Coating Composition Applied Forms Oxide Coating Patents (Class 148/284)
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Patent number: 12208446Abstract: There is provided a powder material that is for densifying a molded article manufactured by an additive layer manufacturing method and improving harness of the molded article. There is provided a powder material for use in additive layer manufacturing containing ceramics and metals, in which a tapped filling rate defined by (tapped density/theoretical density)×100% is 40% or more.Type: GrantFiled: November 8, 2019Date of Patent: January 28, 2025Assignee: FUJIMI INCORPORATEDInventors: Junya Yamada, Hiroyuki Ibe, Nobuaki Kato, Yuta Kato, Yoshikazu Sugiyama
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Patent number: 12157029Abstract: According to an embodiment, a process apparatus performs processing on a byproduct generated in a reaction of a raw material including silicon and a halogen element or in a reaction between a raw material including silicon and a raw material including a halogen element. The apparatus includes a process liquid tank, a processing tank, a supplier and an exhauster. A process target member including the byproduct is introduced into the processing tank. The supplier supplies the process liquid from the process liquid tank to the processing tank and performs processing on the byproduct with the supplied process liquid. The exhauster exhausts a gas generated by reaction between the process liquid and the byproduct from the processing tank.Type: GrantFiled: July 9, 2021Date of Patent: December 3, 2024Assignees: KABUSHIKI KAISHA TOSHIBA, Kioxia Corporation, TOHOKU UNIVERSITYInventors: Kenya Uchida, Hiroyuki Fukui, Ikuo Uematsu, Takeaki Iwamoto, Eunsang Kwon
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Patent number: 12148994Abstract: A radiation absorber device configured to protect a user from radiation from a wireless device, which has a housing made from radiation absorbent material, the housing having an opening, a first chamber and a second chamber, and wherein the first and second chambers are in communication with each other, the first chamber being greater than the second chamber, and wherein the first and second chambers are adapted to together receive a wireless device. The radiation absorber device also has a lid adapted to selectively close the opening of the housing and thus enclose the wireless device therein.Type: GrantFiled: October 20, 2023Date of Patent: November 19, 2024Inventor: Tanvi Mitesh Shah
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Patent number: 11933431Abstract: A threaded connection for pipes includes a pin, a box, a shoulder part plating layer, and a non-shoulder part plating layer. The shoulder part plating layer has an outermost layer formed of a high friction coefficient plating layer, and is arranged on a pin side shoulder part and/or a box side shoulder part. The non-shoulder part plating layer has an outermost layer formed of a low friction coefficient plating layer having a coefficient of friction lower than a coefficient of friction of the high friction coefficient plating layer, and the non-shoulder part plating layer is arranged on at least one of a pin side thread part, a pin side metal seal part, a box side thread part, and a box side metal seal part.Type: GrantFiled: February 7, 2020Date of Patent: March 19, 2024Assignees: NIPPON STEEL CORPORATION, VALLOUREC OIL AND GAS FRANCEInventors: Kazuya Ishii, Kunio Goto, Masaaki Sugino, Yousuke Oku
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Patent number: 11901103Abstract: A magnetic body is constituted by grains of a soft magnetic alloy bonded together via an oxide layer, wherein: the soft magnetic alloy is an alloy containing Si by 1 to 5.5 percent by mass, and Cr or Al by 0.2 to 4 percent by mass in total, as constituent elements, with Fe and unavoidable impurities accounting for the remainder; and the oxide layer contains Si, as well as at least one of Cr and Al, where, among Fe, Si, Cr, and Al, Si is contained in the largest quantity based on mass. The magnetic body can have high magnetic permeability.Type: GrantFiled: February 24, 2020Date of Patent: February 13, 2024Assignee: TAIYO YUDEN CO., LTD.Inventors: Yoko Orimo, Shinsuke Takeoka
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Patent number: 11872713Abstract: Razors cartridges including a guard, a cap, and at least two blades with parallel sharpened edges located between the guard and cap are provided. The first blade has a first color and a second blade has a second color, where the first color is different than the second color. The blade color corresponds to an attribute of the blade (e.g., low cut force) that the color is disposed on or an attribute of the razor cartridge (e.g., sensitive skin). The color of the blade corresponds to a target user of the razor cartridge (e.g., male or female). The first blade defines a blade edge near or nearest the guard and a second blade defines a blade edge near or nearest the cap.Type: GrantFiled: July 30, 2020Date of Patent: January 16, 2024Assignee: The Gillette Company LLCInventors: Laura Xu, Kenneth James Skrobis, Neville Sonnenberg, Ronald Richard Duff, Jr., Joseph Allan DePuydt
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Patent number: 11780013Abstract: An optical mount part having a body that includes a composite of a titanium-zirconium-niobium alloy. The titanium-niobium-zirconium alloy includes titanium, about 13.5 to about 14.5 wt. % zirconium, and about 18 to about 19 weight % (wt. %) niobium. The titanium-niobium-zirconium alloy has a congruent melting temperature of about 1750 to about 1800° Celsius (° C.).Type: GrantFiled: July 30, 2020Date of Patent: October 10, 2023Assignee: RAYTHEON COMPANYInventors: Sunder S. Rajan, Keith Carrigan, Kurt S. Ketola
