2 Si+3.8 Mn+4.5 Cr—expression (2).

Abstract: Disclosed are a metal separator for fuel cells, which exhibits excellent properties in terms of corrosion resistance, electrical conductivity and durability, and a method of manufacturing the same. The metal separator for fuel cells includes a separator-shaped metal matrix and a coating layer formed on the metal matrix. The coating layer has a concentration gradient of a carbon element C and a metal element Me according to a thickness thereof such that the carbon element C becomes gradually concentrated in the coating layer with increasing distance from the metal matrix, and the metal element Me becomes gradually concentrated in the coating layer with decreasing distance from the metal matrix.

Abstract: A ceramic-metal composite includes a ceramic substrate, an active metal brazing alloy layer, and a metal plate bonded to the ceramic substrate through the active metal brazing alloy layer disposed therebetween. The active metal brazing alloy layer contains a transition metal that is at least one element selected from Group-8 elements specified in the periodic table. According to the above configuration, the following composite and device can be provided: the ceramic-metal composite that exhibits high bonding strength, heat cycle resistance, durability, and reliability even if the ceramic-metal composite is used in a power module and a semiconductor device including the ceramic-metal composite.

Abstract: A fastening mechanism includes a basic body made from a base metal, onto which at least one corrosion-resistant layer is applied. A further layer is applied at least partially onto the at least one corrosion-resistant layer. The further layer has a lower coefficient of friction than the at least one corrosion-resistant layer.

Abstract: The invention relates to a body with a substrate (1), an intermediate layer (2) applied on top thereof and a CVD diamond layer (3) applied to the intermediate layer. In order to propose a body coated with CVD diamond and a production process, in which the body has an increased load-bearing capacity under various mechanical loads, provision is made for the intermediate layer to be predominantly metallic, wherein the metal fraction of the intermediate layer consists predominantly of tungsten and/or chromium, and for the intermediate layer to have a roughness defined by an Rz value of 0.5 ?m-3.0 ?m.

Abstract: A metal plate or wire coated with a graphene layer and a method for manufacturing the graphene coated metal plate or wire are provided. The graphene coated metal plate or wire can include a nickel layer or a copper layer coated on an outer surface of the metal plate or wire, and a graphene layer coated on an outer surface of the nickel layer or the copper layer. The graphene coated metal plate or wire can be manufactured by using a chemical vapor deposition equipment or spraying a reduced graphene oxide (RGO) solution or a graphene oxide (GO) solution on the surface.

Abstract: Polycrystalline diamond compacts for use in artificial joints achieve reduced corrosion and improved biocompatibility through the use of solvent metal formulations containing tin and through the control of solvent metal pore size, particularly in inner layers of the compact. Solvent metal formulations containing tin have been discovered which provide sintering ability, part strength, and grind resistance comparable to levels achieved by using CoCrMo solvent metals. It has been discovered that limiting the solvent metal pore size in the diamond layers minimizes or eliminates the occurrence of micro cracks in the solvent metal and significantly reduces the corrosion of the compact as manifested by the release of heavy metal ions from the compact. Polycrystalline diamond compacts which utilize both the solvent metal formulations containing tin and the control of pore sizes achieve significantly reduced corrosion and improved biocompatibility compared to prior art polycrystalline diamond compacts.

Abstract: An article includes a substrate made of carbon fiber and zirconium diboride composites; an chromium layer deposited on the substrate; an chromium diffusing layer formed between the substrate and the chromium layer; and a iridium layer deposited on the chromium layer opposite to the chromium diffusing layer.

Abstract: Free standing articles or articles at least partially coated with substantially porosity free, fine-grained and/or amorphous Co-bearing metallic materials optionally containing solid particulates dispersed therein, are disclosed. The electrodeposited metallic layers and/or patches comprising Co provide, enhance or restore strength, wear and/or lubricity of substrates without reducing the fatigue performance compared to either uncoated or equivalent thickness chromium coated substrate. The fine-grained and/or amorphous metallic coatings comprising Co are particularly suited for articles exposed to thermal cycling, fatigue and other stresses and/or in applications requiring anti-microbial properties.

