Metal Or Metal Oxide Patents (Class 51/309)
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Patent number: 10202309Abstract: A cBN sintered material cutting tool is provided. The cBN cutting tool includes a cutting tool body, which is a sintered material including cBN grains and a binder phase, wherein the sintered material comprises: the cubic boron nitride grains in a range of 40 volume % or more and less than 60 volume %; and Al in a range from a lower limit of 2 mass % to an upper limit Y, satisfying a relationship, Y=?0.1X+10, Y and X being an Al content in mass % and a content of the cubic boron nitride grains in volume %, respectively, the binder phase comprises: at least a Ti compound; Al2O3; and inevitable impurities, the Al2O3 includes fine Al2O3 grains with a diameter of 10 nm to 100 nm dispersedly formed in the binder phase, and there are 30 or more of the fine Al2O3 grains generated in an area of 1 ?m×1 ?m in a cross section of the binder phase.Type: GrantFiled: March 27, 2015Date of Patent: February 12, 2019Assignee: MITSUBISHI MATERIALS CORPORATIONInventors: Kenji Yumoto, Yosuke Miyashita
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Patent number: 10160658Abstract: The present invention relates to cerium oxide particles that have excellent heat resistance especially useful for catalysts, functional ceramics, solid electrolyte for fuel cells, polishing, ultraviolet absorbers and the like, and particularly suitable for use as a catalyst or co-catalyst material, for instance in catalysis for purifying vehicle exhaust gas. The present invention also relates to a method for preparing such cerium oxide particles, and a catalyst, such as for purifying exhaust gas, utilizing these cerium oxide particles.Type: GrantFiled: November 10, 2015Date of Patent: December 25, 2018Assignee: Rhodia OperationsInventors: Naotaka Ohtake, Mitsuhiro Okazumi, Fabien Ocampo
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Patent number: 10155892Abstract: Abrasive particles include: 0.50 to 5.00 weight percent of seed particles for alpha-alumina formation selected from the group consisting of alpha-Fe2O3 seed particles, alpha-Al2O3 seed particles, and combinations thereof; 0.50 to 5.00 weight percent of MgO; 0.02 to 0.40 weight percent of Li2O or a molar equivalent amount of at least one alkali metal oxide selected from the group consisting of: Na2O; K2O; combinations of Na2O and Li2O; combinations of K2O and Li2O; combinations of Na2O and K2O; and combinations of Li2O, Na2O, and K2O; and 91.08 to 99.48 weight percent of Al2O3. Methods of making the abrasive particles and abrasive articles incorporating them are also disclosed.Type: GrantFiled: February 13, 2015Date of Patent: December 18, 2018Assignee: 3M Innovative Properties CompanyInventors: Larry D. Monroe, Grant E. Greske
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Patent number: 10113239Abstract: A cutting tool includes: a base including cemented carbide containing Cr; and a coating layer including a Ti-based layer including at least a layer of Ti(Cx1Ny1Oz1) (0?x1?1, 0?y1?1, 0?z1?1, x1+y1+z1=1), an Al2O3 layer, and an outermost layer of Ti(Cx3Ny3Oz3) (0?x3?1, 0?y3?1, 0?z3?1, x3+y3+z3=1), and a content of Cr contained at a first Ti-based layer of the Ti-based layer is lower than a content of Cr contained in the base, and higher than a content of Cr contained at the Al2O3 layer, and a content of Cr contained at the outermost layer is higher than the content of Cr contained at the Al2O3 layer in a glow-discharge emission spectrometry.Type: GrantFiled: November 26, 2014Date of Patent: October 30, 2018Assignee: KYOCERA CORPORATIONInventors: Hayato Kubo, Kou Ri
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Patent number: 10106714Abstract: A shaped abrasive particle including a body having a length (l), a width (w), and a height (hi), wherein the height is at least about 28% of the width, and a percent flashing (f) of at least about 10% and not greater than about 45% for a total side area of the body.Type: GrantFiled: June 28, 2013Date of Patent: October 23, 2018Assignee: SAINT-GOBAIN CERAMICS & PLASTICS, INC.Inventors: Doruk O. Yener, Jennifer H. Czerepinski, Michael D. Kavanaugh, Samuel S. Marlin, Kristin K. Breder, Sujatha Iyengar
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Patent number: 10053755Abstract: A method for treating a super-hard structure, the method including heating the super-hard structure to a treatment temperature of at least 500 degrees centigrade and cooling the super-hard structure from the treatment temperature to a temperature of less than 200 degrees centigrade at a mean cooling rate of at least 1 degree centigrade per second and at most 100 degrees centigrade per second to provide a treated super-hard structure. A PCBN structure produced by the method may have flexural strength of at least 650 MPa.Type: GrantFiled: May 25, 2012Date of Patent: August 21, 2018Assignee: Element Six LimitedInventors: Declan John Carolan, Neal Murphy, Alojz Ivankovic
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Patent number: 10047248Abstract: A slurry composition for the CMP process includes a dispersion medium, and ceria particles having a NO3 functional group bonded to surfaces thereof. The ceria particles are contained in an amount of about 0.1 parts by weight to about 15 parts by weight based on 100 parts by weight of the dispersion medium.Type: GrantFiled: October 14, 2016Date of Patent: August 14, 2018Assignees: Samsung Electronics Co., Ltd., Industry-University Cooperation Foundation Hanyang UniversityInventors: Ye-hwan Kim, Un-gyu Paik, Ji-hoon Seo
