Abstract: Porous metallic bodies having a substantially uniform pore size of less than about 200 microns and a density of less than about 25 percent theoretical, as well as the method for making them, are disclosed. Group IIA, IIIB, IVB, VB, and rare earth metal hydrides are heated in a confining container at a controlled rate to a temperature of about greater than the temperature at which the hydride decomposes. Hydrogen is removed from the container and the remaining metal is heated during a second stage to a temperature greater than the temperature at which it was previously heated but not greater than the temperature of 1/2 to 2/3 the temperature at which the metal melts at a controlled rate. The resulting porous metallic body produced has a density less than about 25 percent theoretical and a pore size of less than about 200 microns. The metallic particles of the present invention have high inner surface area and possess minimum resistance to gas flow.
Type:
Grant
Filed:
March 13, 1984
Date of Patent:
December 24, 1985
Assignee:
The United States of America as represented by the United States Department of Energy
Abstract: An invar alloy on the basis of iron is formed by an intermetallic compound having a cubic crystal structure of the NaZn.sub.13 type having nominal composition La(FeCoX).sub.13, wherein X is Si or Al. By subjecting the present intermetallic compound after melting to a tempering treatment at 800.degree.-1,000.degree. C. and cooling it in an accelerated manner, a brittle material is obtained which can be ground to form a powder. From this powder, articles having any desired (optionally complicated) shape can be produced by means of powder metallurgy. By mixing powders of two different intermetallic compounds, a material can be obtained having a substantially negligible coefficient of linear thermal expansion in the temperature range from 0.degree. C. to 200.degree. C.
Abstract: In the method according to the invention, Cr powder is poured into a degased mold, which can be made of graphite. On this Cr powder a piece of low-oxygen copper is placed. Subsequently, the mold is closed with a porous cover, which can also be made of graphite. Then the mold is degased in a high-vacuum furnace at room temperature until a pressure of better than 10.sup.-4 mb is reached. Thereafter, the furnace temperature is increased to as high as possible a temperature below the melting point of copper. This furnace temperature is maintained constant until an internal pressure in the furnace of better than 10.sup.-4 mb is reached. Subsequently, without intermediate cooling, the furnace temperature is further increased slowly to a final value of 100 degrees K. to 200 degrees K. above the melting temperature of the copper. This temperature is then maintained until the porosity contained in the Cr powder is completely filled up by the liquid copper.
Type:
Grant
Filed:
July 13, 1983
Date of Patent:
March 5, 1985
Assignee:
Siemens Aktiengesellschaft
Inventors:
Horst Kippenberg, Heinrich Haessler, Manfred Huehnlein
Abstract: A sintered powdered titanium alloy article is provided which has a density approaching theoretical and which is characterized by having physical properties similar to those of a wrought titanium alloy article having the same chemical composition.
Abstract: The invention relates to a process for the production of titanium-based alloy members by powder metallurgy.This process consists of:(a) preparing a titanium or titanium alloy powder having a grain size distribution between 100 and 1000 .mu.m,(b) depositing on said powder a coating of a material such that on contact with the titanium or titanium alloy it forms a liquid phase at a temperature T.sub.1 which is below the allotropic transformation temperature T of the titanium or titanium alloy constituting the said powder,(c) introducing the thus coated powder into a mould, and(d) hot compressing this powder in the mould at a pressure of 10 to 30 MPa at a temperature between T.sub.1 and T for a time such that a complete densification of the powder is obtained.Application to the construction of discs for turbines with integrated blades.
Abstract: An electrode having an electrical capacitance in excess of 10,000 .mu.C/g prepared by sintering a tantalum powder having a grain size finer than 2.5 .mu.m, and the process of preparation.
Abstract: The corrosion resistance of stainless steel powder compacts containing tin and silicon is maximized if the compacts are sintered at temperatures in excess of 2300.degree. F. in highly reductive atmospheres until the ratio of Sn:Si on the surface of the compact is at least about 1:1. Stainless steel powders atomized in an oxidizing atmosphere and containing up to about 1 percent oxygen can be utilized.