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Patent number: 11636970Abstract: The invention provides a powder magnetic core and a method for manufacturing a powder magnetic core through simple compression molding and capable of manufacturing a complicatedly shaped powder magnetic core with reliable high strength and insulating properties. A method for manufacturing a powder magnetic core with a metallic soft magnetic material powder includes: a first step including mixing a soft magnetic material powder and a binder; a second step including compression molding the mixture obtained after the first step; a third step including performing at least one of grinding and cutting on the compact obtained after the second step; and a fourth step including heat-treating the compact after the third step, wherein in the fourth step, the compact is heat-treated so that an oxide layer containing an element constituting the soft magnetic material powder is formed on the surface of the soft magnetic material powder.Type: GrantFiled: June 4, 2019Date of Patent: April 25, 2023Assignee: PROTERIAL, LTD.Inventors: Kazunori Nishimura, Shin Noguchi, Toshio Mihara
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Patent number: 11512380Abstract: The present invention provides a method for manufacturing more beautiful black coated steel sheets by uniformly blackening the coating layer. Specifically, the present invention provides a method for manufacturing black coated steel sheets, which brings Zn—Al—Mg alloy coated steel sheets (1) into contact with steam in a closed container (10), wherein said closed container (10) can maintain a predefined internal pressure through variable control of the amount of steam flowing into said closed container (10) and/or the amount of steam flowing out of said closed container (10), and in said closed container (10) that can maintain said predefined pressure, said Zn—Al—Mg alloy coated steel sheets (1) have contact with the steam introduced into said closed container (10).Type: GrantFiled: January 17, 2018Date of Patent: November 29, 2022Assignee: NIPPON STEEL NISSHIN CO., LTD.Inventors: Masaki Yamamoto, Tadashi Nakano, Ichiro Takahashi, Hiroyuki Nakamizo, Toshiaki Sato, Yoshinobu Kurisu, Yuuki Sakuraba, Yoshitaka Yukura, Tsutomu Ohta, Shinichi Kajimoto, Noboru Suzuki, Masahiko Tsuchiyama, Yuusuke Murai
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Patent number: 11441219Abstract: Embodiments of the present invention provide a technique for forming a film having a high added value appearance quality and excellent hardness on the surface of a steel sheet in a short time.Type: GrantFiled: June 21, 2019Date of Patent: September 13, 2022Assignee: RESEARCH INSTITUTE OF INDUSTRIAL SCIENCE & TECHNOLOGYInventors: Hye Jeong Kim, Gab Sik Byun, Kyung Hwang Lee, Mi Seon Choi
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Patent number: 11180835Abstract: A steel sheet has a predetermined chemical composition, and a surface exhibits an absorption peak at which a reflectance is not less than 50% nor more than 85% in a range of wave numbers of 1200 cm?1 to 1300 cm?1 by a Fourier transform-infrared spectroscopy analysis by a reflection absorption spectrometry method, and does not exhibit an absorption peak in a range of wave numbers of 1000 cm?1 to 1100 cm?1, or exhibits an absorption peak at which a reflectance is 85% or more in the range of wave numbers of 1000 cm?1 to 1100 cm?1, wherein Ni of 3 mg/m2 to 100 mg/m2 adheres to the surface.Type: GrantFiled: September 25, 2015Date of Patent: November 23, 2021Assignee: NIPPON STEEL CORPORATIONInventors: Kohei Ueda, Hiroyuki Kawata, Takayuki Kitazawa, Takeshi Yasui, Hiroyuki Ban
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Patent number: 10684265Abstract: A method for measuring volatile organic compounds includes loading glass containers into an oven, heating the oven, purging the oven with dry clean air, collecting a volumetric portion of an oven exhaust, trapping volatile organic compounds from the volumetric portion, and measuring the volatile organic compounds trapped in the trap. The one or more glass containers are in-tact while measuring the VOCs of the coated glass container. An apparatus includes an oven having an interior volume that is capable of holding one or more in-tact glass containers, a flow meter fluidly connected to the first trap, and a pump fluidly connected to the flow meter. The first trap collects volatile organic compounds from a volumetric portion of the oven exhaust gas. The pump controls a flow rate of the volumetric portion of the oven exhaust gas across the first trap.Type: GrantFiled: September 1, 2017Date of Patent: June 16, 2020Assignee: CORNING INCORPORATEDInventors: Robert Scott Burkhalter, Andrei Gennadyevich Fadeev, John Stephen Peanasky, David Charles Sauer
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Patent number: 10629370Abstract: The method including: applying a graphite-based lubricant to a cavity surface of a die; forming a first graphite-based powder layer by disposing graphite-based powder that does not contain a binder on a cavity surface of a lower punch, forming a magnet powder body by putting magnet powder on the first graphite-based powder layer, and forming a second graphite-based powder layer by disposing graphite-based powder that does not contain a binder on the magnet powder body; and producing a compact by performing press forming using the lower punch and a upper punch while heating the magnet powder body surrounded by the graphite-based lubricant applied to the cavity surface of the die, the first graphite-based powder layer, and the second graphite-based powder layer, and releasing the compact from a forming die.Type: GrantFiled: July 5, 2016Date of Patent: April 21, 2020Assignee: TOYOTA JIDOSHA KABUSHIKI KAISHAInventors: Tomonori Inuzuka, Akira Kano
