Electron Microscope Type Patents (Class 250/311)
  • Publication number: 20130099115
    Abstract: A variant of the Foucault (knife-edge) aperture is disclosed that is designed to provide single-sideband (SSB) contrast at low spatial frequencies but retain conventional double-sideband (DSB) contrast at high spatial frequencies in transmission electron microscopy. The aperture includes a plate with an inner open area, a support extending from the plate at an edge of the open area, a half-circle feature mounted on the support and located at the center of the aperture open area. The radius of the half-circle portion of reciprocal space that is blocked by the aperture can be varied to suit the needs of electron microscopy investigation. The aperture is fabricated from conductive material which is preferably non-oxidizing, such as gold, for example.
    Type: Application
    Filed: December 7, 2012
    Publication date: April 25, 2013
    Applicant: The Regents of the University of California
    Inventor: The Regents of the University of California
  • Patent number: 8426811
    Abstract: An electron microscope according to the present invention includes a phase plate (510) having a thickness which changes in a radial direction, and adjusts a phase difference caused by a difference in electron beam path due to an effect of a spherical aberration when an electron beam is converged by a lens or an image of the electron beam is formed. Accordingly, the phase difference caused by the difference in electron beam path is adjusted, to thereby improve the coherence, so that a phase contrast image of transmitted electrons can be obtained at a higher resolution.
    Type: Grant
    Filed: July 10, 2009
    Date of Patent: April 23, 2013
    Assignee: Hitachi High-Technologies Corporation
    Inventors: Isao Nagaoki, Toshiaki Tanigaki
  • Patent number: 8426812
    Abstract: A method of operating a charged-particle microscope, the method comprising: recording a first image of a first region of an object in a first setting; recording a second image of a second region of the object using the charged-particle microscope in a second setting; reading a third image of a third region using the charged-particle microscope, wherein the first and second regions are contained at least partially within the third region; displaying a representation of the first image at least partly within the displayed third image, wherein the representation of the first image includes a first indicator which is indicative of the first setting; displaying a representation of the second image at least partly within the displayed third image, wherein the representation of the second image includes a second indicator which is indicative of the second setting, and wherein the displayed second indicator is different from the displayed first indicator.
    Type: Grant
    Filed: November 2, 2011
    Date of Patent: April 23, 2013
    Assignee: Carl Zeiss Microscopy Ltd.
    Inventors: Stewart Bean, Roger Rowland, Simon Hees
  • Patent number: 8426810
    Abstract: A method of planar imaging on semiconductor chips using focused ion beam includes the initial step of disposing at least a positioning symbol to designate a testing area. A metal membrane is positioned on the testing area. The testing chip is trimmed to form a first testing chip. A blind opening is cut proximate to the testing area on the first testing chip forms a second testing chip. The second testing chip is mounted on an inclinable platform. The mounted second testing chip is rotated with the inclinable platform. Ion beams are emitted into the opening at an angle of inclination. Ion beams are emitted in the direction of the incident ray to form planar images of different depths parallel to the metal membrane on the testing area.
    Type: Grant
    Filed: January 12, 2012
    Date of Patent: April 23, 2013
    Assignee: Inotera Memories, Inc.
    Inventors: Bi-Jen Chen, Pei-Yi Chen, Chiu Chu Liu
  • Publication number: 20130092836
    Abstract: A transmission electron microscope comprises a high-voltage source for outputting a high voltage at two high-voltage outputs and outputting a control signal at a controller output; a focusing lens for focusing a beam; a monochromator which allows only those particles of the particle beam to pass whose kinetic energy is within an adjustable energy interval; an energy-dispersive component which deflects particles of different kinetic energies differently; a detector; and a controller connected to the controller output, which controls a beam deflector, arranged between the energy-dispersive component and the detector, the monochromator, or the energy-dispersive component in dependence on the control signal, or superposes plural of intensity distributions detected by the detector with an offset relative to one another, which offset is set in dependence on the control signal.
    Type: Application
    Filed: December 23, 2011
    Publication date: April 18, 2013
    Applicant: CARL ZEISS NTS GMBH
    Inventor: Joerg Fober
  • Patent number: 8421010
    Abstract: There is provided a substrate inspection device which uses a charged particle beam and is capable of more quickly extracting a defect candidate than ever before. The configuration of the substrate inspection device is such that a substrate having a circuit pattern is irradiated with a primary charged particle beam, the substrate is moved at a constant speed or at an increasing or a decreasing speed, a position resulting from the movement is monitored, the position of irradiation with the primary charged particle beam is controlled according to the coordinates of the substrate, an image in a partial region on the substrate is captured at a speed lower than the velocity of the movement, a defect candidate is detected based on the captured image, and the detected defect candidate is displayed in a map format.
    Type: Grant
    Filed: August 28, 2009
    Date of Patent: April 16, 2013
    Assignee: Hitachi High-Technologies Corporation
    Inventors: Takashi Hiroi, Yasuhiro Gunji, Hiroshi Miyai, Masaaki Nojiri
  • Patent number: 8421009
    Abstract: A test structure and method thereof for determining a defect in a sample of semiconductor device includes at least one transistor rendered grounded. The grounded transistor is preferably located at at least one end of a test pattern designed to be included in the sample. When the test structure is inspected by charged particle beam inspection, the voltage contrast (VC) of the transistors in the test pattern including the grounded transistor is observed for determination of the presence of defect in the sample.
