Base Metal One Or More Transition Metal Patents (Class 75/245)
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Patent number: 6193930Abstract: Two or more metal or alloy parts (such as catalytic convertor parts) are brazed by melting a homogeneous nickel-based brazing filler alloy containing boron in an amount of not more than 0.2% by weight; converting the molten alloy to a powder of uniform composition; and using the powder as a brazing filler alloy to braze a metal or alloy part to a further metal or alloy part. Typically, the parts are of stainless steel with a relatively high aluminum content; at least one of the parts is generally in the form of a thin foil.Type: GrantFiled: May 26, 1998Date of Patent: February 27, 2001Assignee: Wall Colmonoy LimitedInventor: Norman Allnatt
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Patent number: 6193778Abstract: A method for forming dendritic metal powders, comprising the steps of: (1) heating a powder comprising non-dendritic particles, under conditions suitable for initial stage sintering, to form a lightly sintered material; and (2) breaking the lightly sintered material to form a powder comprising dendritic particles. In one embodiment, the lightly sintered material is broken by brushing the material through a screen. Another aspect of the present invention comprises the dendritic particles that are produced by the method described above. These particles can comprise any suitable metal, such as transition metals, rare earth metals, main group metals or metalloids or an alloy of two or more such metals. The particles can also comprise a ceramic material, such as a metal oxide. These particles are characterized by a dendritic, highly anisotropic, morphology arising from the fusion of substantially non-dendritic particles, and by a low apparent density relative to the substantially non-dendritic starting material.Type: GrantFiled: October 8, 1998Date of Patent: February 27, 2001Assignee: Millipore CorporationInventors: Robert S. Zeller, Christopher J. Vroman
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Patent number: 6193779Abstract: The invention relates a tantalum powder free of alkali and fluorine, which for a relatively small primary particle size has comparatively large secondary particles and is suitable for producing capacitors with a specific charge of between 100,000 and 180,000 &mgr;FV/g at specific residual currents of less than 2nA/&mgr;FV.Type: GrantFiled: August 19, 1999Date of Patent: February 27, 2001Assignee: H. C. Starck GmbH & Co. KGInventors: Karlheinz Reichert, RĂ¼diger Wolf, Christine Rawohl
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Patent number: 6183606Abstract: A method of producing high coercivity FePt—Si3N4 granular composite thin films for magnetic recording media is invented. The method includes magnetron co-sputtering of FePt and Si3N4 targets at controlled sputtering power and sputtering argon gas pressure to form a selective composition of granular FePt—Si3N4 thin film on a low temperature substrate, then post-annealed in vacuum at selective time period and temperature. Two kinds of FePt targets can be used. One is the FePt alloy target. The other one is a composite target consisting of an iron disk overlaid with small Pt pieces. This arrangement provides a wide range of effective target compositions and therefore film compositions. FePt—Si3N4 films were deposited on natural oxidized silicon wafer or quartz glass substrate at room temperature. The as-deposited film has soft magnetic properties and granular structure with soft magnetic &ggr;-FePt particles dispersed in amorphous Si3N4 matrix.Type: GrantFiled: November 3, 1999Date of Patent: February 6, 2001Assignee: National Science Council of Republic of ChinaInventors: Po-Cheng Kuo, Chih-Ming Kuo
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Patent number: 6165623Abstract: A flaked niobium powder is disclosed as well as electrolytic capacitors formed from the flaked niobium powders. Niobium powders having a BET surface area of at least about 0.50 m.sup.2 /g are also disclosed and capacitors made therefrom, as well as niobium powders doped with an oxygen content of at least 2,000 ppm. Methods to reduce DC leakage in a niobium anode are also disclosed.Type: GrantFiled: November 3, 1997Date of Patent: December 26, 2000Assignee: Cabot CorporationInventors: James A. Fife, Jane Jia Liu, Roger W. Steele
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Patent number: 6149705Abstract: A projectile, such as a bullet, is made by combining two different metals in proportions calculated to achieve a desired density, without using lead. A base constituent, made of a material having density greater than lead, is combined with a binder constituent having less density. The binder constituent is malleable and ductile metallic phase material that forms projectile shapes when subjected to a consolidation force, such as compression. The metal constituents can be selected, rationed, and consolidated to achieve desired frangibility characteristics.Type: GrantFiled: March 2, 1998Date of Patent: November 21, 2000Assignee: UT-Battelle, LLCInventors: Richard A. Lowden, Thomas M. McCoig, Joseph B. Dooley
