Producing Alloy Patents (Class 75/351)
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Patent number: 7648555Abstract: Disclosed is a method for carrying out a reaction in a microreaction chamber. Nanoparticles which have been advantageously subjected to specific reactions in the microreaction chamber are used for carrying out the reaction. The obtained reaction product, which is preferably also provided in the form of nanoparticles. can then be removed from the microreaction chamber. Advantageously, the ongoing reaction can be specifically influenced by using the microreaction chamber. Both endothermic and exothermic reactions can be carried out with an accurately predictable result by feeding energy in a dosed manner into/out of the reaction chamber.Type: GrantFiled: September 27, 2006Date of Patent: January 19, 2010Assignee: Siemens AktiengesellschaftInventors: Frank Arndt, Jens Dahl Jensen, Ursus Krüger, Hendrik Rönsch
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Patent number: 7632332Abstract: The present teachings are directed towards methods of producing iron and titanium-containing nanoparticles by reducing iron and titanium-containing precursors with alkali or alkaline-earth metal-containing reducing agents in the presence of a suitable surfactant, and by the thermolysis of iron and titanium-containing precursors without alkali or alkaline-earth metal-containing reducing agents present.Type: GrantFiled: December 12, 2006Date of Patent: December 15, 2009Assignees: Honda Motor Co., Ltd., The Governors of the University of AlbertaInventors: Christopher J. Brooks, Jonathan Veinot, Janet MacDonald, Bryan Rowsell, Victoria Russell
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Publication number: 20090297397Abstract: A system for producing an elemental material or an alloy thereof from a halide of the elemental material or halide mixtures comprising a reactor for introducing the vapor halide of an elemental material or halide mixtures thereof into a liquid phase of a reducing metal of an alkali metal or alkaline earth metal or mixtures thereof present in less than or equal to the amount needed to reduce the halide vapor to the elemental material or alloy resulting in an exothermic reaction between the vapor halide and the liquid reducing metal producing particulate elemental material or alloy thereof and particulate halide salt of the reducing metal, a chamber wherein the reaction products are cooled so that substantially all the particulate elemental material or alloy remains unsintered, and a separator for separating the particulate metal or alloy reaction products from the particulate salt.Type: ApplicationFiled: August 3, 2009Publication date: December 3, 2009Inventors: Richard P. Anderson, Donn Armstrong, Jacobsen Lance
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Patent number: 7621977Abstract: A system and method of producing an elemental material or an alloy from a halide of the elemental material or halide mixtures. The vapor halide of an elemental material or halide mixtures are introduced into a liquid phase of a reducing metal of an alkali metal or alkaline earth metal or mixtures thereof present in excess of the amount needed to reduce the halide vapor to the elemental material or alloy resulting in an exothermic reaction between the vapor halide and the liquid reducing metal. Particulates of the elemental material or alloy and particulates of the halide salt of the reducing metal are produced along with sufficient heat to vaporize substantially all the excess reducing metal. Thereafter, the vapor of the reducing metal is separated from the particulates of the elemental material or alloy and the particulates of the halide salt of the reducing metal before the particulate reaction products are separated from each other.Type: GrantFiled: September 3, 2003Date of Patent: November 24, 2009Assignee: Cristal US, Inc.Inventors: Richard P. Anderson, Donn Armstrong, Jacobsen Lance
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Patent number: 7615096Abstract: A method for manufacturing a metal nanoparticle is provided. The method includes steps of: a) providing a metal salt solution, b) providing a reducing agent, c) providing a protecting agent, d) providing an alkaline solution, e) mixing the salt solution, the reducing agent, the protecting agent and the alkaline solution to form a slurry within a high-gravity field, and f) separating the metal nanoparticle from the slurry.Type: GrantFiled: January 11, 2007Date of Patent: November 10, 2009Assignee: National Taiwan UniversityInventors: Yi-Der Tai, Yao-Hsuan Wang, Ming-Hui Chang
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Publication number: 20090263268Abstract: A raw magnesium alloy powder material having a relatively small crystal grain diameter is obtained by subjecting a starting material powder having a relatively large crystal grain diameter to a plastic working in which the powder is passed through a pair of rolls to undergo compressive deformation or shear deformation. The starting material powder is a magnesium alloy powder having a fine intermetallic compound (21) precipitated and dispersed in a base (22) by a heat treatment. A work strain (22) is formed around the precipitated intermetallic compound (21) in the magnesium alloy powder after processed by the plastic working. The magnesium alloy powder after processed by the plastic working has a maximum size of 10 mm or less and a minimum size of 0.1 mm or more, and the magnesium particle constituting the base (20) has a maximum crystal grain diameter of 20 ?m or less.Type: ApplicationFiled: June 14, 2006Publication date: October 22, 2009Applicants: GOHSYU CO., LTD., KURIMOTO, LTD.Inventors: Katsuyoshi Kondoh, Mitsuhiro Goto, Hideaki Fukui, Kantaro Kaneko, Shuji Shiozaki, Katsuhito Itakura