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Patent number: 10458305Abstract: A base for supporting a catalyst for exhaust gas purification, the base including a honeycomb structure obtained by superposing a metallic flat foil and a metallic wavy foil, characterized in that the wavy foil has offset portions where any adjoining two of the wave phases arranged in the axial direction of the honeycomb structure are offset from each other. The base is further characterized in that an oxide coating film has been formed in a given range of these offset portions which includes exposed edge surfaces that are exposed on the gas-inlet side, that the oxide coating film includes 30-99.9 mass % first alumina, with the remainder comprising at least one of second aluminas, Fe oxides, and Cr oxides, that the first alumina comprises ?-alumina, that the second aluminas comprise one or more of ?-, ?-, ?-, ?-, ?-, and ?-aluminas.Type: GrantFiled: October 4, 2016Date of Patent: October 29, 2019Assignee: NIPPON STEEL CHEMICAL & MATERIAL CO., LTD.Inventors: Tooru Inaguma, Shinji Kawasoe, Yasuhiro Tsumura, Shogo Konya, Masayuki Kasuya, Masafumi Omizu
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Patent number: 10378412Abstract: A metal substrate for catalytic converter for purifying an exhaust gas includes a honeycomb core with metal flat foil and corrugated foil stacked in layers, and an oxide film having a thickness of 0.1 ?m or more and 10 ?m or less is formed in a predetermined range including an exposed end surface exposed toward the gas inlet side. The oxide film contains at least a first alumina including ?-alumina and a Fe oxide. The ?-alumina contains ?-alumina with solid-solved Fe and ?-alumina with no solid-solved Fe. In the oxide film, the content of the first alumina is 30% by mass or more and 99.5% by mass or less, the content of the Fe oxide is 0.5% by mass or more and 40% by mass or less, and the content of Fe is more than 7% by mass and 35% by mass or less.Type: GrantFiled: October 11, 2017Date of Patent: August 13, 2019Assignee: NIPPON STEEL CHEMICAL & MATERIAL CO., LTD.Inventors: Tooru Inaguma, Shinji Kawasoe, Yasuhiro Tsumura, Shogo Konya, Masayuki Kasuya, Takuzo Kako, Masafumi Omizu
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Patent number: 10014431Abstract: Disclosed is a thin film solar cell including a substrate, a first electrode, a light absorbing layer, a buffer layer, a window layer, and a second electrode, wherein a compound layer of MxSy or MxSey (here, M is metal, and x and y each are a natural number) is present in an interface between the first electrode and the light absorbing layer, the thickness of the compound layer of MxSy or MxSey being 150 nm or less.Type: GrantFiled: April 27, 2016Date of Patent: July 3, 2018Assignee: Daegu Gyeongbuk Institute of Science and TechnologyInventors: Kee Jeong Yang, Bo Ram Jeon, Jun Hyoung Sim, Dae Ho Son, Jin Kyu Kang
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Patent number: 9976196Abstract: Hot-stamped steel includes: a steel base metal including a tempered portion having hardness corresponding to 85% or less of the highest quenching hardness defined as a Vickers hardness at a depth position spaced away from a surface layer by ¼ times a sheet thickness in a case of performing water quenching after heating at a temperature equal to or higher than an Ac3 point and retention for 30 minutes; and a Zn coating layer formed on the tempered portion of the base metal. The Zn coating layer includes a solid-solution layer including a solid-solution phase containing Fe and Zn that is solid-soluted in Fe, and a lamella layer including solid-solution phase and a capital gamma phase. In the Zn coating layer, an area ratio of the lamella layer is 30 to 100% and an area ratio of the solid-solution layer is 0 to 70%.Type: GrantFiled: March 31, 2015Date of Patent: May 22, 2018Assignee: NIPPON STEEL & SUMITOMO METAL CORPORATIONInventors: Akihiro Sengoku, Hiroshi Takebayashi
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Patent number: 9932652Abstract: Hot-stamped steel includes: a base metal that is steel including a tempered portion having hardness corresponding to 85% or less of the highest quenching hardness, the highest quenching hardness being defined as a Vickers hardness at a depth position spaced away from a surface by ¼ times a sheet thickness in a case of performing water quenching after heating at a temperature equal to or higher than an Ac3 point and retention for 30 minutes; and a Zn coating layer that is formed on the tempered portion of the base metal. The Zn coating layer includes a solid-solution layer including a solid-solution phase that contains Fe and Zn that is solid-soluted in Fe, and a lamella layer that includes the solid-solution phase and a capital gamma phase. An area ratio of the lamella layer in the Zn coating layer is 20% or less.Type: GrantFiled: March 31, 2015Date of Patent: April 3, 2018Assignee: NIPPON STEEL & SUMITOMO METAL CORPORATIONInventors: Akihiro Sengoku, Hiroshi Takebayashi
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Patent number: 9905580Abstract: The present disclosure relates to the field of display technology and provides a method for manufacturing a TFT, the TFT, an array substrate including the TFT, and a display device. The method includes steps of forming a pattern of a gate electrode on 5 a base substrate, forming a gate insulation layer on the base substrate, and forming patterns of a source electrode and a drain electrode arranged above the gate insulation layer. The method further includes forming an antioxidation metal protection layer on a surface or surfaces of the gate electrode, the source electrode and/or the drain electrode.Type: GrantFiled: July 20, 2015Date of Patent: February 27, 2018Assignee: BOE TECHNOLOGY GROUP CO., LTD.Inventors: Ce Ning, Mingchao Li, Fangzhen Zhang