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Patent number: 10040971Abstract: Disclosed is a polishing agent comprising: water; tetravalent metal hydroxide particles; and an additive, wherein the additive contains at least one of a cationic polymer and a cationic polysaccharide. The present invention can provide a polishing agent which is capable of polishing an insulating film at a high speed with less polishing flaws, and having a high polishing rate ratio of a silicon oxide film and a stopper film, in the CMP technology of flattening insulating film. The present invention can also provide a polishing agent set for storing the polishing agent, and a method for polishing a substrate using this polishing agent.Type: GrantFiled: September 23, 2016Date of Patent: August 7, 2018Assignee: HITACHI CHEMICAL COMPANY, LTD.Inventors: Yousuke Hoshi, Daisuke Ryuzaki, Naoyuki Koyama, Shigeru Nobe
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Patent number: 10011000Abstract: A method of processing a polycrystalline diamond material includes exposing at least a portion of a polycrystalline diamond material to a processing solution, the polycrystalline diamond material including a metallic material disposed in interstitial spaces defined within the polycrystalline diamond material. The method includes exposing an electrode to the processing solution, applying a positive charge to the polycrystalline diamond material, and applying a negative charge to the electrode. An assembly for processing a polycrystalline diamond body includes a polycrystalline diamond body and an electrode that are in electrical communication with a volume of processing solution, and a power source configured to apply a positive charge to the polycrystalline diamond body and a negative charge to the electrode.Type: GrantFiled: September 24, 2015Date of Patent: July 3, 2018Assignee: US SYNTHETIC CORPORATIONInventors: Daren Nathaniel Heaton, Jeremy Brett Lynn, Mark Pehrson Chapman, Oakley D. Bond
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Patent number: 9993878Abstract: A coated cutting tool includes a substrate and a coating layer formed onto the surface of the substrate. The coating layer contains an ?-type aluminum oxide layer. A residual stress value at the (116) plane of the ?-type aluminum oxide layer is greater than 0. A residual stress value at the (012) plane of the ?-type aluminum oxide layer is smaller than 0.Type: GrantFiled: November 7, 2014Date of Patent: June 12, 2018Assignee: TUNGALOY CORPORATIONInventors: Kinya Takahashi, Hiroyuki Satoh
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Patent number: 9981317Abstract: A polycrystalline CVD synthetic diamond work piece for use in a polycrystalline CVD synthetic diamond tool, the polycrystalline CVD synthetic diamond work piece comprising: a working surface; and a rear mounting surface; wherein an average lateral grain size of the rear mounting surface is no less than 10 ?m, and wherein the working surface comprises: (a) smaller diamond grains than the rear mounting surface; (b) an average lateral grain size in a range 10 nm to 15 ?m; and (c) a Raman signal generated by a laser focused on the working surface which exhibits one or more of the following characteristics: (1) an sp3 carbon peak at 1332 cm?1 having a full width half-maximum of no more than 8.Type: GrantFiled: November 20, 2014Date of Patent: May 29, 2018Assignee: Element Six Technologies LimitedInventor: Mark McClymont
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Patent number: 9982177Abstract: A slurry includes abrasive grains and water, wherein the abrasive grains include tetravalent cerium hydroxide particles and produce light transmittance of at least 50%/cm for light with a wavelength of 500 nm in an aqueous dispersion with the content of the abrasive grains adjusted to 1.0 mass %. A polishing liquid includes abrasive grains, an additive and water, wherein the abrasive grains include tetravalent cerium hydroxide particles and produce light transmittance of at least 50%/cm for light with a wavelength of 500 nm in an aqueous dispersion with the content of the abrasive grains adjusted to 1.0 mass %.Type: GrantFiled: January 20, 2011Date of Patent: May 29, 2018Assignee: HITACHI CHEMICAL COMPANY, LTDInventors: Tomohiro Iwano, Hirotaka Akimoto, Takenori Narita, Tadahiro Kimura, Daisuke Ryuzaki
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Patent number: 9980480Abstract: Biocidal roofing granules are prepared by providing a mineral core and at least one biocidal photocatalytic metal oxide. A gel-forming inorganic coating medium is prepared and used to coat the mineral core to form a coating layer having a porous network on the mineral core, and the at least one biocidal photocatalytic metal oxide is disposed in the porous network.Type: GrantFiled: January 11, 2012Date of Patent: May 29, 2018Assignee: CertainTeed CorporationInventors: Sophie Vanpoulle, Van Nhan Nguyen, Alexandra Dekoninck