    Type: Grant
    Filed: April 8, 2009
    Date of Patent: April 16, 2013
    Assignee: Hermes Microvision, Inc.
    Inventor: Hong Xiao
  • Patent number: 8415621
    Abstract: A method for line width measurement, comprising: providing a substrate, wherein a raised line pattern is formed on a surface of the substrate, and the line pattern has a width; forming a first measurement structure and a second measurement structure on opposite sidewalls of the line pattern in the width direction of the line pattern; removing the line pattern; and measuring the spacing between the first measurement structure and the second measurement structure, and obtaining the width of the line pattern by subtracting a predetermined offset from the spacing. The present invention facilitates to reduce the uncertainty associated with the measuring process and to improve the measurement precision.
    Type: Grant
    Filed: July 22, 2011
    Date of Patent: April 9, 2013
    Assignee: Institute of Microelectronics, Chinese Academy of Sciences
    Inventors: Haizhou Yin, Huilong Zhu, Zhijiong Luo
  • Publication number: 20130084491
    Abstract: An object of the present invention is to provide an ambient temperature molten salt having excellent electron conductivity in addition to ion conductivity. The present invention attains the object by providing an ambient temperature molten salt including a first imidazolium salt having a cationic segment represented by the general formula (1) and an anionic segment represented by MX4 (where M is a transition metal and X is a halogen); and a second salt having a cationic segment as a monovalent cation and an anionic segment as a halogen.
    Type: Application
    Filed: October 22, 2010
    Publication date: April 4, 2013
    Applicant: TOYOTA JIDOSHA KABUSHIKI KAISHA
    Inventors: Hirofumi Nakamoto, Fuminori Mizuno
  • Patent number: 8410440
    Abstract: It is an object of the present invention to provide a specimen observation method, an image processing device, and a charged-particle beam device which are preferable for selecting, based on an image acquired by an optical microscope, an image area that should be acquired in a charged-particle beam device the representative of which is an electron microscope. In the present invention, in order to accomplish the above-described object, there are provided a method and a device for determining the position for detection of charged particles by making the comparison between a stained optical microscope image and an elemental mapping image formed based on X-rays detected by irradiation with the charged-particle beam.
    Type: Grant
    Filed: February 16, 2012
    Date of Patent: April 2, 2013
    Assignee: Hitachi High-Technologies Corporation
    Inventors: Eiko Nakazawa, Masahiro Tomita, Hiroyuki Kobayashi
  • Patent number: 8410457
    Abstract: A sample transfer device is provided which can insert to a charged particle beam apparatus a sample to be observed and analyzed under irradiation of a charged particle beam while suppressing to a minimum the time to expose the sample to the atmospheric environment. The sample transfer device for transferring the sample to be observed and analyzed by irradiating the charged particle beam comprises an expansible hollow member capable of accommodating a sample holder mounting the sample, a fixing member for fixing the sample holder within the expansible hollow member, and a sealing member communicating with the interior of the expansible hollow member to open/close an opening through which the sample holder passes.
    Type: Grant
    Filed: January 27, 2011
    Date of Patent: April 2, 2013
    Assignee: Hitachi, Ltd.
    Inventors: Shohei Terada, Tatsumi Hirano, Koichi Watanabe, Yasuichiro Watanabe, Hiromitsu Seino
  • Patent number: 8410439
    Abstract: Multiple detectors arranged in a ring within a specimen chamber provide a large solid angle of collection. The detectors preferably include a shutter and a cold shield that reduce ice formation on the detector. By providing detectors surrounding the sample, a large solid angle is provided for improved detection and x-rays are detected regardless of the direction of sample tilt.
    Type: Grant
    Filed: December 6, 2011
    Date of Patent: April 2, 2013
    Assignee: PEI Company
    Inventors: Hanno Sebastian Von Harrach, Bert Freitag, Pleun Dona
  • Patent number: 8405026
    Abstract: Disclosed herewith is a charged particle beam apparatus capable of controlling each of the probe current and the objective divergence angle to obtain a desired probe current and a desired objective divergence angle in accordance with the diameter of the subject objective aperture. The apparatus is configured to include an objective aperture between first and second condenser lenses to calculate and set a control value of a first condenser lens in accordance with the diameter of the hole of the objective aperture so as to obtain a desired probe current and calculate a control value of a second condenser lens setting device in accordance with the diameter of the hole of the objective divergence angle and the control value of the second condenser lens setting device, thereby setting the calculated control value for the second condenser lens setting device to control the objective divergence angle.