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Patent number: 6126799Abstract: A cermet composite material is made by treating at an elevated temperature a mixture comprising a compound of iron and a compound of at least one other metal, together with an alloy or mixture of copper and a noble metal. The alloy or mixture preferably comprises particles having an interior portion containing more copper than noble metal and an exterior portion containing more noble metal than copper. The noble metal is preferably silver. The cermet composite material preferably includes alloy phase portions and a ceramic phase portion. At least part of the ceramic phase portion preferably has a spinel structure.Type: GrantFiled: February 1, 1999Date of Patent: October 3, 2000Assignee: Alcoa Inc.Inventors: Siba P. Ray, Robert W. Woods, Robert K. Dawless, Robert B. Hosler
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Patent number: 6123896Abstract: A process of consolidating tantalum metal powder to essentially random texture by pressing a preform in a bed of flowable pressure transmitting particles, and the product thereby produced.Type: GrantFiled: January 29, 1999Date of Patent: September 26, 2000Assignee: Ceracon, Inc.Inventors: Henry S. Meeks, III, Marc A. Fleming, Lucile Lansing
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Patent number: 6120620Abstract: A permanent magnet having substantially stable magnetic properties is disclosed having as the active magnetic component a sintered product of compacted particulate iron-boron-rare earth intermetallic material, said sintered product having pores which are substantially non-interconnecting, a density of at least 87 percent of theoretical and a composition consisting essentially of in atomic percent about 13 to about 19 percent rare earth elements, about 4 to about 20 percent boron and about 61 to about 83 percent of iron with or without impurities; where the rare earth content is greater than 50 percent praseodymium with an effective amount of a light rare earth selected from the group consisting of cerium, lanthanum, yttrium and mixtures thereof, and balance neodymium.Type: GrantFiled: February 12, 1999Date of Patent: September 19, 2000Assignee: General Electric CompanyInventors: Mark Gilbert Benz, Juliana Ching Shei
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Patent number: 6117204Abstract: A sintered Ti alloy material and a process for producing the same, which comprises a matrix mainly comprising a Ti alloy, and TiB dispersed and maintained in said matrix, wherein a composition of the sintered Ti alloy material at least comprises from 0.1 to 8.0% by weight of B, from 3.0 to 30.0% by weight of Mo, 50% by weight or more of Ti, and the balance of unavoidable impurities.Type: GrantFiled: September 16, 1998Date of Patent: September 12, 2000Assignee: Kabushiki Kaisha Toyota Chuo KenkyushoInventors: Takashi Saito, Tadahiko Furuta, Hiroyuki Takamiya
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Patent number: 6106957Abstract: A metal-matrix diamond or cubic boron nitride composite and method of making the same are disclosed. The metal-matrix/diamond composite includes grains of diamond uniformly distributed in a metal matrix. Alternatively, grains of cubic boron nitride may be used. Suitable metals for the metal matrix material may include nickel, cobalt, iron, and mixtures or alloys thereof. Other transition metals also may be used. The metal-matrix/diamond or metal-matrix/cubic boron nitride composite has high fracture toughness due to its fine microstructure. Such a metal-matrix/diamond or metal-matrix/cubic boron nitride composite is suitable for use in blanks or cutting elements for cutting tools, drill bits, dressing tools, and wear parts. It also may be used to make wire drawing dies.Type: GrantFiled: March 10, 1999Date of Patent: August 22, 2000Assignee: Smith International, Inc.Inventor: Zhigang Fang
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Patent number: 6090227Abstract: Structural units which come into contact with glass melts and ceramic melts are exposed to strong corrosive attack. Molybdenum is a known material for glass melt electrodes but it is not usable for the majority of highly corrosive glass and ceramic melts. The use of a special molybdenum and/or tungsten alloy as the material for the structural unit reduces corrosion even in the case of contact with highly corrosive glass and ceramic melts.Type: GrantFiled: May 7, 1998Date of Patent: July 18, 2000Assignee: Schwarzkopf Technologies Corp.Inventors: Gerhard Leichtfried, Hans-Peter Martinz, Joachim Disam
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Patent number: 6090191Abstract: The invention relates to the field of producing the means for protecting the alloys on the nickel base against the influence of corrosive media, and more particularly concerns the metal-ceramic coatings used for protecting the flow parts of the turbines of turbopump liquid-propellant rocket engines (LRE). The composition for producing the metal-ceramic coating consists of nickel and of oxides of barium, boron, aluminum, cerium and zirconium at the following percentage of components by mass: nickel--36-58, barium oxide--16-19, boron oxide--7-13, aluminum oxide--6-9, cerium oxide--14-19, zirconium oxide--1-2. The coating is produced of a slip, that is applied to the pieces by dipping, spraying or flooding. The slip layers are dried in the flow of hot air. The coating is fired in a furnace in the inert gas medium, argon for example, at a temperature of 1000-1100.degree. C. during 0.5-1 hour.Type: GrantFiled: September 29, 1999Date of Patent: July 18, 2000Assignee: Oktrytoe Aktsionernoe Obschestvo "Nauchno-Proizvodstvennoe Obiedinenie "Energomash" Imeni Akademika V.P. Glushko"Inventors: Aza Fedorovna Atlanova, Galina Andreevna Babaeva, Evgeny Alexeevich Belov, Dina Ivanovna Dubovik, Jury Alexandrovich Pestov, Margarita Evgenievna Judina, Leonid Vasilievich Cherkasov, Vadim Iliich Semenov, Felix Jurievich Chelkis, Alexandr Mikhailovich Kashkarov, Konstantin Pavlovich Khaplanov