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Patent number: 9963348Abstract: Apparatuses and methods for leaching catalysts from a polycrystalline diamond compact (PDC) may utilize a high pressure jet. For example, a method may include impinging a jet of leaching fluid, including one or both of an acid and a caustic material, on a surface of a PDC disposed on a substrate at a fluid pressure ranging between 125 psi and 10,000.Type: GrantFiled: June 4, 2014Date of Patent: May 8, 2018Assignee: HALLIBURTON ENERGY SERVICES, INC.Inventor: Gary E. Weaver
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Patent number: 9881802Abstract: A polishing liquid includes abrasive grains, an additive and water, wherein the abrasive grains include a tetravalent metal element hydroxide, and produce a liquid phase with a nonvolatile content of 500 ppm or greater when an aqueous dispersion with a content of the abrasive grains adjusted to 1.0 mass % has been centrifuged for 50 minutes at a centrifugal acceleration of 1.59×105 G.Type: GrantFiled: January 31, 2013Date of Patent: January 30, 2018Assignee: HITACHI CHEMICAL COMPANY, LTDInventor: Tomohiro Iwano
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Patent number: 9873185Abstract: A system and process for rapid and uniform curing of grinding wheels (2) to obtain grinding wheels (2) with better durability, at 180-220° C. deploying microwave energy at 800-5000 MHz in which closely fitting green wheel sample holders (1) are made of carbon bearing microwave susceptor materials such as graphite, silicon carbide with tiny holes on the surface. These sample holders (1) help in maintaining the shape and geometry of the final wheels (2) after curing and reduce energy consumption. The performance of the grinding wheels (2) cured by this process is better than those cured by presently used process employing steel plate sample holders of the present state-of-art.Type: GrantFiled: July 17, 2013Date of Patent: January 23, 2018Assignee: Pradeep Metals LimitedInventors: Pradeep Goyal, Shivanand Borkar, Ritesh Jaiswal
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Patent number: 9840649Abstract: A superabrasive material and method of making the superabrasive material are provided. The superabrasive material may comprise a superabrasive crystal having an irregular surface. The superabrasive material further comprises a plurality of structure defects within the superabrasive crystal. The plurality of structure defects may cause micro-chipping when used as grinding materials.Type: GrantFiled: September 16, 2013Date of Patent: December 12, 2017Assignee: DIAMOND INNOVATIONS INC.Inventors: Shuang Ji, Christopher Long, Susanne Sowers, Kai Zhang
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Patent number: 9828528Abstract: The invention provides a chemical-mechanical polishing composition including first abrasive particles, wherein the first abrasive particles are wet-process ceria particles, have a median particle size of about 40 nm to about 100 nm, are present in the polishing composition at a concentration of about 0.005 wt. % to about 2 wt. %, and have a particle size distribution of at least about 300 nm, a functionalized heterocycle, a pH-adjusting agent, and an aqueous carrier, and wherein the pH of the polishing composition is about 1 to about 6. The invention also provides a method of polishing a substrate, especially a substrate comprising a silicon oxide layer, with the polishing composition.Type: GrantFiled: October 31, 2016Date of Patent: November 28, 2017Assignee: Cabot Microelectronics CorporationInventors: Brian Reiss, Dana Sauter Van Ness, Viet Lam, Alexander Hains, Steven Kraft, Renhe Jia
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Patent number: 9790411Abstract: An abrasive article can include a body including a bond material and abrasive particles contained within the bond material. The abrasive particles can include nanocrystalline alumina. The bond material can include an organic material. In an embodiment, the nanocrystalline alumina may have an average crystallite size of not greater than 1.5 microns. In another embodiment, the bond material and the abrasive particles may be mixed and the mixture may cure to form the abrasive article of embodiments herein.Type: GrantFiled: December 30, 2015Date of Patent: October 17, 2017Assignees: SAINT-GOBAIN ABRASIVES, INC., SAINT-GOBAIN ABRASIFSInventors: Yang Zhong, Nilanjan Sarangi, Shu Yang, Ralph Bauer, Stefan Vujcic
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Patent number: 9758697Abstract: The invention provides chemical-mechanical polishing compositions and methods of chemically-mechanically polishing a substrate, especially a substrate comprising a silicon oxide layer, with the chemical-mechanical polishing compositions. The polishing compositions comprise first abrasive particles, wherein the first abrasive particles are wet-process ceria particles, have a median particle size of about 75 nm to about 200 nm, and are present in the polishing composition at a concentration of about 0.005 wt. % to about 2 wt. % a functionalized heterocycle, a cationic polymer selected from a quaternary amine, is cationic polyvinyl alcohol, and a cationic cellulose, optionally a carboxylic acid, a pH-adjusting agent, and an aqueous carrier, and have a pH of about 1 to about 6.Type: GrantFiled: March 5, 2015Date of Patent: September 12, 2017Assignee: Cabot Microelectronics CorporationInventors: Brian Reiss, Dana Sauter Van Ness, Viet Lam, Renhe Jia