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Patent number: 9850563Abstract: Producing a Ni superalloy component in which the superalloy has a ? phase matrix containing intermetallic ?? precipitates. Providing a Ni superalloy casting of the component; solutioning the component by heat treating the casting under vacuum and/or in an inert atmosphere at a temperature above the ?? solvus to homogenize the ? phase; quenching and ageing the solutioned component to grow intermetallic ?? precipitates in the homogenized ? phase. Before the solutioning step: heat treating the casting to produce a thermally grown oxide on the surface, oxide adherent to supress volatilization of Ni from the surface of the casting during the solutioning heat treatment. Performing the solutioning step under a Ni vapor pressure which is sufficient to supress volatilization of Ni from the surface of the casting during the solutioning heat treatment. During the solutioning heat treatment the component is encapsulated in a container protecting the casting from Si-doped contaminants.Type: GrantFiled: February 5, 2015Date of Patent: December 26, 2017Assignee: ROLLS-ROYCE plcInventors: Neil John D'Souza, Kevin Goodwin, Martin Richard Perry
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Patent number: 9040168Abstract: The galvannealed steel sheet includes: a galvannealed layer formed on at least one surface of a steel sheet and contains includes an amount of 0.05 mass % to 0.5 mass % of Al, an amount of 6 mass % of 12 mass % of Fe, and the balance composed of Zn and inevitable impurities; and a mixed layer formed on a surface of the galvannealed layer and includes a composite oxide of Mn, Zn, and P and an aqueous P compound, wherein the composite oxide includes 0.1 mg/m2 to 100 mg/m2 of Mn, an amount of 1 mg/m2 to 100 mg/m2 of P, and Zn, and a P/Mn ratio is 0.3 to 50, and wherein the total size of an area of the mixed layer in which an attached amount of P is equal to or more than 20 mg/m2 is 20% to 80% of a surface area of the mixed layer.Type: GrantFiled: July 12, 2010Date of Patent: May 26, 2015Assignee: NIPPON STEEL & SUMITOMO METAL CORPORATIONInventors: Kazuhiko Honda, Noriyuki Suzuki, Yoichi Ikematsu
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Patent number: 9028667Abstract: A metal material is contacted with a treatment solution containing zirconium and/or titanium compound, and a polyamine compound having a number average molecular weight from 150 to 500,000 and containing from 0.1 mmol to 17 mmol of primary and/or secondary amino group per 1 g of solid content and at least one siloxane unit. Concentration of zirconium and/or titanium compound in the metal surface treatment composition is from 10 ppm to 10,000 ppm with respect to the metal element, and mass ratio of the zirconium and/or titanium element is from 0.1 to 100 with respect to the polyamine compound. The metal material is washed with water after contacted by the treatment solution.Type: GrantFiled: September 13, 2012Date of Patent: May 12, 2015Assignees: Nippon Paint Co., Ltd., Chemetall GmbHInventors: Toshio Inbe, Thomas Kolberg
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Publication number: 20150107722Abstract: The present invention pertains to a method for producing a black-plated steel sheet capable of being blackened in a short amount of time, and exhibiting an excellent ability to maintain a black appearance after processing. As an original sheet, the sheet used is a Zn-plating steel sheet which contains molten Al and Mg and has a Zn-plating layer containing molten Al and Mg, containing Al in the amount of 0.1-22.0 mass %, inclusive, and containing Mg in the amount of 0.1-1.5 mass %, inclusive. The plating layer is blackened by causing the molten-plating steel sheet to contact water vapor inside a tightly sealed container. When doing so, the concentration of oxygen inside the tightly sealed container is 13% or less.Type: ApplicationFiled: April 23, 2013Publication date: April 23, 2015Applicant: NISSHIN STEEL CO., LTDInventors: Tadashi Nakano, Masaya Yamamoto, Hirofumi Taketsu
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Patent number: 8992696Abstract: A method of bonding a metal to a substrate involves forming a plurality of nano-features in a surface of the substrate, where each nano-feature is chosen from a nano-pore and/or a nano-crevice. In a molten state, the metal is over-cast onto the substrate surface, and penetrates the nano-features. Upon cooling, the metal is solidified inside the nano-features, where the solidification of the metal forms a mechanical interlock between the over-cast metal and the substrate.Type: GrantFiled: December 2, 2011Date of Patent: March 31, 2015Assignee: GM Global Technology Operations LLCInventors: Michael J. Walker, Bob R. Powell, Jr., Aihua A. Luo
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Publication number: 20150083276Abstract: The present invention pertains to a method for producing a black-plated steel sheet capable of being blackened in a short amount of time, and exhibiting an excellent ability to maintain a black appearance after processing. As an original sheet, the sheet used is a Zn-plating steel sheet which contains molten Al and Mg and has a Zn-plating layer containing molten Al and Mg, containing Al in the amount of 1.0-22.0 mass %, inclusive, and containing Mg in the amount of 1.5-10.0 mass %, inclusive. The plating layer is blackened by causing the molten-plating steel sheet to contact water vapor inside a tightly sealed container. When doing so, the concentration of oxygen inside the tightly sealed container is 13% or less.Type: ApplicationFiled: April 23, 2013Publication date: March 26, 2015Inventors: Tadashi Nakano, Masaya Yamamoto, Hirofumi Taketsu