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Patent number: 6090178Abstract: A frangible metal bullet, a method for making it, and ammunition made therefrom. The frangible metal bullet is formed from a mixture of metal particles and metal or metalloid binder forming material which is compacted into the desired shape, heated to a temperature above that needed to form at least one intermetallic compound but below the temperature of joining of the metal particles by sintering and below the temperature of formation of substantial amounts of a ductile alloy of the metal of the particles and the metal or metalloid binder forming material and then cooled. Such bullets have sufficient strength to maintain their integrity during firing but disintegrate into powder on impact and can be formulated to be lead-free.Type: GrantFiled: November 5, 1998Date of Patent: July 18, 2000Assignee: SinterFire, Inc.Inventor: Joseph C. Benini
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Patent number: 6074453Abstract: A method of making hydrogen storage powder resistant to fracture in service involves forming a melt having the appropriate composition for the hydrogen storage material, such, for example, LaNi.sub.5 and other AB.sub.5 type materials and AB.sub.5+x materials, where x is from about -2.5 to about +2.5, including x=0, and the melt is gas atomized under conditions of melt temperature and atomizing gas pressure to form generally spherical powder particles. The hydrogen storage powder exhibits improved chemcial homogeneity as a result of rapid solidfication from the melt and small particle size that is more resistant to microcracking during hydrogen absorption/desorption cycling. A hydrogen storage component, such as an electrode for a battery or electrochemical fuel cell, made from the gas atomized hydrogen storage material is resistant to hydrogen degradation upon hydrogen absorption/desorption that occurs for example, during charging/discharging of a battery.Type: GrantFiled: October 28, 1997Date of Patent: June 13, 2000Assignees: Iowa State University Research Foundation, Inc., California Institute of TechnologyInventors: Iver E. Anderson, Timothy W. Ellis, Vitalij K. Pecharsky, Jason Ting, Robert Terpstra, Robert C. Bowman, Charles K. Witham, Brent T. Fultz, Ratnakumar V. Bugga
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Patent number: 6071323Abstract: An alloy target comprises at least one rare earth metal element Tb, Dy, Gd, Sm, Nd, Ho, Tm, and Er with a substantial balance of a transition metal element such as Fe, Co and Ni, and has a substantially homogeneous sintered structure and a permeability of 3 or lower. The alloy target is fabricated by a process comprising steps of melting in a high-frequency furnace or crucible furnace, quenching, pulverization, and firing under pressure. After the alloy target has been used up, it is regenerated by mixing alloy powders (to be regenerated) obtained by the mechanical pulverization of the used-up target with the alloy powders obtained at the pulverization step of the aforesaid process to obtain a mixture, and firing the mixture under pressure.Type: GrantFiled: March 2, 1998Date of Patent: June 6, 2000Assignee: TDKCorporationInventor: Yukio Kawaguchi
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Patent number: 6066191Abstract: Disclosed is a hard molybdenum alloy which exhibits an excellent wear resistance against sliding wear and adhesive wear in a high temperature nonlubricating atmosphere, comprising at least one of nickel (Ni) and cobalt (Co) in an amount of from 14.0 to 43.0% by weight, silicon (Si) in an amount of from 3.0 to 8.0% by weight and molybdenum (Mo) in an amount of not less than 20.0% by weight. Also disclosed is a wear resistant alloy which includes the above hard molybdenum alloy as a reinforcing phase.Type: GrantFiled: May 21, 1998Date of Patent: May 23, 2000Assignee: Kabushiki Kaisha Toyota Chuo KenkyushoInventors: Kouji Tanaka, Takashi Saito, Tadashi Oshima
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Patent number: 6063212Abstract: Heat treated, spray formed articles are disclosed which exhibit crack growth rates and resistance to stress rupture comparable to corresponding, forged articles. The articles are first formed by depositing molten metal droplets, e.g., of IN 718, on a substrate to form a rough article. The articles are HIP'ed and then processed by heat treating, which includes solution, stabilization and precipitation heat treatments. The resultant articles have fine average grain sizes compared to forged and conventionally heat treated material, as well as yield and tensile strengths comparable to forged material. Importantly, the articles also exhibit low crack growth rates and stress rupture resistance, e.g., comparable to forged material, and have an isotropic microstructure. The articles can be used in place of forged articles.Type: GrantFiled: May 12, 1998Date of Patent: May 16, 2000Assignee: United Technologies CorporationInventor: Antonio C. Cabral
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Patent number: 6051044Abstract: A nitrogen containing niobium powder is disclosed as well as electrolytic capacitors formed from the niobium powders. Methods to reduce DC leakage in a niobium anode are also disclosed.Type: GrantFiled: May 4, 1998Date of Patent: April 18, 2000Assignee: Cabot CorporationInventor: James A. Fife