Type:
Grant
Filed:
January 21, 1980
Date of Patent:
February 9, 1982
Assignee:
SCM Corporation
Inventors:
David H. Ro, Erhard Klar, C. I. Whitman
Abstract: Supercorroding magnesium alloys that operate like galvanic cells and react apidly and predictably with seawater to produce heat and hydrogen gas. The alloys are formed by a mechanical process that bonds magnesium and noble metal powder particles together in a strong electrical and mechanical bond. The alloy powders can be compacted and sintered to form barstock, etc., suitable for making self-destructing corroding links.
Type:
Grant
Filed:
August 13, 1979
Date of Patent:
April 28, 1981
Assignee:
The United States of America as represented by the Secretary of the Navy
Inventors:
Sergius S. Sergev, Stanley A. Black, James F. Jenkins
Abstract: Tantalum and tantalum-rich alloys, particularly in wire form, are stabilized against embrittlement by the addition of 50 to 700 parts per million of silicon and optionally with the further addition of 100 to 500 parts per million of carbon.
Abstract: A process for the preparation by sintering of molybdenum based alloys containing at least one reinforcing element, characterized in that at least one addition compound is introduced in the liquid state into molybdenum used in the form of at least one of the members belonging to the group consisting of the salts of molybdenum, the oxides of molybdenum and metallic molybdenum, and in that carbon is then added in sufficient quantity and the intimate member, after reduction of the matrix to the metallic state of molybdenum was used in the form of at least one molybdenum salt or at least one molybdenum oxide, is sintered at a temperature at which the said carbon at least partially reduces the addition compound.The addition compound belongs to the group consisting of the mineral and organic compounds of titanium, zirconium, hafnium, thorium, aluminum, niobium, berylium, boron and the rare earths.
Type:
Grant
Filed:
April 23, 1976
Date of Patent:
September 19, 1978
Assignee:
Cime Bocuze
Inventors:
Geraud Fustier, Jean-Paul Langeron, Joseph DE LA Bastie, Jean Carlizza
Abstract: A process for the preparation by sintering of molybdenum based alloys containing at least one reinforcing element, characterized in that at least one addition compound is introduced in the solid state into molybdenum used in the form of at least one of the components of the group consisting of the salts of molybdenum and the oxides of molybdenum, and that carbon is then added in sufficient quantity and the intimate mixture, after reduction of the molybdenum based component, is sintered at a temperature at which the said carbon at least partially reduces the addition compound.Addition compounds belonging to the group consisting of the mineral and organic compounds of titanium, zirconium, hafnium, thorium, aluminum, niobium, beryllium, boron and the rare earths are used.
Type:
Grant
Filed:
April 23, 1976
Date of Patent:
August 22, 1978
Assignee:
Cime Bocuze
Inventors:
Geraud Fustier, Jean-Paul Langeron, Joseph DE LA Bastie, Jean Carlizza
Abstract: A method for adding reactive elements to molten copper or copper base alloys is disclosed. This method prevents unwanted reactions and oxidation by adding the reactive elements to the molten metal in the form of a powder mixture placed within tubing which is compatible with said molten metal. This filled tubing is sealed and drawn down, if desired, to an appropriate size for rapid melting within said molten metal and consequent rapid dissolution of the reactive elements throughout the molten metal.
Type:
Grant
Filed:
November 4, 1976
Date of Patent:
May 9, 1978
Assignee:
Olin Corporation
Inventors:
Derek E. Tyler, David W. Dickinson, James E. Dore, Abid A. Khan
Abstract: Columbium powder capable of producing anodes of improved electrical capacitance is prepared by the addition of phosphorus-containing materials in amounts from about 5 to about 600 ppm based on elemental phosphorus.
Abstract: Prealloyed powders, particularly of compositions which are difficult to work by conventional means, are subjected to forces such that strain energy is imparted thereto by virtue of which the prealloyed powders manifest low flow stress and a high degree of thermoplasticity.
Type:
Grant
Filed:
September 4, 1975
Date of Patent:
February 14, 1978
Assignee:
The International Nickel Company, Inc.
Inventors:
Timothy E. Volin, John S. Benjamin, Jay M. Larson, Robert L. Cairns
Abstract: Tantalum and tantalum-rich alloys, particularly in wire form, are stabilized against embrittlement by the addition of 50 to 700 parts per million of silicon and optionally with the further addition of 100 to 500 parts per million of carbon.