Miscellaneous Patents (Class 51/293)
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Patent number: 8911521Abstract: Embodiments of the invention relate to methods of fabricating a polycrystalline diamond compacts and applications for such polycrystalline diamond compacts. In an embodiment, a method of fabricating a polycrystalline diamond compact includes at least saturating a sintering aid material with non-diamond carbon to form a carbon-saturated sintering aid material and sintering a plurality of diamond particles in the presence of the carbon-saturated sintering aid particles to form a polycrystalline diamond table.Type: GrantFiled: December 12, 2011Date of Patent: December 16, 2014Assignee: US Synthetic CorporationInventors: David P. Miess, Michael A. Vail, C. Eugene McMurray
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Patent number: 8911522Abstract: Methods of forming inserts for earth-boring tools include providing a material in a pattern adjacent a strip, arranging a plurality of superabrasive particles proximate the pattern, and securing at least some of the plurality of superabrasive particles to the strip. The material is configured to attract or secure the plurality of superabrasive particles. Some methods may include imparting like charges to each of a plurality of superabrasive particles, placing the plurality of superabrasive particles over a strip, and securing the superabrasive particles to the strip. In some methods, a first plurality of superabrasive particles may be placed in an array between a first strip and a second strip. A second plurality of superabrasive particles may be placed in an array between the second strip and a third strip. Methods of forming earth-boring rotary drill bits include forming an insert and securing the insert to a body of the bit.Type: GrantFiled: July 5, 2011Date of Patent: December 16, 2014Assignee: Baker Hughes IncorporatedInventors: Christopher J. Cleboski, Suresh G. Patel, Danny E. Scott, L. Allen Sinor
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Patent number: 8894730Abstract: Provided are an alumina sintered compact containing a titanium compound and an iron compound, wherein the total amount of the TiO2-equivalent content of the titanium compound, the Fe2O3-equivalent content of the iron compound and the alumina content is at least 98% by mass, the total amount of the TiO2-equivalent content of the titanium compound and the Fe2O3-equivalent content of the iron compound is from 5 to 13% by mass, and the ratio by mass of the TiO2-equivalent content of the titanium compound to the Fe2O3-equivalent content of the iron compound (TiO2/Fe2O3) is from 0.85/1.15 to 1.15/0.85; and an abrasive grain and a grain stone using the alumina sintered compact.Type: GrantFiled: October 18, 2011Date of Patent: November 25, 2014Assignee: Showa Denko K.K.Inventors: Shinichiro Tomikawa, Hirokazu Miyazawa, Takeshi Iemura
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Patent number: 8894732Abstract: The invention provides a plurality of polymeric particles embedded with alkaline-earth metal oxide. The gas-filled polymeric microelements have a shell and a density of 5 g/liter to 200 g/liter. The shell has an outer surface and a diameter of 5 ?m to 200 ?m with the outer surface of the shell of the gas-filled polymeric particles having alkaline-earth metal oxide-containing particles embedded in the polymer. The alkaline-earth metal oxide-containing particles have an average particle size of 0.01 to 3 ?m distributed within each of the polymeric microelements to coat less than 50 percent of the outer surface of the polymeric microelements.Type: GrantFiled: May 11, 2012Date of Patent: November 25, 2014Assignee: Rohm and Haas Electronic Materials CMP Holdings, Inc.Inventors: Andrew R. Wank, Donna M. Alden, David B. James
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Patent number: 8888879Abstract: In an embodiment, a method of non-destructively testing a polycrystalline diamond (“PCD”) element includes providing a PCD element including a plurality of bonded diamond grains defining a plurality of interstitial regions, at least a portion of the plurality of interstitial regions including one or more interstitial constituents disposed therein. The method further includes exposing the PCD element to neutron radiation from a neutron radiation source, receiving a portion of the neutron radiation that passes through the PCD element, and determining at least one characteristic of the PCD element at least partially based on the portion of the neutron radiation received. For example, the at least one characteristic may be the presence and distribution of metal-solvent catalyst, residual metal-solvent catalyst, an infiltrant, residual infiltrant, or other interstitial constituents within a PCD element.Type: GrantFiled: October 6, 2011Date of Patent: November 18, 2014Assignee: US Synthetic CorporationInventors: Debkumar Mukhopadhyay, Kenneth E. Bertagnolli