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Patent number: 5993513Abstract: A method for controlling oxygen in valve metal materials. The method includes deoxidizing a valve metal material, typically tantalum, niobium, or alloys thereof, and leaching the material in an acid leach solution at a temperature lower than room temperature. In one embodiment of the present invention, the acid leach solution is prepared and cooled to a temperature lower than room temperature prior to leaching the deoxidized valve metal material. The method of the present invention has been found to lower both the oxygen and fluoride concentrations in valve metal materials, as the use of reduced acid leach temperatures provide lower oxygen for a given quantity of a leach acid, such as hydrofluoric acid.Type: GrantFiled: April 5, 1996Date of Patent: November 30, 1999Assignee: Cabot CorporationInventor: James A. Fife
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Patent number: 5989673Abstract: Chromium-tantalum oxides (Cr-TaO.sub.x), including chromium-tantalum pentoxide (Cr-Ta.sub.2 O.sub.5), chromium-tantalum tetrioxide (Cr-Ta.sub.2 O.sub.4 or Cr-TaO.sub.2), sputtering targets containing them, and their manufacture are disclosed. The targets are characterized by high density, uniform TaO.sub.x distribution, low impedance and stable plasma during the sputtering. The Cr-Ta oxides are used as a thin film sublayer to improve the coercivity and other characteristics of magnetic recording media deposited on metallic or non-metallic substrates used in hard disks for data storage.Type: GrantFiled: June 30, 1997Date of Patent: November 23, 1999Assignees: Sony Corporation, Materials Research CorporationInventors: Wei Xiong, Hung-Lee Hoo
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Patent number: 5984996Abstract: Methods for the manufacture of nanostructured metals, metal carbides, and metal alloys are presented, such metals including nanostructured aluminum, chromium, iron, molybdenum, vanadium, and steel. Preferably, the nanostructured steel is of the M50 type, and comprises iron, molybdenum, chromium, vanadium and carbon. Synthesis of M50 steel further comprising nanostructured aluminum, aluminum oxide, or aluminum nitride is also described. In accordance with an important feature of this invention, the grain size of the metals and metal alloys is in the nanometer range. In accordance with the method of the present invention, the nanostructured metals, metal carbides, and metal alloys are prepared via chemical synthesis from aluminum, iron, molybdenum, chromium and vanadium starting materials. Decomposition of metal precursors or co-precipitation or precipitation of metal precursors is followed by consolidation of the resulting nanostructured powders.Type: GrantFiled: October 9, 1996Date of Patent: November 16, 1999Assignee: The University of ConnecticutInventors: Kenneth E. Gonsalves, Sri Prakash Rangarajan
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Patent number: 5972068Abstract: The vacuum valve contact material of the present invention is manufactured by a step of mixing an anti-arc constituent powder and a conductive constituent powder, a step of forming, and a step of sintering the formed body below the melting point of the conductive constituent, and has improved arc interruption performance.Type: GrantFiled: March 6, 1998Date of Patent: October 26, 1999Assignee: Kabushiki Kaisha ToshibaInventors: Tsuneyo Seki, Atsushi Yamamoto, Takashi Kusano, Tsutomu Okutomi
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Patent number: 5972067Abstract: A disclosed gradient function material seal cap for discharge lamp bulb is produced by molding and thereafter firing a slurry which contains a plurality of groups of particles having different specific gravities. The plurality of groups of particles include at least a first group of particles and a second group of particles. The first group of particles comprises a group of non-metal particles having a specific gravity ranging from about 3 to 7 and a maximum particle diameter equal to or smaller than a deflocculation limit, said nonmetal particles being made of one or more materials selected from the group consisting of an oxide, a carbide, a nitride, and an oxynitride. The second group of particles comprises a group of metal particles having a specific gravity which is about 1.5 times the specific gravity of said first group of particles, and particle diameters distributed across the deflocculation limit.Type: GrantFiled: August 17, 1998Date of Patent: October 26, 1999Assignee: Toto Ltd.Inventors: Hirotaka Ishibashi, Koichi Hayashi, Hiroyuki Nagayama
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Patent number: 5943546Abstract: A disclosed gradient function material is produced by molding and thereafter firing a slurry which contains a plurality of groups of particles having different specific gravities. The plurality of groups of particles include at least a first group of particles and a second group of particles. The first group of particles comprises a group of non-metal particles having a specific gravity ranging from about 3 to 7 and a maximum particle diameter equal to or smaller than a deflocculation limit, said non-metal particles being made of one or more materials selected from the group consisting of an oxide, a carbide, a nitride, and an oxynitride. The second group of particles comprises a group of metal particles having a specific gravity which is about 1.5 times the specific gravity of said first group of particles, and particle diameters distributed across the deflocculation limit.Type: GrantFiled: November 29, 1995Date of Patent: August 24, 1999Assignee: Toto Ltd.Inventors: Hirotaka Ishibashi, Koichi Hayashi, Hiroyuki Nagayama