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Publication number: 20090257907Abstract: SmCo-based alloy nanoparticles composed mainly of a SmCo-based alloy containing Sm and Co as constituent elements, wherein the content of metal elements other than Sm and Co is 0.05-20 wt % with respect to the SmCo-based alloy.Type: ApplicationFiled: March 4, 2009Publication date: October 15, 2009Applicants: TDK Corporation, Tokyo University of Science Educational Foundation Administrative OrganizationInventors: Mamoru Satoh, Naoki Toshima, Mutsuko Kinjo, Haruki Kinjo, Shiho Tokonami
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Publication number: 20090226753Abstract: The present invention provides metal nanowires including at least silver, and a metal other than silver, wherein the metal other than silver has a standard electrode potential more positive than the standard electrode potential of silver, and the metal nanowires have a long-axis length of 1 ?m or more and a short-axis length of 300 nm or less.Type: ApplicationFiled: March 5, 2009Publication date: September 10, 2009Applicant: FUJIFILM CorporationInventor: Kenji NAOI
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Patent number: 7582134Abstract: Provided is an aerosol method, and accompanying apparatus, for preparing powdered products of a variety of materials involving the use of an ultrasonic aerosol generator (106) including a plurality of ultrasonic transducers (120) underlying and ultrasonically energizing a reservoir of liquid feed (102) which forms droplets of the aerosol. Carrier gas (104) is delivered to different portions of the reservoir by a plurality of gas delivery ports (136) delivering gas from a gas delivery system. The aerosol is pyrolyzed to form particles, which are then cooled and collected. The invention also provides powders made by the method and devices made using the powders.Type: GrantFiled: October 31, 2006Date of Patent: September 1, 2009Assignee: Cabot CorporationInventors: Mark J. Hampden-Smith, Toivo T. Kodas, Quint H. Powell, Daniel J. Skamser, James Caruso, Clive D. Chandler
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Publication number: 20090208364Abstract: The invention concerns a method for making a thermoelectric element consisting mainly of a crystalline alloy having a cubic structure, the alloy comprising a first constituent having at least a first element selected among the transition metals, a second constituent having at least one element selected among column XIV, XV or XVI of the periodic table, and a third constituent having at least one constituent selected among rare earths, alkalis, alkaline earths or actinides. The method includes making the alloy in the form of nanopowders by mechanosynthesis. The invention also concerns the thermoelectric material obtained by implementing said method.Type: ApplicationFiled: April 5, 2006Publication date: August 20, 2009Applicant: Centre National de la Recherche Scientifique (CNRS)Inventors: David Berardan, Eric Alleno, Claude Godart, Eric Leroy
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Patent number: 7575621Abstract: A process for the production of metal nanoparticles. Nanoparticles are formed by combining a metal compound with a solution that comprises a polyol and a substance that is capable of being adsorbed on the nanoparticles. The nanoparticles are precipitated by adding a nanoparticle-precipitating liquid in a sufficient amount to precipitate at least a substantial portion of the nanoparticles and of a protic solvent in a sufficient amount to improve the separation of the nanoparticles from the liquid phase.Type: GrantFiled: January 13, 2006Date of Patent: August 18, 2009Assignee: Cabot CorporationInventors: Karel Vanheusden, Hyungrak Kiim, Aaron D. Stump, Allen B. Schult, Mark J. Hampden-Smith, Chuck Edwards, Anthony R. James, James Caruso, Toivo T. Kodas, Scott Thomas Haubrich, Mark H. Kowalski
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Patent number: 7566357Abstract: Methods for producing finely divided copper or copper alloy powders are described, from compositions containing metal ions and an alkanolamine, preferably monoethanolamine, wherein the alkanolamine acts as a primary reducing agent. In preferred embodiments the methods for producing micron and submicron copper powder utilize precursor compositions containing copper ions in the form of submicron particles of copper carbonate, copper hydroxide, copper oxides, or any combination thereof, and utilize monoethanolamine (or optionally but less preferably hydrazine), and preferably additionally containing caustic and a reducing sugar.Type: GrantFiled: March 14, 2007Date of Patent: July 28, 2009Assignee: Phibro Wood, LLCInventor: Gang Zhao
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Publication number: 20090155630Abstract: A method of producing alloy nanoparticles includes the steps of: adding a metallic salt, a reducing agent, a stabilizing ligand, and an organic iron complex to an organic solvent selected from the group consisting of 2-20C hydrocarbon, alcohol, ether, and ester in an inert gas atmosphere to obtain a reaction liquid; and stirring the reaction liquid while heating the reaction liquid to a predetermined temperature. The grain diameter of the alloy nanoparticle is controlled by regulating the amount of the stabilizing ligand.Type: ApplicationFiled: January 31, 2005Publication date: June 18, 2009Inventors: Satoru Momose, Hiroyoshi Kodama, Nobutaka Ihara, Takuya Uzumaki
