Treating Polymer Containing Material Or Treating A Solid Polymer Or A Resinifiable Intermediate Condensation Product Patents (Class 528/480)
  • Patent number: 8541513
    Abstract: Disclosed are terminal-modified difunctional sulfur-containing polymers that are the reaction products of a sulfur-containing diol, an aldehyde or a ketone, and a compound containing a functional group. Compositions comprising the terminal-modified difunctional sulfur-containing polymers useful as sealants are also disclosed.
    Type: Grant
    Filed: March 18, 2011
    Date of Patent: September 24, 2013
    Assignee: PRC-DeSoto International, Inc.
    Inventors: Stephen J. Hobbs, Gregory J. McCollum, Lawrence G. Anderson, Renhe Lin
  • Patent number: 8530531
    Abstract: Method for the recycling of polyvinyl butyral based on obtaining recycled polyvinyl butyral (PVB) from laminated glass which is shattered and the polyvinyl butyral (PVB) is separated. The sheet obtained is cut into pieces and cleaned to eliminate dirt and foreign matter. The solid state PVB is subjected to a first polyvinyl butyral (PVB) purification stage with a chemical treatment with a first reagent and a final chemical treatment with a second reagent. The obtained purified polyvinyl butyral is suitable to be used in the manufacture of laminated glass.
    Type: Grant
    Filed: March 27, 2008
    Date of Patent: September 10, 2013
    Assignee: L'Urederra Fundacion para el Desarrollo Technologico y Social
    Inventors: Claudio Fernández Acevedo, Luis Martínez de Morentín Osaba, Edurne Osés Arteta, Germán Medina Herrera, María Antonia Fernández Fernández
  • Patent number: 8530618
    Abstract: Process for recovering a polymer by injection of steam, and optionally liquid water, into a solution of this polymer comprising a polar aprotic organic solvent (PAOS) that has an azeotrope with water and an apolar organic compound that is miscible with the PAOS and immiscible with water and that acts as a phase separation agent (PSA), the boiling point of which is below that of the water/PAOS azeotrope, the amount of steam injected being sufficient to give rise to the substantial removal of the PSA via stripping and that of the PAOS via azeotropic distillation, and the total amount of water being sufficient to give rise to the precipitation of the polymer, this process being characterized in that the polymer solution also comprises an alcohol, at least during the precipitation of the polymer.
    Type: Grant
    Filed: September 18, 2008
    Date of Patent: September 10, 2013
    Assignee: Solvay
    Inventors: Jean-Christophe Lepers, Denis Geets, Jean-Raphael Caille
  • Patent number: 8530608
    Abstract: What is disclosed is a water-based adhesive composition that is an aqueous dispersion or emulsion of a polymer component having functional groups that are inactive in a reversible manner in the adhesive composition as prepared; and a water-soluble, or water emulsion, or dispersion of a cross linker component having functional groups wherein the functional groups are inactive in a reversible manner in the adhesive composition as prepared. Preferably the adhesive composition has a pH of from 7 to 11 and a volatile stabilizing base component is used to inactivate the functional groups and to provide the pH. The functional groups in the polymer component and the cross linker component are activated when the volatile base is removed during lamination heat treatment. The adhesive composition can be used to adhere a variety of plastic films to metal substrates without reliance on non-water-based adhesives.
    Type: Grant
    Filed: September 24, 2010
    Date of Patent: September 10, 2013
    Assignee: Henkel AG & Co. KGaA
    Inventors: John D. McGee, Brian D. Bammel
  • Patent number: 8524859
    Abstract: In the production of isobutylene-based elastomers the product obtained from the polymerization process is often in the form of a stream. Described herein are an apparatus and a process for removal of hydrocarbon liquids from the elastomer. The process comprises the steps of obtaining a stream comprising hydrocarbon liquids, either solvents or diluents, and an isobutylene-based elastomer; passing the stream through a kneader to volatize the hydrocarbon liquids from the elastomer.
    Type: Grant
    Filed: March 23, 2011
    Date of Patent: September 3, 2013
    Assignee: ExxonMobil Chemical Patents Inc.
    Inventors: Yu Feng Wang, Richard C-M Yeh
  • Patent number: 8524789
    Abstract: A process for recovering waste latex material from a manufacturing plant, treating the recovered waste latex material, and subsequently utilizing the recovered and treated waste latex material in a manufacturing plant. Waste latex material is recovered and treated to provide a fine, sand-like material that is suitable for reintroduction into a latex adhesive manufacturing process.