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Patent number: 5913256Abstract: A solid object having controlled frangibility, such as a bullet or a container for explosives, is made by combining two different metals in proportions calculated to achieve a desired density, without using lead. A wetting material is deposited on the base constituent which is made of a relative dense, hard material. The wetting material enhances the wettability of the base constituent with the binder constituent, which is lighter and softer than the base constituent.Type: GrantFiled: November 10, 1997Date of Patent: June 15, 1999Assignee: Lockheed Martin Energy Systems, Inc.Inventors: Richard A. Lowden, Thomas M. McCoig, Joseph B. Dooley, Cyrus M. Smith
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Patent number: 5897830Abstract: A consumable billet for melting and casting a metal matrix composite component is made of a consolidated powder metal matrix composite having a titanium or titanium alloy matrix reinforced with particles. The preferred billet is a blended and sintered powder metal composite billet incorporating titanium carbide or titanium boride into a Ti--6Al--4V alloy.Type: GrantFiled: December 6, 1996Date of Patent: April 27, 1999Assignee: Dynamet TechnologyInventors: Stanley Abkowitz, Susan M. Abkowitz, Paul F. Weihrauch, Harold L. Heussi, Walter Zimmer
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Patent number: 5886269Abstract: A substrate serving as a heat sink for a semiconductor efficiently radiates heat from a semiconductor element mounted thereon. The substrate consists of a composite alloy metal which consists of a sintered body of a metal powder having a high melting point such as W and Mo impregnated with a filling metal such as Cu and Ag, wherein the sintered body of a metal powder having a high melting point has a grain size composition of a combination of a plurality of powder groups having statistically different average grain sizes from group to group, and the powder of each group is dispersed uniformly.Type: GrantFiled: February 14, 1996Date of Patent: March 23, 1999Assignee: Nippon Tungsten Co., Ltd.Inventors: Yasunao Kai, Akira Mishima, Shinji Gotoh, Chiaki Yamasaki
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Patent number: 5877437Abstract: Numerous products can be formed by combining a low melting matrix made up of one or more metals and high melting, high density metal particles and wherein the products can be formed by adding the high density particles to a molten matrix metal and casting same, mixing powders of all the metals together, compacting and sintering at a temperature in the low end of the melting range of the matrix alloy, or by mixing the high density particles into a paste of the matrix alloy and molding. These methods and compositions are particularly adaptable for use in forming low or non-toxic high density projectiles, such as, shot, bullets and pellets having a density comparable to that of lead while avoiding problems of toxicity associated with the use of lead.Type: GrantFiled: September 16, 1996Date of Patent: March 2, 1999Inventor: Victor C. Oltrogge
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Patent number: 5852248Abstract: Shaped article replicas which are proportionately accurate replicas of a shaped article and which are equal, greater or smaller in size than said shaped article are made by preparing a swellable polymer cavity mold from said shaped article; immersing said swellable polymer cavity mold in a swelling agent system under conditions which will enlarge said cavity mold to a predetermined extent; forming a powder compact in said casting mold or a replica thereof and heating said powder compact to produced a proportionately accurate solid replica of a predetermined size.Type: GrantFiled: May 21, 1998Date of Patent: December 22, 1998Assignee: Den-Mat CorporationInventor: Thomas Chadwick
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Patent number: 5850047Abstract: A method of producing copper powder having little variation in its particle size and an excellent monodispersion properties. A copper complex ion solution is prepared from a copper-containing solution and a complexing agent, then a reducing agent is added to the copper complex ion solution to precipitate metallic copper. The copper-containing solution herein contains copper sulfate, copper formate, copper pyrophosphate, copper chloride or copper carbonate and the complexing agent is at least one carboxylate or phosphate.Type: GrantFiled: March 11, 1997Date of Patent: December 15, 1998Assignee: Murata Manufacturing Co., Ltd.Inventors: Hiroji Tani, Naoaki Ogata
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Patent number: 5834640Abstract: This invention relates to a method or process of forming a sintered article of powder metal, and particularly relates to a process of forming a sintered article of powder metal by blending combinations of finely ground ferro alloys (either singly or in combination with other ferro alloys) with elemental iron powder and other additives and then high temperature sintering of the article in a reducing atmosphere to produce sintered parts with oxygen contents less than 250 parts per million (ppm). More particularly the ferro alloys admixed to the base iron have a mean particle size of approximately 8 to 12 microns, having previously been ground to size in an inert atmosphere.Type: GrantFiled: August 10, 1995Date of Patent: November 10, 1998Assignee: Stackpole LimitedInventors: Rohith Shivanath, Peter Jones