Abstract: Object is to provide a surface-treated copper foil free from chromium in the surface-treatment layer and excellent in peel strength of a circuit and chemical resistance against to degradation of the peel strength after processing into a printed wiring board. To achieve the object, the surface-treated copper foil having a surface-treatment layer on a bonding surface of a copper foil for manufacturing a copper-clad laminate by laminating it to an insulating resin substrate has the surface-treatment layer formed by depositing a metal component having high melting point not lower than 1400° C. by dry process film formation method to the bonding surface of the copper foil after the cleaning treatment and further depositing a carbon component to the surface.

Abstract: The present invention provides a battery or supercapacitor current collector which is prelithiated. The prelithiated current collector comprises: (a) an electrically conductive substrate having two opposed primary surfaces, and (b) a mixture layer of carbon (and/or other stabilizing element, such as B, Al, Ga, In, C, Si, Ge, Sn, Pb, As, Sb, Bi, Te, or a combination thereof) and lithium or lithium alloy coated on at least one of the primary surfaces, wherein lithium element is present in an amount of 1% to 99% by weight of the mixture layer. This current collector serves as an effective and safe lithium source for a wide variety of electrochemical energy storage cells, including the rechargeable lithium cell (e.g. lithium-metal, lithium-ion, lithium-sulfur, lithium-air, lithium-graphene, lithium-carbon, and lithium-carbon nanotube cell) and the lithium ion based supercapacitor cell (e.g, symmetric ultracapacitor, asymmetric ultracapacitor, hybrid supercapacitor-battery, or lithium-ion capacitor).

Abstract: The present disclosure relates to brazed coated diamond-containing materials and methods of producing brazed coated diamond-containing materials. The method for brazing the coated diamond-containing material may include bringing a braze metal into contact with the refractory metal layer and a substrate; heating at least the braze metal above the melting temperature of the braze metal; and bringing the braze metal into contact with the substrate to form a braze metal layer to join the diamond-containing material, braze metal layer, and substrate together. An advantage of the method may include that the brazing step may be performed in air, under ambient pressure, and without the need for a protective layer.

Abstract: The object of the present invention is to provide a slide member excellent in wear resistance and highly reliable over a long period by improving the adhesion property (anti-flaking property) of a diamond-like-carbon coating in the slide member including the diamond-like-carbon coating. The sliding member includes a substrate; and a diamond-like-carbon film including layers serially stacked in order of a first layer, a second layer and a hard carbon layer, in which the substrate is formed of an alloy steel containing at least one element selected from the group consisting of V, Cr, Nb, Mo, Ta and W, in which the first layer contains at least one element selected from the group consisting of V, Cr, Nb, Mo, Ta and W, and in which the first layer adheres to the substrate.

Abstract: A sliding member for a compressor includes a base metal, a first layer and a second layer. The base metal is made of an aluminum-based metal. The first layer is formed on or over the base metal and made of a nickel-based plating layer containing at least one material of nitrogen (N), silicon (Si), titanium (Ti), chromium (Cr) and aluminum (Al) as an additive. The second layer is formed on the surface of the first layer and made of a diamond-like carbon layer containing the same additive as the additive contained in the first layer.

Abstract: The present invention discloses a heat conductive composite substrate having heat dissipation properties and a manufacturing method thereof. The heat conductive composite substrate comprises a heat dissipation substrate and a metal diamond composite layer physically disposed on the heat dissipation substrate for passing heat energy to the heat dissipation substrate. The metal diamond composite layer is a growth substance including at least one kind metal, and the growth substance is distributed with plural diamond particles therein.

Abstract: An object of the present invention is to provide a copper foil with carrier sheet which permits releasing of the carrier sheet from the copper foil layer even when hot pressing at a temperature exceeding 300° C. is applied in the production of a printed wiring board. In order to achieve the object, a copper foil with physically releasable carrier sheet having a copper foil layer on the surface of the carrier sheet through a bonding interface layer, characterized in that the bonding interface layer is composed of a metal layer and a carbon layer. It is preferable for the bonding interface layer to be composed of a metal layer of 1 nm to 50 nm thick and a carbon layer of 1 nm to 20 nm thick.

Abstract: The present invention discloses corrosion and wear-resistant claddings comprising hard particles and an alloying addition dispersed in a nickel-based alloy matrix. The alloying addition comprises at least one of molybdenum or copper. The cladding does not include cobalt-bonded tungsten carbide particles.

Abstract: A diamond substrate having a contact, wherein the contact comprises a diamond-like-carbon (DLC) layer on at least part of a surface of the diamond substrate; and at least one metal layer on at least part of the surface of the DLC layer. Methods for producing the same and devices comprising such a substrate are also described.

