By Coalescing Or Aggregating Patents (Class 430/137.14)
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Publication number: 20110136058Abstract: A method of making toner particles, including: mixing, at less than about 17° C. and without homogenizing, a resin emulsion with a coagulant, a colorant, an optional wax, and optional additives, to form pre-aggregated particles in a slurry; heating the slurry to form aggregated toner particles; freezing aggregation of the particles in the slurry once at a desired aggregated particle size; and further heating the aggregated particles in the slurry to coalesce the aggregated particles into toner particles.Type: ApplicationFiled: December 3, 2009Publication date: June 9, 2011Applicant: XEROX CORPORATIONInventors: Kimberly D. NOSELLA, Tie Hwee NG, Allan K. CHEN, Abdisamed SHEIK-QASIM, David KURCEBA, Shigang QIU, Santiago FAUCHER
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Publication number: 20110136059Abstract: A method of manufacturing a double emulsion with narrow dispersed phase particle size distribution comprising: providing an organic phase comprising solid hydrocolloid particles dispersed in an organic solvent; and dispersing the organic phase in an aqueous phase in the presence of a controlled amount of stabilizing agent to form an emulsion of droplets of the organic phase dispersed in the external aqueous phase, wherein the hydrocolloid particles in the organic phase droplets are swelled with water from the external aqueous phase to form internal droplets of an aqueous phase in the organic phase droplets, thereby forming a double emulsion comprising droplets of the organic phase of controlled narrow particle size distribution in the external aqueous phase, where the organic phase droplets contain internal droplets of an aqueous phase.Type: ApplicationFiled: December 3, 2009Publication date: June 9, 2011Inventor: Xiqiang Yang
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Patent number: 7955774Abstract: An electrostatic image developing toner comprising a non-crystalline polyester resin, wherein the non-crystalline polyester resin is obtained by copolymerizing monomers in the presence of a titanium catalyst; the monomers comprise a polyhydric alcohol component and a monomer containing a sulfonic acid group, the polyhydric alcohol component comprises a propylene oxide adduct of bisphenol A, a ratio of an amount of the monomer containing a sulfonic acid group to the total amount of the non-crystalline polyester resin is 0.1 mol % to 20 mol %, and a content of titanium is 1 ppm to 1000 ppm by weight based on the amount of the resin. The invention also provides a method for producing the same, an electrostatic image developer and image forming method using the toner.Type: GrantFiled: December 8, 2005Date of Patent: June 7, 2011Assignee: Fuji Xerox Co., Ltd.Inventors: Hideo Maehata, Susumu Yoshino, Noriyuki Mizutani, Satoshi Yoshida
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Publication number: 20110129774Abstract: A process for making a resin emulsion suitable for use in forming toner particles including an oil component incorporated into the latex core of the toner particles.Type: ApplicationFiled: December 2, 2009Publication date: June 2, 2011Applicant: XEROX CORPORATIONInventors: Valerie M. Farrugia, Kimberly D. Nosella, Edward Graham Zwartz, Barkev Keoshkerian
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Publication number: 20110129773Abstract: A toner including a binder resin comprising a modified polyester having an ester bond and a chemical bond other than the ester bond, and a crystalline polyester; and a release agent comprising a microcrystalline wax comprising a hydrocarbon having 20 to 80 carbon atoms which comprises 55 to 70% by weight of a linear hydrocarbon. The microcrystalline wax has an acid value of from 0.1 to 20 mgKOH/g and a melting point of from 65 to 90° C. The melting point is a temperature at which a local maximum endothermic peak is observed in a differential thermal curve measured by differential scanning calorimetry (DSC). The release agent is dispersed in the toner with a dispersion diameter of from 0.06 to 1.50 ?m.Type: ApplicationFiled: November 3, 2010Publication date: June 2, 2011Inventors: Hyo SHU, Fumihiro Sasaki, Hiroshi Yamashita, Masaki Watanabe, Junichi Awamura, Tsuyoshi Sugimoto, Teruki Kusahara, Satoshi Ogawa, Ryota Inoue, Daisuke Inoue
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Patent number: 7951519Abstract: A toner for development of an electrostatic image includes at least a crystalline polyester resin and a colorant. The toner shows a dielectric loss index ?? of 0.1 or less at 0.1 Hz and 500 V at 30° C. and 90% RH.Type: GrantFiled: March 20, 2008Date of Patent: May 31, 2011Assignee: Fuji Xerox Co., Ltd.Inventors: Eisuke Iwazaki, Shuji Sato, Atsushi Sugawara, Hiroshi Nakazawa
