Free Carbon Containing Component Patents (Class 428/634)
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Patent number: 4863809Abstract: An etching and fluorinating treatment is disclosed for modifying the surface properties of magnetic data storage media and sliders for magnetic data transducing heads. Media enclosed within a plasma chamber is first exposed to an argon plasma for cleaning, then exposed to a plasma mixture including argon with either fluorine or carbon tetrafluoride, maintained at a pressure of approximately half of atmospheric pressure, at a temperature of about 100.degree. C. An electrical field is generated for forming argon, carbon and fluorine ions. The argon ions etch the carbon overcoat of the disc, while the carbon and fluorine ions combine with the carbon to form extended chain fluoropolymers, and also penetrate the carbon layer. Sliders are treated in a plasma mixture of argon and CF.sub.4. During such treatment, carbon and fluorine ions penetrate exposed surface areas of the slider, and form a reaction product of solid lubricant film.Type: GrantFiled: March 10, 1988Date of Patent: September 5, 1989Assignee: Magnetic Peripherals, Inc.Inventors: Amarjit S. Brar, Jagdish P. Sharma
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Patent number: 4859541Abstract: A safe having a wall comprising spaced steel plates, a sheathing layer between the plates consisting of hard non-metallic grains of e.g., boron carbide, silicon carbide, boron nitride, diamonds, ceramic oxides and hard metallic grains of e.g., cast iron, metal carbides, nitrides, borides, and silicides, said grains being bound together and to said plates by a hard solder mass having a copper or nickel base. The sheathing layer contains 30-70% by volume of said non-metallic grains (having a grain size of 5 to 20 mm) and metallic grains (having a grain size of 1 to 6 mm) and from 70% to 30% of said hard solder. The ratio of said non-metallic to said metallic grains is 2-4 parts to 1 part by volume. A method for making the sheathing layer is also disclosed.Type: GrantFiled: February 3, 1987Date of Patent: August 22, 1989Assignees: Metallgesellschaft AG, Bode Panzer AktiengesellschaftInventors: Heinz Maxeiner, Gerhard Kruske, Hartwig Reimann
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Patent number: 4853294Abstract: An improved metal, alloy, or intermetallic matrix composite containing carbon reinforcing fibers is formed. The carbon reinforcing fibers are protected from interaction with the matrix material by an inner and an outer barrier layer. The outer layer is any one of the group of stable, non-reactive ceramic materials used to protect fibers, and the inner layer is a ductile, low density, oxygen desorbing rare earth metal. The carbon fibers are particularly useful in forming composites with a titanium aluminide matrix.Type: GrantFiled: June 28, 1988Date of Patent: August 1, 1989Assignee: United States of America as represented by the Secretary of the NavyInventors: Richard K. Everett, William F. Henshaw
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Patent number: 4847168Abstract: A slicing saw blade comprising a substrate disc and a blade edge consisting essentially of a ultra-hard material deposited along a peripheral edge of said substrate disc, said substrate disc being made of a steel consisting essentially of, by weight, not more than 0.10% of C, more than 1.0% but not more than 3.0% of Si, less than 0.5% of Mn, from 4.0% to 8.0% of Ni, from 12.0% of 18.0% of Cr, from 0.5% to 3.5% of Cu, not more than 0.15% of N and not more than 0.004% of S, the sum of C and N being at least 0.10%, the balance being Fe and inavoidable impurities. The saw blade is useful for the production of wafers of a semiconductive material, and has a long service life.Type: GrantFiled: December 19, 1987Date of Patent: July 11, 1989Assignee: Nisshin Steel Co., Ltd.Inventors: Sadao Hirotsu, Kazuo Hoshino, Sadayuki Nakamura
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Patent number: 4847883Abstract: The present invention concerns a support of carbonaceous material for a rotary target of X-ray tubes. The support is formed of two parts which are fixed with respect to each other, one part being of a carbon/carbon composite which provides mechanical strength and the other part being of polycrystalline graphite for receiving a refractory metal, by virtue of its coefficient of expansion. A thermal contact is provided between the two parts. The invention is especially applicable to targets of X-ray tubes which rotate at a high speed, 20,000 RPM and above.Type: GrantFiled: January 27, 1987Date of Patent: July 11, 1989Assignee: Le Carbone LorraineInventor: Jacques Fourre