    Type: Grant
    Filed: July 9, 2012
    Date of Patent: September 3, 2013
    Assignee: C & H Services Of North Georgia, LLC
    Inventor: James Craig Hankins
  • Patent number: 8519093
    Abstract: A process for the continuous thermal treatment of mixed substances, especially of solutions, suspensions and emulsions, wherein the continuous treatment of the mixed substances is divided into a main vaporization and a degassing stage, in which instance the main vaporization and the degassing take place in each case takes place in a separate mixer-kneader.
    Type: Grant
    Filed: February 5, 2010
    Date of Patent: August 27, 2013
    Assignee: List Holding AG
    Inventors: Andreas Diener, Pierre-Alain Fleury, Thomas Isenschmid, Alfred Kunz, Alain Schwick, Manuel Steiner, Daniel Witte
  • Patent number: 8519094
    Abstract: Process for heating a polymer-containing stream being transferred from a polymerization reactor to a separation zone or device, by passing the stream through at least two heaters operating in parallel, each heater having at least one transfer line for the stream and a heater for heating the transfer line. The average particle of the polymer is below 3 mm, the temperature of the polymer-containing stream at the outlet of all heaters is maintained above the dew point of the stream, and no heater has a volumetric flowrate of polymer-containing stream more than three times that of any other heater.
    Type: Grant
    Filed: April 15, 2009
    Date of Patent: August 27, 2013
    Assignee: Ineos Manufacturing Belgium NV
    Inventors: Daniel Marissal, Marc Parisel, Brent Walworth
  • Patent number: 8513378
    Abstract: The present invention provides a method for producing a water-absorbing resin powder. The method includes a polymerization step, a drying step, a pulverization step, a classification step, and a surface cross-linking step. It further includes an additional step, performed before the surface cross-linking step, in which at least part of the classified polymer is supplied again to the same or a different pulverization step. The circulation pulverization ratio in the pulverization step is higher than 1.50.
    Type: Grant
    Filed: September 16, 2010
    Date of Patent: August 20, 2013
    Assignee: Nippon Shokubai Co., Ltd.
    Inventors: Sayaka Machida, Kazushi Torii, Yoko Shirai, Hiroyuki Ikeuchi, Kunihiko Ishizaki
  • Patent number: 8513364
    Abstract: A production method of a water-absorbent resin includes the steps of: obtaining a hydrogel by supplying monomer liquid to a reaction device so that the monomer liquid is polymerized; and detaching the hydrogel from the reaction device, wherein the reaction device's surface in contact with the monomer liquid at a position where polymerization occurs is made of a fluororesin having a melt viscosity of less than 1×108 poise at 380° C. On this account, it is possible to obtain a water-absorbent resin having less amounts of an extractable content with high productivity and it is possible to carry out continuous production for an extended period of time.
    Type: Grant
    Filed: January 20, 2006
    Date of Patent: August 20, 2013
    Assignee: Nippon Shokubai Co., Ltd.
    Inventors: Masazumi Sasabe, Sumio Okuda, Yorimichi Dairoku, Shuji Kanzaki, Yoshihiro Kita, Motohiro Imura
  • Patent number: 8492512
    Abstract: The disclosed process comprises freeze-drying a biodegradable implant device comprised or one or more polyesters to thereby reduce moisture content in the device.
    Type: Grant
    Filed: August 30, 2011
    Date of Patent: July 23, 2013
    Assignee: Surmodics Pharmaceuticals, Inc.
    Inventors: Adrian Raiche, Brandon Smith, Kehley Miller
  • Patent number: 8486530
    Abstract: A method of reducing a volatile organic compound of composite resin particles comprising the step of: blowing a gas from a bottom part of a container in order to fluidize composite resin particles containing a polyolefin-based resin and a polystyrene-based resin in the container until an amount of volatile organic compounds contained in the whole composite resin particles becomes 50 ppm or less, wherein the gas has a temperature of (T?40) to (T?10)° C. when a softening temperature of the composite resin particles is defined as T° C.
    Type: Grant
    Filed: March 24, 2010
    Date of Patent: July 16, 2013
    Assignee: Sekisui Plastics Co., Ltd.
    Inventors: Hideyasu Matsumura, Shinji Ishida
  • Patent number: 8487049
    Abstract: A process is described for recycling superabsorbent polymer fines into a process that includes treating the superabsorbent polymer fines with caustic and a polymerization step for making the superabsorbent polymer gel. The process requires treating the superabsorbent polymer fines with a caustic, followed by mixture with polymerizable monomer solution, and polymerizing the mixture of the superabsorbent polymer fines and monomer to form the aqueous fluid absorbent polymer. In the process, the fines are incorporated into the new polymer gel and become indistinguishable there from. The gel may then be comminuted into a particulate dried and then separated into a portion having a desired minimum particle size in a fines portion having less than the desired size. The particulate may then be coated with a surface crosslinking agent and surface additives and heated for surface conversion.