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Publication number: 20150030875Abstract: The present invention relates to a Zn—Mg alloy-coated steel sheet with excellent blackening resistance and excellent coating adhesion and to a method for manufacturing same. Provided are a Zn—Mg alloy-coated steel sheet with excellent blackening resistance and excellent adhesion and a method for manufacturing same, the steel sheet comprising: a substrate steel sheet; a Zn—Fe intermetallic compound layer formed on the substrate steel sheet; a first Zn—Mg coating layer formed on the Zn—Fe intermetallic compound layer and comprising a Zn—Fe intermetallic compound in which the content of Zn is 95% by weight or higher; a second Zn—Mg coating layer formed on the first Zn—Mg coating layer and comprising a Zn—Mg intermetallic compound in which the content of Zn is 80 to 95% by weight; and an oxide film formed on the second Zn—Mg coating layer and comprising a metallic oxide.Type: ApplicationFiled: December 27, 2012Publication date: January 29, 2015Inventors: Dong-Yoeul Lee, Kyung-Hoon Nam, yong-Hwa Jung, Seok-Jun Hong, Tae-Yeob Kim, Young-Jin Kwak, Mun-Jong Eom, Woo-Sung Jung
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Patent number: 8906170Abstract: An alloy casting having a protective layer disposed on a surface of the casting is provided. The protective layer is resistant to liquid metal attack, and wherein the protective layer includes an oxide of an element present in the alloy. A method of forming a protective layer on a surface of the alloy casting is also provided. The method includes disposing the alloy in a mold, and oxidizing an element of the alloy to form a protective layer on the surface of the casting.Type: GrantFiled: June 24, 2008Date of Patent: December 9, 2014Assignee: General Electric CompanyInventors: Michael Frances Xavier Gigliotti, Jr., Stephen Francis Rutkowski, Shyh-Chin Huang, Roger John Petterson, Luana Emiliana Iorio, Andrew John Elliott
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Patent number: 8894777Abstract: A surface treatment method of a magnesium alloy article includes, instead of forming a primer on a magnesium alloy based composite first, directly performing a hairline finish process on the magnesium alloy based composite, to form a hairline structure on a surface of the magnesium alloy based composite, and performing a chemical oxidation process on the magnesium alloy based composite, to form a glossy film covering the hairline structure on the magnesium alloy based composite, thereby forming a magnesium alloy article structure. Alternatively, another chemical oxidation process is performed before the hairline finish process, to form an oxide film on the surface of the magnesium alloy based composite.Type: GrantFiled: September 25, 2011Date of Patent: November 25, 2014Assignee: Getac Technology CorporationInventor: Chun-Hsiang Chen
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Patent number: 8852359Abstract: A method of bonding a metal to a substrate involves forming an oxide layer on a surface of the substrate, and in a molten state, over-casting the metal on the substrate surface. The over-casting drives a reaction at an interface between the over-cast metal and the oxide layer to form another oxide. The other oxide binds the metal to the substrate surface upon solidification of the over-cast metal.Type: GrantFiled: December 2, 2011Date of Patent: October 7, 2014Assignee: GM Global Technology Operations LLCInventors: Michael J. Walker, Anil K. Sachdev, Bob R. Powell, Jr., Aihua A. Luo
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Publication number: 20140296077Abstract: A method, system, and apparatus for fabricating a high-strength Superconducting cable comprises pre-oxidizing at least one high-strength alloy wire, coating at least one Superconducting wire with a protective layer, and winding the high-strength alloy wire and the Superconducting wire to form a high-strength Superconducting cable.Type: ApplicationFiled: April 2, 2013Publication date: October 2, 2014Inventor: Tengming Shen
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Publication number: 20140295194Abstract: There is provided a heat resistant ferritic steel including a base material including, by mass percent, C: 0.01 to 0.3%, Si: 0.01 to 2%, Mn: 0.01 to 2%, P: at most 0.10%, S: at most 0.03%, Cr: 7.5 to 14.0%, sol.Al: at most 0.3%, and N: 0.005 to 0.15%, the balance being Fe and impurities, and an oxide film that is formed on the base material and contains 25 to 97% of Fe and 3 to 75% of Cr. This heat resistant ferritic steel is excellent in photoselective absorptivity and oxidation resistance.Type: ApplicationFiled: November 21, 2012Publication date: October 2, 2014Applicant: NIPPON STEEL & SUMITOMO METAL CORPORATIONInventors: Yoshitaka Nishiyama, Hiroshi Matsuo, Shunichi Otsuka
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Publication number: 20140261897Abstract: Embodiments of the present invention relate generally to methods of treating metal surfaces to enhance adhesion or binding to substrates, and devices formed thereby. In some embodiments of the present invention, methods of achieving improved bonding strength without roughening the topography of a metal surface are provided. The metal surface obtained by this method provides strong bonding to resin layers. The bonding interface between the treated metal and the resin layer exhibits resistance to heat, moisture, and chemicals involved in post-lamination process steps, and therefore can suitably be used in the production of PCB's. Methods according to some embodiments of the present invention are especially useful in the fabrication of high density multilayer PCB's, in particular for PCB's having circuits with line/spacing of equal to and less than 10 microns.Type: ApplicationFiled: July 6, 2010Publication date: September 18, 2014Applicant: Atotech Deutschland GmbHInventors: Jen-Chieh Wei, Zhiming Liu, Steven Z. Shi, Werner G. Kuhr