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Patent number: 8888877Abstract: The invention involves a method of preparing an alkaline-earth metal oxide-containing polishing pad useful for polishing at least one of semiconductor, magnetic and optical substrates. The method includes introducing a feed stream of gas-filled polymeric microelements into a gas jet, the polymeric microelements having varied density, varied wall thickness and varied particle size. The method passes the polymeric microelements in the gas jet adjacent a Coanda block, the Coanda block having a curved wall for separating the polymeric microelements with Coanda effect, inertia and gas flow resistance. Then it separates various alkaline earth metal oxide constituents from the curved wall of the Coanda block to clean the polymeric microelements.Type: GrantFiled: May 11, 2012Date of Patent: November 18, 2014Assignee: Rohm and Haas Electronic Materials CMP Holdings, Inc.Inventors: Donna M. Alden, David B. James, Andrew R. Wank, James Murnane
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Publication number: 20140332283Abstract: Earth-boring tools may have a body, a cutting element attached to the body at a first location, and a formation-engaging structure attached to the body at a second location. The formation-engaging structure may be movable during a drilling operation between a first position and a second position. In the first position, the formation-engaging structure may be located rotationally behind the cutting element at a first radial distance from a longitudinal axis of the body at which the cutting element will at least initially shield the formation-engaging structure from engaging a formation. In the second position, the formation-engaging structure may be located at a different second radial distance from the longitudinal axis of the body at which the formation-engaging structure will engage a formation.Type: ApplicationFiled: May 13, 2013Publication date: November 13, 2014Inventors: Eric Do, Juan Miguel Bilen, Philip Christof Schulte, Jason E. Hoines
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Patent number: 8870986Abstract: An abrasive article including a bonded abrasive body having abrasive particles contained within a bond material, the bond material including a vitreous material formed from a mixture having aluminum oxide (Al2O3), bismuth oxide (Bi2O3), and boron oxide (B2O3), and wherein the mixture includes an amount (wt %) of aluminum oxide less than an amount (wt %) of bismuth oxide and the amount (wt %) of aluminum oxide is less than an amount (wt %) of boron oxide.Type: GrantFiled: June 28, 2013Date of Patent: October 28, 2014Assignees: Saint-Gobain Abrasives, Inc., Saint-Gobain AbrasifsInventors: Sophie Papin, Cécile Jousseaume, Nilanjan Sarangi, Sandhya Jayaraman Rukmani
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Patent number: 8864858Abstract: Embodiments of the invention relate to methods of fabricating polycrystalline diamond compacts (“PDCs”) and applications for such PDCs. In an embodiment, a method of fabricating a PDC includes providing a polycrystalline diamond (“PCD”) table in which a catalyst is disposed throughout, leaching the PCD table with a gaseous leaching agent to remove catalyst from the PCD table and bonding the at least partially leached PCD table to a substrate to form a PDC.Type: GrantFiled: December 13, 2011Date of Patent: October 21, 2014Assignee: US Synthetic CorporationInventors: Julie Ann Kidd, Michael A. Vail, Kenneth E. Bertagnolli
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Patent number: 8864859Abstract: The present application relates to polishing pads for chemical mechanical planarization (CMP) of substrates, and methods of fabrication and use thereof. The pads described in this invention are customized to polishing specifications where specifications include (but not limited to) to the material being polished, chip design and architecture, chip density and pattern density, equipment platform and type of slurry used. These pads can be designed with a specialized polymeric nano-structure with a long or short range order which allows for molecular level tuning achieving superior thermo-mechanical characteristics. More particularly, the pads can be designed and fabricated so that there is both uniform and nonuniform spatial distribution of chemical and physical properties within the pads.Type: GrantFiled: November 28, 2007Date of Patent: October 21, 2014Assignee: NexPlanar CorporationInventors: Pradip K. Roy, Manish Deopura, Sudhanshu Misra
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Patent number: 8858662Abstract: Methods of forming a polycrystalline table comprise disposing a plurality of particles comprising a superabrasive material, a substrate comprising a hard material, and a catalyst material in a mold. The plurality of particles is partially sintered in the presence of the catalyst material to form a brown polycrystalline table having a first permeability attached to an end of the substrate. The substrate is removed from the brown polycrystalline table and catalyst material is removed from the brown polycrystalline table. The brown polycrystalline table is then fully sintered to form a polycrystalline table having a reduced, second permeability. Intermediate structures formed during a process of attaching a polycrystalline table to a substrate comprise a substantially fully leached brown polycrystalline table. The substantially fully leached brown polycrystalline table comprises a plurality of interbonded grains of a superabrasive material.Type: GrantFiled: March 4, 2011Date of Patent: October 14, 2014Assignee: Baker Hughes IncorporatedInventors: Anthony A. DiGiovanni, Nicholas J. Lyons, Derek L. Nelms, Danny E. Scott