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Patent number: 9724424Abstract: A quartz or otherwise similar crystal (‘host crystal’) embedded with minerals, metals, homeopathic, organic/inorganic, and magnetic materials (which allow for magnetic interactions) and the method for embedded ‘host crystal’ with said materials is disclosed. The ‘host crystal’ can be any size, shape, cut, or color of crystal. A hole/depression is first drilled/etched anywhere on the quartz or similar ‘host crystal’, this hole is then filled with a chosen combination of materials using force/compression, and are semi-permanently sealed by compressing metal flake or powder onto/into the top of the material-filled hole in the ‘host crystal’.Type: GrantFiled: March 15, 2013Date of Patent: August 8, 2017Inventors: DeCauter Ward Stoppelbein, Carly Ann Babb
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Patent number: 9701043Abstract: An object of the present invention is to provide a dicing blade which does not cause cracking and breaking even in a workpiece formed from a brittle material, and can stably perform cutting process in a ductile mode on the workpiece with high precision. A dicing blade 26 which performs the cutting process on the workpiece is integrally formed of a diamond sintered body 80 which is formed by sintering diamond abrasive grains 82 so as to have a discoid shape, and a content of the diamond abrasive grains 82 of the diamond sintered body 80 is 80 vol % or more. It is preferable that recessed parts which are formed on a surface of the diamond sintered body 80 are continuously provided in an outer circumferential part of the dicing blade 26 along a circumferential direction.Type: GrantFiled: April 24, 2013Date of Patent: July 11, 2017Assignees: Tokyo Seimitsu Co., Ltd., Shin-Nihon Tech Inc.Inventors: Takashi Fujita, Yasuo Izumi, Junji Watanabe
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Patent number: 9694426Abstract: There is provided a cutting tool having high wear resistance and fracture resistance by reducing the occurrence of thermal cracking on a cutting edge even during a cutting process of a heat-resistant alloy in which the cutting edge reaches high temperatures. The cutting tool is made from a cemented carbide that is composed mainly of a WC phase and contains 11.5-12.5% by mass of Co and 0.2-0.6% by mass of Cr in terms of Cr3C2. The WC phase has a mean particle size of 0.85-1.05 ?m, an antimagnetic force (Hc) of 13.0-16.0 kA/m, and a Rockwell hardness (HRA) of 89.5-90.5.Type: GrantFiled: November 29, 2013Date of Patent: July 4, 2017Assignee: KYOCERA CORPORATIONInventor: Takahiko Makino
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Patent number: 9676077Abstract: An abrasive article includes a body having abrasive grains contained within a bond material comprising a metal or metal alloy, wherein the body comprises a ratio of VAG/VBM of at least about 1.3, wherein VAG is the volume percent of abrasive grains within the total volume of the body and VBM is the volume percent of bond material within the total volume of the body.Type: GrantFiled: December 30, 2015Date of Patent: June 13, 2017Assignees: SAINT-GOBAIN ABRASIVES, INC., SAINT-GOBAIN ABRASIFSInventors: Srinivasan Ramanath, Kenneth A. Saucier, Rachana Upadhyay
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Patent number: 9669508Abstract: A grinding wheel assembly for use in a sharpening system includes a grinding wheel configured to be mounted in the sharpening system to carry out sharpening operations in which the grinding wheel removes material from a blade to be sharpened, such as the blade of an ice skate. The grinding wheel assembly further includes an identification tag attached to the grinding wheel, the identification tag having (1) secure memory including a usage location for persistently and securely storing a usage tracking value, and (2) interface circuitry for engaging in communication with a transceiver of the sharpening system to enable electronic circuitry of the sharpening system to both read from and write to the usage location to track usage of the grinding wheel for sharpening operations. The memory may also store other data including user-specific system parameters usable to customize operation, and fault information usable to diagnose fault conditions.Type: GrantFiled: October 24, 2014Date of Patent: June 6, 2017Assignee: VELASA SPORTS, INC.Inventors: Russell K. Layton, Jr., Daniel A. Beaudet, Ivan D. Goryachev
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Patent number: 9656297Abstract: A pretreatment solution and process for pretreating steel substrates with an aqueous solution to form a thin partially crosslinked layer that passivates the steel surface and inhibits the formation of flash rust, in which the thin partially crosslinked layer is dried in ambient air, and the dried layer enhances the cathodic disbondment resistance of the overlying paint system. In the process an aqueous precursor solution (A) containing at least one amino-functional silane, at least one of a dissolved silicate or a dissolved aluminate and at least a metal salt; is mixed with an aqueous precursor solution (B) containing at least an epoxy resin. The molar amount of amino-functional silane in precursor solution (A) is at considerably lower than the stoichiometric amount that is needed for completing the crosslinking reaction with the epoxy resin in precursor solution (B) so that unreacted epoxy groups are made available for further crosslinking with the overlying paint.Type: GrantFiled: June 24, 2013Date of Patent: May 23, 2017Assignee: NEI CorporationInventor: Jiong Liu