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Patent number: 5792288Abstract: An alloy made of Titanium, Aluminum, Vanadium, and Copper. The combination enhances the strength of the metal. Such alloy can be used where high strength metal is required. When Molybdenum Sulfide is added to the alloy, it will provide a solid lubricating substance, which will reduce the friction coefficient by forming secondary structures, thus suppressing the phenomena of setting, which is typical for titanium alloys. Such alloy can be used where wear and tear is high under variable pressure such as gears. It can also be used where objects are moving with high velocity such as weapons.Type: GrantFiled: January 16, 1996Date of Patent: August 11, 1998Assignee: Mite Ltd.Inventors: Rusk Masih, Nikolay Manoukian
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Patent number: 5772701Abstract: A method for manufacturing tantalum capacitors includes preparing a tantalum compact by cold pressing tantalum powder, placing the compact, along with loose refractory metal powder, in a microwave-transparent casket to form an assembly, and heating the assembly for a time sufficient to effect at least partial sintering of the compact and the product made by the method.Type: GrantFiled: September 5, 1996Date of Patent: June 30, 1998Assignee: Lockheed Martin Energy Research CorporationInventors: April D. McMillan, Robert E. Clausing, William F. Vierow
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Patent number: 5768679Abstract: An article essentially consisting of one or more of Ti-Al intermetallic compounds is fabricated so as to have a volume ratio of voids of 0.2 to 3.5% and a maximum size of voids less than 50 .mu.m, by preparing a mixture of materials selected from a group consisting of Ti, Ti alloys, Al, Al alloys, and Ti-Al compounds, having a composition suitable for forming a desired Ti-Al intermetallic compound, and heating the mixture so that the mixture may be sintered. Typically, the temperature and pressure for the heating or sintering process, and the particle size of the material are appropriately selected so that a desired porosity and a desired range of void sizes may be obtained. The mechanical strength of the article according to the present invention is not only improved (as compared to the conventional Ti-Al intermetallic compounds) but is highly predictable, or, in other words, highly reliable.Type: GrantFiled: September 3, 1996Date of Patent: June 16, 1998Assignee: NHK Spring R & D Center Inc.Inventors: Kohei Taguchi, Michihiko Ayada, Hideo Shingu
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Patent number: 5758253Abstract: A process for producing sintered titanium-graphite having improved wear resistance and low frictional characteristics is described. The said process which produces titanium-graphite composites having a triphasic structure with controlled porosity and a graphite lubricating film, comprises sintering a mixture of titanium and graphite powders in which the percentage of graphite may vary from 4 to 8 percent at temperatures from about 800.degree. C. to 1600.degree. C., for about 1/2 to 2 hours, under a compaction pressure of 0.17 to 0.62 MPa. The composites have applications in biomedical engineering and other fields of engineering due to their biocompatibility, strength and improved wear resistance.Type: GrantFiled: October 7, 1996Date of Patent: May 26, 1998Assignee: National University of SingaporeInventors: Swee Hin Teoh, Rajendran Thampuran, James Cho Hong Goh, Winston Kar Heng Seah
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Patent number: 5718778Abstract: A chromium target is disclosed for use in the formation of chromium films or sheets of reduced thickness by means of sputtering. The target has a recrystallized structure represented by the equation, A/B.ltoreq.0.6, where A is the diffraction intensity of the (110) planes as determined by X-ray diffraction of a sputtered surface, and B is the diffraction intensity as determined from the sum of the (110), (200) and (211) planes. The target preferably has a deflective strength of above 500 MPa and an average crystal grain of below 50 .mu.m. The chromium target is produced by subjecting a starting chromium material to at least one stage of plastic working at a temperature of not higher than 1,000.degree. C., and subsequently by heat-treating the resulting chromium material for recrystallization at a temperature of higher than the recrystallization temperature of the chromium material but not higher than 1,200.degree. C.Type: GrantFiled: March 29, 1996Date of Patent: February 17, 1998Assignee: Hitachi Metals, Ltd.Inventors: Hideo Murata, Shigeru Taniguchi
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Patent number: 5698800Abstract: The present invention provides a mixed raw material which is capable of producing a porous metal sintered product having high porosity and fine and uniform pores. The mixed raw material for producing a porous metal sintered product is a composition including 0.05 to 10% of water-insoluble hydrocarbon organic solvent having 5 to 8 carbon atoms, 0.05 to 5% of surfactant, 0.5 to 20% of water-soluble resin binder, 5 to 80% of metallic powder having an average particle size of 0.5 to 500 .mu.m, optionally 0.1 to 40% of combustible agent for accelerating pore formation, and optionally, 0.1 to 15% of plasticizer consisting of at least one of polyhydric alcohols, oils and fats, ethers and esters, with a balance of water.Type: GrantFiled: August 2, 1996Date of Patent: December 16, 1997Assignee: Mitsubishi Materials CorporationInventors: Koji Hoshino, Toru Kohno