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Patent number: 8852304Abstract: Thermally stable diamond bonded materials and compacts include a diamond body having a thermally stable region and a PCD region, and a substrate integrally joined to the body. The thermally stable region has a microstructure comprising a plurality of diamond grains bonded together by a reaction with a reactant material. The PCD region extends from the thermally stable region and has a microstructure of bonded together diamond grains and a metal solvent catalyst disposed interstitially between the bonded diamond grains. The compact is formed by subjecting the diamond grains, reactant material, and metal solvent catalyst to a first temperature and pressure condition to form the thermally stable region, and then to a second higher temperature condition to both form the PCD region and bond the body to a desired substrate.Type: GrantFiled: January 19, 2010Date of Patent: October 7, 2014Assignee: Smith International, Inc.Inventor: Stewart N. Middlemiss
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Patent number: 8851058Abstract: Wear indicators for abrasive articles are presented. Specifically, indicator marks that are parallel to a bonding edge of a grinding element are presented. Tools comprising a carrier element and one or more grinding elements comprising one or more indicators are also presented.Type: GrantFiled: December 16, 2010Date of Patent: October 7, 2014Assignees: Saint-Gobain Abrasives, Inc., Saint-Gobain AbrasifsInventors: Marc Linh Hoang, Rodolphe Martin
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Patent number: 8845773Abstract: Abrasive particles which are shaped abrasive particles each with an opening are described. The shaped abrasive particles are formed from alpha alumina and have a first face and a second face separated by a thickness t. The opening in each of the shaped abrasive particles can improve grinding performance by reducing the size of a resulting wear flat, can provide a reservoir for grinding aid, and can improve adhesion to a backing in a coated abrasive article.Type: GrantFiled: February 16, 2012Date of Patent: September 30, 2014Assignee: 3M Innovative Properties CompanyInventors: Dwight D. Erickson, Scott R. Culler, Negus B. Adefris, John T. Boden, John D. Haas
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Patent number: 8840693Abstract: Coated particles comprise a core particle comprising a superhard material and having an average diameter of between 1 ?m and 500 ?m. A coating material is adhered to and covers at least a portion of an outer surface of the core particle, the coating material comprising an amine terminated group. A plurality of nanoparticles selected from the group consisting of carbon nanotubes, nanographite, nanographene, non-diamond carbon allotropes, surface modified nanodiamond, nanoscale particles of BeO, and nanoscale particles comprising a Group VIIIA element is adhered to the coating material.Type: GrantFiled: June 22, 2011Date of Patent: September 23, 2014Assignee: Baker Hughes IncorporatedInventors: Soma Chakraborty, Oleksandr Kuznetsov, Gaurav Agrawal
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Publication number: 20140273775Abstract: Disclosed is a tool for finishing a work piece where the tool includes multiple pieces of abrasive material (sandpaper) mounted to a cylindrical housing and carrying a shank for mounting the tool to a portable electric drill or drill press or bench motor. The drill is powered to rotate the shank and housing in a first direction and the sheets of abrasive material are mounted at spaced locations around the periphery of the housing and wrapped in an opposite direction to the direction of rotation of the shank and housing, The sheet of abrasive material is cut from the end opposite to the attached end to form a plurality of finger-like projections which are not secured but tend to move outward when the housing is rotated. The fingers provide a yieldable abrasive surface which can adapt to the contours of the work piece and allow for finishing an irregular work piece.Type: ApplicationFiled: March 15, 2013Publication date: September 18, 2014Inventor: Arturo M. Ottolenghi
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Patent number: 8834588Abstract: The present invention relates to polycrystalline Al2O3 bodies based on melted aluminum oxide having a mean crystallite size of the primary crystals between 20 ?m and 100 ?m and a closed macroporosity between 10% by volume and 30% by volume. The polycrystalline Al2O3 bodies may be obtained by tapping out and quenching a liquid aluminum oxide melt and simultaneous seeding of the pouring stream with seed crystals and can be used advantageously for the production of abrasive materials and refractory products.Type: GrantFiled: August 15, 2011Date of Patent: September 16, 2014Assignee: Center for Abrasives and Refractories Research & Development C.A.R.R.D. GmbHInventor: Sebastian Sachse