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Patent number: 9650712Abstract: In one aspect, articles are described herein comprising refractory coatings employing an inter-anchored multilayer architecture. Articles having refractory coatings described herein, in some embodiments, are suitable for high wear and/or abrasion applications such as metal cutting operations. A coated article described herein comprises a substrate and a coating deposited by CVD adhered to the substrate, the coating including a refractory layer comprising a plurality of sublayer groups, a sublayer group comprising a Group IVB metal nitride sublayer and an adjacent layer alumina sublayer, the Group IVB metal nitride sublayer comprising a plurality of nodules interfacing with the alumina sublayer.Type: GrantFiled: December 8, 2014Date of Patent: May 16, 2017Assignee: KENNAMETAL INC.Inventors: Zhenyu Liu, Yixiong Liu
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Patent number: 9636800Abstract: A cubic nitride compact containing a polycrystalline mass of cubic boron nitride particles, present in an amount of at least 70 percent by volume, and a binder phase, which is metallic in character. In addition, a compact in which the binder phase is preferably superalloy in character.Type: GrantFiled: December 19, 2012Date of Patent: May 2, 2017Assignee: ELEMENT SIX ABRASIVES S.A.Inventors: Anton Raoul Twersky, Nedret Can
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Patent number: 9597774Abstract: A cubic nitride compact having a polycrystalline mass of cubic boron nitride particles, present in an amount of at least 70 percent by volume and a binder phase, which is metallic in character. In addition, a compact in which the binder phase is preferably superalloy in character.Type: GrantFiled: December 11, 2007Date of Patent: March 21, 2017Assignee: ELEMENT SIX ABRASIVES S.A.Inventors: Anton Raoul Twersky, Nedret Can
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Patent number: 9566649Abstract: A coated cutting tool has a base material of a WC-based cemented carbide and a film formed on the surface of the base material by a chemical vapor deposition method. The coated cutting tool has a rake face, a flank face and a cutting edge ridgeline part positioned between the rake face and the flank face being provided, wherein a total film thickness of the entire film is 3 to 20 ?m in an average film thickness, and one or more oblique cracks where an extension angle of the crack to the surface of the film is 45° or less are present at the rake face within 300 ?m from the cutting edge ridgeline part.Type: GrantFiled: September 24, 2012Date of Patent: February 14, 2017Assignee: Tungaloy CorporationInventor: Yusuke Hirano
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Patent number: 9539701Abstract: An abrasive article includes a bonded abrasive body having abrasive particles comprising microcrystalline alumina (MCA) contained within a bond material. In an embodiment, the bonded abrasive body has a strength ratio (MOR/MOE) of at least about 0.80. Additionally, the bonded abrasive body may have a MOR of at least 40 MPa for a MOE or at least about 40 GPa and the bonded abrasive body may be capable of grinding a workpiece that includes metal at a speed of at least about 60 m/s at a material removal rate of at least about 0.4 in3/min/in (258 mm3/min/mm).Type: GrantFiled: March 30, 2012Date of Patent: January 10, 2017Assignees: SAINT-GOBAIN ABRASIVES, INC., SAINT-GOBAIN ABRASIFSInventors: Nilanjan Sarangi, Renaud Fix, Stephen Woods, Jim M. Gaffney, John Campaniello, John R. Besse, Stephen E. Fox
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Patent number: 9505952Abstract: The invention provides a chemical-mechanical polishing composition including first abrasive particles, wherein the first abrasive particles are wet-process ceria particles, have a median particle size of about 40 nm to about 100 nm, are present in the polishing composition at a concentration of about 0.005 wt. % to about 2 wt. %, and have a particle size distribution of at least about 300 nm, a functionalized heterocycle, a pH-adjusting agent, and an aqueous carrier, and wherein the pH of the polishing composition is about 1 to about 6. The invention also provides a method of polishing a substrate, especially a substrate comprising a silicon oxide layer, with the polishing composition.Type: GrantFiled: March 5, 2015Date of Patent: November 29, 2016Assignee: Cabot Microelectronics CorporationInventors: Brian Reiss, Dana Sauter Van Ness, Viet Lam, Alexander Hains, Steven Kraft, Renhe Jia
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Patent number: 9480970Abstract: The present invention relates to a carrier for supporting a catalyst for a spacecraft thruster and to a method for preparing the same, and more particularly, to a catalyst carrier for a spacecraft thruster and method for preparing the same, in which the diameter and distribution of pores of the carrier are controlled using a pore inducing material to lengthen the life of the catalyst.Type: GrantFiled: December 21, 2010Date of Patent: November 1, 2016Assignee: Korea Aerospace Research InstituteInventors: Su Kyum Kim, Myoung Jong Yu, Sung June Cho, Sang Ryool Lee