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Patent number: 5698008Abstract: A contact material for a vacuum valve including, a conductive constituent including at least copper, an arc-proof constituent including at least chromium and an auxiliary constituent including at least one selected from the group consisting of tungsten, molybdenum, tantalum and niobium. The contact material is manufactured by quench solidification of a composite body of the conductive constituent, the arc-proof constituent and the auxiliary constituent.Type: GrantFiled: February 21, 1995Date of Patent: December 16, 1997Assignee: Kabushiki Kaisha ToshibaInventors: Tsuneyo Seki, Tsutomu Okutomi, Atsushi Yamamoto, Takashi Kusano
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Patent number: 5641921Abstract: This invention is directed toward a material which is used to coat or create a surface for machine cutting tools, all types of drill bit teeth, saw teeth, bearing surfaces valve seats, nozzles and the like, thereby producing surfaces which are highly abrasion and erosion resistant. Furthermore, this invention includes some of the possible methods for producing such a material given that the methods and apparatus required provide a significant cost reduction over those required for producing prior art surface materials with similar abrasion and erosion resistant properties. More specifically, the material set forth can be formed at relatively low temperatures and relatively low pressures by sintering mixtures for a relatively short period of time.Type: GrantFiled: August 22, 1995Date of Patent: June 24, 1997Assignee: Dennis Tool CompanyInventors: Mahlon Denton Dennis, Barton Hampshire
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Patent number: 5628044Abstract: High purity iron-zinc intermetallic calibration standards are produced using a slow diffusion technique. The alloys are pure to greater than 99.5 wt % and are homogenous to greater than 98%. The alloys can be used to calibrate instrumentation used to monitor and measure galvanneal and galvanized coatings. The alloy calibration standards for each of the iron-zinc phases allows instrumentation correction factors to be determined for iron-zinc coating analysis.Type: GrantFiled: June 2, 1995Date of Patent: May 6, 1997Assignee: Old Dominion UniversityInventors: Desmond C. Cook, Richard G. Grant, Patricia S. Cook
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Patent number: 5618397Abstract: Metal silicide targets are provided for sputtering which have a density of at least 99%, no more than one coarse silicon phase 10 .mu.m or larger in size that appears, per square millimeter, on the sputter surface, and an oxygen content of at most 150 ppm. They are made by a method which comprises finely grinding a synthesized silicide powder, vacuum annealing the finely ground powder in a hot press die without the application of pressure, and thereafter compacting and sintering the compact to a density of at least 99% by hot pressing. Alternatively, the finely ground powder is vacuum annealed as a presintered body at a density ratio of 50 to 75%, and thereafter is compacted and sintered.Type: GrantFiled: April 17, 1995Date of Patent: April 8, 1997Assignee: Japan Energy CorporationInventors: Osamu Kano, Yasuhiro Yamakoshi, Junichi Anan, Koichi Yasui
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Patent number: 5608174Abstract: The invention relates to a chromium-based alloy which has a chromium content of more than 65% by weight and the following composition: 0.005 to 5% by weight of one or more oxides of the rare earth elements and 0.1 to 32% by weight of one or more metals selected from the group comprising iron, nickel and cobalt, the remainder being chromium.The alloy may furthermore contain up to 30% by weight of one ore more metals selected from the group comprising Al, Ti, Zr and Hf, up to 10% by weight of one or more metals selected from the group comprising V, Nb, Mo, Ta, W and Re and up to 1% by weight of C and/or N and/or B and/or Si.Compared with pure chromium the alloy has a substantially improved oxidation resistance and improved corrosion resistance, in particular with respect to vanadium pentoxide.Type: GrantFiled: May 15, 1995Date of Patent: March 4, 1997Inventors: Ralf Eck, Gunter Kneringer, Wolfgang Kock
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Patent number: 5607780Abstract: Disclosed are a target material for magneto-optical recording medium having a structure formed by sintering of an RE-TM phase (A) having a composition with an RE content higher than that of the composition of an intermetallic compound represented by the chemical formula TM.sub.2 RE, and a TM-RE phase (B) having a composition with an RE content equal to or lower than that of the composition of an intermetallic compound represented by the chemical formula TM.sub.2 E, wherein RE denotes at least one rare earth element selected from the group of elements consisting of Nd, Gd, Tb, Dy, Ho and Er, and TM denotes at least one element selected from the group of metals of the iron group which consists of Fe, Co and Ni; and a process for producing the same.Type: GrantFiled: May 20, 1994Date of Patent: March 4, 1997Assignee: Hitachi Metals, Ltd.Inventors: Kaoru Masuda, Takashi Meguro