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Patent number: 8828110Abstract: A composite body has a material layer formed from aggregated diamond nanorods (ADNRs); The ADNR material layer has a first surface and a substrate. The first surface of the diamond material layer and the substrate are bonded together under high pressure and high temperature.Type: GrantFiled: September 23, 2011Date of Patent: September 9, 2014Inventor: Robert Frushour
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Patent number: 8821604Abstract: A polycrystalline diamond compact includes a substrate and a polycrystalline diamond table attached to the substrate. The polycrystalline diamond table includes an upper surface and at least one peripheral surface. Diamond grains of the polycrystalline diamond table define a plurality of interstitial regions. The polycrystalline diamond table includes a region having silicon carbide positioned within at least some of the interstitial regions thereof. In an embodiment, the first region extends over only a selected portion of the upper surface and/or at least a portion of the at least one peripheral surface. In another embodiment, the first region substantially contours the upper surface and a chamfer.Type: GrantFiled: February 22, 2011Date of Patent: September 2, 2014Assignee: US Synthetic CorporationInventor: Mohammad N. Sani
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Patent number: 8821603Abstract: A hard composite member produced by a rapid omni-directional compaction process that includes the steps of: providing a pre-compaction composite comprising a substrate, a superhard member and a layer of braze between the substrate and the superhard member; placing the pre-compaction composite in a pressure transmitting material contained within a shell to form an isostatic die assembly; heating the isostatic die assembly to a temperature at which the pressure-transmitting material is capable of fluidic flow and wherein the temperature ranges between greater than the melting point of the braze layer and less than or equal to about 1200° C.; and in a forging press, compressing the isostatic die assembly to consolidate the pre-compaction composite under omnidirectional pressure at a pressure equal to or greater than about 60,000 psi into a dense, consolidated body.Type: GrantFiled: March 8, 2007Date of Patent: September 2, 2014Assignee: Kennametal Inc.Inventors: Jonathan W. Bitler, Sara Kiani
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Patent number: 8821605Abstract: The present invention relates to sintered abrasive grit agglomerates based on aluminum oxide, having homogeneously distributed nanoscale pores in the range of 100-300 nm, with a pore volume of at least 15%. The average diameter of primary particles of the aluminum oxide primary particles is less than 5 ?m, wherein said primary particles are connected to each other without additional adhesive agent.Type: GrantFiled: July 21, 2009Date of Patent: September 2, 2014Assignee: Center for Abrasives and Refractories Research & Development C.A.R.R.D. GmbHInventors: Maria Christina DiDavide, Reiner Kunz
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Patent number: 8821606Abstract: A metal bonded grinding stone is manufactured by heating and pressurizing a material including abrasive grains, a cobalt, a tungsten disulfide and a copper tin alloy to obtain a sintered product, and rapid-cooling the sintered product.Type: GrantFiled: July 21, 2010Date of Patent: September 2, 2014Assignee: Honda Motor Co., Ltd.Inventors: Masato Ujihashi, Toshiya Hirata, Kazuhiko Kitanaka, Naohide Unno, Hiroshi Sugiyama, Noriyuki Namba
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Patent number: 8814965Abstract: A cubic boron nitride sintered body is excellent in wear resistance. The cubic boron nitride sintered body has about 30 to about 70% by volume of cubic boron nitride; and as the reminder, a binder phase having at least one selected from an oxide, carbide, nitride and boride of Ti, Al, Zr, Y, Ce, Mg or Ca and mutual solid solutions thereof; and inevitable impurities, wherein the cubic boron nitride sintered body contains ?-type Al2O3, ZrB2, ZrO2 and ZrO, and when an X-ray diffraction intensity of a (110) plane of ?-type Al2O3 is represented by Ia, an X-ray diffraction intensity of a (101) plane of ZrB2 is represented by Izb, and an X-ray diffraction intensity of a (111) plane of ZrO is represented by Izo, (Izb/Ia) which shows a ratio of Izb based on Ia satisfies 0.13?(Izb/Ia)?0.30, and (Izo/Ia) which shows a ratio of Izo based on Ia satisfies 0.05?(Izo/Ia)?0.20.Type: GrantFiled: November 11, 2010Date of Patent: August 26, 2014Assignee: Tungaloy CorporationInventor: Sho Yokoshi
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Patent number: 8814967Abstract: An abrasive article includes a bonded abrasive having a body made of abrasive grains contained within a composite bond material. The composite bond material can include an organic material and a metal material. The body can also include a filler material made of a superabrasive material. In an embodiment, the filler material can have an average particle size at least about 10 times less than an average particle size of the abrasive grains.Type: GrantFiled: June 29, 2012Date of Patent: August 26, 2014Assignees: Saint-Gobain Abrasives, Inc., Saint-Gobain AbrasifsInventors: Rachana Upadhyay, Srinivasan Ramanath