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Patent number: 9446502Abstract: Precursor alpha alumina abrasive particles in a mold are subjected to a drying process that cracks or fractures at least a majority of the precursor abrasive particles into at least two pieces thereby producing abrasive shards having a smaller size than the mold cavity from which they were made. The smaller abrasive shards, once formed, could be reassembled like jigsaw puzzle pieces to reproduce the original cavity shape of the mold from which they were made. The cracking or fracturing of the precursor abrasive particles is believed to occur by ensuring that the surface tension of the abrasive dispersion to the walls of the mold is greater than the internal attractive forces of the abrasive dispersion as the abrasive dispersion is dried within the mold cavity.Type: GrantFiled: September 8, 2011Date of Patent: September 20, 2016Assignee: 3M Innovative Properties CompanyInventors: Dwight D. Erickson, Scott R. Culler, Negus B. Adefris, John T. Boden, John D. Haas
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Patent number: 9403282Abstract: A diamond-containing blade includes a blade body having at proximal end a connection part to be fitted into a gripper; and an edge longitudinally formed along one side of the blade body, wherein the blade is manufactured by a process in which a powder mixture for constituting the edge, including 20 wt % or less of diamond particles coated with Ti and having a particle size of 20 ?m or less and residual Ti powder or Ti alloy powder, is charged in a space of a mold corresponding to the edge, Ti powder or Ti alloy powder for constituting the blade body is charged in another space of the mold corresponding to the blade body, the charged powders are pressed to obtain a molded product, the molded product is sintered to obtain a sintered body, and then an edge of the sintered body is sharpened.Type: GrantFiled: September 10, 2012Date of Patent: August 2, 2016Assignee: FOREVER CO., LTD.Inventor: Kimiko Sueda
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Patent number: 9394592Abstract: The invention relates to hard-metal body comprising a hard-metal, the hard-metal comprising tungsten carbide grains and metal binder comprising cobalt having a concentration of tungsten dissolved therein, the body comprising a surface region adjacent a surface and a core region remote from the surface, the surface region and the core region being contiguous with each other; the mean binder fraction of the core region being greater than that of the surface region; the mean carbon concentration within the binder being higher in the surface region than in the core region; to tools comprising same and methods of making same.Type: GrantFiled: January 3, 2014Date of Patent: July 19, 2016Assignee: ELEMENT SIX GMBHInventors: Igor Yuri Konyashin, Sebastian Ralf Hlawatschek, Bernd Heinrich Ries, Frank Friedrich Lachmann
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Patent number: 9382602Abstract: The present invention relates to tungsten-rhenium coated compounds, materials formed from tungsten-rhenium coated compounds, and to methods of forming the same. In embodiments, tungsten and rhenium are coated on ultra hard material particles to form coated ultra hard material particles, and the coated ultra hard material particles are sintered at high temperature and high pressure.Type: GrantFiled: August 30, 2012Date of Patent: July 5, 2016Assignee: Smith International, Inc.Inventors: Yahua Bao, Scott L. Horman
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Patent number: 9346978Abstract: A polishing liquid comprising an abrasive grain, an additive, and water, wherein the abrasive grain includes a hydroxide of a tetravalent metal element, produces absorbance of 1.00 or more for light having a wavelength of 400 nm in an aqueous dispersion having a content of the abrasive grain adjusted to 1.0 mass %, and produces light transmittance of 50%/cm or more for light having a wavelength of 500 nm in an aqueous dispersion having a content of the abrasive grain adjusted to 1.0 mass %, and a difference between a NO3? concentration of an aqueous dispersion having a content of the abrasive grain adjusted to 1.0 mass % and a NO3? concentration after retaining the aqueous dispersion at 60° C. for 72 hours is 200 ppm or less.Type: GrantFiled: March 26, 2013Date of Patent: May 24, 2016Assignee: HITACHI CHEMICAL COMPANY, LTD.Inventors: Tomohiro Iwano, Hisataka Minami, Toshiaki Akutsu, Koji Fujisaki
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Patent number: 9334561Abstract: The present invention relates to a coated cutting tool comprising a substrate and a multilayered (Ti,Al)N coating. The coating comprises three zones: a first zone (A) closest to the substrate, a second zone (B) adjacent to the first zone and a third outermost zone (C). All three zones each comprises a multilayered aperiodic structure of (Ti,Al)N, where the average composition for each zone is different from each other and where the ratio between the thickness of the zone C and zone B is between 1.3 and 2.2 and where zzone C>Zzone B, where z is the average composition for each zone of the ratio z=Ti/Al. The coating has a low residual stress.Type: GrantFiled: February 26, 2013Date of Patent: May 10, 2016Assignee: SANDVIK INTELLECTUAL PROPERTY ABInventor: Bjorn Ericsson