Abstract: A rigid composite structure includes a tubular body made from a metallic material and having a first bore formed therein along a longitudinal axis, and one or more segments formed from a super hard material disposed within the first bore. Each segment has a hole formed in the center thereof, and the segments may be positioned end-to-end and adjacent to one another to align the center holes about the longitudinal axis and form a second bore. The segments can be held under compression within the first bore of the tubular body. The segments may be made of super hard materials such as natural diamond, synthetic diamond, polycrystalline diamond, single crystalline 10 diamond, cubic boron nitrate or other superhard composite materials which exhibit low thermal expansion rates and are generally chemically inert. The resultant rigid composite structure may possess higher tolerances to high pressures and high temperatures within the second bore.

Abstract: Object is to provide a surface-treated copper foil free from chromium in the surface-treatment layer and excellent in peel strength of a circuit and chemical resistance against to degradation of the peel strength after processing into a printed wiring board. To achieve the object, the surface-treated copper foil having a surface-treatment layer on a bonding surface of a copper foil for manufacturing a copper-clad laminate by laminating it to an insulating resin substrate has the surface-treatment layer formed by depositing a metal component having high melting point not lower than 1400° C. by dry process film formation method to the bonding surface of the copper foil after the cleaning treatment and further depositing a carbon component to the surface.

Abstract: A method for manufacturing composite bodies is provided by applying a firmly adhering layer to substrates composed of plastic or metal, particularly stainless steel, brass, aluminum, or zinc, it is provided that a layer composed of carbon is deposited on the substrate by means of chemical vapor deposition and a hard material layer is deposited on the carbon layer by means of physical vapor deposition.

Abstract: Disclosed is a method of assembling a metallic-graphite structure (10) including arranging one or more layers of graphite fiber material (12) and locating at least one metallic sheet (18) adjacent to the one or more layers of graphite fiber material (12). The at least one metallic sheet (18) is secured to the one or more layers of graphite fiber material (12) via brazing. Further disclosed is a metallic-graphite structure (10) including one or more layers of graphite fiber material (12) and at least one metallic sheet (18) located adjacent to the one or more layers of graphite fiber material (12). The at least one metallic sheet (18) is secured to the one or more layers of graphite fiber material (12) via brazing.

Abstract: Disclosed is an aluminum-diamond composite having both high thermal conductivity and thermal expansion coefficient close to those of semiconductor elements, which is improved in platability in the surface and surface roughness so that the composite becomes suitable for use as a heat sink of a semiconductor element of the like. Specifically disclosed is a plate-like aluminum-diamond composite containing diamond particles and a metal mainly composed of aluminum. The aluminum-diamond composite is composed of a composite part and surface layers formed on both sides of the composite part, and the surface layers are composed of a material containing a metal mainly composed of aluminum. The diamond particle content is 40-70% by volume of the entire aluminum-diamond composite.

Abstract: A component for use in a high vacuum environment, the component including a core of non-magnetic Hastelloy with a cladding of nickel-iron covering the core at least in part. The component can be, for example, at least one of a gate valve for use in a high vacuum environment of an electron gun, a bearing, a slide way, a gate valve bearing, a rotary slide, a linear slide, an electron beam column, and electron beam chamber, and a vacuum chamber. In this manner, because the final mechanical tolerance is controlled by machining instead of part assembling, extremely high alignment accuracy is obtained. The final part provides field shielding as provided by the nickel alloy shell, low stray field provided by the non-magnetic Hastelloy, good vacuum performance, and tight mechanical tolerance control. Also, because Hastelloy has the advantage of a low oxidation rate in comparison to stainless steel and titanium, there is less contamination buildup due to conditions such as electron beam bombardment.

Abstract: A nanostructured composite electrode is provided that includes a pair of conductive metal foils and a multiplicity of ordered nanostructures formed on each conductive metal foil. The ordered nanostructures include functionalized carbon multi-walled nanotubes electrophoretically deposited onto the metal foils. The ordered nanostructures also include synthesized nanoparticles electrophoretically deposited onto each of the carbon multi-walled nanotubes and the metal foils in proportion to the concentration of the carbon multi-walled nanotubes while in a stable colloidal suspension with the synthesized nanoparticles during electrophoretic deposition.