    Type: Grant
    Filed: September 4, 2009
    Date of Patent: March 26, 2013
    Assignee: Hitachi High-Technologies Corporation
    Inventors: Tomoyasu Shojo, Muneyuki Fukuda, Naomasa Suzuki, Noritsugu Takahashi
  • Patent number: 8405047
    Abstract: The present invention relates to a specimen box for an electron microscope, comprising a first substrate, a second substrate, one or more photoelectric elements, and a metal adhesion layer. The first substrate has a first surface, a second surface, a first concave, and one or more first through holes, wherein the first through holes penetrate through the first substrate. The second substrate has a third surface, a forth surface, and a second concave. The photoelectric element is disposed between the first substrate and the second substrate. In addition, the metal adhesion layer is disposed between the first substrate and the second substrate to form a space for a specimen contained therein. Besides, the present specimen box further comprises one or more plugs. When the plugs are assembled into the first through holes to seal the specimen box, the in-situ observation can be accomplished by using the electron microscope.
    Type: Grant
    Filed: April 18, 2012
    Date of Patent: March 26, 2013
    Assignee: National Chiao Tung University
    Inventors: Chih Chen, King-Ning Tu
  • Patent number: 8405027
    Abstract: A scanning confocal transmission electron microscope includes a descan deflector and a corrector below the sample. The microscope uses a detector that is preferably significantly larger than the resolution of the microscope and is positioned in the real image plane, which provides improved contrast, particularly for light elements.
    Type: Grant
    Filed: July 14, 2011
    Date of Patent: March 26, 2013
    Assignee: Fei Company
    Inventors: Sorin Lazar, Bert Henning Freitag, Peter Christiaan Tiemeijer
  • Patent number: 8405053
    Abstract: A focused ion beam apparatus, including: a specimen transferring unit having a probe to which a micro-specimen extracted from a specimen, can be joined through a joining deposition film, for transferring the micro-specimen to a sample holder; and wherein, the specimen transferring unit holds the probe which is joined through the joining deposition film to the micro-specimen extracted from the specimen, and the sample stage moves so that the sample holder mounted on the holder clasp is provided into an irradiated range of the focused ion beam, and the specimen transferring unit approaches the probe to the sample holder, and the gas nozzle supplies the deposition gas so that the micro-specimen is fixed to the sample holder through a fixing deposition film, and the ion beam irradiating optical system irradiates the focused ion beam to the micro-specimen fixed to the sample holder for various procedures.
    Type: Grant
    Filed: February 14, 2011
    Date of Patent: March 26, 2013
    Assignee: Hitachi, Ltd.
    Inventors: Satoshi Tomimatsu, Kaoru Umemura, Yuichi Madokoro, Yoshimi Kawanami, Yasunori Doi
  • Patent number: 8405025
    Abstract: A scanning electron microscope includes an electron beam source which emits an electron beam, a beam current controller which controls a beam current of the electron beam, an electron beam converger which converges the electron beam on a surface of a sample, an electron beam scanner which scans the electron beam on the surface of the sample, a table which mounts the sample and moves at least in one direction, a detector which detects a secondary electron or a reflected electron emanated from the sample by the scan of the electron beam, an image former which forms an image of the sample based on a detection value of the detector, an image processor which processes the image formed by the image former. The beam current controller controls the beam current of the electron beam by changing transmittance of the electron beam in an irradiation path of the electron beam.
    Type: Grant
    Filed: October 2, 2008
    Date of Patent: March 26, 2013
    Assignee: Hitachi High-Technologies Corporation
    Inventors: Toshifumi Honda, Hiroshi Makino
  • Publication number: 20130068947
    Abstract: A pattern inspection apparatus includes: an irradiator irradiating a sample with an electron beam; an electron detector detecting an amount of electrons generated on the sample having a pattern formed thereon, by the irradiation of the electron beam; an image processor generating a SEM image of the pattern on the basis of the electron amount; and a controller acquiring defect position information on the pattern formed on the sample from an optical defect inspection device is provided. The controller specifies a defect candidate pattern from the SEM image and judges whether a defect in the defect candidate pattern is to be transferred onto a wafer. The controller determines a view field of the SEM image and specifies the defect candidate pattern from information on patterns in the SEM image in the view field.
    Type: Application
    Filed: October 31, 2011
    Publication date: March 21, 2013
    Inventors: Takayuki Nakamura, Tsutomu Murakawa
  • Patent number: 8401269
    Abstract: The present invention relates to a system and method for automatic measurements and calibration of computerized magnifying instruments. More particularly, the method includes an automatic calibration aspect, which includes obtaining an optimized digital image of a reference object including at least one standardized landmark feature, and establishing calibration parameters based on one or more measured attributes of the landmark feature. The method further describes a calibration aspect, which includes providing calibration parameters, obtaining a digital image including at least one known attribute, measuring the at least one known attribute and comparing the measured value with the known value. The method further includes an aspect of automatic measurement of an attribute of one or more object, which includes retrieving calibration parameters, acquiring a digital image and measuring the attribute.
    Type: Grant
    Filed: March 13, 2007
    Date of Patent: March 19, 2013
    Assignee: Clemex Technologies Inc.
    Inventors: Sylvain Laroche, Clement Forget
  • Patent number: 8399832
    Abstract: A calibration standard specimen is provided to have formed therein calibrating patterns of a lattice shape discontinuously arrayed, and particular alignment patterns respectively disposed near the calibrating patterns so that the positioning of the specimen can be made to match the calibrating patterns to the measurement points.