    Type: Grant
    Filed: November 9, 2012
    Date of Patent: July 16, 2013
    Assignee: Evonik Stockhausen, LLC
    Inventors: Gonglu Tian, Scott J. Smith, Janet Pate-Linton
  • Patent number: 8481607
    Abstract: A surface treatment method for a fluororesin molded body, which is a method for treating a surface of an ETFE molded body by using a glow discharge generated by a pulsed electric field having a voltage-rising time of at most 10 ?sec in a nitrogen atmosphere under a pressure in the vicinity of atmospheric pressure; which comprises carrying out a plurality of glow discharge treatments at intervals of at least 0.01 sec so that the discharge density of each of the glow discharges is from 40 to 200 W·min/m2, and that the total discharge density of the glow discharges is from 220 to 800 W·min/m2. Further, an ETFE molded body subjected to a surface treatment by the surface treatment method.
    Type: Grant
    Filed: July 26, 2012
    Date of Patent: July 9, 2013
    Assignee: Asahi Glass Company, Limited
    Inventors: Hiroshi Aruga, Koichi Oda
  • Patent number: 8481675
    Abstract: A process for recycling a polymer blend necessarily containing PLA, comprising grinding, compacting, dissolving in a solvent of PLA, removing the undissolved contamining polymers, alcoholysis depolymerisation reaction and purification steps.
    Type: Grant
    Filed: March 31, 2010
    Date of Patent: July 9, 2013
    Assignee: Galactic S.A.
    Inventors: Philippe Coszach, Jean-Christophe Bogaert, Jonathan Willocq
  • Patent number: 8470897
    Abstract: A process for devulcanizing crosslinked elastomer particles comprising applying an alternating electric field to a composition comprising crosslinked elastomer particles under compression. The alternating electric field preferably has a frequency between 1 and 100 MHz and a voltage between 1000 and 10,000 V, and may be applied between an apparatus that continuously conveys the particles through the field.
    Type: Grant
    Filed: July 18, 2011
    Date of Patent: June 25, 2013
    Assignee: Vertex L.L.C.
    Inventor: Michel Marc
  • Patent number: 8470962
    Abstract: A method of preventing bubble formation during or after thermoforming polyester sheet comprising heating the polyester sheet to about 100-165° F. for at least about 1 hour prior to thermoforming the sheet.
    Type: Grant
    Filed: January 27, 2011
    Date of Patent: June 25, 2013
    Assignee: MYCONE Dental Supply Co., Inc.
    Inventor: David E. Nelson
  • Patent number: 8466257
    Abstract: Methods and apparatus for the recovery and purification of solid salt compositions from an organic liquid containing epoxy resin and at least one of epihalohydrin and solvent to obtain purified salt and/or brine compositions that may be useful in industrial processes.
    Type: Grant
    Filed: February 9, 2009
    Date of Patent: June 18, 2013
    Assignee: Dow Global Technologies LLC
    Inventors: Thomas C. Young, Ha Q. Pham, Shuji Maeda
  • Patent number: 8445187
    Abstract: A hardmask composition includes an organic solvent and one or more aromatic ring-containing polymers represented by Formulae 1, 2 and 3:
    Type: Grant
    Filed: July 14, 2011
    Date of Patent: May 21, 2013
    Assignee: Cheil Industries, Inc.
    Inventors: Kyong Ho Yoon, Jong Seob Kim, Dong Seon Uh, Hwan Sung Cheon, Chang Il Oh, Min Soo Kim, Jin Kuk Lee
  • Patent number: 8431677
    Abstract: Method for purifying a conventional polymer stream (PE, PP, PET, PVC, etc.) contaminated with not more than 50% PLA, comprising steps for the suspension of the polymer with solubilisation of the PLA fraction and the recovery of the purified polymer after separation.
    Type: Grant
    Filed: July 14, 2010
    Date of Patent: April 30, 2013
    Assignee: Galactic S. A.
    Inventors: Philippe Coszach, Jonathan Willocq
  • Patent number: 8431683
    Abstract: A process for recycling a polymer blend necessarily containing PLA, comprising grinding, compacting, dissolving in a solvent of PLA, removing the undissolved contaminating polymers, hydroloysis depolymerization reaction and purification steps.