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Patent number: 9303462Abstract: A cutter assembly includes a substrate and at least one island. The substrate includes a surface circumscribed by a peripheral edge, a flank surface extending from the peripheral edge, and at least one pocket with an opening on the surface and spaced apart from the peripheral edge. The at least one pocket extends from the opening towards an interior of the substrate. The at least one island is in the at least one pocket, and the at least one island includes a cutting surface that is exposed by the opening of the at least one pocket.Type: GrantFiled: December 29, 2011Date of Patent: April 5, 2016Assignee: Diamond Innovations, Inc.Inventors: Yuanbo Lin, Bruce J. Reierson, Joseph M. Rhodes, John W. Lucek
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Patent number: 9303305Abstract: A method for applying a non-magnetic, abrasive, wear-resistant hardfacing material to a surface of a drill string member includes providing a non-magnetic drill string member formed of a non-magnetic material, the drill string member having an outer surface. It also includes providing a non-magnetic hardfacing precursor material comprising a plurality of non-magnetic, sintered carbide pellets and a non-magnetic matrix material; heating a portion of the non-magnetic hardfacing precursor material to a temperature above the melting point of the matrix material to melt the matrix material. It further includes applying the molten non-magnetic matrix material and the plurality of non-magnetic, sintered carbide pellets to the exterior surface of the drill string member; and solidifying the molten non-magnetic matrix material to form a layer of a non-magnetic hardfacing material having a plurality of non-magnetic, sintered carbide pellets dispersed in the hardfacing material.Type: GrantFiled: January 27, 2012Date of Patent: April 5, 2016Assignee: BAKER HUGHES INCORPORATEDInventors: James L. Overstreet, Jimmy W. Eason, Travis Puzz
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Patent number: 9287127Abstract: A wafer polishing process includes polishing a central area on the back side of a wafer, polishing a peripheral area on the back side of the wafer, buffing the central area, and buffing the peripheral area. The process can significantly reduce scratch-related wafer breakage, can correct focus spots on wafers, and can replace cleaning processes that use chemical etchants. Polishing and buffing can include polishing and buffing the bevel region. Further improvements include polishing with abrasive pads having a soft backing, polishing or buffing with pads having relatively soft abrasive particles, polishing or buffing with abrasive pads made from abrasive particles that have been sorted and selected for regularity of shape, irrigating the surface being polished or buffed with an aqueous solution that includes a friction-reducing agent, and buffing with abrasive pads having 20 k or finer grit or non-abrasive pads.Type: GrantFiled: February 17, 2014Date of Patent: March 15, 2016Assignee: Taiwan Semiconductor Manufacturing Co., Ltd.Inventors: Shen-Nan Lee, Teng-Chun Tsai, Hsin-Hsien Lu, Chang-Sheng Lin, Kuo-Cheng Lien, Kuo-Yin Lin, Wen-Kuei Liu, Yu-Wei Chou
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Patent number: 9283637Abstract: Tools for friction stir welding can be made with fewer process steps, lower cost techniques, and/or lower cost ingredients than other state-of-the-art processes by utilizing improved compositions and processes of fabrication. Furthermore, the tools resulting from the improved compositions and processes of fabrication can exhibit better distribution and homogeneity of chemical constituents, greater strength, and/or increased durability. In one example, a friction stir weld tool includes tungsten and rhenium and is characterized by carbide and oxide dispersoids, by carbide particulates, and by grains that comprise a solid solution of the tungsten and rhenium. The grains do not exceed 10 micrometers in diameter.Type: GrantFiled: January 22, 2013Date of Patent: March 15, 2016Assignee: Battelle Memorial InstituteInventors: Glenn J. Grant, John G. Frye, Jin Yong Kim, Curt A. Lavender, Kenneth Scott Weil
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Patent number: 9272392Abstract: Embodiments relate to polycrystalline diamond compacts (“PDCs”) and methods of manufacturing such PDCs in which an at least partially leached polycrystalline diamond (“PCD”) table is infiltrated with a low viscosity cobalt-based alloy infiltrant. In an embodiment, a method includes forming a PCD table in the presence of a metal-solvent catalyst in a first high-pressure/high-temperature (“HPHT”) process. The method includes at least partially leaching the PCD table to remove at least a portion of the metal-solvent catalyst therefrom to form an at least partially leached PCD table. The method includes subjecting the at least partially leached PCD table and a substrate to a second HPHT process effective to at least partially infiltrate the at least partially leached PCD table with a cobalt-based alloy infiltrant having a composition at or near a eutectic composition of the cobalt-based alloy infiltrant.Type: GrantFiled: October 18, 2011Date of Patent: March 1, 2016Assignee: US SYNTHETIC CORPORATIONInventors: Debkumar Mukhopadhyay, Jair J. Gonzalez
