Plural Diverse X-ray Analyses Patents (Class 378/46)
  • Patent number: 7856081
    Abstract: This invention is directed towards finding, locating, and confirming threat items and substances. The inspection system is designed to detect objects that are made from, but not limited to, special nuclear materials (“SNM”) and/or high atomic number materials. The system employs advanced image processing techniques to analyze images of an object under inspection (“OUI”), which includes, but is not limited to baggage, parcels, vehicles and cargo, and fluorescence detection.
    Type: Grant
    Filed: March 13, 2008
    Date of Patent: December 21, 2010
    Assignee: Rapiscan Systems, Inc.
    Inventor: Kristian R. Peschmann
  • Patent number: 7844090
    Abstract: A method of deriving a quantitative measure of a degree of calcification of a blood vessel such as an aorta by processing an image such as an X-ray image of at least a part of the blood vessel containing said calcification comprises: taking a starting set of digital data representative of an image of at least part of a blood vessel containing a calcification set against a background; estimating the boundary of the calcification; using inpainting to replace digital data in said starting set representing the calcification with data extrapolating the boundary of the background to extend over the area of calcification, and so generating an inpainted set of digital data; and computing the difference between the starting set of digital data and the inpainted set of digital data to obtain a quantitative measure of the degree of calcification of the blood vessel.
    Type: Grant
    Filed: June 2, 2006
    Date of Patent: November 30, 2010
    Assignee: Nordic Bioscience Imaging A/S
    Inventors: Marleen De Bruijne, Mads Nielsen, Claus Christiansen, Lars A. Conrad-Hansen, Francois B. Lauze
  • Patent number: 7796726
    Abstract: An X-ray diffraction and X-ray fluorescence instrument for analyzing samples having no sample preparation includes a X-ray source configured to output a collimated X-ray beam comprising a continuum spectrum of X-rays to a predetermined coordinate and a photon-counting X-ray imaging spectrometer disposed to receive X-rays output from an unprepared sample disposed at the predetermined coordinate upon exposure of the unprepared sample to the collimated X-ray beam. The X-ray source and the photon-counting X-ray imaging spectrometer are arranged in a reflection geometry relative to the predetermined coordinate.
    Type: Grant
    Filed: February 14, 2007
    Date of Patent: September 14, 2010
    Assignee: University of Maryland, Baltimore County
    Inventors: Keith Gendreau, Jose Vanderlei Martins, Zaven Arzoumanian
  • Patent number: 7702067
    Abstract: A method, instrument, and computer program software product for characterizing a sample with respect to the presence of a specified element, either as a constituent of a surface layer or of the bulk of the sample. Intensities of fluorescent emission at two characteristic emission lines are compared to establish whether the specified element is disposed above the bulk of the sample. In the case where the specified element is disposed above the bulk of the sample, an areal density of the specified element is determined, whereas in the case where the specified element is disposed within the bulk of the sample, a volumetric concentration of the specified element within the sample is determined.
    Type: Grant
    Filed: September 5, 2008
    Date of Patent: April 20, 2010
    Assignee: Thermo Niton Analyzers LLC
    Inventors: Lee Grodzins, John Pesce
  • Patent number: 7700820
    Abstract: The present disclosure is generally directed to a process for controlling the quality of manufactured absorbent articles, the process including incorporating into an absorbent article at least a portion of a wetness sensing system that is configured to detect the presence of a substance, the wetness sensing system comprising at least one metallic conductive element; and passing the absorbent article in proximity to a foreign material sensor employing x-ray technology, the foreign material sensor adapted to detect the presence of foreign material to confirm whether foreign material has been incorporated into the article.
    Type: Grant
    Filed: November 30, 2006
    Date of Patent: April 20, 2010
    Assignee: Kimberly-Clark Worldwide, Inc.