Abstract: A composite-plated article in which carbon nanofibers are used, and an adequate degree of strength is obtained thereby. Carbon nanofibers having microparticles bonded thereto are used. On reacting with carbon and forming a compound, the microparticles will be securely bonded to the carbon nanofibers, and a high-strength composite-plated article is obtained.

Abstract: A method of forming a well-anchored carbon nanotube (CNT) array, as well as thermal interfaces that make use of CNT arrays to provide very high thermal contact conductance. A thermal interface is formed between two bodies by depositing a continuous array of carbon nanotubes on a first of the bodies so that, on mating the bodies, the continuous array is between surface portions of the first and second bodies. The thermal interface preferably includes a multilayer anchoring structure that promotes anchoring of the continuous array of carbon nanotubes to the first body. The anchoring structure includes a titanium bond layer contacting the surface portion of the first body, and an outermost layer with nickel or iron catalytic particles from which the continuous array of carbon nanotubes are nucleated and grown. Additional thermal interface materials (TIM's) can be used in combination with the continuous array of carbon nanotubes.

Abstract: A highly corrosion-resistant member that is equipped with: a substrate made of stainless steel; an intermediate layer coated on at least a part of a surface of the substrate; and an amorphous carbon film coated on at least a part of a surface of the intermediate layer is completed by forming the intermediate layer and amorphous carbon film at such a low temperature that a temperature of the surface of the substrate is 450° C. or less. Another highly corrosion-resistant member that is equipped with: a substrate made of stainless steel, substrate whose superficial-layer portion is subjected to nitriding treatment; and an amorphous carbon film coated on at least a part of a surface of the superficial-layer portion is completed by carrying out the nitriding treatment and a formation of the amorphous carbon film at such a low temperature that a temperature of a surface of said substrate is 450° C. or less.

Abstract: The present invention relates to a magnesium-based composite material includes at least two magnesium-based metallic layers; and at least one magnesium-based composite layer respectively sandwiched by the at least two magnesium-based metallic layers. The present invention also relates to a method for fabricating a magnesium-based composite material, the method includes the steps of: (a) providing at least two magnesium-based plates; (b) providing a plurality of nanoscale reinforcements; (c) sandwiching the nanoscale reinforcements between the at least two magnesium-based plates to form a preform; and (d) hot pressing the preform to achieve the magnesium-based composite material.

Abstract: To provide a novel high strength polyethylene multifilament which consists of a plurality of filaments having high strengths and uniform internal structures, and showing a narrow variation in the strengths of the monofilaments, and which has been difficult to be provided by the conventional gel spinning method. A high strength polyethylene multifilament consisting of a plurality of filaments which are characterized in that the crystal size of monoclinic crystal is 9 nm or less; the stress Raman shift factor is ?5.0 cm?1/(cN/dTex) or more; the average strength is 20 CN/dTex or higher; the knot strength retention of each monofilament is 40% or higher; CV indicating a variation in the strengths of the monofilaments is 25% or lower; the elongation at break is from 2.5% inclusive to 6.0% inclusive; the fineness of each filament is 10 dTex or less; and the melting point of the filaments is 145° C. or higher.

Abstract: An exemplary embodiment discloses a thermoformed composite powder metallurgy based material including a matrix of sintered metal particles including at least one of a metal and metal alloy; and carbon fibers within said matrix having an orientation and shape derived from a precursor fibrous matte.

Abstract: The present invention relates to a magnesium-based composite material includes a magnesium-based metallic material, and at least one nanoscale reinforcement film disposed therein. The present invention also relates to a method for fabricating the above-described a magnesium-based composite material, the method includes the steps of: (a) providing at least two magnesium-based plates; (b) providing at least one nanoscale reinforcement film; (c) sandwiching the at least one nanoscale reinforcement film between the at least two magnesium-based plates to form a preform; and (d) hot rolling the preform to achieve the magnesium-based composite material.

Abstract: A composite body which can withstand high thermal stresses is formed by high-temperature soldering at least a part of a high-temperature-resistant, metallic or nonmetallic component and at least a part of a high-temperature-resistant, nonmetallic component. Prior to soldering, a metallic barrier layer, which is impervious to the solder melt, of one or more elements selected from the group consisting of V, Nb, Ta, Cr, Mo, W, Ti, Zr, Hf and alloys thereof, is deposited on that surface of each nonmetallic component which is to be soldered. Solder material, barrier layer and soldering conditions are adapted to one another in such a manner that during the soldering operation the metallic barrier layer remains at least partially in the solid state, so that after the soldering operation it is still present in a thickness of at least 10 ?m at least over the majority of the soldering surface.