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Publication number: 20110123917Abstract: In the present invention, provided is a toner suitable for fixing at low temperature, which exhibits excellent performance against thermal stress as well as mechanical stress with no generation of blocking even during storage for a long duration in an unused state, and also with no generation of tacking of toner images after fixing. Also disclosed is a toner comprising at least a binder resin, a colorant and a wax, the toner comprising a fatty acid ester wax comprising a hydroxyl group, and an aliphatic alcohol.Type: ApplicationFiled: September 11, 2009Publication date: May 26, 2011Applicant: KONICA MINOLTA BUSINESS TECHNOLOGIES, INC.Inventors: Kenji Hayashi, Mikio Kouyama, Hiroaki Obata, Noriyuki Kimpara, Hiroshi Nagasawa
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Publication number: 20110123916Abstract: A decolorable electrophotographic toner, containing a color former compound, a color developing agent, a binder resin, and a release agent, wherein the toner has a pH of from 6 to 9 when dispersed in water with a pH of from 5.5 to 7 at a mass ratio of toner/water of 1/10.Type: ApplicationFiled: November 22, 2010Publication date: May 26, 2011Applicant: TOSHIBA TEC KABUSHIKI KAISHAInventor: Satoshi Araki
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Publication number: 20110123919Abstract: A decolorable electrophotographic toner, which is produced by forming a coloring agent that imparts a color to the toner by heating a leuco dye and a color development and erasure controlling agent having a color developable structure that develops a color by reacting with the leuco dye and also having a decolorable structure that erases the color by inhibiting the contact of the leuco dye with the color developable structure in a dispersion liquid, thereby developing a color, pulverizing the coloring agent in the dispersion liquid by a high-pressure pulverization method, obtaining coloring agent particles maintained in a color developed state by cooling the pulverized coloring agent in the dispersion liquid to a temperature lower than the melting initiation temperature of the color development and erasure controlling agent at a cooling rate at which the color development and erasure controlling agent is not crystallized, and aggregating and fusing the coloring agent particles, binder resin particles, and relType: ApplicationFiled: November 5, 2010Publication date: May 26, 2011Applicant: TOSHIBA TEC KABUSHIKI KAISHAInventor: Takashi Urabe
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Publication number: 20110123923Abstract: A method for producing a decolorable toner comprising: forming particles containing a color former compound, a color developing agent, and a binder resin; forming first aggregated particles by aggregating and fusing the particles containing the color former compound, the color developing agent, and the binder resin in a dispersion medium; and forming second aggregated particles by aggregating and fusing the first aggregated particles and a binder resin in a dispersion medium.Type: ApplicationFiled: November 19, 2010Publication date: May 26, 2011Applicant: TOSHIBA TEC KABUSHIKI KAISHAInventor: Masahiro Ikuta
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Publication number: 20110117486Abstract: The present disclosure provides polyesters suitable for use in forming toners. In embodiments, a polyester may be subjected to phase inversion emulsification, in which charge control agents are added so that the polyester emulsion includes charge control agents therein. The resulting polyester emulsion with charge control agents may then be utilized to form toner particles.Type: ApplicationFiled: November 16, 2009Publication date: May 19, 2011Applicant: XEROX CORPORATIONInventors: Robert D. Bayley, Yuhua Tong, Timothy L. Lincoln, Grazyna Kmiecik-Lawrynowicz, Maura A. Sweeney
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Patent number: 7943283Abstract: Processes for producing toner are provided which utilize reactive coalescing agents in forming the toner particles, as well as toners produced by such processes.Type: GrantFiled: December 20, 2006Date of Patent: May 17, 2011Assignee: Xerox CorporationInventors: Zhen Lai, Yuhua Tong, Christopher M. Wolfe, Chieh-Min Cheng
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Patent number: 7939236Abstract: The present disclosure relates to chemically processed toner that makes use of aqueous dispersions of release agent and/or pigment and solutions of a polymeric resin binder. The polymer solution may be prepared in an organic solvent wherein the organic solvent has some level of solubility in water. The polymer solution may then be combined with an aqueous dispersion of pigment and/or release agent which dispersions may include an aqueous polyelectrolyte and/or an aqueous dispersion of colloidal particles. This may be followed by agglomerating and forming particles of toner of a desired number and/or volume average particle size and/or degree of circularity.Type: GrantFiled: February 22, 2007Date of Patent: May 10, 2011Assignee: Lexmark International, Inc.Inventors: Bradley Leonard Beach, Jing X. Sun