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Publication number: 20090151512Abstract: A method for producing an alloy fine particle colloid by heating and evaporating a raw material binary alloy which is in a solid state in an ambient temperature and pressure environment in a reduced-pressure environment, cooling a generated vapor for condensation and solidification and collecting a formed alloy fine particle in a liquid medium, wherein (1) when an atomic fraction of a component element in the raw material alloy is defined as X, a component ratio of each of the elements of the raw material alloy is regulated such that a fraction of a vapor pressure of the component element to the total vapor pressure of the raw material alloy falls within the range of from (X?0.1) to (X+0.1); and (2) the raw material binary alloy is an alloy species which forms a homogeneous alloy phase in an alloy ingot. Thus, an alloy fine particle colloid is rationally and efficiently produced.Type: ApplicationFiled: April 25, 2007Publication date: June 18, 2009Inventor: Isao Nakatani
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Patent number: 7547347Abstract: A method of synthesizing nanoparticles includes: combining at least one stabilizing agent, at least one precursor and an ionic liquid to form a reaction mixture; heating the reaction mixture to a predetermined temperature to form the nanoparticles and cause the nanoparticles to self-separate from the reaction mixture; and collecting the nanoparticles from the reaction mixture. Ionic liquid from which the nanoparticles are separated may be reused.Type: GrantFiled: May 15, 2006Date of Patent: June 16, 2009Assignee: University of RochesterInventors: Hong Yang, Yong Wang
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Patent number: 7544229Abstract: The present invention discloses a novel method for the production of metallic nano-powder. This cost-effective, simple process is customized for a full-scale production of metallic nano-powders containing a first metal, and comprising the following of forming an alloy comprising said first metal and at least one soluble metal; applying first thermal treatment in the manner homogenized alloy is obtained; applying a cold work to the homogenized alloy so thin strips are obtained; applying a second thermal treatment to the alloy until a phase composition of predetermined characteristics is obtained; subjecting the said alloy to a leaching agent adapted to effectively leach out the least one soluble metal; filtering and washing the powder; washing the powder; drying the powder; coating the powder with chemicals; and then de-agglomerating the coated powder. The present invention also discloses a cost-effective and highly pure metallic powder produced by the method defined above.Type: GrantFiled: June 19, 2003Date of Patent: June 9, 2009Assignee: Cima NanoTech Israel Ltd.Inventors: Arkady Garbar, Fernando De La Vega, Einat Matzner
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Publication number: 20090139372Abstract: It is to propose a method of producing super-micro powders of pure metal-alloy in which cheap materials can be used and the production is efficient. In the production method of pure metal super-micro powder by heating a starting material containing a metal chloride and reducing the resulting vapor of the metal chloride with hydrogen gas, an elementary metal constituting the metal chloride is added to the starting material containing the metal chloride and a metal chloride having a large valence among metal chlorides having two or more valence is used as the metal chloride. Also, in the production method of alloy super-micro powder, a metal chloride is used as one to (number of all alloying components—1) alloying components in the starting material and an elemental metal is used as the other alloying component.Type: ApplicationFiled: November 5, 2003Publication date: June 4, 2009Applicants: ISHIHARA CHEMICAL CO, LTD, JFE MINERAL COMPANY, LTD.,Inventors: Yasunori Yonehana, Yoshinao Chisaki, Fumitaka Tsukihashi
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Patent number: 7537636Abstract: A method of making a superfine alloy comprises: incorporating a grain growth inhibitor polymeric precursor into a composition for synthesis of a superfine material; synthesizing the superfine material from the composition comprising the incorporated precursor; incorporating an alloy additive into the composition for synthesis of the superfine material before synthesizing the superfine material, or alternatively, into the as-synthesized superfine material to produce a superfine alloy-grain growth inhibitor polymeric precursor composite; and treating the superfine alloy-grain growth inhibitor polymeric precursor composite to convert the grain growth inhibitor polymeric precursor to a grain growth inhibitor.Type: GrantFiled: May 8, 2007Date of Patent: May 26, 2009Assignee: Inframat CorporationInventors: Danny T. Xiao, Chris W. Strock, Donald M. Wang, Peter R. Strutt