    Inventors: Darold Dean Tippey, Perry Allen Bush, Timothy Patrick Clare
  • Patent number: 7664223
    Abstract: A beam collimator arrangement for scanned-slot x-ray imaging having one or several collimators in an x-ray apparatus is disclosed. The beam collimator arrangement includes an x-ray source; an x-ray image receiver positioned to receive x-rays from the x-ray source; a compressor or means for compressing a female breast to be examined where the compressor is positionable between the x-ray source and the x-ray image receiver; and the beam collimator is positioned between the x-ray source and the compressor. The beam collimator arrangement is arranged on a carrying structure to displace the beam collimator arrangement between a first position when no x-ray exposure is conducted and a second position before x-ray exposure is initiated.
    Type: Grant
    Filed: February 12, 2002
    Date of Patent: February 16, 2010
    Assignee: Sectra Mamea AB
    Inventors: Mats Danielsson, Theresa Lammroth, Lénnart Rapp
  • Patent number: 7646846
    Abstract: The press formability of a galvanized steel sheet including an oxide film, which has a thickness of 10 nm to 100 nm, as a surface layer is nondestructively speedily evaluated.
    Type: Grant
    Filed: September 22, 2005
    Date of Patent: January 12, 2010
    Assignee: JFE Steel Corporation
    Inventors: Wataru Tanimoto, Hisato Noro
  • Patent number: 7643662
    Abstract: Systems and methods are provided for accessing three dimensional representation of an anatomical surface and flattening the anatomical surface so as to produce a two dimensional representation of an anatomical surface. The two dimensional surface can be augmented with computed properties such as thickness, curvature, thickness and curvature, or user defined properties. The rendered two dimensional representation of an anatomical surface can be interacted by user so as to deriving quantitative measurements such as diameter, area, volume, and number of voxels.
    Type: Grant
    Filed: August 15, 2006
    Date of Patent: January 5, 2010
    Assignee: General Electric Company
    Inventor: David T Gering
  • Patent number: 7636460
    Abstract: A method of producing an improved straightened reformat is presented in which cross sections are calculated perpendicular to an elongate subject described within an object data set, a reference direction is determined in each cross sectional slice and a new object data set is created by concatenating the cross sectional slices, each cross sectional slice orientated so that the reference directions in the cross sectional slices are aligned. Various methods are presented by which the reference direction is determined within each cross sectional slice, including propagation from an original reference direction and optimization using determined reference directions as boundary conditions.
    Type: Grant
    Filed: July 31, 2003
    Date of Patent: December 22, 2009
    Assignee: Koninklijke Philips Electronics N.V.
    Inventor: Bert Leo Alfons Verdonck
  • Patent number: 7634054
    Abstract: Provided are an X-ray tube and an X-ray analysis apparatus, which can be further reduced in size as well as in weight and more efficiently detect a fluorescent X-ray and the like to increase sensitivity.
    Type: Grant
    Filed: July 18, 2008
    Date of Patent: December 15, 2009
    Assignee: SII NanoTechnology Inc.
    Inventors: Yoshiki Matoba, Yutaka Ikku
  • Patent number: 7616734
    Abstract: A method for nondestructively obtaining measurement information of a region within one or more ultra-hard polycrystalline constructions comprises conducing a first measurement using x-ray fluorescence by directing x-rays onto a surface of the diamond body, receiving x-ray fluorescence from the diamond body, and deriving measurement information regarding the region therefrom. A second method can be used on the same or other ultra-hard polycrystalline constructions to obtain measurement information regarding the region in a manner that is relatively more time efficient than the first method to facilitate use of the measurement method on a large number of constructions. The second measurement can be selected from the group including beta backscatter, x-ray radioscopy, eddy current, magnetic induction, and microresistance. In an example embodiment, the method is used to determine the thickness of a region within the diamond body that comprises less catalyst material than another region within the body.
    Type: Grant
    Filed: May 8, 2007
    Date of Patent: November 10, 2009
    Assignee: Smith International, Inc.