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Patent number: 9254553Abstract: An abrasive article includes a body having abrasive grains contained within a bond material comprising a metal or metal alloy, wherein the body comprises a ratio of VAG/VBM of at least about 1.3, wherein VAG is the volume percent of abrasive grains within the total volume of the body and VBM is the volume percent of bond material within the total volume of the body.Type: GrantFiled: March 21, 2014Date of Patent: February 9, 2016Assignees: Saint-Gobain Abrasives, Inc., Saint-Gobain AbrasifsInventors: Srinivasan Ramanath, Kenneth A. Saucier, Rachana Upadhyay
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Patent number: 9238267Abstract: Cutting insert made of hard metal, cermet or ceramic substrate body with multi-layer coating applied thereto by CVD methods. The coating has a total thickness of 5 to 40 ?m and, starting from the substrate surface, has one or more hard material layers, an alpha aluminum oxide (?-Al2O3) layer of a layer thickness of 1 to 20 ?m and optionally at least portion-wise over the ?-Al2O3 layer one or more further hard material layers as decorative or wear recognition layers. The ?-Al2O3 layer has a crystallographic preferential orientation characterized by a texture coefficient TC (0 0 12)?5 for the (0 0 12) growth direction. The ?-Al2O3 layer has an inherent stress in the region of 0 to +300 MPas, and the substrate within a region of 0 to 10 ?m from the substrate surface has an inherent stress minimum in the region of ?2000 to ?400 MPas.Type: GrantFiled: September 17, 2012Date of Patent: January 19, 2016Assignee: Walter AGInventors: Dirk Stiens, Sakari Ruppi, Thomas Fuhrmann
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Patent number: 9233422Abstract: A superhard cutter element for machining a workpiece comprising wood, metal, ceramic material or composite material, the superhard cutter comprising a superhard structure (140) having a rake side (110) and a flank side (120), the rake side (110) and the flank side (120) enclosing a wedge angle ?; and a protective layer (170) bonded to the superhard structure (140) at a rake interface (180) on the rake side (110), the protective layer (170) being softer than the material of the superhard structure (140).Type: GrantFiled: May 14, 2010Date of Patent: January 12, 2016Assignee: ELEMENT SIX LIMITEDInventors: Peter Michael Harden, Anthony Joseph Cooper
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Patent number: 9234113Abstract: The invention provides a dispersion of particles of rutile titanium oxide wherein the particles of rutile titanium oxide have a D50 in a range of 1 to 15 nm and a D90 of 40 nm or less in particle size distribution as determined by a dynamic light scattering method; a specific surface area in a range of 120 to 180 m2/g as determined by a BET method; and a rate of weight loss of 5% or less as obtained by heating the particles of rutile titanium oxide from 105° C. to 900° C.Type: GrantFiled: February 15, 2010Date of Patent: January 12, 2016Assignee: SAKAI CHEMICAL INDUSTRY CO., LTD.Inventors: Atsushi Nomura, Kenichi Nakagawa, Takanori Morita
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Patent number: 9228252Abstract: A hard alloy and a cutting tool. The hard alloy includes a hard phase and a binder phase. The hard phase includes: a main phase containing 50-70 mass % of WC, 15-30 mass % of TiCN, and 0-10 mass % of at least one kind of carbide, nitride or carbonitride of one or more non-W, non-Ti periodic table Group 4, 5 or 6 metal; a WC phase; and a composite hard phase. The binder phase includes 6 to 12 mass % of at least one of Co and Ni. The hard alloy includes a surface portion at a surface thereof, the surface portion having a WC content higher than that of an internal portion thereof. An average size of grains in the WC phase in the surface portion is larger than an average size of grains in the WC phase in the internal portion.Type: GrantFiled: June 27, 2012Date of Patent: January 5, 2016Assignee: KYOCERA CORPORATIONInventors: Hideyoshi Kinoshita, Katsuhiro Hanaki, Kouji Hirosaki
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Patent number: 9221153Abstract: A method for preparing a sintered metal matrix diamond saw blade used for cutting a QFN packaging device includes steps of: preparing metal matrix by employing metal powder and inorganic filler, wet-mixing and stirring the metal matrix, adding diamond grains to form a mixed material with evenly distributed diamond grains, performing the mixed material through cold pressing for pre-shaping, preparing a sintered metal matrix diamond saw blade blank through hot-pressing sintering, and finally machine-shaping the sintered metal matrix diamond saw blade blank to meet the dimensional requirements. The firm interface metallurgical bond is formed between the metal matrix and the diamond grains by the hot-pressing sintering process, which enhances holding force of the metal matrix on the diamond grains, in such a manner that abrasive grains are not easy to fall off untimely during cutting, thus prolonging service life of the sintered metal matrix diamond saw blade.Type: GrantFiled: June 10, 2011Date of Patent: December 29, 2015Assignee: XI' AN JIAOTONG UNIVERSITYInventors: Junma Nan, Kewei Xu