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Patent number: 8814968Abstract: A thermally conductive sand shell molding system allows for controlling heat flow in a molten metal infiltrate powdered metal drill bit molding system to differentially cool the mold system to control differential shrinking and accompanying stress concentrations.Type: GrantFiled: January 13, 2011Date of Patent: August 26, 2014Assignee: National Oilwell Varco, L.P.Inventors: Alan Honggen Jiang, Harold Sreshta
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Patent number: 8808414Abstract: The present invention provides a technique of improving wear resistance of a Sialon sintered body. The Sialon sintered body has a Sialon phase including at least a ?-Sialon and a 12H-Sialon among an ?-Sialon, the ?-Sialon and the 12H-Sialon. A ratio of a second Sialon total content, which is a sum of the contents of the ?-Sialon and the 12H-Sialon, to a first Sialon total content, which is a sum of contents of the ?-Sialon, the ?-Sialon and the 12H-Sialon, is greater than 20% and not greater than 55%, and a ratio of the content of the 12H-Sialon to the first Sialon total content is not less than 2% and not greater than 55%.Type: GrantFiled: March 11, 2010Date of Patent: August 19, 2014Assignee: NGK Spark Plug Co., Ltd.Inventors: Hiroko Nakayama, Ryoji Toyoda
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Patent number: 8790429Abstract: The reactor for polycrystalline silicon is a reactor for polycrystalline silicon in which a silicon seed rod installed inside the reactor is heated by supplying electricity, a raw material gas supplied inside the reactor is allowed to react, thereby producing polycrystalline silicon on the surface of the silicon seed rod, and specifically, the reactor for polycrystalline silicon is provided with a raw material gas supply port installed on the bottom of the reactor and a raw material gas supply nozzle attached to the raw material gas supply port so as to be communicatively connected and extending upward, in which the upper end of the raw material gas supply nozzle is set to a height in a range from ?10 cm to +5 cm on the basis of the upper end of the electrode which retains the silicon seed rod.Type: GrantFiled: June 27, 2012Date of Patent: July 29, 2014Assignee: Mitsubishi Materials CorporationInventors: Toshihide Endoh, Toshiyuki Ishii, Masaaki Sakaguchi, Naoki Hatakeyama
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Patent number: 8790430Abstract: Embodiments of the invention relate to polycrystalline diamond compacts (“PDCs”) comprising a preformed polycrystalline diamond (“PCD”) table including a thermally-stable region having a copper-containing material disposed interstitially between bonded diamond grains thereof, and methods of fabricating such PDCs. In an embodiment, a PDC includes a substrate, and a preformed PCD table having an interfacial surface bonded to the substrate and a generally opposing upper surface. The PCD table includes a plurality of diamond grains exhibiting diamond-to-diamond bonding therebetween and defining a plurality of interstitial regions. The preformed PCD table further includes a first region extending inwardly from the upper surface that includes a copper-containing material disposed therein and a second region extending inwardly from the interfacial surface that includes a nickel-containing material disposed therein.Type: GrantFiled: November 30, 2012Date of Patent: July 29, 2014Assignee: US Synthetic CorporationInventors: David P. Miess, Michael A. Vail, Kenneth E. Bertagnolli, C. Eugene McMurray, Paul Douglas Jones
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Patent number: 8784517Abstract: Embodiments of the invention relate to polycrystalline diamond compacts (“PDCs”) including a pre-sintered polycrystalline diamond (“PCD”) table that may exhibit a non-cylindrical-shaped geometry and/or may have been partially graphitized prior to bonding to a substrate in a high-pressure/high-temperature process (“HPHT”). The disclosed PDCs may be used in a variety of applications, such as rotary drill bits, mining tools, drill bits, bearing apparatuses, wire-drawing dies, machining equipment, and other articles and apparatuses.Type: GrantFiled: March 4, 2010Date of Patent: July 22, 2014Assignee: US Synthetic CorporationInventors: Jair J. Gonzalez, David P. Miess, Mark P. Chapman, Steven L. Choate, D. Bart Crockett, Jeffery A. Gerber
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Patent number: 8784518Abstract: Herein are disclosed an apparatus and method for reaction injection molding of polyurethane foam. In the method, a recirculation loop containing polyols along with an effective amount of water, and a recirculation loop containing isocyanates, are each partially evacuated.Type: GrantFiled: January 11, 2012Date of Patent: July 22, 2014Assignee: 3M Innovative Properties CompanyInventors: Elizabeth Anna Benson-Sargent, David R. Dow, Grady A. Dunham, Douglas E. Earl, Jeffrey P. Lenzendorf