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Patent number: 8834651Abstract: A method using a continuous annealing furnace where a cooling method of a cooling zone including part or all of the temperature range of the steel sheet of 600 to 250° C. following the heating for recrystallization is one or more of gas cooling, effusion cooling, and cooling pipe cooling, or a joint cold rolled steel sheet/hot dip galvanized steel sheet facility having such a continuous annealing furnace, to continuously anneal cold rolled steel sheet to produce high strength cold rolled steel sheet, characterized by exposing the steel sheet surface to an iron-oxidizing atmosphere in the steel sheet temperature range to make the surface oxidize, pickling the sheet at the outlet side of the annealing furnace, then iron- or Ni-plating the sheet to 1 to 50 mg/m2.Type: GrantFiled: January 9, 2008Date of Patent: September 16, 2014Assignee: Nippon Steel & Sumitomo Metal CorporationInventors: Kenichiro Matsumura, Kohji Yanaba, Yuuki Yasuda
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Publication number: 20140251502Abstract: Embodiments of the present invention relate generally to methods of treating metal surfaces to enhance adhesion or binding to substrates, and devices formed thereby. In some embodiments of the present invention, methods of achieving improved bonding strength without roughening the topography of a metal surface are provided. The metal surface obtained by this method provides strong bonding to resin layers. The bonding interface between the treated metal and the resin layer exhibits resistance to heat, moisture, and chemicals involved in post-lamination process steps, and therefore can suitably be used in the production of PCB's. Methods according to some embodiments of the present invention are especially useful in the fabrication of high density multilayer PCB's, in particular for PCB's having circuits with line/spacing of equal to and less than 10 microns.Type: ApplicationFiled: May 16, 2014Publication date: September 11, 2014Applicant: Atotech Deutschland GmbHInventors: Jen-Chieh Wei, Zhiming Liu, Steven Z. Shi, Werner G. Kuhr
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Patent number: 8828151Abstract: Disclosed is an easily handleable composition for metal surface treatment which enables to achieve foundation surface concealment, coating adhesion and corrosion resistance equal to or higher than those obtained by the conventional metal surface treatment compositions. This composition for metal surface treatment places no burden on the environment. Also disclosed are a method for treating the surface of a metal material wherein such a composition for metal surface treatment is used, and a metal material treated by such a metal surface treatment method. Specifically disclosed is a metal surface treatment composition used for a treatment of a metal surface, which composition contains a zirconium compound and/or titanium compound substantially not containing fluorine, and an inorganic acid and/or a salt thereof. This metal surface treatment composition has a pH of not less than 1.5 but not more than 6.5.Type: GrantFiled: May 24, 2012Date of Patent: September 9, 2014Assignee: Chemetall GmbHInventors: Toshio Inbe, Thomas Kolberg
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Patent number: 8771439Abstract: The invention is directed to a method for producing a titanium aluminide intermetallic alloy composition having an improved wear resistance, the method comprising heating a titanium aluminide intermetallic alloy material in an oxygen-containing environment at a temperature and for a time sufficient to produce a top oxide layer and underlying oxygen-diffused layer, followed by removal of the top oxide layer such that the oxygen-diffused layer is exposed. The invention is also directed to the resulting oxygen-diffused titanium aluminide intermetallic alloy, as well as mechanical components or devices containing the improved alloy composition.Type: GrantFiled: April 1, 2009Date of Patent: July 8, 2014Assignee: UT-Battelle, LLCInventors: Jun Qu, Hua-Tay Lin, Peter J. Blau, Vinod K. Sikka
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Publication number: 20140150997Abstract: A heat pipe processing method includes steps of providing a metal tube with openings at two ends, where an inner wall of the metal tube has a capillary structure surface; and oxidizing the capillary structure surface so as to form an oxidized structure surface. In another embodiment, a heat pipe includes is provided, including a metal tube, a working fluid, and a first oxidized structure. An inner wall of the metal tube has a first area. The working fluid is filled in the metal tube. The first oxidized structure is formed on the inner wall defined by the first area, and the working fluid has a first contact angle on the first oxidized structure.Type: ApplicationFiled: July 19, 2013Publication date: June 5, 2014Inventors: Cheng-We TU, Kuo-Hsiang Chien, Ming-Shan Jeng