    Inventors: Loel Gene Corbett, Nephi Mourik
  • Patent number: 7595489
    Abstract: A method of identifying a material using an x-ray emission characteristic is provided. X-ray data representing a monitored x-ray emission characteristic is obtained from a specimen in response to an incident energy beam. A dataset is also obtained, this comprising composition data of a plurality of materials. The material of the specimen is contained within the dataset. Predicted x-ray data are calculated for each of the materials in the dataset using the composition data. The obtained and the predicted x-ray data are compared and the likely identity of the material of the specimen is determined, based upon the comparison.
    Type: Grant
    Filed: June 28, 2006
    Date of Patent: September 29, 2009
    Assignee: Oxford Instruments Analytical Limited
    Inventor: Peter John Statham
  • Patent number: 7592591
    Abstract: An electron probe X-ray analyzer capable of automatically setting appropriate analytical conditions if there are unknown compounds by performing analysis under the analytical conditions adapted for analysis points having different compositions in a case where the numerous analysis points having the plural compositions are analyzed by WDS (wavelength-dispersive X-ray spectrometer). At each analysis point, the analyzer performs quantitative analysis using EDS (energy-dispersive X-ray spectrometer) permitting easy and quick analysis. Based on the results, chemical compounds are identified. If the results indicate that there is any new compound, analytical conditions adapted for the new compound are selected. If the new compound is already registered in a database, the analytical conditions are read from the database. Then, quantitative analysis is performed using WDS.
    Type: Grant
    Filed: April 9, 2007
    Date of Patent: September 22, 2009
    Assignee: Jeol Ltd.
    Inventor: Satoshi Notoya
  • Patent number: 7579591
    Abstract: Method and apparatus for performing sample analysis using both the WDS and an energy-dispersive X-ray spectrometer (EDS). The analysis starts with irradiating the sample with an electron beam. Characteristic X-rays emanating from the sample are spectrally dispersed and detected by the WDS. The intensities of the characteristic X-rays at positions where the characteristic X-ray peaks are detected are measured. At this time, the background intensities of the characteristic X-rays at the positions where the characteristic X-ray peaks are detected are found based on a mean atomic number calculated using values which are derived by quantitative analysis based on the characteristic X-ray intensities measured by the EDS at the corresponding analysis positions on the sample. The background intensities are subtracted from the peak intensities at the positions where the characteristic X-ray peaks are detected by the WDS. Thus, the net characteristic X-ray intensities are found.
    Type: Grant
    Filed: November 13, 2007
    Date of Patent: August 25, 2009
    Assignee: Jeol Ltd.
    Inventor: Masaru Takakura
  • Patent number: 7551714
    Abstract: A system and methods for identifying contents of an enclosure such as an air cargo container. A three-dimensional image indicative of at least one of the CT number and the density of contents of the enclosure is obtained using penetrating radiation such as x-rays. If one or more suspect regions are identified among contents of the enclosure, a collimated neutron beam is activated to traverse each suspect region and fluorescent emission from the suspect region is detected, allowing material within the suspect region to be characterized based at least on the detected fluorescent emission. Additionally, the collimated neutron beam may be employed for neutron imaging of the contents of the enclosure.
    Type: Grant
    Filed: April 27, 2007
    Date of Patent: June 23, 2009
    Assignee: American Science and Engineering, Inc.
    Inventor: Peter J. Rothschild
  • Publication number: 20090086905
    Abstract: One aspect relates to inducing at least one induced X-ray fluorescing photon within an at least some matter of an at least a portion of an at least one individual responsive to a substantial single input energy event based at least partially on an at least some input energy being applied to the at least some matter of the at least the portion of the at least one individual; and detecting the at least one induced X-ray fluorescing photon; and X-ray fluorescence visualizing, imaging, or information providing within the at least some matter of the at least the portion of the at least one individual responsive to the detecting the at least one induced X-ray fluorescing photon.