    Type: Grant
    Filed: June 30, 2008
    Date of Patent: March 19, 2013
    Assignee: Hitachi High-Technologies
    Inventors: Takeshi Mizuno, Hiroki Kawada
  • Publication number: 20130062520
    Abstract: A charged particle apparatus is equipped with a third stigmator positioned between the objective lens and a detector system, as a result of which a third degree of freedom is created for reducing the linear distortion. Further, a method of using said three stigmators, comprises exciting the first stigmator to reduce astigmatism when imaging the sample, exciting the second stigmator to reduce astigmatism when imaging the diffraction plane, and exciting the third stigmator to reduce the linear distortion.
    Type: Application
    Filed: April 13, 2012
    Publication date: March 14, 2013
    Applicant: FEI Company
    Inventors: Alexander Henstra, Maarten Bischoff, Uwe Luecken, Peter Christiaan Tiemeijer
  • Publication number: 20130062519
    Abstract: An electron microscope is provided that can automatically adjust the optical axis even in a state of deviation of the optical axis according to which the position of an electron beam on a fluorescent plate cannot be verified after replacement of an electron source. The microscope measures current of a fluorescent plate and determining whether the fluorescent plate is irradiated with an electron beam or not; without irradiation, controls a deflector to move the electron beam such that the fluorescent plate is irradiated with the electron beam; and, with irradiation, controls the deflector such that the current becomes a local maximum and a magnitude of luminance acquired from the image of the electron beam with which the fluorescent plate is irradiated becomes a local maximum.
    Type: Application
    Filed: April 20, 2011
    Publication date: March 14, 2013
    Inventors: Toshiyuki Oyagi, Takafumi Yotsuji, Yasuyuki Nodera, Isao Nagaoki
  • Patent number: 8395130
    Abstract: A mount (100, 200) for holding an electron microscopy sample carrier (310) comprises a base plate (101) having an opening (103) through a middle region thereof and a support surface (107) for the sample carrier (310) extending at least partly around the opening (103), a holding apparatus (104a, 104b) for frictionally engaged holding of the sample carrier (310) on the support surface (107) being provided on the base plate (101), the holding apparatus (104a, 104b) comprising at least two mutually independent clip elements (104a, 104b) that extend from the base plate (101) toward the opening (103) and by means of which edge regions (313a, 313b), spaced apart from one another, of the electron microscopy sample carrier (310) are holdable on the support surface (107). The invention further encompasses a loading apparatus for loading a mount with an electron microscopy sample carrier, and a method for using the loading apparatus.
    Type: Grant
    Filed: November 28, 2011
    Date of Patent: March 12, 2013
    Assignee: Leica Microsystems (Schweiz) AG
    Inventor: Leander Gächter
  • Patent number: 8387227
    Abstract: A method for making a TEM micro-grid is provided. The method includes the following steps. A carrier, a carbon nanotube structure, and a protector are provided. The carrier defines a first through opening. The protector defines a second through opening. The protector, the carbon nanotube structure and the carrier are stacked such that the carbon nanotube structure is located between the carrier and the protector. The second through opening at least partly overlaps with the first through opening.
    Type: Grant
    Filed: November 11, 2010
    Date of Patent: March 5, 2013
    Assignee: Beijing FUNATE Innovation Technology Co., Ltd.
    Inventors: Liang Liu, Li Fan, Chen Feng, Li Qian, Yu-Quan Wang
  • Patent number: 8389937
    Abstract: A transmission electron microscope includes an electron beam source to generate an electron beam. Beam optics are provided to converge the electron beam. An aberration corrector corrects the electron beam for at least a spherical aberration. A specimen holder is provided to hold a specimen in the path of the electron beam. A detector is used to detect the electron beam transmitted through the specimen. The transmission electron microscope may operate in an incoherent mode and may be used to locate a sequence of objects on a molecule.
    Type: Grant
    Filed: June 7, 2011
    Date of Patent: March 5, 2013
    Assignee: Mochii, Inc.
    Inventors: Christopher Su-Yan Own, Andrew Bleloch, William Andregg
  • Patent number: 8389935
    Abstract: A lower pole piece of an electromagnetic superposition type objective lens is divided into an upper magnetic path and a lower magnetic path. A voltage nearly equal to a retarding voltage is applied to the lower magnetic path. An objective lens capable of acquiring an image with a higher resolution and a higher contrast than a conventional image is provided. An electromagnetic superposition type objective lens includes a magnetic path that encloses a coil, a cylindrical or conical booster magnetic path that surrounds an electron beam, a control magnetic path that is interposed between the coil and sample, an accelerating electric field control unit that accelerates the electron beam using a booster power supply, a decelerating electric field control unit that decelerates the electron beam using a stage power supply, and a suppression unit that suppresses electric discharge of the sample using a control magnetic path power supply.