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Patent number: 7939237Abstract: A method for making toners to include clay composites. The clay composites are incorporated into emulsion of toner and used in making toner via emulsion aggregation. Such toners may have a core and/or a shell and the clay composites may be included with the core, the shell or both.Type: GrantFiled: August 17, 2007Date of Patent: May 10, 2011Assignee: Xerox CorporationInventors: Maria N. V. McDougall, Richard P. N. Veregin, Guerino G. Sacripante, Valerie M. Farrugia
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Publication number: 20110104604Abstract: Disclosed is a manufacturing method of a toner including a vinyl series resin being a polymer of a radical polymerizable monomer, and a coloring agent, the method comprising: dispersing a crystalline organic compound having an unsaturated bond in an aqueous medium to prepare a dispersion liquid of the crystalline organic compound; causing a radical polymerization reaction between an unsaturated bond part of the crystalline organic compound and the radical polymerizable monomer after adding the radical polymerizable monomer to the dispersion liquid of the crystalline organic compound, to prepare a dispersion liquid of resin particles including the obtained polymer; and mixing at least the dispersion liquid of the resin particles and a dispersion liquid of coloring agent particles, and aggregating the resin particles and the coloring agent particles to form toner particles.Type: ApplicationFiled: November 1, 2010Publication date: May 5, 2011Applicant: KONICA MINOLTA BUSINESS TECHNOLOGIES, INC.Inventors: Kenji HAYASHI, Hiroaki OBATA, Yukio HOSOYA, Kouji SHIBATA, Mikio KOUYAMA
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Publication number: 20110104609Abstract: The present disclosure provides processes for producing resins suitable for use in forming toner compositions. In embodiments, the processes described herein comprise formation of latexes, including latexes for use in toners, produced without use of solvents.Type: ApplicationFiled: November 2, 2009Publication date: May 5, 2011Applicant: XEROX CORPORATIONInventors: Shigang QIU, Santiago FAUCHER, John ABATE, Allan CHEN, Ke ZHOU
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Publication number: 20110097665Abstract: A method of making toner particles, including cold homogenizing at a temperature below room temperature a resin emulsion, a colorant, an optional wax, and optional additives with a coagulant to form a toner slurry; heating the toner slurry to form aggregated toner particles; freezing aggregation of the particles in the slurry once at a desired aggregated particle size; and further heating the aggregated particles in the slurry to coalesce the aggregated particles into toner particles.Type: ApplicationFiled: October 22, 2009Publication date: April 28, 2011Applicant: XEROX CORPORATIONInventors: Kimberly D. Nosella, Tie Hwee Ng, Allan K. Chen, Abdisamed Sheik-Qasim, Melanie L. Davis
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Publication number: 20110097664Abstract: A method of making toner particles, including mixing at least one emulsion of at least one resin, a colorant, an optional wax, and optional additives to form a slurry; heating the slurry to form aggregated particles in the slurry; freezing aggregation of the particles with a buffer solution; and heating the aggregated particles in the slurry to coalesce the particles into toner particles.Type: ApplicationFiled: October 22, 2009Publication date: April 28, 2011Applicant: XEROX CORPORATIONInventors: Kimberly D. NOSELLA, Allan K. Chen, Abdisamed SHEIK-QASIM, Melanie L. DAVIS, Zhen LAI
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Patent number: 7932010Abstract: There are provided a toner, a method of manufacturing the toner, a two-component developer, a developing device, and an image forming apparatus, which are excellent in a charge rising property, environmental stability, and life stability during printing and which cause less fogging. The toner contains a core particle containing binder resin and colorant, and a coating layer which contains resin and a charge control agent and is formed on a surface of the core particle. At least a part of the resin contained in the coating layer is melt-bonded to the core particle, and the charge control agent is dispersed and immobilized in the coating layer. The dispersed charge control agent has a dispersion diameter of less than 1 ?m.Type: GrantFiled: October 10, 2008Date of Patent: April 26, 2011Assignee: Sharp Kabushiki KaishaInventors: Saori Yamada, Yoshitaka Kawase, Yoshiaki Akazawa