    Type: Grant
    Filed: March 31, 2010
    Date of Patent: April 30, 2013
    Assignee: Galactic S.A.
    Inventors: Philippe Coszach, Jean-Christophe Bogaert, Jonathan Willocq
  • Patent number: 8426480
    Abstract: Methods of reclaiming plastic from infectious medical waste and manufacturing medical devices from reclaimed plastic are described. Medical devices made from plastic reclaimed from infectious medical waste are also described.
    Type: Grant
    Filed: September 16, 2010
    Date of Patent: April 23, 2013
    Assignee: Becton, Dickinson and Company
    Inventors: Richard Ji, Kenneth McCord
  • Patent number: 8420702
    Abstract: Process for recycling a fiber reinforced polymer article, according to which the article, eventually cut in fragments, is dissolved in a solvent capable of dissolving the polymer but not the fibers and which is susceptible of forming an azeotrope with water, forming a solution; the fibers are recovered from the solution; the fibers are washed with solvent by putting them in the form of a slurry in the solvent and by agitating the slurry and/or by making the solvent circulate through it; the washed fibers are recovered from the slurry; and the recovered fibers are submitted to a stripping with steam in order to substantially remove the solvent.
    Type: Grant
    Filed: May 7, 2009
    Date of Patent: April 16, 2013
    Assignee: Solvay S.A.
    Inventors: Jacques Van Weynbergh, Stephane Noel
  • Patent number: 8420703
    Abstract: The purpose of the present invention is to provide a method for collecting effective components from polyester fiber waste containing polyalkylene telephthalate as the main component, more specifically to provide a method for separating and removing foreign matters (mainly cotton) contained in polyester fiber waste. The purpose of the invention can be achieved by a method for separating and removing foreign matters from polyester waste, which includes throwing polyester fiber waste that contains polyalkylene telephthalate as the main component and foreign matters other than the polyalkylene telephthalate into a depolymerization reaction tank, subjecting a part or all of the polyester fiber to a depolymerization reaction with alkylene glycol to give a depolymerization reaction liquid, and then continuously or intermittently feeding the liquid to a foreign matter-separating and removing apparatus having specified characteristics.
    Type: Grant
    Filed: February 19, 2008
    Date of Patent: April 16, 2013
    Assignee: Teijin Fibers Limited
    Inventors: Kouji Mukai, Minoru Nakashima
  • Patent number: 8415402
    Abstract: A method for separating a polymer from carbon black in devulcanized rubber, the method comprising steps of inserting devulcanized rubber into a bath of a solvent, dissolving a polymer out of the devulcanized rubber and into a solution of the solvent and the polymer, removing the solution from the bath without disturbing an un-dissolved residue comprising carbon black, and recovering the un-dissolved residue.
    Type: Grant
    Filed: October 29, 2009
    Date of Patent: April 9, 2013
    Assignee: Rubreco Inc.
    Inventors: Brian Harrison, Hurdon Hooper, Ross Gilders, Leo Cheung, Matthew Ness
  • Patent number: 8410245
    Abstract: Solid-state shear pulverization of semi-crystalline polymers and copolymers thereof and related methods for enhanced crystallization kinetics and physical/mechanical properties.
    Type: Grant
    Filed: February 2, 2009
    Date of Patent: April 2, 2013
    Assignee: Northwestern University
    Inventors: John M. Torkelson, Cynthia Pierre, Amanda Flores
  • Patent number: 8404753
    Abstract: A method of degrading a water-soluble, synthetic polymeric film being at least partially covered with a paint material. The method includes placing the film in an extractor apparatus and separating the paint material from the film. The paint material is collected from a water-based solution with a filtration media. The film is degraded in the extractor apparatus.
    Type: Grant
    Filed: November 15, 2010
    Date of Patent: March 26, 2013
    Inventor: Robert Joseph Hanlon, Jr.
  • Patent number: 8399598
    Abstract: The object of this invention is to provide a copolycarbonate that is excellent in heat resistance, thermal stability and moldability and that uses a renewable resource as a raw material. This invention is a copolycarbonate including 50 to 99 mol % of a carbonate constituent unit (1) of the following formula and 50 to 1 mol% of a carbonate constituent unit (2) derived from an aliphatic diol having a boiling point of 180° C. or higher under reduced pressure of 4×10?3 MPa.