    Type: Grant
    Filed: April 14, 2009
    Date of Patent: March 5, 2013
    Assignee: Hitachi High-Technologies Corporation
    Inventors: Muneyuki Fukuda, Naomasa Suzuki, Tomoyasu Shojo, Noritsugu Takahashi
  • Patent number: 8384050
    Abstract: Disclosed are embodiments of an ion beam sample preparation thermal management apparatus and methods for using the embodiments. The apparatus comprises an ion beam irradiating means in a vacuum chamber that may direct ions toward a sample, a shield blocking a portion of the ions directed toward the sample, and a shield retention stage with shield retention means that replaceably and removably holds the shield in a position. The shield has datum features which abut complementary datum features on the shield retention stage when the shield is held in the shield retention stage. The shield has features which enable the durable adhering of the sample to the shield for processing the sample with the ion beam. The complementary datum features on both shield and shield retention stage enable accurate and repeatable positioning of the sample in the apparatus for sample processing and reprocessing. A heat sink means is configured to conduct heat away from the sample undergoing sample preparation in the ion beam.
    Type: Grant
    Filed: April 7, 2011
    Date of Patent: February 26, 2013
    Assignee: Gatan, Inc.
    Inventors: Steven Thomas Coyle, John Andrew Hunt
  • Publication number: 20130043386
    Abstract: The method disclosed in this specification includes: acquiring a dark-field image produced by capturing an image of a sample with a scanning transmission electron microscope by detecting electrons scattered at angles between a first angle to the optical axis of the scanning transmission electron microscope and a second angle which is larger than the first angle; acquiring a bright-field image captured simultaneously with the dark-field image by detecting electrons scattered within a third angle which is smaller than the first angle; generating a reverse image by reversing lightness and darkness of the dark-field image; and generating a difference image each of whose pixels has a brightness value equal to the difference between the brightness of the corresponding pixel in the reverse image and the brightness of the corresponding pixel in the bright-field image.
    Type: Application
    Filed: June 29, 2012
    Publication date: February 21, 2013
    Applicant: FUJITSU LIMITED
    Inventor: Takashi YAMAZAKI
  • Publication number: 20130043387
    Abstract: A transmission electron microscope includes an electron beam source to generate an electron beam. Beam optics are provided to converge the electron beam. An aberration corrector comprising either a foil or a set of concentric elements corrects the electron beam for at least a spherical aberration. A specimen holder is provided to hold a specimen in the path of the electron beam. A detector is used to detect the electron beam transmitted through the specimen. The transmission electron microscope may be configured to operate in a dark-field mode in which a zero beam of the electron beam is not detected. The microscope may also be capable of operating in an incoherent illumination mode.
    Type: Application
    Filed: October 22, 2012
    Publication date: February 21, 2013
    Applicant: MOCHII, INC. (D/B/A VOXA)
    Inventor: MOCHII, INC. (D/B/A VOXA)
  • Patent number: 8378299
    Abstract: A column for a charged particle beam device is described. The column includes a charged particle emitter for emitting a primary charged particle beam as one source of the primary charged particle beam; a biprism adapted for acting on the primary charged particle beam so that two virtual sources are generated; and a charged particle beam optics adapted to focus the charged particle beam simultaneously on two positions of a specimen corresponding to images of the two virtual sources.
    Type: Grant
    Filed: March 10, 2011
    Date of Patent: February 19, 2013
    Assignee: ICT Integrated Circuit Testing Gesellschaft fur Halbleiterpruftechnik MBH
    Inventor: Jürgen Frosien
  • Publication number: 20130037712
    Abstract: An optical phase plate system and method for enhancing phase contrast in electron beam imaging includes a transmission electron microscope (TEM) having a back focal plane; an optical cavity having a high internal surface reflectance, the center of the optical cavity located at the back focal plane of the TEM, the optical cavity having first and second ports arranged oppositely along a symmetrical axis of the optical cavity to admit an electron beam provided by the TEM through the first port to pass through and focus at the center of the optical cavity, and to exit through the second port, and wherein the optical cavity further has an optical port on an axis transverse to and intersecting the electron beam axis to admit a laser beam; a laser coupled to the optical cavity to provide a laser beam of a selected wavelength to enter the optical cavity through the optical port, wherein the laser beam is multiply reflected from the high internal surface reflectance to provide a high intensity standing wave optical ph
    Type: Application
    Filed: June 4, 2012
    Publication date: February 14, 2013
    Applicant: REGENTS OF THE UNIVERSITY OF CALIFORNIA
    Inventors: Robert GLAESER, Jian Jin, Radostin Danev, Holger Mueller, John Spence
  • Publication number: 20130032713
    Abstract: An electron detector includes a plurality of assemblies, the plurality of assemblies including a first assembly having a first SiPM and a first scintillator made of a first scintillator material directly connected to an active light sensing surface of the first SiPM, and a second assembly having a second SiPM and a second scintillator made of a second scintillator material directly connected to an active light sensing surface of the second SiPM, wherein the first scintillator material and the second scintillator material are different than one another. Alternatively, an electron detector includes an assembly including an SiPM and a scintillator member having a front surface and a back surface, the scintillator member being a film of a scintillator material directly deposited on to an active light sensing surface of the SiPM.