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Patent number: 7932011Abstract: An electrophotographic toner comprising a resin and a colorant, wherein: (i) a toner particle comprises a domain in the toner particle, the domain comprising a polar wax having a first polar group and a non-polar wax; and (ii) the resin contains a second polar group.Type: GrantFiled: February 24, 2006Date of Patent: April 26, 2011Assignee: Konica Minolta Business Technologies, Inc.Inventors: Takamasa Ueda, Mikio Koyama, Kazuya Isobe
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Patent number: 7931876Abstract: The invention provides a method and an apparatus for manufacturing a developer, which can manufacture a developer having a uniform and fine particle shape in a narrow particle size distribution and having a coloring agent highly dispersed therein at the primary particle level, the method and apparatus at the same time enabling continuous and efficient production without opening and closing a reactor. The method comprises the steps of: dissolving a binding resin component in a supercritical or subcritical fluid so that the binding resin component is blended with a coloring agent component; and reducing the solubility of the binding resin component in the supercritical or subcritical fluid so that the binding resin component is precipitated in the form of particles with the coloring agent component dispersed in the interior thereof.Type: GrantFiled: December 17, 2008Date of Patent: April 26, 2011Assignee: Sharp Kabushiki KaishaInventors: Shinichi Nakano, Yasuhiro Shibai, Keiichi Kikawa
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Publication number: 20110091803Abstract: An emulsion aggregation toner composition includes toner particles including: an amorphous polyester resin; an optional crystalline resin; an optional colorant; an optional wax; an optional coagulant; and a polymeric or oligomeric hydroxy ketone photo initiator capable of initiating crosslinking of said polyester resin, wherein at least one of the amorphous polyester resin and the optional crystalline resin when present is unsaturated.Type: ApplicationFiled: October 15, 2009Publication date: April 21, 2011Applicant: XEROX CORPORATIONInventors: Ke ZHOU, Daryl W. VANBESIEN, Edward G. ZWARTZ, Guerino G. SACRIPANTE, Karen A. MOFFAT
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Publication number: 20110091801Abstract: The present disclosure provides toners and methods for their production. In embodiments, the amount of coagulant utilized in producing those toners may be less than amounts currently in use, which may have a beneficial effect by reducing the time for coalescence. Modified waxes may also be utilized which provide excellent gloss and charging characteristics.Type: ApplicationFiled: October 15, 2009Publication date: April 21, 2011Applicant: XEROX CORPORATIONInventors: Mark E. Mang, Grazyna Kmiecik-Lawrynowicz, Maura A. Sweeney, Timothy L. Lincoln
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Publication number: 20110086306Abstract: A toner having charge control agents which impart excellent triboelectric charging characteristics. In embodiments, the charge control agents include copolymers formed by an emulsion polymerization process.Type: ApplicationFiled: October 8, 2009Publication date: April 14, 2011Applicant: XEROX CORPORATIONInventors: Robert D. Bayley, Yuhua Tong, Timothy L. Lincoln, Grazyna E. Kmiecik-Lawrynowicz, Maura A. Sweeney, Daniel W. Asarese, Susan J. LaFica, Mark E. Mang
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Publication number: 20110086302Abstract: An emulsion aggregation toner composition includes toner particles including: an unsaturated polymeric resin, such as amorphous resins, crystalline resins, and combinations thereof; an optional colorant; an optional wax; an optional coagulant; and an IR absorber. The use of an IR absorber may permit formation of color toners that have uniform gloss and crease properties, i.e., the IR absorbers may prevent gloss and crease differences between color and black toners.Type: ApplicationFiled: October 9, 2009Publication date: April 14, 2011Applicant: XEROX CORPORATIONInventors: Ke Zhou, Edward Graham Zwartz, Karen Ann Moffat, Guerino G. Sacripante, T. Brian McAneney, Jordan H. Wosnick, Valerie M. Farrugia
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Patent number: 7923191Abstract: The present disclosure relates to chemically processed toner. The toner may be prepared by an emulsion aggregation method by forming a polyester dispersion wherein the polyester has an acid value of about 5 to about 50 and a particle size of about 50 to about 500 nanometers. The polyester dispersion may then be combined with a pigment and/or release agent dispersion wherein the pigment and/or release agent dispersion may contain a dispersant. This may then be followed by heating and recovering agglomerated toner particles wherein the toner particles may have a mean particle size of about 3 to about 15 microns and an average degree of circularity of between about 0.90 to about 1.0.Type: GrantFiled: July 26, 2007Date of Patent: April 12, 2011Assignee: Lexmark International, Inc.Inventors: Craig Michael Bertelsen, Ligia Aura Bejat, Michael James Bensing, John Joseph Kraseski, Matthew T. Martinkovic, Jing X. Sun