    Type: Application
    Filed: September 28, 2007
    Publication date: April 2, 2009
    Inventors: Edward S. Boyden, Roderick A. Hyde, Muriel Y. Ishikawa, Edward K.Y. Jung, Eric C. Leuthardt, Robert W. Lord, Nathan P. Myhrvold, Dennis J. Rivet, Michael A. Smith, Clarence T. Tegreene, Thomas A. Weaver, Charles Whitmer, Lowell L. Wood, JR., Victoria Y.H. Wood
  • Publication number: 20090067573
    Abstract: A method for analyzing a sample includes directing one or more beams of X-rays to impinge on an area of a surface of the sample on which a layer of nano-particles of a selected element has been formed. Secondary X-ray radiation from the area is detected responsively to the one or more beams. A distribution of the nano-particles on the surface is characterized based on the detected radiation.
    Type: Application
    Filed: September 6, 2007
    Publication date: March 12, 2009
    Inventors: Boris Yokhin, Alexander Tokar, Alexander Krokhmal, Asher Peled, Dileep Agnihotri
  • Patent number: 7495217
    Abstract: In some embodiments, techniques are described for combining an X-ray detector (e.g., for providing EPMA) and an electron detector (e.g., for providing AES) to provide a tool for determining film compositions and thicknesses on a specimen, such as a semiconductor structure or wafer. In one embodiment, a system includes a beam generator configurable to direct a beam towards a specimen. The electron beam may generate Auger electrons and X-rays. The system may also include at least one electron detector disposed adjacent to (e.g., above) the specimen to detect electrons and measure their energies emanating from a top layer of the specimen. One or more X-ray detectors may be disposed adjacent to the specimen to detect X-rays.
    Type: Grant
    Filed: May 21, 2007
    Date of Patent: February 24, 2009
    Assignee: KLA-Tencor Corporation
    Inventors: Ying Gao, Gary Janik
  • Patent number: 7463758
    Abstract: A method of deriving a quantitative measure of a degree of calcification of a blood vessel such as an aorta by processing an image such as an X-ray image of at least a part of the blood vessel containing said calcification comprises: taking a starting set of digital data representative of an image of at least part of a blood vessel containing a calcification set against a background; estimating the boundary of the calcification; using inpainting to replace digital data in said starting set representing the calcification with data extrapolating the boundary of the background to extend over the area of calcification, and so generating an inpainted set of digital data; and computing the difference between the starting set of digital data and the inpainted set of digital data to obtain a quantitative measure of the degree of calcification of the blood vessel.
    Type: Grant
    Filed: June 2, 2005
    Date of Patent: December 9, 2008
    Assignee: Nordio Bioscience A/S
    Inventors: Lars A. Conrad-Hansen, Marleen de Bruijne, Francois Bernard Lauze, Claus Christiansen, Mads Nielsen
  • Patent number: 7457451
    Abstract: Systems, methods and apparatus are provided through which in one aspect, a three-dimensional (3D) image of an object is constructed from a plurality of two-dimensional (2D) images of the object using a specialized filter. In some embodiments, the specialized filter implements a linear ramp function, a windowing function, and/or a polynomial function. In some embodiments, the 3D image is back-projected from the filtered two-dimensional images, yielding a 3D image that has improved visual distinction of overlapping anatomic structures and reduced blurring.
    Type: Grant
    Filed: December 4, 2007
    Date of Patent: November 25, 2008
    Assignee: General Electric Company
    Inventors: Jiang Hsieh, Stephen W. Metz, Gopal B. Avinash, Baojun Li, John Michael Sabol
  • Patent number: 7432501
    Abstract: An ionising particle analyser comprises a source of ionising particles, a charged particle detector, and an ionisable gas located between the source and the detector. The analyser further comprises a charged particle impeding device located between the source and the detector. The charged particle impeding device is arranged to be maintained in a first configuration at a potential to impede the passage of charged particles and pass uncharged particles.
    Type: Grant
    Filed: August 27, 2004
    Date of Patent: October 7, 2008
    Assignee: Council for the Central Laboratory of the Research Councils
    Inventors: James Edmond Bateman, Gareth Derbyshire
  • Patent number: 7428293
    Abstract: There is provided a fluorescent X-ray analysis apparatus in which a detection lower limit has been improved by reducing an X-ray generating subsidiarily and detected. The fluorescent X-ray analysis apparatus is one which possesses an X-ray source irradiating a primary X-ray, and a detector in which a collimator having a through-hole in its center part has been placed in a front face, and in which, by the detector, there is detected a primary fluorescent X-ray which generates from a sample by irradiating the primary X-ray to a sample, and passes through the through-hole of the collimator.