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Patent number: 8778039Abstract: The invention relates to an elastically deformable composite material suitable to be processed further into sheet-like abrasive products, comprising a sheet-like supporting base coated or impregnated with a prepolymer material which obtains thermosetting properties when thermally post-cured, or consisting of a coated or impregnated supporting base, characterized in that the supporting base comprises at least one layer of bonded fibers selected among inorganic fibers and organic synthetic fibers, if necessary mixed with natural fibers. Moreover, it relates to a method for the manufacture of the composite material.Type: GrantFiled: July 20, 2011Date of Patent: July 15, 2014Assignee: Bamberger Kaliko Textile Finishing GmbHInventors: Peter Klenner, Klaus Fuessmann, Waldfried Weier
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Patent number: 8771390Abstract: A vitrified superabrasive product includes a superabrasive component and a vitrified bond component in which the superabrasive component is dispersed, wherein the vitrified bond component defines pores occupying greater than about 50% of the total volume of the vitrified superabrasive product. The vitrified superabrasive product can be in the form of a grinding tool, such as a grinding wheel. A superabrasive mixture includes a glass powder, a superabrasive grit, a binder and a silicon carbide. The mixture can be in the form of a green body, which is fired under an atmosphere and pressure, and at a temperature sufficient to form a porous vitrified superabrasive product.Type: GrantFiled: July 9, 2012Date of Patent: July 8, 2014Assignees: Saint-Gobain Abrasives, Inc., Saint-Gobain AbrasifsInventors: Rachana D. Upadhyay, Gilles Querel, Pradyumna Gupta, Richard W. J. Hall
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Patent number: 8771389Abstract: A method of forming one or more TSP compacts is provided. The method includes placing one or more TSP material layers in an enclosure and surrounding each TSP material layer with at least one of a pre-sintered tungsten carbide powder, pre-cemented tungsten carbide powder, tungsten carbide powder, or partially sintered tungsten carbide substrates. The method also includes exposing the enclosure to a high temperature high pressure process wherein the at least one of a pre-sintered tungsten carbide powder, pre-cemented tungsten carbide powder, tungsten carbide powder, or partially sintered tungsten carbide substrates bond to the TSP material layers forming a stack of TSP material layers including the TSP material layers one over the other with tungsten carbide bonded to each of the TSP material layers and encapsulating each of the TSP material layers.Type: GrantFiled: May 6, 2010Date of Patent: July 8, 2014Assignee: Smith International, Inc.Inventors: Madapusi K. Keshavan, Monte Russell
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Patent number: 8764862Abstract: The disclosure provides a super abrasive element containing a substantially catalyst-free thermally stable polycrystalline diamond (TSP) body having pores and a contact surface, a base adjacent the contact surface of the TSP body; and an infiltrant material infiltrated in the base and in the pores of the TSP body at the contact surface. The disclosure additionally provides earth-boring drill bits and other devices containing such super abrasive elements. The disclosure further provides methods and mold assemblies for forming such super abrasive elements via infiltration and hot press methods.Type: GrantFiled: April 26, 2012Date of Patent: July 1, 2014Assignee: Halliburton Energy Services, Inc.Inventors: Brian Atkins, Seth G. Anderle, Robert W. Arfele, Ram L. Ladi, Brandon Paul Linford, Jason Keith Wiggins, Kevin Duy Nguyen, Jiang Qian, Kenneth Eugene Bertagnolli, Shawn Casey Scott, Debkumar Mukhopadhyay, Michael Alexander Vail
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Patent number: 8764863Abstract: A method of forming a shaped abrasive particle includes forming a first mixture and a second mixture in a single forming process into an integral precursor shaped abrasive particle, wherein the first mixture has a different composition than a composition of the second mixture.Type: GrantFiled: December 31, 2012Date of Patent: July 1, 2014Assignee: Saint-Gobain Ceramics & Plastics, Inc.Inventors: Doruk O. Yener, Paul Braun
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Patent number: 8758463Abstract: In one aspect, a vacuum-sealed can is used during the bonding process to improve the properties of an infiltrated TSP cutting element. In one embodiment, ultra hard diamond crystals and a catalyst material are sintered to form a polycrystalline diamond material (PCD). This PCD material is leached to remove the catalyst, forming a thermally stable product (TSP). The TSP material and a substrate are placed into an enclosure such as a can assembly, heated, and subjected to a vacuum in order to remove gas, moisture and other residuals that can inhibit infiltration of the infiltrant into the TSP layer. The can assembly is then subjected to high temperature, high pressure bonding to bond the TSP material to the substrate. During bonding, material from the substrate infiltrates the TSP layer.Type: GrantFiled: August 6, 2010Date of Patent: June 24, 2014Assignee: Smith International, Inc.Inventors: Peter T Cariveau, Ronald K Eyre, Yi Fang