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Patent number: 4842945Abstract: A stainless steel with black transparent appearance suitable for use as a decorative architectural material. The stainless steel material has a stainless steel substrate and a thin graphite film formed on the substrate, the thin graphite film having a thickness not greater than 1 .mu.m and containing 10 to 75 wt % of carbon existing in a state of diamond. This stainless steel material is produced by chemical vapor deposition process making use of a capacitance-coupled type high-frequency plasma, having the steps of preparing a stainless steel material as a substrate; placing the substrate in an atmosphere of a mixture gas which contains both hydrogen gas and an inert gas together with a hydrocarbon gas; and causing a reaction by applying a D.C. voltage of 100 to 600 V using the substrate as a cathode; thereby forming, on the substrate, a thin graphite film having a thickness not greater than 1 .mu.m and containing 10 to 75 wt % of carbon existing in a state of diamond.Type: GrantFiled: May 26, 1987Date of Patent: June 27, 1989Assignee: Nippon Steel CorporationInventors: Wataru Ito, Satoshi Ito
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Patent number: 4772111Abstract: An optical mirror in which a mirror surface formation material, e.g. aluminum, is coated on a substrate consisting of a c/c composite and having a predetermined shape. The coated mirror surface formation material layer is ultrahigh precision machined to a small thickness such that its deformation is suppressed by the substrate.Type: GrantFiled: March 30, 1987Date of Patent: September 20, 1988Assignees: Agency of Industrial Science & Technology, Ministry of International Trade & IndustryInventors: Hirofumi Shimura, Yuji Enomoto, Yusei Noguchi, Yoshitaka Tatsue, Hidenori Shinno
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Patent number: 4772514Abstract: A protective layer for carbonaceous materials, especially graphite electrodes, applied by plasma-coating method comprised of 65-98 .sup.w /o of metal aluminum, 1-20 .sup.w /o of combined metal silicon with silica (SiO.sub.l) and up to 15 .sup.w /o of oxygenous compounds of aluminum. The resistivity of the layer is 0.07.10.sup.-6 ohm.m up to 0.3.10.sup.-6 ohm.m at 20.degree. C. and 0.12.10.sup.-6 ohm.m up to 0.7.10.sup.-6 ohm.m at 400.degree. C.The method of producing the protective layer comprises the following steps of directing a plasma flame of a water stabilized plasma burner toward the carbonaceous material, and feeding into a plasma flame a particulate composition comprising between about 85 .sup.w /o to about 99 .sup.w /o of metallic aluminum having a particle size of between about 0.09 to about 0.180 mm and between about 1 to about 15 .sup.w /o of silicon having a particle size of between about 0.07 to about 0.165 mm.Type: GrantFiled: February 26, 1987Date of Patent: September 20, 1988Assignee: Ceskoslovenska akademie vedInventors: Karel Neufuss, Ales Macku, Antonin Forejt, Pavel Kasik
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Patent number: 4766040Abstract: Temperature resistant abrasive polycrystalline diamond bodies are described, intended for use as tools in various mechanical operations like turning, milling, drilling, sawing and drawing, having different additions, i.e. amount and composition, of binding, fluxing, catalyst metals at different distances from the working surface. Preferably the metal concentration of the polycrystalline diamond body is decreasing towards the working surface while the metal composition is varied in a way that gives a mechanically stiffer matrix that also has a lower thermal expansion.In one embodiment the diamond body is high pressure-high temperature-bonded to a supporting body, e.g. of cemented carbide, in order to facilitate the clamping of the tool. In another embodiment the diamond body is brazed to a supporting body or used in a surface-set rock drill bit, i.e. held by a braze metal.Type: GrantFiled: June 26, 1987Date of Patent: August 23, 1988Assignee: Sandvik AktiebolagInventors: Lars H. Hillert, Mats G. Waldenstrom
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Patent number: 4753852Abstract: A magnetic recording medium for high density recording comprising a non-magnetic substrate, a Cr undercoat and a magnetic Ni-Cr-Co alloy thin layer formed on the substrate. The magnetic alloy thin layer has a thickness of from 400 to 1200 angstrom and a Cr content of from 3 to 17 atomic percent. As a result, improved magnetic characteristics and corrosion resistance of the medium are ensured.Type: GrantFiled: March 21, 1986Date of Patent: June 28, 1988Assignee: Victor Company of Japan, Ltd.Inventors: Makoto Mizukami, Toshio Kato, Toshikazu Nishihara, Toshiro Abe, Akihiro Kimura
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Patent number: 4686150Abstract: An antenna reflector comprising a face skin of graphite fiber reinforced epoxy (GFRE) material is coated with a layer of chromium. The chromium is then coated with aluminum and a protective coating of silicon dioxide is then deposited over the aluminum. The chromium has a thickness sufficiently thin to provide good coverage of the pores of the GFRE material and to minimize distortion causing poor bond due to differences in the coefficient of thermal expansion of the different materials in the presence of temperature cycles. The aluminum is sufficiently thick to provide good reflecting characteristics to minimize the polarizing effects of the graphite face skins.Type: GrantFiled: January 17, 1986Date of Patent: August 11, 1987Assignee: RCA CorporationInventors: Eric Talley, Raj N. Gounder