    Type: Application
    Filed: August 3, 2012
    Publication date: February 7, 2013
    Inventors: Nicholas C. Barbi, Richard B. Mott
  • Publication number: 20130028042
    Abstract: A method for calibrating an apparatus for measuring shape factor is provided, wherein the method comprises determining aspect ratios for each of a plurality of kaolin samples and measuring the shape factors of each of the plurality of kaolin samples using the apparatus, wherein each of the kaolin samples includes potassium oxide in an amount less than about 0.1% by weight of each of the kaolin samples. The method further includes calibrating the apparatus based on a correlation between the aspect ratios and the shape factors.
    Type: Application
    Filed: January 30, 2012
    Publication date: January 31, 2013
    Applicant: Imerys Pigments, Inc.
    Inventors: Robert J. Pruett, Jondahl Davis, Roger Wygant
  • Publication number: 20130026363
    Abstract: The present invention provides a scanning charged particle beam device including a sample chamber (8) and a detector. The detector has: a function of detecting light at least ranging from the vacuum ultraviolet region to the visible light region, of light (17) having image information which is obtained by a light emission phenomenon of gas scintillation when the sample chamber is controlled to a low vacuum (1 Pa to 3,000 Pa); and a function of detecting ion currents (11, 13) having image information which are obtained by cascade amplification of electrons and gas molecules. Accordingly, it becomes possible to realize a device which can deal with observation of various samples. Further, an optimal configuration of the detection unit is devised, to thereby make it possible to add value to an obtained image and provide users in wide-ranging fields with the observation image.
    Type: Application
    Filed: October 2, 2012
    Publication date: January 31, 2013
    Applicant: HITACHI HIGH-TECHNOLOGIES CORPORATION
    Inventor: HITACHI HIGH-TECHNOLOGIES CORPORATION
  • Patent number: 8362426
    Abstract: The SEM has a dynamic range reference value setting unit for setting dynamic range reference values, a dynamic range adjustment unit for receiving an observation image signal delivered out of a secondary electron detector, adjusting the dynamic range of the observation image signal on the basis of the dynamic range reference values and outputting the thus adjusted observation image signal as an observation image signal after adjustment, a display image generation unit for determining luminous intensity levels of individual pixels of an image to be displayed based on the observation image signal after adjustment to generate a display image, a histogram generation unit for generating a histogram of luminous intensity levels of the display image and extracting, as a luminous intensity peak value, at which the frequency of luminous intensity is maximized, and a display unit for displaying the generated histogram and the extracted luminous intensity peak value.
    Type: Grant
    Filed: September 14, 2006
    Date of Patent: January 29, 2013
    Assignee: Hitachi High-Technologies Corporation
    Inventors: Atsushi Kobaru, Katsuhiro Sasada, Hiroki Kawada
  • Patent number: 8362443
    Abstract: An objective lens for focussing charged particles includes a magnetic lens and an electrostatic lens whose components are displaceable relative to each other. The bore of the outer pole piece of the magnetic lens exhibits a diameter Da which is larger than a diameter Di of the bore of the inner pole piece of the magnetic lens. The following relationship is satisfied: 1.5·Di?Da?3·Di. The lower end of the inner pole piece is disposed in a distance of at least 2 mm offset from the inner end of the outer pole piece in a direction of the optical axis.
    Type: Grant
    Filed: April 18, 2012
    Date of Patent: January 29, 2013
    Assignee: Carl Zeiss Microscopy GmbH
    Inventor: Volker Drexel
  • Patent number: 8362428
    Abstract: A transmission electron microscope has a target body position on the electron optical axis of the microscope, and an electrically conductive body off the axis of the microscope. The microscope also has an electron source for producing an axial electron beam. In use, the beam impinges upon a target body located at the target body position. The microscope further has a system for simultaneously producing a separate off-axis electron beam. In use, the off-axis electron beam impinges on the electrically conductive body causing secondary electrons to be emitted therefrom. The electrically conductive body is located such that the emitted secondary electrons impinge on the target body to neutralise positive charge which may build up on the target body.
    Type: Grant
    Filed: June 5, 2008
    Date of Patent: January 29, 2013
    Assignee: Medical Research Council
    Inventors: John Berriman, Peter Rosenthal
  • Patent number: 8357913
    Abstract: An improved method and apparatus for extracting and handling samples for STEM analysis. Preferred embodiments of the present invention make use of a micromanipulator and a hollow microprobe probe using vacuum pressure to adhere the microprobe tip to the sample. By applying a small vacuum pressure to the lamella through the microprobe tip, the lamella can be held more securely and its placement controlled more accurately than by using electrostatic force alone. By using a probe having a beveled tip and which can also be rotated around its long axis, the extracted sample can be placed down flat on a sample holder. This allows sample placement and orientation to be precisely controlled, thus greatly increasing predictability of analysis and throughput.