    Type: Grant
    Filed: April 16, 2009
    Date of Patent: March 19, 2013
    Assignee: Teijin Limited
    Inventors: Toshiyuki Miyake, Masami Kinoshita
  • Patent number: 8399576
    Abstract: Disclosed is a phosphorous containing phenol novolac resin, having a structure as below: In the above formula, Z is selected from — or —CH2—. Each Y is independently selected from —, —CH2—, —C(CH3)2—, —S—, —SO2—, —O—, —CO—, or —N?N—. Each X is independently selected from a hydrogen or phosphorous containing group, wherein the hydrogen and phosphorous containing group have a molar ratio of 1:0.1 to 0.1:1. Each R1 is independently selected from a hydrogen or C1-5 alkyl group. Each R2 is independently selected from a C1-5 alkyl group. m is an integer of 1 to 10, and n is 0 or 1.
    Type: Grant
    Filed: February 4, 2011
    Date of Patent: March 19, 2013
    Assignee: Grand Tek Advance Material Science Co., Ltd.
    Inventors: Shang-Wei Tang, Hsueh-Tso Lin, Kuan-Ching Chen, Dick Zhong
  • Patent number: 8399607
    Abstract: The present invention generally relates to a pad transfer printing method for making colored hydrogel contact lenses with good image quality. More specifically, the present invention relates to make and use a pad transfer printing pad comprises an addition-cure room temperature vulcanized silicon, which has subjected to post-heat treating. The post-heat treated pad transfer printing pad is characterized by having a reduced silicone residue release by at least 50 percent relative to a control transfer pad having identical composition without post heat treating.
    Type: Grant
    Filed: December 15, 2010
    Date of Patent: March 19, 2013
    Assignee: Novartis AG
    Inventors: Jimmie E. April, Jr., Richard Charles Breitkopf, Robert Carey Tucker
  • Patent number: 8394866
    Abstract: A method for preparing contaminated plastics ground into flakes, such as RPET or such polymers, having at least decontamination and SSP treatment steps, with at least one reactor, with heating to the process temperature taking place essentially outside the reactor. Also, a device for carrying out the method, and having at least one decontamination reactor and at least one SSP reactor, a device for heating plastic flakes to the process temperature being arranged upstream of the decontamination reactor. Also an SSP reactor having at least two individual reactors, and preferably between 3 and 7 individual reactors.
    Type: Grant
    Filed: March 15, 2006
    Date of Patent: March 12, 2013
    Assignee: Krones AG
    Inventors: Thomas Friedlaender, Thomas Rieckmann, Frank Marx
  • Patent number: 8394416
    Abstract: The present invention relates to a novel one step process for preparing cross-linked poly(allylamine) polymers or salts thereof using the novel cross-linking agent of Formula (IV). This invention also relates to the compound of Formula (IV) as well as to a process to obtain it. The cross-linked poly(allylamine) polymers of the invention are useful in medicine as substrate-binding polymers.
    Type: Grant
    Filed: July 16, 2008
    Date of Patent: March 12, 2013
    Assignee: Chemo Ibérica, S.A.
    Inventors: Sabrina Bianchi, Valter Castelvetro, Giovanni Marras, Sonja Bellomi, Graziano Castaldi, Gianpiero Ventimiglia
  • Patent number: 8383764
    Abstract: The invention relates to block polymers, for example, arborescent copolymer compounds, and to methods of making and purifying such compounds. In one embodiment, the invention relates to arborescent polymer compounds that contain one or more styrene polymeric blocks in combination with one or more isobutylene polymeric blocks. In another embodiment, the invention relates to methods for purifying arborescent polymer compounds that contain at least one styrene polymeric block in combination with at least one isobutylene polymeric block.
    Type: Grant
    Filed: May 17, 2007
    Date of Patent: February 26, 2013
    Assignee: The University of Akron
    Inventor: Judit E. Puskas
  • Patent number: 8378063
    Abstract: A process for producing fluoropolymer particles includes preparing a solution/dispersion containing fluoropolymer dissolved/dispersed in a first solvent such that the swelling of fluoropolymer by the first solvent is from 50 to 1,200%, and mixing the solution/dispersion with a second solvent such that fluoropolymer forms particles and the swelling of fluoropolymer by the mixture of the first and second solvents is from 0 to 100%. WC/WB is in the range of from 1 to 5, WB represents mass of the first solvent, WC/ represents mass of the second solvent, WC/WB represents a ratio of the mass of the second solvent to the mass of the first solvent. SBC/SB is at most 0.5. SBC represents the swelling by the mixture of the first and second solvents, SB represents the swelling by the first solvent, and SBC/SB represents a ratio of the swelling by the mixture to the swelling by the first solvent.