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Publication number: 20090107584Abstract: Solder compositions and methods of forming solders are provided. The solder compositions exhibit desirable melting characteristics. In addition, the solder compositions may be useful in joining heat sensitive components such as sensors, system-in-package, memory, and MEMS devices.Type: ApplicationFiled: September 29, 2008Publication date: April 30, 2009Applicant: NanoDynamics, Inc.Inventors: SUVANKAR SENGUPTA, Ramachandra R. Revur
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Patent number: 7524355Abstract: A method is disclosed for producing an energetic metastable nano-composite material. Under pre-selected milling conditions a mixture of powdered components are reactively milled. These components will spontaneously react at a known duration of the pre-selected milling conditions. The milling is stopped at a time at which the components have been compositionally homogenized to produce nanocomposite powder, but prior to said known duration, and thereby before the spontaneous reaction occurs. The milled powder is recovered as a highly reactive nanostructured composite for subsequent use by controllably initiating destabilization thereof.Type: GrantFiled: November 12, 2004Date of Patent: April 28, 2009Assignee: New Jersey Institute of TechnologyInventors: Edward Leonid Dreizin, Mirko Schoenitz
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Patent number: 7503959Abstract: Metal particles that can be alloyed with rhenium are dispersed as a main component in a gas phase, a rhenium oxide vapor is made to be present around these particles, the rhenium oxide is reduced, and the rhenium precipitated on the surface of the main component metal particles as a result of this reduction is diffused under a high temperature into the main component metal particles, which gives a rhenium-containing alloy powder including the main component metal and rhenium. The powder thus obtained preferably contains 0.01 to 50 wt % rhenium, has an average particle size of 0.01 to 10 ?m, and is made into a conductor paste by being uniformly mixed and dispersed in an organic vehicle along with other additives as needed.Type: GrantFiled: October 16, 2006Date of Patent: March 17, 2009Assignee: Shoei Chemical Inc.Inventors: Yuji Akimoto, Kazuro Nagashima, Masayuki Maekawa, Hidenori Ieda, Yasuhiro Kamahori
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Publication number: 20090014423Abstract: The present invention provides a radiofrequency plasma apparatus for the production of nanoparticles and method for producing nanoparticles using the apparatus. The apparatus is designed to provide high throughput and makes the continuous production of bulk quantities of high-quality crystalline nanoparticles possible. The electrode assembly of the plasma apparatus includes an outer electrode and a central electrode arranged in a concentric relationship to define an annular flow channel between the electrodes.Type: ApplicationFiled: July 10, 2007Publication date: January 15, 2009Inventors: Xuegeng Li, Maxim Kelman, Mason Terry, Elena Rogojina, Eric Schiff, Karel Vanheusden
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Publication number: 20090013824Abstract: Disclosed are a method of fabricating a binary alloy nanostructure by using metal oxides, metal substances or metal halides of metal elements used to form a binary alloy and/or binary alloy substances as a precursor through a vapor phase synthesis method and a binary alloy nanostructure fabricated by the same. More particularly, the present invention provides a method of fabricating a binary alloy nanowire or nanobelt which comprises placing a precursor on the front part of a reaction furnace and a substrate on the rear part of the furnace, and heat treating both of them under inert gas atmosphere to produce the nanowire or nanobelt and, in addition, a binary alloy nanowire or nanobelt fabricated by the method according to the present invention.Type: ApplicationFiled: July 7, 2008Publication date: January 15, 2009Inventors: Bong Soo Kim, June Ho In, Krishna Kumar, Hyo Tcheri Lhee, Yeong Dong Yoo
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Patent number: 7470309Abstract: The present invention relates to an economically excellent method for manufacturing ultra fine tungsten carbide-cobalt composite powder having tungsten compound and cobalt compound as its raw material. More particularly, the present invention provides a manufacturing method comprising a process for mixing tungsten compounds, cobalt compounds, grain-grown inhibitor compounds and oxide in a mechanical method, a calcination process for removing ammonia and moisture of the mixed powder and forming it into an composite oxide, a reduction process for manufacturing said calcined powder into pure metal powder, a mixing process for adding carbon source to said reduced powder, and a carburization process for manufacturing the mixed powder into a tungsten carbide-cobalt composite powder, which is the final form. Using the manufacturing method of the present invention, ultra-fine tungsten carbide-cobalt composite powder having an ultra-fine particle size of 0.1˜0.2 ?m, 0.2˜0.3 ?m,0.3˜0.Type: GrantFiled: April 27, 2006Date of Patent: December 30, 2008Assignee: Nanotech Co., Ltd.Inventors: Sang-Myun Kim, Hyun-Ho Lee, Min-Sun Hur