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Publication number: 20110069992Abstract: A method of manufacturing toner particles capable of decreasing the manufacturing costs by simplifying the manufacturing apparatus and by decreasing the number of the steps, as well as to provide toner particles, a two-component developer, a developing apparatus and an image forming apparatus are provided. A high-pressure homogenizer is constituted by a tank, a feed pump, a high-pressure pump, a heat exchanger, a nozzle, a first depressurizing module, a cooling unit, a second depressurizing module and a take-out port arranged in this order. A flow path constituted in the first depressurizing module has a straight portion tilted with respect to a direction in which the aqueous slurry passes and a portion for relaxing the flow of the aqueous slurry.Type: ApplicationFiled: November 30, 2010Publication date: March 24, 2011Applicant: SHARP KABUSHIKI KAISHAInventors: Katsuru Matsumoto, Keiichi Kikawa, Nobuhiro Maezawa
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Patent number: 7910275Abstract: Embodiments include a chemical toner composition having a first resin including a styrene vinyl copolymer and having a Tg of from about 46 to about 56° C., b) a second resin including a styrene vinyl copolymer having a Tg of from about 55 to about 65° C., c) a distilled wax having a heat of crystallization and a heat of enthalpy, both from about 1.0 to about 4.0 J/g for every weight percent of the wax used in the chemical toner composition, and wherein the wax has a peak melting point of from about 70 to about 99° C., and d) a colorant, wherein the chemical toner has a gloss of from about 30 to about 80 GGU.Type: GrantFiled: November 14, 2005Date of Patent: March 22, 2011Assignee: Xerox CorporationInventors: Raj D. Patel, David J. Sanders, Christine Anderson, Allan K. Chen, Daryl W. Vanbesien, Patricia A. Burns
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Patent number: 7910276Abstract: Disclosed herein are emulsion aggregation toner particles having less than about 15 atomic percent oxygen in relation to a total atomic percent of 100 for all elements on the surface thereof. Such toner particles exhibit lower marks on print defects.Type: GrantFiled: July 12, 2007Date of Patent: March 22, 2011Assignee: Xerox CorporationInventors: Karen A. Moffat, Juan A. Morales-Tirado, Thomas P. Debies, William H. Hollenbaugh, Jr., Emily L. Moore, Nancy S. Hunt
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Patent number: 7910279Abstract: A method of manufacturing aggregate particles capable of obtaining aggregate particles having high mechanical strength, small particle size, with narrow particle size distribution width by preventing interfusion of bubbles in the aggregate particles during stirring is provided. Aggregate particles are manufactured by stirring a resin particle slurry including resin particles dispersed in an aqueous medium and contained in a stirring vessel by a stirring section having a impeller and two or more screen members disposed so as to surround the impeller in the stirring vessel and each formed with a plurality of slits and aggregating the resin particles.Type: GrantFiled: November 8, 2007Date of Patent: March 22, 2011Assignee: Sharp Kabushiki KaishaInventors: Nobuhiro Maezawa, Katsuru Matsumoto, Keiichi Kikawa
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Patent number: 7901857Abstract: The present invention provides a toner for developing an electrostatic latent image comprising at least a core layer including at least a coloring agent and a first binder resin, and a shell layer for covering the core layer and including a second binder resin, wherein two local maximum values of the tangent loss (tan ?) of the dynamic visco-elasticity are present in a temperature range of 90° C. or less, with one of the local maximum values present in a range of less than 60° C., and the other local maximum value present in a range of 60° C. or more and 90° C. or less. Moreover, a production method for the toner for developing an electrostatic latent image, a developer for developing an electrostatic latent image, using the toner, and an image forming method are provided.Type: GrantFiled: July 15, 2005Date of Patent: March 8, 2011Assignee: Fuji Xerox Co., Ltd.Inventors: Hiroshi Nakazawa, Takao Ishiyama, Masanobu Ninomiya