    Type: Grant
    Filed: December 22, 2009
    Date of Patent: February 19, 2013
    Assignee: Asahi Glass Company, Limited
    Inventors: Susumu Saito, Tetsuji Shimohira, Takashi Saeki, Junichi Tayanagi
  • Patent number: 8362197
    Abstract: There is provided a method for producing a resin particle capable of unprecedentedly realizing both excellent heat resistant keeping property and melting property. The present invention is a method for producing a resin particle (X) comprising the step of treating a resin particle (B) containing a resin (A) composed of a crystalline part (a) containing, as an essential constitutional component, a polyester (p1) not containing an aromatic ring or a polyester (p2) containing an aromatic ring, and produced by polycondensation of a polyol component and a polycarboxylic acid component, and a noncrystalline part (b), with liquid or supercritical carbon dioxide (C), and removing (C), wherein a heat of fusion measured by differential scanning calorimetry (DSC) of the obtained (X) satisfies the following relational formula (1): 0?H2/H1?0.
    Type: Grant
    Filed: May 20, 2009
    Date of Patent: January 29, 2013
    Assignee: Sanyo Chemical Industries, Ltd.
    Inventors: Yasuhiro Shindo, Sho Kim
  • Patent number: 8362198
    Abstract: There is provided a method for producing a resin particle capable of unprecedentedly realizing both excellent heat resistant keeping property and melting property. The present invention is a method for producing a resin particle (X) comprising the step of treating a resin particle (B) containing a resin (A) composed of a crystalline part (a) containing, as an essential constitutional component, a polyester (p1) not containing an aromatic ring or a polyester (p2) containing an aromatic ring, and produced by polycondensation of a polyol component and a polycarboxylic acid component, and a noncrystalline part (b), with liquid or supercritical carbon dioxide (C), and removing (C), wherein a heat of fusion measured by differential scanning calorimetry (DSC) of the obtained (X) satisfies the following relational formula (1): 0?H2/H1?0.
    Type: Grant
    Filed: February 18, 2011
    Date of Patent: January 29, 2013
    Assignee: Sanyo Chemical Industries, Ltd.
    Inventors: Yasuhiro Shindo, Sho Kim
  • Patent number: 8362200
    Abstract: A process for the salt-free coagulation of polymer dispersions in a rotor/stator assembly is disclosed. The rotor/stator assembly includes a casing, a rotor shaft rotatably mounted within the casing, a rotor having a conical surface affixed to the rotor shaft, and a stator affixed to the casing and concentrically associated with the rotor. The conical surface faces a surface of the stator to form an adjustable shear gap, which is surrounded by an annular space. A polymer dispersion is fed into the assembly and conveyed through the shear gap. During this conveyance, the polymer dispersion is precipitated at a predetermined shear rate and a predetermined shear deformation. The polymer dispersion is discharged from the assembly through an outlet neck, and the assembly is flushed with water using one or more ports formed in at least one of a pipeline coupled to the axial feed neck, the stator, and the casing.
    Type: Grant
    Filed: February 8, 2006
    Date of Patent: January 29, 2013
    Assignee: BASF Aktiengesellschaft
    Inventors: Norbert Güntherberg, Wolfgang Fischer, Manfred Radulla
  • Patent number: 8357773
    Abstract: The disclosure relates to a steam stripping process for producing purified polyimides, e.g., polyetherimide homopolymers and polyetherimide copolymers. The process can include contacting an initial polyimide with steam to remove a volatile species from the initial polyimide to produce a purified polyimide. The purified polyimide can have a weight average molecular weight of from 5,000 to 80,000 Daltons. The weight average molecular weight of the purified polyimide can be greater than or equal to 90% of the weight average molecular weight of the initial polyimide. The purified polyimide can have less than 44 ppm of a volatile species, having a molecular weight of less than 250 Daltons. The polyimide can have less than 10 ppm of a metal cation.
    Type: Grant
    Filed: October 31, 2011
    Date of Patent: January 22, 2013
    Assignee: Sabic Innovative Plastics IP B.V.
    Inventors: Robert R. Gallucci, Robert Hossan, Daniel F. Lowery
  • Patent number: 8357726
    Abstract: A process for devulcanizing crosslinked elastomer particles comprising applying an alternating radio frequency dielectric field to a composition comprising crosslinked elastomer particles. The alternating radio frequency dielectric field preferably has a frequency between 1 and 100 MHz and a voltage between 1000 and 10,000 V.