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Patent number: 7465333Abstract: A precursor halide compound is reduced to a predetermined product at substantially ambient conditions. The halide is added to an anhydrous liquid reaction medium containing one or more alkali metals or alkaline earth metals as reductants. The metal reductants are dispersed as very small globules in the liquid by cavitation of the liquid, such as by application of high intensity ultrasonic vibrations or high-shear mixing to the reaction vessel. Continued cavitation of the liquid medium affects low temperature reduction of the precursor halide(s) to produce a metal, metal alloy, metal compound, ceramic material, metal matrix-ceramic composite material, or the like. The practice may be applied, for example, to titanium tetrachloride, alone or with other chlorides, to produce titanium metal, titanium alloys (for example Ti-6Al-4V), and titanium compounds (TiSi2).Type: GrantFiled: August 17, 2006Date of Patent: December 16, 2008Assignee: GM Global Technology Operations, Inc.Inventors: Ion C. Halalay, Michael P. Balogh, Michael K. Carpenter
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Publication number: 20080295645Abstract: A precursor halide compound is reduced to a predetermined product at substantially ambient conditions. The halide is added to an anhydrous liquid reaction medium containing one or more alkali metals or alkaline earth metals as reductants. The metal reductants are dispersed as very small globules in the liquid by cavitation of the liquid, such as by application of high intensity ultrasonic vibrations or high-shear mixing to the reaction vessel. Continued cavitation of the liquid medium affects low temperature reduction of the precursor halide(s) to produce a metal, metal alloy, metal compound, ceramic material, metal matrix-ceramic composite material, or the like. The practice may be applied, for example, to titanium tetrachloride, alone or with other chlorides, to produce titanium metal, titanium alloys (for example Ti-6Al-4V), and titanium compounds (TiSi2).Type: ApplicationFiled: August 17, 2006Publication date: December 4, 2008Applicant: GM Global Technology Operations, Inc.Inventors: Ion C. Halalay, Michael P. Balogh, Michael K. Carpenter
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Patent number: 7455713Abstract: A titanium halide and, optionally, other precursor halides compound are reduced to a predetermined titanium product, suitably at or near ambient conditions. Titanium tetrachloride, for example, is added to an anhydrous liquid reaction medium containing one or more alkali metals or alkaline earth metals as reductants. The metal reductants are dispersed as very small globules in the liquid by cavitation of the liquid reaction medium, such as by application of high intensity ultrasonic vibrations or high-shear mixing to the reaction vessel. Continued cavitation of the liquid medium affects relatively low temperature reduction of the precursor halide(s) to produce a titanium-containing product such as titanium metal, a titanium alloy or compound, or a titanium matrix-ceramic composite material, or the like.Type: GrantFiled: August 17, 2006Date of Patent: November 25, 2008Assignee: GM Global Technology Operations, Inc.Inventors: Ion C. Halalay, Michael P. Balogh
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Patent number: 7419528Abstract: A metallic article made of metallic constituent elements is fabricated from a mixture of nonmetallic precursor compounds of the metallic constituent elements. The mixture of nonmetallic precursor compounds contains more of a base-metal element, such as nickel, cobalt, iron, iron-nickel, and iron-nickel-cobalt than any other metallic element. The mixture of nonmetallic precursor compounds is chemically reduced to produce a metallic superalloy material, without melting the metallic superalloy material. The metallic superalloy material is consolidated to produce a consolidated metallic article, without melting the metallic superalloy material and without melting the consolidated metallic article.Type: GrantFiled: February 19, 2003Date of Patent: September 2, 2008Assignee: General Electric CompanyInventors: Clifford Earl Shamblen, Andrew Philip Woodfield, Eric Allen Ott, Michael Francis Xavier Gigliotti
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Patent number: 7416579Abstract: Nanometer sized particles containing titanium and platinum are prepared by a sonochemical process. Compounds of the metals are dissolved, suspended, or diluted in a low vapor pressure liquid medium, preferably at a sub-ambient temperature. A reducing gas is bubbled through the liquid as it is subjected to cavitation to affect the reductive decomposition of the metal compounds. Titanium and platinum are co-precipitated in very small particles.Type: GrantFiled: July 8, 2005Date of Patent: August 26, 2008Assignee: GM Global Technology Operations, Inc.Inventors: Ion C. Halalay, Michael Kevin Carpenter
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Patent number: 7416697Abstract: A method for preparing an article of a base metal alloyed with an alloying element includes the steps of preparing a compound mixture by the steps of providing a chemically reducible nonmetallic base-metal precursor compound of a base metal, providing a chemically reducible nonmetallic alloying-element precursor compound of an alloying element, and thereafter mixing the base-metal precursor compound and the alloying-element precursor compound to form a compound mixture. The compound mixture is thereafter reduced to a metallic alloy, without melting the metallic alloy. The step of preparing or the step of chemically reducing includes the step of adding an other additive constituent. The metallic alloy is thereafter consolidated to produce a consolidated metallic article, without melting the metallic alloy and without melting the consolidated metallic article.Type: GrantFiled: May 17, 2004Date of Patent: August 26, 2008Assignee: General Electric CompanyInventors: Andrew Philip Woodfield, Eric Allen Ott, Clifford Earl Shamblen, Michael Francis Xavier Gigliotti