    Type: Grant
    Filed: October 20, 2007
    Date of Patent: January 22, 2013
    Assignee: FEI Company
    Inventors: Enrique Agorio, James Edgar Hudson, Michael Tanguay, Jason Arjavac, Gerhard Daniel
  • Patent number: 8357894
    Abstract: An improved microcalorimeter-type energy dispersive x-ray spectrometer provides sufficient energy resolution and throughput for practical high spatial resolution x-ray mapping of a sample at low electron beam energies. When used with a dual beam system that provides the capability to etch a layer from the sample, the system can be used for three-dimensional x-ray mapping. A preferred system uses an x-ray optic having a wide-angle opening to increase the fraction of x-rays leaving the sample that impinge on the detector and multiple detectors to avoid pulse pile up.
    Type: Grant
    Filed: August 10, 2010
    Date of Patent: January 22, 2013
    Assignee: FEI Company
    Inventors: Milos Toth, Michael R. Scheinfein, Eric Silver, David Narum
  • Patent number: 8357897
    Abstract: A charged particle beam device enabling prevention of degradation of reproducibility of measurement caused by an increase of the beam diameter attributed to an image shift and having a function of dealing with device-to-device variation. The charged particle beam device is used for measuring the dimensions of a pattern on a specimen using a line profile obtained by detecting secondary charged particles emitted from the specimen when the specimen is scanned with a primary charged particle beam converged on the specimen. A lookup table in which the position of image shift and the variation of the beam diameter are associated is prepared in advance by actual measurement or calculation and registered. When the dimensions are measured, image processing is carried out so as to correct the line profile for the variation of the beam diameter while the lookup table is referenced, and thereby the situation where the beam diameter is effectively equal is produced irrespective of the position of the image shift.
    Type: Grant
    Filed: January 26, 2010
    Date of Patent: January 22, 2013
    Assignee: Hitachi High-Technologies Corporation
    Inventors: Chie Shishido, Atsushi Miyamoto, Mayuka Iwasaki, Tomofumi Nishiura, Go Kotaki
  • Patent number: 8354638
    Abstract: An electron detection device including: one scintillator 31 having an opening through which an electron beam emitted from an electron gun passes; a plurality of photoguides 22 of the same shape, which are bonded to the scintillator and disposed symmetrically about an optical axis; and a photomultiplier tube which is connected to one side of each of the photoguides 22, the side opposing to the optical axis side, and converts light into electrical signals, the light being emitted by the scintillator 31 receiving light through the photoguide 22. The photoguides 22 are joined so as to equally divide the scintillator 31 symmetrically about the optical axis. Moreover, a position and an area of a portion bonded to the scintillator 31, in each of the photoguides 22, are the same among the photoguides 22.
    Type: Grant
    Filed: February 14, 2011
    Date of Patent: January 15, 2013
    Assignee: Advantest Corp.
    Inventor: Tsuguo Kurata
  • Publication number: 20130009058
    Abstract: An electron microscope which utilizes a polarized electron beam and can obtain a high contrast image of a sample is provided. The microscope includes: a laser; a polarization apparatus that polarizes a laser beam into a circularly polarized laser beam; a semiconductor photocathode that is provided with a strained superlattice semiconductor layer and generates a polarized electron beam when irradiated with the circularly polarized laser beam; a transmission electron microscope that utilizes the polarized electron beam; an electron beam intensity distribution recording apparatus arranged at a face reached by the polarized electron beam that has transmitted through the sample. An electron beam intensity distribution recording apparatus records an intensity distribution before and after the polarization of the electron beam is reversed, and a difference acquisition apparatus calculates a difference therebetween.
    Type: Application
    Filed: February 22, 2011
    Publication date: January 10, 2013
    Applicant: NATIONAL UNIVERSITY CORPORATION NAGOYA UNIVERSITY
    Inventors: Nobuo Tanaka, Tsutomu Nakanishi, Yoshikazu Takeda, Hidefumi Asano, Koh Saitoh, Toru Ujihara, Makoto Kuwahara
  • Publication number: 20130009056
    Abstract: An arrangement and a method for imaging, examining and processing a sample using electrons. The arrangement comprises an electron microscope for providing electrons, a chamber with a sample holder on which a sample is positionable such that it can be imaged, examined and processed using the electrons. A system for magnetic field compensation in at least one spatial direction, including a compensation coil, wherein a wall of the chamber has an accommodation area, in sections thereof, for a portion of the compensation coil. Generally, only the chamber in which the sample is arranged is considered as a compensation volume. It suffice to reduce the compensation volume to the sensitive region of the electron microscope, since it is in the chamber, shortly following a final focusing and filtering, where the electron beam is most sensitive in terms of image quality when subjected to external electromagnetic interference.
    Type: Application
    Filed: July 3, 2012
    Publication date: January 10, 2013
    Applicant: INTEGRATED DYNAMICS ENGINEERING GMBH
    Inventor: Peter A. Kropp
  • Patent number: 8350214
    Abstract: Provided is a multi-beam type charged particle beam applied apparatus in an implementable configuration, capable of achieving both high detection accuracy of secondary charged particles and high speed of processing characteristically different specimens. An aperture array (111) includes plural aperture patterns. A deflector (109) for selecting an aperture pattern through which a primary beam passes is disposed at the position of a charged particle source image created between an electron gun (102), i.e., a charged particle source, and the aperture array (111). At the time of charge-control beam illumination and at the time of signal-detection beam illumination, an aperture pattern of the aperture array (111) is selected, and conditions of a lens array (112), surface electric-field control electrode (118) and the like are switched in synchronization with each beam scanning. Thus, the charges are controlled and the signals are detected at different timings under suitable conditions, respectively.