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Patent number: 5606141Abstract: The present invention relates to a strip-like current feeder based on molybdenum-yttrium oxide, for electric lamps with a metal/glass sealing. In addition to molybdenum-yttrium oxide, the strip material contains 0.03 to 1.0% by weight cerium oxide and the ratio of cerium oxide to yttrium oxide amounts to 0.1 to 1. As compared to known current feeders, the current feeder according to the present invention has a distinctly enhanced resistance to corrosion or oxidation.Type: GrantFiled: June 19, 1995Date of Patent: February 25, 1997Assignee: Schwarzkopf Technologies CorporationInventor: Gerhard Leichtfried
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Patent number: 5602350Abstract: The present invention discloses an improved method for compacting powdered materials, including ferrous alloys, non-ferrous metals or non-metal powders, wherein the improved method includes the use of an improved lubricant during the compaction process. The improved lubricant includes vinyl halides, generally, and polytetrafluroethylene, specifically. In a preferred embodiment of the present invention, 0.2 to 0.6 wt. % of the vinyl halide is added to the powdered form of the compactable material before the compaction and sintering of the compactable material.Type: GrantFiled: May 15, 1995Date of Patent: February 11, 1997Assignee: The Penn State Research FoundationInventors: Randall M. German, Anthony Griffo, Tracy Potter
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Patent number: 5577424Abstract: A nitrogen-containing sintered hard alloy in which the content of the binder phase is at the highest level in an area to a depth of between 3 .mu.m and 500 .mu.m from its surface and its content in this area is between 1.1 and 4 times the average content of the binder phase in the entire alloy. Below this area, the content of the binder phase decreases gradually so that its content becomes equal to the average content of the binder phase at a depth of 800 .mu.m or less. The content of the binder phase in the surface layer is 90% or less of its maximum value. The depth of 800 .mu.m is a value at which the thermal conductivity is kept sufficiently high and at the same time a tool can keep high resistance to plastic deformation during cutting.Type: GrantFiled: March 28, 1995Date of Patent: November 26, 1996Assignee: Sumitomo Electric Industries, Ltd.Inventors: Kazutaka Isobe, Keiichi Tsuda, Nobuyuki Kitagawa, Toshio Nomura
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Patent number: 5571304Abstract: Oxide dispersion strengthened (ODS) Ni-base alloy foils are made directly from powders of these alloys by hot pressing. These ODS Ni-base alloy foils are characterized by having a thickness of 0.017 in. or less, and by the fact that they are fine-grained and substantially free of nitrogen and deformation induced defects. The as-pressed ODS Ni-base alloy foils are adapted for subsequent forming operations, including cold rolling. The reduction in thickness imparted in a single pass to an Ni-base alloy foil through cold-rolling was about 8%. The total reduction in thickness was about 55% based upon a plurality of such passes. For reductions in thickness greater than 20%, annealing is employed for stress relief.Type: GrantFiled: June 27, 1994Date of Patent: November 5, 1996Assignee: General Electric CompanyInventors: Ann M. Ritter, Melvin R. Jackson, Paul L. Dupree, Donald N. Wemple, Jr.
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Patent number: 5567891Abstract: A permanent magnet is provided which is comprised of, by atomic percent: 10-24% R; 2-28% boron, 0.1-18.12% hydrogen; and balance being M. R is at least one element selected from La, Ce, Pr, Nd, Pm, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu, Y and Sc, and M is at least one metal selected from Fe, Co, Ni, Li, Be, Mg, Rs, Si, Ti, V, Cr, Mn, Cu, Zn, Ga Ge, Zn, Nb, Mo, Ru, Rh, Pd, Ag, Sb, Te, Hf, Ta, W, Re, Os, Ir, Pt, Au, and Bi. A process for producing the rare earth element-metal-hydrogen boron magnets is also disclosed wherein the magnetic materials are treated in an atmosphere having partial pressures of hydrogen containing gas at temperatures below the phase transformation temperature of the rare earth element-metal hydrides prior to sintering.Type: GrantFiled: May 8, 1995Date of Patent: October 22, 1996Assignee: YBM Technologies, Inc.Inventors: Jacob G. Bogatin, Andrey Belov
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Patent number: 5545248Abstract: A titanium-base sintered alloy which comprises a TiC and/or TiN or Ti(C,N) solid solution accounting for 5 to 70 vol %, with the remainder being composed of two components. The first component is at least one species selected from the group consisting of Groups Va and VIa metallic elements, except Cr, or at least one species selected from the group consisting of carbides, nitrides, and carbonitrides of Groups Va and VIa metallic elements, except Cr. The second component is titanium. The first component accounts for 1 to 30 vol % and the second component accounts for 70 to 99 vol % of the total amount of the first and second components. The alloy produces a preferred result when the content of TiC or TiN is 35 to 70 vol % and the first component accounts for 1 to 15 vol % of the remainder. It is desirable that the TiC, TiN, and the first component of the remainder be in the form of a solid solution.Type: GrantFiled: February 14, 1995Date of Patent: August 13, 1996Assignee: Nippon Tungsten Co., Ltd.Inventors: Kei Tokumoto, Tetsunori Kitada, Hironobu Shinoaki, Shigeya Sakaguchi