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Patent number: 8758461Abstract: An abrasive article includes a shaped abrasive particle including a body having a first height (h1) at a first end of the body defining a corner between an upper surface, a first side surface, and a second side surface, and a second height (h2) at a second end of the body opposite the first end defining an edge between the upper surface and a third side surface, wherein the average difference in height between the first height and the second height is at least about 50 microns. The body also includes a bottom surface defining a bottom area (Ab) and a cross-sectional midpoint area (Am) defining an area of a plane perpendicular to the bottom area and extending through a midpoint of the particle, the body has an area ratio of bottom area to midpoint area (Ab/Am) of not greater than about 6.Type: GrantFiled: December 30, 2011Date of Patent: June 24, 2014Assignee: Saint-Gobain Ceramics & Plastics, Inc.Inventors: Doruk O. Yener, Jennifer H. Czerepinski, Sujatha Iyengar, Michael D. Kavanaugh
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Patent number: 8753413Abstract: Embodiments of the invention relate to polycrystalline diamond compacts (“PDCs”) comprising a polycrystalline diamond (“PCD”) table including a catalyst material therein that has been implanted with ions (e.g., carbon ions) and/or infiltrated from a host material implanted with carbon ions. In an embodiment, a PDC comprises a substrate and a PCD table bonded to the substrate. The PCD table includes a plurality of bonded diamond grains defining a plurality of interstitial regions. The PCD table includes an upper surface from which a region inwardly extends. At least a portion of the interstitial regions of the region includes a catalyst material disposed therein. At least a portion of the catalyst material may be at least saturated with carbon.Type: GrantFiled: November 9, 2011Date of Patent: June 17, 2014Assignee: US Synthetic CorporationInventor: Michael A. Vail
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Patent number: 8753412Abstract: An outer blade cutting wheel comprising an annular thin disc base of cemented carbide and a blade section is manufactured by disposing permanent magnet pieces on the side surfaces and inward of the outer periphery of the base to produce a magnetic field, providing magnetic coated diamond and/or CBN abrasive grains such that the magnetic field may act on the grains, causing the grains to be magnetically attracted to the base outer periphery, and electroplating or electroless plating whereby the abrasive grains are bound to the base outer periphery to form the blade section.Type: GrantFiled: April 29, 2010Date of Patent: June 17, 2014Assignee: Shin-Etsu Chemical Co., Ltd.Inventors: Masaki Kasashima, Yuhito Doi, Harukazu Maegawa, Takehisa Minowa
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Patent number: 8741005Abstract: A method of processing a polycrystalline diamond material is disclosed. According to the method, a metal-solvent catalyst is leached from a polycrystalline diamond material by exposing at least a portion of the polycrystalline diamond material to a leaching composition. The leaching composition includes water, a complexing agent, and hydrofluoric acid.Type: GrantFiled: January 7, 2013Date of Patent: June 3, 2014Assignee: US Synthetic CorporationInventor: Andrew E. Dadson
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Patent number: 8734550Abstract: Embodiments of the present invention relate to PDCs including a PCD table having an exterior cutting region that exhibits enhanced thermal stability. In one embodiment, a method comprises forming an assembly including a first region having non-diamond carbon material and a second region having a plurality of diamond particles. The method comprises subjecting the assembly to heat and pressure sufficient to form the PDC. In another embodiment, a PDC comprises a substrate and a PCD table bonded to the substrate. The PCD table comprises an exterior cutting region including a plurality of elongated diamond grains that are generally randomly oriented. The PCD table comprises a main region positioned between the substrate and exterior cutting region, and including a plurality of bonded diamond grains. In another embodiment, the first region may include coarse-sized diamond particles instead of non-diamond carbon material.Type: GrantFiled: October 26, 2010Date of Patent: May 27, 2014Assignee: US Synthetic CorporationInventor: Mohammad N. Sani
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Patent number: 8734753Abstract: A method is provided of etching a diamond particle including the step of heating the particle at a temperature of about 700° C. or greater in the presence of water vapor to form an etched particle. Also provided is an etched particle having a core and a surface. The core is formed of sp3 hybridized carbon atoms covalently bonded together, and the surface has substantially no chlorine atoms, oxygen atoms or oxygen species.Type: GrantFiled: December 30, 2010Date of Patent: May 27, 2014Assignee: Engis CorporationInventors: Ion C. Benea, Benjamin Rosczyk, Laura Fitzgerald
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Patent number: 8728185Abstract: Shaped abrasive particles comprising a ceramic and comprising a first plate integrally joined to a second plate at a predetermined angle?.Type: GrantFiled: August 3, 2011Date of Patent: May 20, 2014Assignee: 3M Innovative Properties CompanyInventor: Negus B. Adefris