    Type: Grant
    Filed: March 28, 2007
    Date of Patent: September 23, 2008
    Assignee: SII Nanotechnology Inc.
    Inventors: Takayuki Fukai, Yoshiki Matoba
  • Publication number: 20080205593
    Abstract: An analytical instrument is disclosed having both XRF and spark emission spectroscopy capabilities. In a particularly advantageous embodiment, a field portable XRF device is removably coupled to the instrument by means of a docking station. A first surface of the sample is irradiated with an X-ray beam, and the X-ray radiation fluorescently emitted from the sample is detected and analyzed to acquire elemental composition data. The instrument is further provided with a spark source located proximal a second surface of the sample and a detector for sensing the radiation emitted from the spark-excited material. The combined instrument enables the acquisition of complementary elemental composition data by XRF and spark emission spectroscopy without having to transport a sample between separate instruments.
    Type: Application
    Filed: February 23, 2007
    Publication date: August 28, 2008
    Inventor: Ravisekhar Yellepeddi
  • Patent number: 7391892
    Abstract: According to one embodiment, the present technique provides a phantom for testing imaging device. The exemplary phantom includes a first portion having groups of vessels, which are filled with a radiographically opaque substance (i.e., a contrast agent). The each group of vessels may extend from a central region of the first portion to the periphery of the central portion. The phantom may also include a second portion having a testing region. By way of example, the testing region may comprise a series of rings, each ring being configured to attenuate X-ray radiation differently. Adventurously, each ring may comprise materials configured to emulate different types and amounts of human tissue. For example, the exemplary phantom may include a ring, which emulates bone tissue, and a second ring, which emulates soft tissue. Moreover, each ring may be configured to emulate different amounts of tissue.
    Type: Grant
    Filed: November 26, 2003
    Date of Patent: June 24, 2008
    Assignee: GE Medical Systems, Inc.
    Inventor: Paul J. Gerwin
  • Patent number: 7375327
    Abstract: A method and device to accurately obtain very small quantity of wear of the order of nanometers of a protective film on the surface of a sliding member. A quantity of wear on the surface of a measurement sample including a base and a coating layer is measured by making a spectrum of the surface elements in a reference sample using a surface-element analysis device which analyzes elements on the surface of a substance from an energy spectrum of charged particles obtained by applying excited ionization radiation on the reference sample equivalent to the measurement and by measuring charged particles generated from the surface of the substance. A step of obtaining signal intensity ratios of plural elements from the spectrum is repeated a plurality of times while the surface of the reference sample is being etched and calibration curves which indicate a distribution of the signal intensity ratios of the plural elements in the reference sample are made.
    Type: Grant
    Filed: November 7, 2005
    Date of Patent: May 20, 2008
    Assignee: Kabushiki Kaisha Toshiba
    Inventors: Masahiko Yoshiki, Makoto Kato
  • Patent number: 7366282
    Abstract: This invention is directed towards finding, locating, and confirming threat items and substances. The inspection system is designed to detect objects that are made from, but not limited to, special nuclear materials (“SNM”) and/or high atomic number materials. The system employs advanced image processing techniques to analyze images of an object under inspection (“OUI”), which includes, but is not limited to baggage, parcels, vehicles and cargo, and fluorescence detection.
    Type: Grant
    Filed: October 15, 2005
    Date of Patent: April 29, 2008
    Assignee: Rapiscan Security Products, Inc.
    Inventor: Kristian R. Peschmann
  • Patent number: 7366374
    Abstract: An optic device, system and method for imaging are described. The optic device includes a first solid phase layer having a first index of refraction with a first photon transmission property and a second solid phase layer having a second index of refraction with a second photon transmission property, the solid phase layers being situated between an output face and a non-flat input face. The first and second layers are conformal to each other. The imaging system includes a source of electrons and a target, with an array of the optic devices coupled thereto to form limited cone beams of X-ray radiation.