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Patent number: 7407527Abstract: A synthetic method of fabricating highly crystalline and monodisperse nanoparticles of metals, multi-metallic alloys, monometallic oxides and multi-metallic oxides without a size selection process are disclosed. A typical synthetic method comprises the steps of, synthesis of a metal surfactant complex from the reaction of a metal precursor and a surfactant, high temperature thermal decomposition of the metal surfactant complex to produce monodisperse metal nanoparticles, and completing the formation of synthesized metal, metal alloy or metal oxide nanoparticles by adding a poor solvent followed by centrifuging. For obtaining highly crystalline monodisperse nanoparticles, additional steps are necessary as described in the invention. The resulting nanoparticles have excellent magnetic property for many applications.Type: GrantFiled: January 22, 2002Date of Patent: August 5, 2008Assignee: Seoul National University Industry FoundationInventor: Taeghwan Hyeon
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Patent number: 7404842Abstract: A hydrogen storage system is described that can fabricated under ambient atmospheric conditions and humidity. The hydrogen storage system includes hydrogen-absorbing alloy particles, such as ABx-type alloys, for example LaNi4.7Al0.3, AB/A2B-type alloys, for example Mg2Ni, and AB2-type alloys, and group VIII transition metal particles, such as Pd, Pt, Ni, Ru, and/or Re, that are mechanically alloyed. The mechanically alloyed particles are stable and retain their hydrogen-absorbing efficiency even after prolonged exposure to air and water. Binders and solvent can be added to produce low-viscosity inks. The hydrogen storage system can be used with fuel cells that can be microfabricated and optionally be integrated with electronic devices.Type: GrantFiled: January 23, 2004Date of Patent: July 29, 2008Inventors: Jesse Wainright, Joe Payer, Chung-Chiun Liu, Laurie Dudik, Xi Shan, Seth Levine
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Publication number: 20080175740Abstract: A method for manufacturing of iron- respectively micro-alloyed steel powders, starting from fluffy spray roasted iron oxides exhibiting a specific surface area in excess of 2.0 m2/g and residual chloride contents over 440 ppm Cl?, decrease the chloride content in two steps to less than 100 ppm, the specific surface area (BET) of to a pre-selected value of less than 10.0 m2/g, preferably between 0.1 and 2.0 m2/g and reduce the pre-sintered granules exhibiting a bulk density in excess of 1.200 g/dm3.Type: ApplicationFiled: December 3, 2007Publication date: July 24, 2008Applicant: Dr. Michael J. RuthnerInventor: Michael J. RUTHNER
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Publication number: 20080145687Abstract: A method of producing titanium metal from a titanium-containing material includes the steps of producing a solution of M?TiF6 from the titanium-containing material, selectively precipitating M?2TiF6 from the solution by the addition of (M?)aXb and using the selectively precipitated M?2TiF6 to produce titanium. M? is a cation of the type which forms a hexafluorotitanate, M? is selected from ammonium and the alkali metal cations, X is an anion selected from halide, sulphate, nitrite, acetate and nitrate and a and b are 1 or 2.Type: ApplicationFiled: December 14, 2005Publication date: June 19, 2008Inventor: Gerard Pretorius
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Publication number: 20080134836Abstract: The present teachings are directed towards methods of producing iron and titanium-containing nanoparticles by reducing iron and titanium-containing precursors with alkali or alkaline-earth metal-containing reducing agents in the presence of a suitable surfactant, and by the thermolysis of iron and titanium-containing precursors without alkali or alkaline-earth metal-containing reducing agents present.Type: ApplicationFiled: December 12, 2006Publication date: June 12, 2008Inventors: Christopher J. Brooks, Jonathan Veinot, Janet MacDonald, Bryan Rowsell, Victoria Russell
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Patent number: 7384447Abstract: Nickel powder batches including coated nickel-containing particles and methods for producing the same. The coated nickel-containing particles having have a small particle size, narrow size distribution and a spherical morphology. The present invention is also directed to devices incorporating the coated nickel-containing particles.Type: GrantFiled: November 1, 2004Date of Patent: June 10, 2008Assignee: Cabot CorporationInventors: Toivo T. Kodas, Mark J. Hampden-Smith, James Caruso, Quint H. Powell, Clive D. Chandler, Daniel J. Skamser