    Type: Grant
    Filed: January 20, 2010
    Date of Patent: January 22, 2013
    Assignee: Vertex L.L.C.
    Inventor: Michel Marc
  • Patent number: 8354046
    Abstract: Highly ordered Ge films are prepared directly on single crystal Si substrates by applying an aqueous coating solution having Ge-bound polymer onto the substrate and then heating in a hydrogen-containing atmosphere. A coating solution was prepared by mixing water, a germanium compound, ethylenediaminetetraacetic acid, and polyethyleneimine to form a first aqueous solution and then subjecting the first aqueous solution to ultrafiltration.
    Type: Grant
    Filed: September 11, 2009
    Date of Patent: January 15, 2013
    Assignee: Los Alamos National Security, LLC
    Inventors: Quanxi Jia, Anthony K. Burrell, Eve Bauer, Filip Ronning, Thomas Mark McCleskey, Guifu Zou
  • Patent number: 8344035
    Abstract: A process for making a carbonaceous material and a carbonous residue from scrap tires is disclosed. Tires are digested in an oil product. Steel and glass fibers are separated. A product enhancing additive comprising halogen based organic or inorganic compounds is added. The resulting carbonaceous material is then cured to create the final product. The produced carbonous residue is well suited for capture of mercury. The present invention has the benefits of providing a use for scrap tires that would otherwise require disposal in a landfill, and also produces a product useful for capturing a harmful element, thereby providing multiple environmental and economic benefits.
    Type: Grant
    Filed: September 13, 2010
    Date of Patent: January 1, 2013
    Assignee: Senergy LLC
    Inventors: Alfred G. Comolli, David L. Tanner
  • Patent number: 8344190
    Abstract: Process for producing fluorinated olefins from fluorinated materials, the process comprising thermally decomposing the fluoropolymers into fluoroolefins in a reactor having a feeding zone where the fluorinated materials are fed into the reactor and a decomposition zone where the fluorinated materials are thermally decomposed and wherein the thermal decomposition is carried out in the presence of microwave irradiation.
    Type: Grant
    Filed: September 30, 2009
    Date of Patent: January 1, 2013
    Assignee: 3M Innovative Properties Company
    Inventors: Klaus Hintzer, Gunther J. Kaempf, Thomas Kolbeck, Tilman C. Zipplies, Monika A. Willert-Porada, Thorsten Gerdes, Achim Schmidt-Rodenkirchen
  • Patent number: 8338562
    Abstract: The invention relates to a biocompatible, non-biodegradable, and non-toxic polymer of formula (I), comprising of three monomeric units, selected from 1-Vinylpyrrolidone (VP), N-Isopropylacrylamide (NIPAM), and ester of Maleic anhydride and Polyethylene glycol (MPEG), cross-linked with a bi-functional vinyl derivative, of high purity and substantially free of respective toxic monomeric contaminants, and a process for preparation thereof. The invention further relates to nanoparticulate pharmaceutical compositions of poorly water-soluble drugs or compounds comprising the polymer of the invention, which are safe, less-toxic and convenient for bedside administration to patients in need thereof. Furthermore, the invention relates to a highly selective method for preparation of nanoparticulate pharmaceutical compositions of poorly water-soluble drugs or compounds.
    Type: Grant
    Filed: December 26, 2006
    Date of Patent: December 25, 2012
    Assignee: Fresenius Kabi Oncology Limited
    Inventors: Anand C. Burman, Rama Mukherjee, Dhiraj Khattar, Sanjoy Mullick, Manu Jaggi, Manoj Kumar Singh, Mukesh Kumar, Deepak Prusthy, Pawan Kumar Gupta, Rajendran Praveen, Shobhit Singh
  • Patent number: 8334325
    Abstract: The present invention relates to a method for preferentially breaking cross-links in a vulcanised rubber, thereby de-vulcanising the rubber, by the use of a supercritical fluid, such as carbon dioxide. The supercritical fluid maintained at an appropriate solubility parameter, swells the vulcanised rubber to a state of equilibrium swell. The cross links (3) become fully extended and under strain to hold the internal pressures caused by the solvent swelling affect of the supercritical gas. When equilibrium swell has been achieved, the pressure within the processing vessel is rapidly dropped to a level of not less than 60% of the level at which saturation took place, causing a degassing and expansion of the supercritical fluid that has been absorbed within the vulcanised rubber. The resulting three dimensional separation of the rubber molecules will put a further rapid strain on the cross links, causing them to break (7), thereby giving the affect of de-vulcanization.