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Patent number: 7901862Abstract: It is intended to provide a method includes the step of forming agglomerated particles by agglomerating fine particulate mixture containing a binder resin and a colorant. In the step of forming agglomerated particles, a cationic organic coagulating agent having an average molecular weight of from 1000 to 100000 is added to a liquid dispersion containing fine particles.Type: GrantFiled: October 2, 2008Date of Patent: March 8, 2011Assignees: Kabushiki Kaisha Toshiba, Toshiba Tec Kabushiki KaishaInventors: Tsuyoshi Itou, Takayasu Aoki, Takashi Urabe, Motonari Udo, Yasuhito Noda, Satoshi Araki, Masahiro Ikuta, Takafumi Hara
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Patent number: 7901859Abstract: A chemical toner composition including a polymer polymerized from starting ingredients comprising a resin monomer and a release agent monomer.Type: GrantFiled: April 10, 2007Date of Patent: March 8, 2011Assignee: Xerox CorporationInventors: Daryl W Vanbesien, Edward G Zwartz, Cuong Vong, Maria N V McDougall, Timothy P Bender, Jennifer L Belelie, Tyler Norsten
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Publication number: 20110053076Abstract: The present disclosure provides methods for incorporating a dye into latex particles via a supercritical fluid microencapsulation technique, in order to achieve improved dispersion of a colorant in the latex and an increase in color gamut.Type: ApplicationFiled: August 25, 2009Publication date: March 3, 2011Applicant: XEROX CORPORATIONInventors: Maura A. Sweeney, Grazyna Kmiecik-Lawrynowicz, Robert D. Bayley
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Publication number: 20110053079Abstract: The present disclosure provides processes for the preparation of unsaturated polyesters. In embodiments, a process of the present disclosure includes reacting an organic diol with a cyclic alkylene carbonate in the presence of a first catalyst to thereby form a polyalkoxy diol, optionally adding thereto a further amount of cyclic alkylene carbonate in the presence of a second catalyst, and subsequently polycondensing the resulting mixture with a dicarboxylic acid in combination with an anhydride.Type: ApplicationFiled: August 27, 2009Publication date: March 3, 2011Applicant: XEROX CORPORATIONInventor: Guerino G. Sacripante
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Publication number: 20110053078Abstract: An emulsion aggregation toner composition includes toner particles including: an unsaturated polymeric resin, such as amorphous resins, crystalline resins, and combinations thereof; an optional colorant; an optional wax; an optional coagulant; and a photoinitiator. By optimizing the particle size of the emulsion, the aggregant concentration utilized in the emulsion aggregation process, and the solids content of the emulsion, toners may be produced capable of generating images with non-contact fusing that have high gloss.Type: ApplicationFiled: September 3, 2009Publication date: March 3, 2011Applicant: XEROX CORPORATIONInventors: Edward Graham Zwartz, Guerino G. Sacripante
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Patent number: 7897318Abstract: The present disclosure relates to a process for producing a toner particulate composition from aqueous dispersions containing aggregates of a polymer binder and other toner ingredients. An ionic surfactant may be used to form the dispersion along with an ionic polymer flocculent wherein the ionic polymer flocculent undergoes a molecular conformational change, which may be triggered by pH adjustment, leading to flocculation and particle growth.Type: GrantFiled: November 29, 2007Date of Patent: March 1, 2011Assignee: Lexmark International, Inc.Inventors: Trent Duane Peter, Tao Yu
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Publication number: 20110045395Abstract: An electrostatic image developing toner includes toner particles that contain a binding resin, a coloring agent and a release agent and that have D50 of from about 2.0 ?m to about 8.0 ?m, D50 standing for a volume-average particle size of the toner particles; and non-colored release agent particles, wherein out of the non-colored release agent particles, those ranging in volume-average particle size of from about 0.8 to about 1.2 times a value of D50 are present in a proportion of about 50 or below per 5,000 of the toner particles.Type: ApplicationFiled: January 28, 2010Publication date: February 24, 2011Applicant: FUJI XEROX CO., LTD.Inventors: Yoshimasa FUJIWARA, Masaaki SUWABE
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Publication number: 20110045403Abstract: A toner composition including toner particles, wherein the toner particles are prepared by a method in which toner constituents including at least a binder resin and a colorant are kneaded upon application of heat to prepare a toner constituent mixture; the toner constituent mixture is dissolved or swelled in an organic solvent capable of dissolving or swelling at least the binder resin to prepare an oil phase liquid; the oil phase liquid is emulsified in an aqueous liquid to prepare an emulsion; the emulsion is coagulated; and then the coagulated emulsion is dried to prepare the toner particles.Type: ApplicationFiled: October 29, 2010Publication date: February 24, 2011Inventors: Hiroshi Yamashita, Masami Tomita, Shigeru Emoto, Tsunemi Sugiyama