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Patent number: 8721751Abstract: An abrasive article including an abrasive body having abrasive grains made of microcrystalline alumina contained within a bond material, wherein the bond material comprises a total content of alumina of at least about 15 mol %.Type: GrantFiled: December 2, 2010Date of Patent: May 13, 2014Assignees: Saint-Gobain Abrasives, Inc., Saint-Gobain AbrasifsInventors: Gilles Querel, Sandhya Jayaraman Rukmani, Muthu Jeevanantham, Kelley McNeal, Maike Hillers
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Patent number: 8721752Abstract: A PCD cutting element for use in earth boring drill bits where die interstices remote from the working surface are filled with a catalyzing material and the interstices adjacent to the working surface are substantially free of the catalyzing material is described. An intermediate region between the substantially free portion and filled portion has a plurality of generally conically sectioned catalyst-free projections which taper down, extending to a second depth from the planar working surface, preferably about 0.5 times or more of the first depth.Type: GrantFiled: August 14, 2008Date of Patent: May 13, 2014Assignee: Reedhycalog UK LimitedInventors: John Michael Fuller, Douglas Caraway, Graham Richard Watson
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Publication number: 20140120811Abstract: A method for producing at least one abrasive unit that has at least two abrasive bodies connected at least partially to each other via at least one perforation includes trimming at least one edge of the abrasive unit with at least one laser cutting method. The edge of the abrasive unit is at least partially formed by the laser cutting method so as to have at least one curvature.Type: ApplicationFiled: October 29, 2013Publication date: May 1, 2014Applicant: Robert Bosch GmbHInventors: Adrian Schoch, Stephan Fritsch
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Patent number: 8709114Abstract: A method of manufacturing polishing layers for use in chemical mechanical polishing pads is provided, wherein a plurality of polishing layers are derived from a cake, wherein the formation of density defects in the cake and the surface roughness of the polishing layers formed are minimized.Type: GrantFiled: March 22, 2012Date of Patent: April 29, 2014Assignee: Rohm and Haas Electronic Materials CMP Holdings, Inc.Inventors: Brian T. Cantrell, Kathleen McHugh, James T. Murnane, George H. McClain, Durron A. Hutt, Robert A. Brady, Christopher A. Young, Jeffrey Borcherdt Miller
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Patent number: 8702825Abstract: A method of forming a cutting element that includes filling at least one non-planar region on an upper surface of a carbide substrate with a diamond mixture, subjecting the substrate and the diamond mixture to high pressure high temperature sintering conditions to form a reduced-CTE substrate having polycrystalline diamond that extends a depth into the reduced-CTE substrate in an interface region, and an upper surface made of a composite surface of diamond and carbide, and attaching a polycrystalline diamond body to the composite surface of the reduced-CTE substrate is disclosed.Type: GrantFiled: February 9, 2011Date of Patent: April 22, 2014Assignee: Smith International, Inc.Inventors: Yuelin Shen, Youhe Zhang, Jibin Shi, Yuri Burhan, Gregory T. Lockwood
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Patent number: 8689909Abstract: An insert for an earth-boring tool includes a body and a coating disposed over at least a portion of the body. The coating comprises a ceramic comprising boron, aluminum, and magnesium. Polycrystalline diamond compact cutting elements may include a hard polycrystalline material, a supporting substrate, and a coating disposed over at least a portion of the hard polycrystalline material. An earth-boring drill bit may include a bit body and at least one polycrystalline diamond compact cutting element secured to the bit body. The polycrystalline diamond compact cutting element may have a coating comprising a ceramic of boron, aluminum, and magnesium, and may be disposed over at least a portion of a hard polycrystalline material. A method of forming an insert for an earth-boring tool may include forming a protective coating including a ceramic of boron, aluminum, and magnesium over a cutting element.Type: GrantFiled: October 17, 2011Date of Patent: April 8, 2014Assignee: Baker Hughes IncorporatedInventor: Anthony A. DiGiovanni
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Publication number: 20140094101Abstract: This invention relates to a conditioner for a CMP (Chemical Mechanical Polishing) pad, which is used in a CMP process which is part of the fabrication of a semiconductor device, and more particularly, to a CMP pad conditioner in which the structure of the cutting tips is such that the change in the wear of the polishing pad is not great even when different kinds of slurry are used and when there are changes in pressure of the conditioner, and to a method of manufacturing the same.Type: ApplicationFiled: May 15, 2012Publication date: April 3, 2014Applicants: SAMSUNG ELECTRONICS CO., LTD., EHWA DIAMOND INDUSTRIAL CO., LTD.Inventors: Seh Kwang Lee, Youn Chul Kim, Joo Han Lee, Jae Kwang Choi, Jae Phil Boo