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Patent number: 8741075Abstract: A method of producing a hot press-formed member having good corrosion resistance comprises subjecting a zinc-based plated steel sheet to heat treatment by heating to a temperature region of 600-750° C. at a rate of temperature increase up to 600° C. of at most 50° C. per second followed by cooling to 550° C. or below to form a steel blank which has a zinc oxide layer in its uppermost surface portion and below it a zinc-iron alloy phase having an Fe content of at least 25 mass %. This steel blank is heated to a temperature of at least its Ac3 point, then press formed immediately at a temperature of at least its Ac3 point, and then rapidly cooled. The hot press-formed member has a surface region with zinc oxide and iron-zinc solid solution phases and not containing an intermetallic compound phase or a pure zinc phase.Type: GrantFiled: June 26, 2012Date of Patent: June 3, 2014Assignees: Nippon Steel & Sumitomo Metal Corporation, Toyoda Iron Works Co., Ltd.Inventors: Kazuhito Imai, Masanobu Ichikawa
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Patent number: 8734603Abstract: The invention relates to a method for producing a friction element (3) comprising the steps: providing a metal main body (10), hardening the main body (10) on at least part of its surface (11, 12) in a salt bath, wherein the salt bath hardening is the final method step, and no further processing of the hardened surface (11, 12) is performed. Furthermore, the invention relates to a friction element produced according to this method and a friction component comprising the latter.Type: GrantFiled: December 1, 2011Date of Patent: May 27, 2014Assignee: Miba Frictec GmbHInventors: Zisis Tsioptsias, Gerhard Hartner
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Patent number: 8728252Abstract: A process for treating a non-ferrous metal component, comprising placing the component into a process chamber at an elevated temperature, biasing the component to have a potential capable of attracting ions, introducing oxygen into the chamber at a pressure such that a glow discharge comprising oxygen ions is generated, the process chamber additionally comprising a glow discharge ionization enhancing means, and activating the glow discharge ionization enhancing means thereby increasing charged species density of the glow discharge, the oxygen ions flowing towards the component and colliding the surface thereof at least some of which diffuse into the component.Type: GrantFiled: March 24, 2008Date of Patent: May 20, 2014Assignees: Tecvac Limited, The University of SheffieldInventors: Junia Cristina Avelar Batista Wilson, Elliott Ashley Fielding Spain, Jonathan Housden, Allan Matthews, Adrian Leyland
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Patent number: 8652272Abstract: A bath containing nickel ions and formic acid is injected into a film-forming aqueous solution flowing in a circulation pipe connected to a feed water pipe made of carbon steel in a BWR plant. This solution is supplied into the pipe through the circulation pipe, and a nickel metal film is formed on an inner surface of the pipe. After the film is formed, a film-forming aqueous solution containing iron (II) ions, formic acid, nickel ions, hydrogen peroxide, and hydrazine is supplied to the pipe. A nickel ferrite film is formed on the surface of the nickel metal film in the pipe. The nickel ferrite film comes into contact with water containing dissolved oxygen at or above 150° C. to transform the nickel metal film into a nickel ferrite film. A thick nickel ferrite film is formed on the inner surface of the feed water pipe.Type: GrantFiled: January 22, 2013Date of Patent: February 18, 2014Assignee: Hitachi-GE Nuclear Energy, Ltd.Inventors: Tsuyoshi Ito, Hideyuki Hosokawa, Yukio Hirama, Motoaki Sakashita, Makoto Nagase
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Patent number: 8652271Abstract: A bath containing nickel ions and formic acid is injected into a film-forming aqueous solution flowing in a circulation pipe connected to feed water pipe made of carbon steel in a BWR plant. This film-forming aqueous solution is supplied into the feed water pipe through the circulation pipe, and then, a nickel metal film is formed on an inner surface of the feed water pipe. After the nickel metal film is formed, a film-forming aqueous solution containing iron (II) ions, formic acid, nickel ions, hydrogen peroxide, and hydrazine is supplied to the feed water pipe. A nickel ferrite film is formed on the surface of the nickel metal film in the feed water pipe. Then, the nickel ferrite film is come into contact with water containing dissolved-oxygen at 150° C. or above to transform the nickel metal film into a nickel ferrite film. A thick nickel ferrite film is formed on the inner surface of the feed water pipe. Corrosion of the carbon steel member composing the plant can further reduce.Type: GrantFiled: August 3, 2010Date of Patent: February 18, 2014Assignee: Hitachi-GE Nuclear Energy, Ltd.Inventors: Tsuyoshi Ito, Hideyuki Hosokawa, Yukio Hirama, Motoaki Sakashita, Makoto Nagase
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Publication number: 20140027021Abstract: A method for manufacturing a conductive film roll includes the following steps: (a) preparing a first roll by rolling up a film substrate; (b) laminating a first transparent conductor layer on a first surface of the film substrate while rewinding the film substrate from the first roll; (c) forming a metal layer on the first transparent conductor layer; (d) forming a metal oxide layer on a surface of the metal layer; (e) forming a second transparent conductor layer on a second surface of the film substrate; (f) forming a second metal layer on the second transparent conductor layer; and (g) rolling up the film substrate where all film formation steps have been completed in the form of a roll, in which an entire process of the aforementioned steps is continuously performed in a film formation apparatus.Type: ApplicationFiled: July 19, 2013Publication date: January 30, 2014Inventors: Nozomi Fujino, Hiroyuki Takao, Kuniaki Ishibashi