    Type: Grant
    Filed: January 4, 2010
    Date of Patent: January 8, 2013
    Assignee: Hitachi High-Technologies Corporation
    Inventors: Hiroki Otaki, Momoyo Enyama, Hiroya Ohta
  • Patent number: 8351115
    Abstract: A complex type microscopic device includes a slider unit moving a stage, an optical microscope, a scanning electron microscope with an electron axis intersecting with an optical axis of the optical microscope, an optical measurement/observation unit having a magnification between those of the scanning electron microscope and the optical microscope and co-using an objective lens with the optical microscope, and a control unit controlling the entire device, and a display unit having a display screen. During display of a low-magnification optical microscopic image, the control unit controls the display unit to display, on the image, a representation to designate an area to be observed at a magnification of the optical measurement/observation unit, and to display, on the image, another representation to designate an area to be observed at a magnification of the scanning electron microscope during display of a high-magnification optical microscopic image.
    Type: Grant
    Filed: October 14, 2009
    Date of Patent: January 8, 2013
    Assignee: Kabushiki Kaisha TOPCON
    Inventors: Hisashi Isozaki, Fumio Ohtomo, Kazuo Nunokawa
  • Patent number: 8344320
    Abstract: A lens adjustment method and a lens adjustment system which adjust a plurality of multi-pole lenses of an electron spectrometer attached to a transmission electron microscope, optimum conditions of the multi-pole lenses are determined through simulation based on a parameter design method using exciting currents of the multi-pole lenses as parameters.
    Type: Grant
    Filed: January 6, 2011
    Date of Patent: January 1, 2013
    Assignee: Hitachi High-Technologies Corporation
    Inventors: Shohei Terada, Yoshihumi Taniguchi, Kazutoshi Kaji
  • Patent number: 8347410
    Abstract: Disclosed is a method for examining a sample using a scanning tunneling microscope, wherein before or during image recording, a contrast agent is applied to at least one location on the tip of the scanning tunneling microscope and/or on the sample, which is part of the tunneling contact during the image recording, while a temperature less than or equal to the condensation temperature of the contrast agent is set at this location. A corresponding scanning tunneling microscope is disclosed.
    Type: Grant
    Filed: November 7, 2008
    Date of Patent: January 1, 2013
    Assignee: Forschungszentrum Juelich GmbH
    Inventors: Ruslan Temirov, Sergey Subach, Frank Stefan Tautz
  • Patent number: 8343769
    Abstract: An immersion solution for a microscope, the immersion solution including a metal-halogeno complex anion containing bromine or iodine and one or more types of metal elements M selected from Sn, In, Bi, Sb, Zn and Al, and an imidazolium cation, a pyridinium cation, a pyrrolidinium cation or an ammonium cation. The immersion solution includes an ionic liquid that transmits light having a predetermined wavelength, has a refractive index of no less than 1.60 and is used for a fluorescence microscope.
    Type: Grant
    Filed: December 8, 2011
    Date of Patent: January 1, 2013
    Assignee: Olympus Medical Systems Corp.
    Inventors: Hiroaki Kinoshita, Atsushi Niwa, Masahiro Sato
  • Patent number: 8338804
    Abstract: One of principal objects of the present invention is to provide a sample dimension measuring method for detecting the position of an edge of a two-dimensional pattern constantly with the same accuracy irrespective of the direction of the edge and a sample dimension measuring apparatus. According to this invention, to accomplish the above object, it is proposed to correct the change of a signal waveform of secondary electrons which depends on the direction of scanning of an electron beam relative to the direction of a pattern edge of an inspection objective pattern. It is proposed that when changing the scanning direction of the electron beam in compliance with the direction of a pattern to be measured, errors in the scanning direction and the scanning position are corrected. In this configuration, a sufficient accuracy of edge detection can be obtained irrespective of the scanning direction of the electron beam.
    Type: Grant
    Filed: March 7, 2011
    Date of Patent: December 25, 2012
    Assignee: Hitachi High-Technologies Corporation
    Inventors: Hidetoshi Morokuma, Akiyuki Sugiyama, Ryoichi Matsuoka, Takumichi Sutani, Yasutaka Toyoda
  • Patent number: RE44035
    Abstract: An instrument system is controlled to acquire an optical image of an object, with the optical image defining a first coordinate system. The object is positioned in a second coordinate system and a point in the optical image is selected. The object is repositioned so that a point on the object corresponding to the selected point in the optical image is positioned at a predetermined point in the second coordinate system. Alternatively, movement of the object causes an indicia on the optical image to move to a point thereon corresponding to the point on the object that is positioned at the predetermined point in the second coordinate system.
    Type: Grant
    Filed: January 28, 2009
    Date of Patent: March 5, 2013
    Assignee: FEI Company
    Inventors: Frederick H. Schamber, Cornelis G. van Beek, Nicholas Ritchie