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Patent number: 7887983Abstract: The present invention relates to a process for preparing a toner for electrophotography containing a resin binder and a colorant, including the step of preparing fine particles of the resin binder to have a volume-median particle size (D50) of from 0.05 to 3 ?m in an aqueous medium in the presence of a nonionic surfactant within a temperature range of from 10° C. below to 10° C. above a cloud point of the nonionic surfactant; and a toner for electrophotography obtained by the process as defined above, wherein the toner contains 60% by weight or more of a crystalline polyester and has a volume-median particle size (D50) of from 1 to 7 ?m. The toner obtained according to the process of the present invention can be suitably used, for example, in development of a latent image formed in electrophotography, electrostatic recording method, electrostatic printing method, or the like.Type: GrantFiled: August 9, 2005Date of Patent: February 15, 2011Assignee: Kao CorporationInventors: Shinichi Sata, Yoshinobu Ishikawa, Nobumichi Kamiyoshi
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Patent number: 7887986Abstract: A method of manufacturing toner particles capable of decreasing the manufacturing costs by simplifying the manufacturing apparatus and by decreasing the number of the steps, as well as to provide toner particles, a two-component developer, a developing apparatus and an image forming apparatus are provided. A high-pressure homogenizer is constituted by a tank, a feed pump, a high-pressure pump, a heat exchanger, a nozzle, a first depressurizing module, a cooling unit, a second depressurizing module and a take-out port arranged in this order. A flow path constituted in the first depressurizing module has a straight portion tilted with respect to a direction in which the aqueous slurry passes and a portion for relaxing the flow of the aqueous slurry.Type: GrantFiled: August 8, 2008Date of Patent: February 15, 2011Assignee: Sharp Kabushiki KaishaInventors: Katsuru Matsumoto, Keiichi Kikawa, Nobuhiro Maezawa
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Publication number: 20110033795Abstract: A toner which can be improved in both low-temperature fixability and offset resistance is disclosed, comprising a colorant and a binder resin containing a polyester ionomer resin which has been reacted with a polyvalent isocyanate compound.Type: ApplicationFiled: July 22, 2009Publication date: February 10, 2011Applicant: KONICA MINOLTA BUSINESS TECHNOLOGIES, INC.Inventors: Mikio Kouyama, Kenji Hayashi, Hiroaki OBata, Noriyuki Kimpara, Hiroshi Nagasawa
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Publication number: 20110027712Abstract: The present disclosure provides toner compositions able to prevent the formation of mold or bacterial growth during storage. In embodiments, toners may include at least one biocide that prevents the formation of mold and/or bacteria in a toner composition, including any emulsion that may be utilized in forming the toner composition. In embodiments, the biocide may also improve charging characteristics of the toner.Type: ApplicationFiled: July 28, 2009Publication date: February 3, 2011Applicant: XEROX CORPORATIONInventors: Kimberly D. Nosella, Maria N.V. McDougall, Melanie Lynn Davis
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Publication number: 20110027710Abstract: A process for making a self-emulsifying granule suitable for use in forming latex emulsions includes contacting a resin with a solid or highly concentrated surfactant, a solid neutralization agent and water in the absence of an organic solvent to form a mixture, melt mixing the mixture, and forming self-emulsifying granules of the melt mixed mixture. Self-emulsifying granules are also provided and configured to form a latex emulsion when added to water, which may then be utilized to form a toner.Type: ApplicationFiled: July 30, 2009Publication date: February 3, 2011Applicant: XEROX CORPORATIONInventors: Santiago Faucher, Joo T. Chung, Shigang Qiu, Fumii Higuchi
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Patent number: 7879523Abstract: A toner composition including toner particles, wherein the toner particles are prepared by a method in which toner constituents including at least a binder resin and a colorant are kneaded upon application of heat to prepare a toner constituent mixture; the toner constituent mixture is dissolved or swelled in an organic solvent capable of dissolving or swelling at least the binder resin to prepare an oil phase liquid; the oil phase liquid is emulsified in an aqueous liquid to prepare an emulsion; the emulsion is coagulated; and then the coagulated emulsion is dried to prepare the toner particles.Type: GrantFiled: January 12, 2009Date of Patent: February 1, 2011Assignee: Ricoh Company LimitedInventors: Hiroshi Yamashita, Masami Tomita, Shigeru Emoto, Tsunemi Sugiyama