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Patent number: 8623153Abstract: The present application discloses a method for producing a stable ultra thin metal film that comprises the following steps: a) deposition, on a substrate, of an ultra thin metal film, such as an ultra thin film of nickel, chromium, aluminum, or titanium; b) thermal treatment of the ultra thin metal film, optionally in combination with an O2 treatment; and c) obtaining a protective oxide layer on top of the ultra thin metal film.Type: GrantFiled: June 10, 2009Date of Patent: January 7, 2014Assignee: Fundacio Institut de Ciencies FotoniquesInventors: Valerio Pruneri, Luis Martinez Montblanch, Stefano Giurgola, Paolo Vergani
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Publication number: 20130340894Abstract: The present technology provides an illustrative method for preparing shaped nanoparticles. The method includes passing a metal vapor to a shaping apparatus and condensing the metal vapor within the shaping apparatus to form selectively-shaped metal nanoparticles. The method may also include forming the metal vapor by heating a bulk metal. In an embodiment, the shaping apparatus comprises a mesh separator that include a plurality of nano-sized, square-shaped pores or a plurality of shaping cups that includes a plurality of recesses.Type: ApplicationFiled: March 7, 2013Publication date: December 26, 2013Applicant: Empire Technology Development LLCInventor: David Max ROUNDHILL
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Publication number: 20130329849Abstract: A nuclear-fuel pin including a linear element made of a metal nuclear-fuel material consisting of uranium and/or plutonium, and cladding including Fe and Cr or an alloy including at least both of said elements, comprises a main shell provided around the linear nuclear-fuel element, said shell including threads or fibers made of SiC. A method for producing a nuclear-fuel pin is also provided.Type: ApplicationFiled: October 4, 2011Publication date: December 12, 2013Applicant: Commissariat a L'Energie Atomique et aux Energies AlternativesInventor: Fabrice Mazaudier
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Patent number: 8574396Abstract: A method for adhesively bonding a metallic substrate and a component together includes treating the metallic substrate to form an oxide layer thereon, treating the oxide layer with a conversion coating solution to form a bond promoter coating on the oxide layer, and depositing an adhesive material on the bond promoter coating to bond the component and the metallic substrate together.Type: GrantFiled: August 30, 2010Date of Patent: November 5, 2013Assignee: United Technologies CorporationInventors: Promila P. Bhaatia, Joseph Parkos
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Patent number: 8562751Abstract: A dry cleaning method of a substrate processing apparatus includes forming a metal oxide by oxidizing a metal film adhered to the inside of a processing chamber of the substrate processing apparatus; forming a complex by reacting the metal oxide with ?-diketone; and sublimating the complex to be removed. A cleaning gas containing oxygen and ?-diketone is supplied into the processing chamber while heating the inside of the processing chamber. A flow rate ratio of oxygen to ?-diketone in the cleaning gas is set such that a formation rate of the metal oxide is lower than a formation rate of the complex.Type: GrantFiled: January 17, 2012Date of Patent: October 22, 2013Assignees: Tokyo Electron Limited, Central Glass Company, LimitedInventors: Isao Gunji, Yusaku Izawa, Hitoshi Itoh, Tomonori Umezaki, Yuta Takeda, Isamu Mori
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Publication number: 20130266892Abstract: A method of reducing the formation of electrically resistive scale on a an article comprising a silicon-containing ferritic stainless subjected to oxidizing conditions in service includes, prior to placing the article in service, subjecting the article to conditions under which silica, which includes silicon derived from the steel, forms on a surface of the steel. Optionally, at least a portion of the silica is removed from the surface to placing the article in service. A ferritic stainless steel alloy having a reduced tendency to form silica on at least a surface thereof also is provided. The steel includes a near-surface region that has been depleted of silicon relative to a remainder of the steel.Type: ApplicationFiled: April 30, 2013Publication date: October 10, 2013Applicant: ATI PROPERTIES, INC.Inventor: James M. Rakowski
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Publication number: 20130257639Abstract: A radiowave absorber of an embodiment includes: core-shell particles each including: a core portion that contains at least one magnetic metal element selected from a first group including Fe, Co, and Ni, and at least one metal element selected from a second group including Mg, Al, Si, Ca, Zr, Ti, Hf, Zn, Mn, rare-earth elements, Ba, and Sr; and a shell layer that coats at least part of the core portion, and includes an oxide layer containing at least one metal element selected from the second group and contained in the core portion; and a binding layer that binds the core-shell particles, and has a higher resistance than the resistance of the core-shell particles. The volume filling rate of the core-shell particles in the radiowave absorber is not lower than 10% and not higher than 55%.Type: ApplicationFiled: November 20, 2012Publication date: October 3, 2013Inventors: Toshihide Takahashi, Tomohiro Suetsuna, Koichi Harada, Seiichi Suenaga