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Patent number: 7384596Abstract: A method for preparing a metallic article made of metallic constituent elements includes furnishing a mixture of nonmetallic precursor compounds of the metallic constituent elements. The method further includes chemically reducing the mixture of nonmetallic precursor compounds to produce an initial metallic material, without melting the initial metallic material, and consolidating the initial metallic material to produce a consolidated metallic article, without melting the initial metallic material and without melting the consolidated metallic article.Type: GrantFiled: July 22, 2004Date of Patent: June 10, 2008Assignee: General Electric CompanyInventors: Andrew Philip Woodfield, Clifford Earl Shamblen, Eric Allen Ott, Michael Francis Xavier Gigliotti
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Patent number: 7361205Abstract: The invention relates to a method of producing granules made of high purity metal or metal alloy, in particular based on chromium, the method being characterized in that it comprises the steps consisting in: preparing a metal or a metal alloy having non-metallic inclusions essentially comprising oxides of the base metal; pelletizing the metal or the alloy with a reducing agent in order to form the pellets or tablets; treating the pellets or tablets in a vacuum in order to enable the reducing agent to react on the inclusions without substantial sublimation of the metal or the metals of the alloy; and eliminating a surface layer from the pellets or tablets. The invention is applicable to manufacturing mechanical parts out of superalloys.Type: GrantFiled: January 20, 2003Date of Patent: April 22, 2008Assignee: Delachaux S.A.Inventor: Philippe Liebaert
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Patent number: 7354472Abstract: A method of producing a refractory metal powder by (A) combining (i) an oxide particle component and (ii) a reducing agent; (B) forming a substantially uniform mixture of (i) and (ii); (C) continuously feeding the mixture into a furnace; (D) igniting the mixture at a reaction zone and starting a reaction that is sufficiently exothermic to form a high temperature flash; (E) starting a reaction that is sufficiently exothermic to form a high temperature self-sustaining flash; and (F) producing a free-flowing reduced oxide powder.Type: GrantFiled: June 21, 2004Date of Patent: April 8, 2008Assignee: H.C. Starck Inc.Inventors: Leonid Natan Shekhter, Edward V. McCormick, Leah F. Simkins, Edward K. Schiele
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Patent number: 7354471Abstract: Provided are silver-containing powders and a method and apparatus for manufacturing the silver-containing particles of high quality, of a small size and narrow size distribution. An aerosol is generated from liquid feed and sent to a furnace, where liquid in droplets in the aerosol is vaporized to permit formation of the desired particles, which are then collected in a particle collector. The aerosol generation involves preparation of a high quality aerosol, with a narrow droplet size distribution, with close control over droplet size and with a high droplet loading suitable for commercial applications.Type: GrantFiled: September 24, 2004Date of Patent: April 8, 2008Assignee: Cabot CorporationInventors: Mark J. Hampden-Smith, Toivo T. Kodas, Quint H. Powell, Daniel J. Skamser, James Caruso, Clive D. Chandler
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Patent number: 7351272Abstract: A method of controlling the size and morphology of powder made by the subsurface injection of a halide vapor into a liquid metal is disclosed. A reaction zone is established and the temperature thereof or the time the powder remains therein is controlled to change powder characteristics.Type: GrantFiled: September 3, 2003Date of Patent: April 1, 2008Assignee: International Titanium Powder, LLCInventors: Donn Reynolds Armstrong, Richard Paul Anderson, Lance E. Jacobsen
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Patent number: 7335245Abstract: The present teachings are directed toward single metal and alloy nanoparticles and synthesis methods for preparing single metal and alloy nanoparticles.Type: GrantFiled: September 17, 2004Date of Patent: February 26, 2008Assignees: Honda Motor Co., Ltd., The Research Foundation of the State University of New YorkInventors: Ting He, Chuan-Jian Zhong, Jin Luo, Mathew M. Maye, Li Han, Nancy N. Kariuki, Lingyan Wang
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Publication number: 20080019858Abstract: An atomised pre-alloyed iron-based powder which comprises by weight-% 10.5-30 Cr ??3-15 Al ??5-20 Cu max 0.1 C max 0.2 N max 3.0 Mn max 2.5 Si max 3.0 Mo balance essentially only iron and unavoidable impurities.Type: ApplicationFiled: June 25, 2007Publication date: January 24, 2008Inventors: Ove H. Mars, Ingrid Hauer
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Patent number: 7309374Abstract: In contrast to current industrial practice where alloying powders are added to starting powder metallurgy compositions either as powder mixtures or fully prealloyed powders, the present invention posits a diffusion bonded nickel-copper precursor additive mixture for direct one step addition to the starting powder metallurgy master blend composition. Segregation and dusting are substantially reduced and the mechanical properties of the resultant compact are improved.Type: GrantFiled: April 4, 2005Date of Patent: December 18, 2007Assignee: Inco LimitedInventors: Tajpreet Singh, Scott Thomas Campbell, Thomas Francis Stephenson, Ouan Min Yang