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Patent number: 4686080Abstract: A composite compact component made of a composite compact consisting of a diamond or BN powder bonded to a hard sintered alloy base during a sintering operation, and a substrate composed of steel or a hard sintered alloy bonded to the base of the composite compact through a high strength filler metal or alloy having a melting point of at least the liquidus point of the hard sintered alloy base. A process of making set composite compact component is also disclosed as well as a drill bit containing said composite compact component and variations thereof.Type: GrantFiled: December 9, 1985Date of Patent: August 11, 1987Assignee: Sumitomo Electric Industries, Ltd.Inventors: Akira Hara, Masaya Miyake, Shuji Yazu
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Patent number: 4677032Abstract: A thin film metal alloy medium for vertical recording has a magnetic film structure of individual films, each film being made up of a non-magnetic layer and a magnetic layer. In a preferred embodiment of the medium, each of the layers is a cobalt-chromium-tantalum (CoCrTa) alloy, the tantalum concentration being varied in the different layers in order to provide either the non-magnetic or the magnetic properties to the layers. The medium also includes a soft magnetic underlayer film structure between the substrate and the magnetic film structure to provide a magnetic flux return path. Each film in the underlayer film structure comprises a CoCrTa non-magnetic layer and a CoCrTa magnetic layer, each magnetic layer being sufficiently thin such that the underlayer film structure exhibits in-plane magnetization with no perpendicular magnetic anisotropy.Type: GrantFiled: September 23, 1985Date of Patent: June 30, 1987Assignee: International Business Machines CorporationInventor: Clifford J. Robinson
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Patent number: 4654276Abstract: An improved cobalt-platinum (CoPt) thin film metal alloy media for horizontal magnetic recording has a coercivity substantially greater than prior CoPt thin film metal alloy media. A tungsten underlayer between the substrate and the CoPt magnetic layer improves the coercivity above that of media wiht conventional underlayers, such as chromium. The coercivity of the CoPt layer can be increased even further if the CoPt film is deposited in such a manner as to form an intermetallic compound of Co.sub.3 W in the interface region between the tungsten underlayer and the CoPt magnetic layer. The tungsten underlayer also improves the magnetic properties of the media when the magnetic layer is an alloy of cobalt-platinum-chromium (CoPtCr).Type: GrantFiled: April 29, 1986Date of Patent: March 31, 1987Assignee: International Business Machines CorporationInventors: Richard H. Ahlert, James K. Howard, Grace S. Lim
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Patent number: 4652499Abstract: An improved cobalt-platinum (CoPt) thin film metal alloy media for horizontal magnetic recording has a squareness greater than prior CoPt thin film metal alloy media. An underlayer of a body-centered-cubic (BCC) chromium-based alloy with a lattice cell constant greater than chromium (Cr), such as chromium-vanadium (CrV), is formed between the substate and the CoPt magnetic layer. The underlayer also improves the magnetic properties of the media when the magnetic layer is an alloy of cobalt-platinum-chromium (CoPtCr).Type: GrantFiled: April 29, 1986Date of Patent: March 24, 1987Assignee: International Business MachinesInventor: James K. Howard
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Patent number: 4605343Abstract: A sintered polycrystalline diamond compact having an integral metallic heat sink bonded to and covering at least the outer diamond surface is used to increase compact life when the compact is used for material removal without a fluid coolant.Type: GrantFiled: September 20, 1984Date of Patent: August 12, 1986Assignee: General Electric CompanyInventors: Louis E. Hibbs, Jr., George C. Sogoian
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Patent number: 4504553Abstract: An infrared radiation reflecting substrate, having deposited thereon a first layer formed from a metal or an alloy, and a second layer deposited on the first layer and consisting of a solar radiation absorbing amorphous material, such as amorphous carbon. The substrate can be formed from an infrared radiation reflecting layer deposited on a primary substrate.Type: GrantFiled: March 30, 1983Date of Patent: March 12, 1985Assignee: Commissariat a l'Energie AtomiqueInventors: Andre Aubert, Jean Valignat, Christophe Wyon