Abstract: The selective growth of vertically aligned, highly dense carbon nanotube (CNT) arrays using a thermal catalytic chemical vapor deposition (CCVD) method via selection of the supporting layer where the thin catalyst layer is deposited on. A thin iron (Fe) catalyst deposited on a supporting layer of tantalum (Ta) yielded CCVD growth of the vertical dense CNT arrays. Cross-sectional transmission electron microscopy revealed a Vollmer-Weber mode of Fe island growth on Ta, with a small contact angle of the islands controlled by the relative surface energies of the supporting layer, the catalyst and their interface. The as-formed Fe island morphology promoted surface diffusion of carbon atoms seeding the growth of the CNTs from the catalyst surface.

Abstract: A contact surface. for electrical contacts may include an Ag layer deposited on a copper-based substrate using galvanic methods. The Ag layer includes finely dispersed graphite particles in a quantity of, e.g., 1 to 3 weight % of the Ag layer, the graphite particles having a length in the range of, e.g., 0.5 to 20 ?m.

Abstract: Multiple layers of nickel phosphorous coatings are formed by electroless plating onto a base metal substrate such as a turbine component. In one embodiment, a first nickel layer metallurgical bonded by a heat treatment process to a surface of the base metal substrate, the first nickel layer containing about 4 to about 6 weight percent phosphorous with the balance being essentially nickel; and a second nickel layer deposited onto the first layer, the second nickel layer containing about 8 to about 12 weight percent phosphorous with the balance being essentially nickel, wherein the first and second layers are formed by electroless plating. In this manner, adhesion is maximized without degrading the properties of the second layer such as corrosion resistance and ductility. Also disclosed are processes for forming the multilayered nickel phosphorus coatings.

Abstract: An electrical component includes a conductive substrate, a tin layer formed on the substrate, and a barrier coating formed on the tin layer to impede tin whisker growth. The barrier coating includes a polymer matrix, and abrasive particles that are dispersed about the matrix.

Abstract: A method of fabricating an interconnect structure is described. A substrate is provided. A patterned interfacial metallic layer is formed on the substrate. An amorphous carbon insulating layer or a carbon-based insulating layer is formed covering the substrate and the interfacial metallic layer. A conductive carbon line or plug is formed in the amorphous carbon or carbon-based insulating layer electrically connected with the interfacial metallic layer. An interconnect structure is also described, including a substrate, a patterned interfacial metallic layer on the substrate, an amorphous carbon insulating layer or a carbon-based insulating layer on the substrate, and a conductive carbon line or plug disposed in the amorphous carbon or carbon-based insulating layer and electrically connected with the interfacial metallic layer.

Abstract: An exemplary core insert includes a main body having a central protruding portion and a peripheral flange portion surrounding the central protruding portion, and a multilayer film formed on the central protruding portion. The multilayer film includes a nickel-phosphorus layer formed on the central protruding portion, a chromium layer formed on the nickel-phosphorus layer, a chromium nitride layer formed on the chromium layer, and a diamond-like carbon layer formed on the chromium nitride layer. The core insert has excellent hardness, good corrosion resistance, good wear resistance, high adhesion, and a long operational lifetime.

Abstract: The invention relates to a diamond electrode with synthetically produced, electrically conductive (doped) diamonds. The surface has diamond particles (5) embedded in a metal or metal alloy layer so as to produce a conductive connection to the metal or metal alloy.

Abstract: A heat conductor that improves heat conductivity is provided. The heat conductor has a first heat conductive region and a second heat conductive region. The first heat conductive region is configured by lamination of a first metal member and a graphite member. The second heat conductive region is configured by lamination of the first metal member and a second metal member.

Abstract: In order to produce a wire electrode having a core consisting of a copper/zinc alloy and to produce a specific sheath layer, the sheath layer is coated onto the core at a temperature at which no diffusion occurs. The wire electrode is subsequently heated at a heating speed higher than 10° C. per second, briefly annealed at temperatures above 500° C. and subsequently cooled again very rapidly at cooling speeds higher than 10° C. per second.