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Patent number: 7297179Abstract: A method of producing (1) metal particles or (2) metal fine-particles, which contains: jetting out two solutions of (1) a metal salt solution and a reducing agent solution, or (2) a metal ion-containing solution and a hydroxide ion-containing solution, from respective nozzles to a mixing chamber, to give a mixed reaction solution; and discharging the mixed reaction solution from a discharging port having a diameter smaller than a diameter of the mixing chamber, wherein one of the two solutions is made into straightly-going flow, which is jetted from a nozzle having a diameter smaller than the diameter of the mixing chamber to the mixing chamber, and the other solution is jetted out, as flow substantially orthogonal to the straightly-going flow, to a position before a position where eddy viscosity generated by the straightly-going flow would be maximum.Type: GrantFiled: September 26, 2003Date of Patent: November 20, 2007Assignee: Fujifilm CorporationInventor: Katsuhisa Ohzeki
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Patent number: 7291201Abstract: A method for making Nano-scale lead-free solder includes the following steps of: forming a mixture solution Sn-Ag or Sn-Ag-Cu; making NaBH4, NaOH and alkyl C12H25OSO3Na to a reducing dispersing solution; producing reactant Sn-Ag or Sn-Ag-Cu by means of the oxidation reduction method; and adding 95% ethanol to be mixed, and cleaning the reactant by using a supersonic vibrator for removing boron (B) and sulfur (S) atom which adhere to the reactant, thereby producing the Nano-scale (0.1˜100 nm) lead-free solder Sn-3.5Ag or Sn-3.5Ag-xCu (x=0.2˜1.0).Type: GrantFiled: August 30, 2004Date of Patent: November 6, 2007Assignee: National Tsing Hua UniversityInventors: Jeng-Gong Duh, Li-Yin Hsiao
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Patent number: 7288134Abstract: Dumbbell-shaped or flower-shaped nanoparticles and a process of forming the same, wherein the process comprises forming a mixture of a nanoparticle with a precursor in a first solvent, wherein the nanoparticle comprises a hydrophobic outer coating; heating the mixture; cooling the mixture to room temperature; modifying the hydrophobic outer coating into a hydrophilic outer coating; precipitating a solid product from the mixture, and dispersing the product in a second solvent. The nanoparticles comprise any of a semiconducting, magnetic, and noble metallic material, wherein the nanoparticles comprise a first portion comprising any of PbSe, PbS, CdSe, CdS, ZnS, Au, Ag, Pd, and Pt, and wherein the precursor comprises any of a cationic, neutral or particulate Au, Ag, Pd, Pt, or transition metal (Fe, Co, Ni) precursors of Fe(CO)5, Co(CO)8, Ni(CO)4 or their analogues. The first and second solvents comprise any of alkanes, arenes, ethers, nitrites, ketones, and chlorinated hydrocarbons.Type: GrantFiled: September 10, 2004Date of Patent: October 30, 2007Assignee: International Business Machines CorporationInventors: Shouheng Sun, Heng Yu, Shan X. Wang
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Patent number: 7270694Abstract: A process comprising: reacting a silver compound with a reducing agent comprising a hydrazine compound in the presence of a thermally removable stabilizer in a reaction mixture comprising the silver compound, the reducing agent, the stabilizer, and an optional solvent, to form a plurality of silver-containing nanoparticles with molecules of the stabilizer on the surface of the silver-containing nanoparticles.Type: GrantFiled: October 5, 2004Date of Patent: September 18, 2007Assignee: Xerox CorporationInventors: Yuning Li, Yiliang Wu, Beng S. Ong
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Patent number: 7258722Abstract: Any one of a Ti-containing water-soluble salt, metatitanic acid (TiO(OH)2) slurry and ultra fine titanium oxide powder, and a transition metal containing metal salt are dissolved in water to prepare a raw material mixture. The raw material is spray-dried to obtain precursor powder, which is calcined to form ultra fine Ti/transition metal complex oxide and is then mixed with nano-sized carbon particles and subjected to reduction and carburization in a non-oxidizing atmosphere.Type: GrantFiled: December 30, 2003Date of Patent: August 21, 2007Assignee: Korea Institute of Machinery and MaterialsInventors: Byoung Kee Kim, Seong Hyeon Hong, Yong Won Woo
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Patent number: 7244287Abstract: The present invention relates to a method of producing a magnetic particle including forming a layer containing an alloy particle that can form a CuAu-type or Cu3Au-type hard magnetic ordered alloy phase on a support, oxidizing the layer, and annealing the layer in a non-oxidizing atmosphere. The invention also relates to a method of producing a magnetic particle including producing an alloy particle that can form a hard magnetic ordered alloy phase, oxidizing the alloy particle, and annealing the particle in a non-oxidizing atmosphere, and a magnetic particle produced by the foregoing production method. Further, the invention relates to a magnetic recording medium comprising a magnetic layer containing a magnetic particle and a method of producing a magnetic recording medium including forming a layer containing an alloy that can form the foregoing hard magnetic ordered alloy phase, oxidizing the layer, and annealing the layer in a non-oxidizing atmosphere.Type: GrantFiled: July 22, 2004Date of Patent: July 17, 2007Assignee: Fujifilm CorporationInventors: Yasushi Hattori, Koukichi Waki, Keizo Ogawa