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Patent number: 4503125Abstract: A protective overcoating is disclosed for a magnetic alloy thin-film recording disc that includes a magnetic alloy film formed on a disc-shaped substrate or coated substrate. The protective overcoating is formed by first sputtering onto the magnetic medium an interfacial layer of titanium, and then sputtering onto the titanium a layer of carbon. The sputtered carbon provides wear-resisting lubricity, while the titanium interface promotes the adhesion of the sputtered carbon to the magnetic medium of the recording disc.Type: GrantFiled: June 5, 1981Date of Patent: March 5, 1985Assignee: Xebec, Inc.Inventors: Carl W. Nelson, Michael B. Vye
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Patent number: 4419389Abstract: A method for manufacturing a composite material which includes carbon material in a matrix metal by first applying tetraisopropyltitanate to the carbon material so as to wet it, next drying the carbon material which is wetted with the tetraisopropyltitanate, and then combining the carbon material with the matrix metal. This drying may be done by heating up the carbon material which is wetted with the tetraisopropyltitanate to a temperature of 50.degree. C. to 200.degree. C. in the atmosphere. The tetraisopropyltitanate may be dissolved in ethanol when it is being applied to the carbon material. The matrix metal may be a metal selected from the group consisting of aluminum, magnesium, aluminum alloy, and magnesium alloy.Type: GrantFiled: August 30, 1982Date of Patent: December 6, 1983Assignees: Toray Industries, Toyota Jidosha Kabushiki KaishaInventors: Tadashi Donomoto, Atsuo Tanaka, Masahiro Okada, Atsushi Kitamura, Tetsuyuki Kyono
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Patent number: 4411963Abstract: A thin film of magnetic recording material is sputter deposited over a base layer of gold and tantalum on a polished substrate. A protective layer of gold and tantalum is deposited overlaying the magnetic recording film. A solid lubricant layer such as carbon, preferably in the form of graphite, gold, silver, tin, molybdenum disulfide, and tungsten disulfide is sputter deposited or ion plated over the protective layer to reduce wear. The recording contacting portion of the recording head is similarly coated with a solid lubricant material. Other suitable protective materials include tantalum, niobium, tungsten and nitrides and carbides of such metals. In a preferred method for making such recording members, the layers are successively sputter deposited in an evacuated sputter chamber, whereby the recording layers and protective coatings are formed in a continuous process requiring only one pump down.Type: GrantFiled: July 6, 1981Date of Patent: October 25, 1983Inventor: Harry E. Aine
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Patent number: 4400442Abstract: There are provided fiber reinforced structures formed of one or more layers of reinforcing fibers contained in an electroformed, superplastic, nickel-cobalt matrix.Type: GrantFiled: July 13, 1981Date of Patent: August 23, 1983Assignee: Rockwell International CorporationInventors: Jack R. Lewis, Robert J. Walter
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Patent number: 4374900Abstract: The present invention relates to a composite diamond compact for a wire drawing die, in which a part or all of the circumference of a diamond sintered body is surrounded by a cermet consisting of a hard compound of (Mo, W)C type carbide crystals containing molybdenum as a predominant component, bonded by an iron group metal, and the binder phase of the diamond sintered body contains an iron group metal and fine carbide crystals containing molybdenum as a predominant component.Type: GrantFiled: June 29, 1979Date of Patent: February 22, 1983Assignee: Sumitomo Electric Industry, Ltd.Inventors: Akio Hara, Shuji Yazu
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Patent number: 4358923Abstract: Disclosed are processes and articles for composite electroless coatings comprising at least two distinct layers, the first layer comprising a metal and/or a metal alloy plus particulate matter and the second layer comprising a metal and/or a metal alloy and being substantially free of particulate matter.Type: GrantFiled: November 14, 1980Date of Patent: November 16, 1982Assignee: Surface Technology, Inc.Inventor: Nathan Feldstein
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Patent number: 4358922Abstract: Disclosed are processes and articles for composite electroless coatings comprising at least two distinct layers, the first layer comprising a metal and/or a metal alloy plus particulate matter and the second layer comprising a metal and/or a metal alloy and being substantially free of particulate matter.Type: GrantFiled: April 10, 1980Date of Patent: November 16, 1982Assignee: Surface Technology, Inc.Inventor: Nathan Feldstein