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Publication number: 20110020745Abstract: The present invention relates to, in the toner including toner particles having a biding agent resin, colorings and a release agent, an electrostatic image developing toner, its composition, and a preparation method thereof. The electrostatic image developing toner is prepared by the method comprising: (1) preparing an inorganic dispersion medium; (2) dispersing/dissolving a polymerizable monomer mixture; (3) micronizing the liquid obtained in step (2) in the liquid obtained in step (1) with high shear force in order to create droplets; (4) performing radical polymerization of the micronized droplets obtained in step (3); (5) aggregating particles obtained in step (4); (6) fusing the aggregate obtained in step (5); (7) cleaning and drying the toner obtained by step (6); and (8) adding additives to impart electrification and fluidity to a toner obtained by step (7).Type: ApplicationFiled: March 12, 2009Publication date: January 27, 2011Inventors: Jae-Goang Yu, Ho-Geun Jo
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Publication number: 20110014558Abstract: According to one embodiment, a method for producing a developing agent including aggregating fine particles of a toner material containing a binder resin and a coloring agent in a dispersion liquid in which the fine particles are dispersed in an aqueous medium to form aggregated particles, and washing the aggregated particles and drying the washed aggregated particles, forming toner particles is provided. An electrical conductivity of the toner particles is measured by a toner electrical conductivity evaluation method. A sample toner is prepared by adhering an additive to surfaces of the toner particles, and a content ratio of a sodium element to a carbon element in a region to which the additive is not adhered of the toner is measured. The washing of the toner particles is repeated until each of the measurement values becomes a predetermined reference value or less.Type: ApplicationFiled: July 8, 2010Publication date: January 20, 2011Applicants: KABUSHIKI KAISHA TOSHIBA, TOSHIBA TEC KABUSHIKI KAISHAInventors: Masahiro Ikuta, Takayasu Aoki, Takashi Urabe, Tsuyoshi Itou, Motonari Udo, Satoshi Araki, Takafumi Hara, Yasuhito Noda, Taishi Takano, Yasuo Goto, Junichi Ishikawa
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Publication number: 20110014559Abstract: The present disclosure provides violet toners and methods for their production. In embodiments, methods of the present disclosure include systems which may be utilized to predict the color properties of a violet toner, thereby permitting adjustment of the pigment loading and/or target mass per unit area.Type: ApplicationFiled: July 20, 2009Publication date: January 20, 2011Applicant: XEROX CORPORATIONInventors: Jordan H. Wosnick, Suxia Yang, Richard P.N. Veregin, Karen A. Moffat
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Publication number: 20110014565Abstract: A method of manufacturing a toner including supplying a fluid containing a resin and a coloring agent to a retaining member including a film having multiple discharge orifices, discharging droplets of the fluid from the multiple discharge orifices at a speed of from 2 to 4 m/s by applying a pulse voltage having a trapezoid waveform to a piezoelectric body having a surface provided substantially parallel to the film to move the surface in a direction away from the film relative to a reference position of the surface followed by holding the surface there for a predetermined time, and bringing the surface back to the reference position; and solidifying droplets of the fluid discharged from the multiple discharge orifices to form mother particles.Type: ApplicationFiled: July 12, 2010Publication date: January 20, 2011Inventors: Yoshihiro NORIKANE, Yohichiroh Watanabe, Masaru Ohgaki, Shinji Aoki, Yasutada Shitara, Andrew Mwaniki Mulwa
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Publication number: 20110008722Abstract: Toners are provided which include a resin including at least one baroplastic polymer. The baroplastic polymer, in embodiments, may be a block copolymer with discrete low glass transition temperature (Tg) domains and high Tg domains that plasticize one another at ambient temperature when subjected to pressures of from about 500 psi (about 3.45 MPa) to about 10,000 psi (about 69 MPa), enabling them to be extruded and molded without heat. The resulting polymers, in turn, may then be utilized to form toners.Type: ApplicationFiled: July 10, 2009Publication date: January 13, 2011Applicant: XEROX CORPORATIONInventors: Jordan H. Wosnick, Karen Ann Moffat