    Type: Grant
    Filed: August 12, 2008
    Date of Patent: December 18, 2012
    Assignee: Rubber-Regen LLP
    Inventors: Michiel Jan Dees, Philip James Hough
  • Patent number: 8334361
    Abstract: A method of treating oil-based paint waste is provided which includes removing at least a portion of the solvent contained in the paint waste and emulsifying the paint waste to form a paint waste residue. The paint waste residue can be combined with varying amounts of water-based paint waste, emulsifiers, a virgin latex polymer, and a plasticizer to form various roofing products including an elastomeric sealer, a primer, and elastomeric caulk. A bedding cement is also provided which includes water-based paint, sand, and an optional plasticizer. The roofing products may be used in combination to form a strong, water-resistant roofing composite overlay for new or existing roof structures.
    Type: Grant
    Filed: August 31, 2011
    Date of Patent: December 18, 2012
    Assignee: Polymer Recycling, LLC
    Inventor: Michael Joseph Gerace
  • Patent number: 8329856
    Abstract: The present invention relates to a preparation method for a biodegradable polymer microparticle and a microparticle prepared by the method. More particularly, the present invention relates to a method for preparing a polymer microparticle, wherein the method includes the steps of: dissolving a biodegradable polyester-based polymer in DMSO (Dimethyl Sulfoxide); spraying the solution in a low temperature hydrocarbon solution to provide a frozen DMSO microparticle; adding the microparticle in a low temperature salt aqueous solution to dissolve DMSO; and removing salt. The present invention provides a method for preparing a novel polymer microsphere which can be injected through a syringe due to excellent physical properties (such as biocompatibility, biodegradability, porosity, mechanical strength) and the microcarrier's size-adjustability, and can be easily mass-produced.
    Type: Grant
    Filed: June 13, 2011
    Date of Patent: December 11, 2012
    Assignee: Regen Biotech Inc.
    Inventors: Gun Poong Kim, Yong Hoon Lee, Kun Pil Lee
  • Patent number: 8329768
    Abstract: A method and apparatus for separating non-biogenic plastic from biogenic waste. A stream of waste materials is delivered through an inlet into a conduit in which the biogenic waste drops out the bottom. The non-biogenic plastic is drawn upwardly by a separator in the form of pressurized gas fed tangentially through two ports in an opposite direction with each other to create a vacuum in the conduit.
    Type: Grant
    Filed: August 28, 2009
    Date of Patent: December 11, 2012
    Inventors: Kevin P. Furnary, Earl T. Balkum
  • Patent number: 8329858
    Abstract: A method of controlling oil-absorbing properties of a silicone rubber powder characterized by keeping a silicone rubber powder in hot storage at a temperature in the range of 40° C. to 150° C. or in cold storage at a temperature in the range of 0° C. to 10° C.
    Type: Grant
    Filed: December 13, 2010
    Date of Patent: December 11, 2012
    Assignee: Dow Corning Toray Co., Ltd.
    Inventors: Kazuhiko Ando, Junichi Uchiyama
  • Patent number: 8318895
    Abstract: A process is described for recycling superabsorbent polymer fines into a process that includes treating the superabsorbent polymer fines with caustic and a polymerization step for making the superabsorbent polymer gel. The process requires treating the superabsorbent polymer fines with a caustic, followed by mixture with polymerizable monomer solution, and polymerizing the mixture of the superabsorbent polymer fines and monomer to form the aqueous fluid absorbent polymer. In the process, the fines are incorporated into the new polymer gel and become indistinguishable there from. The gel may then be comminuted into a particulate dried and then separated into a portion having a desired minimum particle size in a fines portion having less than the desired size. The particulate may then be coated with a surface crosslinking agent and surface additives and heated for surface conversion.
    Type: Grant
    Filed: August 2, 2012
    Date of Patent: November 27, 2012
    Assignee: Evonik Stockhausen, LLC
    Inventors: Gonglu Tian, Scott J. Smith, Janet Pate-Linton
  • Patent number: 8314206
    Abstract: In one embodiment, a block copolymer-containing composition includes PS-b-PXVP and a lithium salt, where “X” is 2 or 4. All lithium salt is present in the composition at no greater than 1 ppm by weight. In one embodiment, a homogenous block copolymer-including comprising has PS-b-PXVP present in the composition at no less than 99.99998% by weight, where “X” is 2 or 4. Methods of forming such compositions are disclosed.
    Type: Grant
    Filed: December 2, 2008
    Date of Patent: November 20, 2012
    Assignee: Micron Technology, Inc.
    Inventors: Dan Millward, Scott Sills