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Patent number: 4358506Abstract: As an article for manufacture, a tin, lead, indium, alloys of each with a carbide or carbonyl former in an admixture for forming said tin, lead and indium, wettable graphite composites which will not dewet upon heating; methods for preparing the composites of various shapes, layers, coatings, and sandwiches, of alloys, preforms and metal-graphite etc, structures are also disclosed.Type: GrantFiled: October 24, 1980Date of Patent: November 9, 1982Inventors: Josef Intrater, Gene Bertoldo
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Patent number: 4341823Abstract: The present invention comprises a process of preparing metal matrix composites which are reinforced by ceramic or graphite fibers, wherein the fibers are pretreated; first by a nickel coating, then by a second coating which is sacrificed when the fibers are ultimately immersed in a liquid metallic bath which becomes the matrix of the composite material formed. Usually the second coating is copper.In addition, a third coating on the fibers comprising a noble metal such as silver may also be used for certain matrix metal materials. Preferably the thickness of the nickel coating is a minimum of 0.5 micrometers and the second sacrificial coating is a minimum of 0.5 micrometers. After the fibers have been coated with the two or more successive coatings, they are incorporated into a metal matrix composite material by immersion in a molten bath of the desired matrix metal, or by placing the fibers in a suitable mold and casting the molten metal matrix around them, or by other suitable means.Type: GrantFiled: January 14, 1981Date of Patent: July 27, 1982Assignee: Material Concepts, Inc.Inventors: Richard W. Sexton, David M. Goddard
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Patent number: 4226917Abstract: A composite joint system is disclosed in which a composite structure containing carbon fibers embedded in a copper matrix in any configuration, e.g. in one direction, in random directions, in mesh form, spirally or radially is joined to another structure through a brazing material such as solder, Al brazer or Ag brazer. A film of metal such as Ni, Cr, Mo, W, Ta, Ti, Zr, V, an alloy of one or some of such metals, or the combination of some thereof is interposed between the composite structure and the brazing material. The metal film has a good wettability to both the composite structure material and the brazing material.Type: GrantFiled: April 12, 1978Date of Patent: October 7, 1980Assignee: Hitachi, Ltd.Inventors: Masao Tsuruoka, Hideyuki Yagi, Keiichi Morita, Keiichi Kuniya
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Patent number: 4223075Abstract: Metals constituting the matrix of carbon (graphite) filament reinforced composites are alloyed with titanium and boron to prevent or reduce the migration of the titanium-boron coating applied to the filaments prior to their impregnation with the metal matrix materials.Type: GrantFiled: January 21, 1977Date of Patent: September 16, 1980Assignee: The Aerospace CorporationInventors: William C. Harrigan, Jr., Robert H. Flowers, Silas P. Hudson
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Patent number: 4215180Abstract: An oxide-coated cathode for electron tubes which comprises a base metal plate made of an alloy comprising nickel as a main component and 2% by weight or more of at least one high-melting point metal, an oxide layer coated on the base metal plate comprising at least one oxide of a reducing element, a carbon coating layer coated on the oxide layer, and an alkaline earth oxide layer capable of emitting electrons coated on the carbon coating layer can maintain electron emitting life for a long period of time due to the prevention of interfacial reaction between the base metal plate and the alkaline earth oxide layer by the oxide layer and the carbon coating layer.Type: GrantFiled: January 18, 1979Date of Patent: July 29, 1980Assignee: Hitachi, Ltd.Inventors: Akira Misumi, Yukio Suzuki, Kazuo Sunahara
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Patent number: RE32464Abstract: A thin film of magnetic recording material is sputter deposited over a base layer of gold and tantalum on a polished substrate. A protective layer of gold and tantalum is deposited overlaying the magnetic recording film. A solid lubricant layer such as carbon, preferably in the form of graphite, gold, silver, tin, molybdenum disulfide, and tungsten disulfide is sputter deposited or ion plated over the protective layer to reduce wear. The recording contacting portion of the recording head is similarly coated with a solid lubricant material. Other suitable protective materials include tantalum, niobium, tungsten and nitrides and carbides of such metals. In a preferred method for making such recording members, the layers are successively sputter deposited in an evacuated sputter chamber, whereby the recording layers and protective coatings are formed in a continuous process requiring only one pump down.Type: GrantFiled: April 16, 1986Date of Patent: July 28, 1987Inventor: Harry E. Aine