    Type: Grant
    Filed: May 22, 2007
    Date of Patent: April 29, 2008
    Assignee: General Electric Company
    Inventors: Susanne Madeline Lee, Forrest Frank Hopkins, Peter Michael Edic, Joseph John Manak, William Eugene Powell, III
  • Patent number: 7358494
    Abstract: The material composition of a thin film formed on a substrate or covered by a cap layer that shares one or more elements with the thin film can be determined by combining characteristic material data, such as characteristic x-ray data, from a material composition analysis tool, such as an electron probe-based x-ray metrology (EPMA) operation, with thickness data and (optionally) possible material phases for the thin film. The thickness data and/or the material phase options can be used to determine, for example, the penetration depth of a probe e-beam of the EPMA tool. Based on the penetration depth and the thin film thickness, the characteristic x-ray data from the EPMA operation can be analyzed to determine the composition (e.g., phase or elemental composition) of the thin film. An EPMA tool can include ellipsometry capabilities for all-in-one thickness and composition determination.
    Type: Grant
    Filed: June 15, 2005
    Date of Patent: April 15, 2008
    Assignee: KLA-Tencor Technologies Corporation
    Inventors: Ying Gao, Moshe Sarfaty
  • Patent number: 7342995
    Abstract: A specific macromolecule crystal evaluating device according to the present invention is equipped with a sample detecting stage for detecting a protein crystal in a sample container, an X-ray measuring stage that is spaced from the sample detecting stage and carries out X-ray diffraction measurement of the protein crystal, a feeding unit for feeding the sample container from the sample detecting stage to the X-ray measuring stage, and a central processing unit for recognizing the position of the protein crystal on the basis of the information achieved in the sample detecting stage and controlling the feeding unit on the basis of the position information to position the protein crystal to a sample disposing portion of the X-ray measuring stage.
    Type: Grant
    Filed: August 18, 2004
    Date of Patent: March 11, 2008
    Assignees: Rigaku Corporation, RIKEN
    Inventors: Takahisa Sato, Akihito Yamano, Shoichi Yasukawa, Hiroki Yoshida, Kensaku Hamada
  • Patent number: 7331714
    Abstract: A multifunctional hard x-ray nanoprobe instrument for characterization of nanoscale materials and devices includes a scanning probe mode with a full field transmission mode. The scanning probe mode provides fluorescence spectroscopy and diffraction contrast imaging. The full field transmission mode allows two-dimensional (2-D) imaging and tomography. The nanoprobe instrument includes zone plate optics for focusing and imaging. The nanoprobe instrument includes a stage group for positioning the zone plate optics. The nanoprobe instrument includes a specimen stage group for positioning the specimen. An enhanced laser Doppler displacement meter (LDDM) system provides two-dimensional differential displacement measurement in a range of nanometer resolution between the zone-plate optics and the sample holder. A digital signal processor (DSP) implements a real-time closed-loop feedback technique for providing differential vibration control between the zone-plate optics and the sample holder.
    Type: Grant
    Filed: September 29, 2005
    Date of Patent: February 19, 2008
    Assignee: UChicago Argonne, LLC
    Inventors: Deming Shu, Jorg M. Maser, Barry Lai, Franz Stefan Vogt, Martin V. Holt, Curt A. Preissner, Robert P. Winarski, Gregory B. Stephenson
  • Patent number: 7312446
    Abstract: Systems and methods for process monitoring based upon X-ray emission induced by a beam of charged particles such as electrons or ions. Concept as expressed herein.
    Type: Grant
    Filed: October 8, 2003
    Date of Patent: December 25, 2007
    Assignee: Applied Materials, Israel, Ltd.
    Inventor: Dror Shemesh
  • Patent number: 7310436
    Abstract: Systems, methods and apparatus are provided through which in one aspect, a three-dimensional (3D) image of an object is constructed from a plurality of two-dimensional (2D) images of the object using a specialized filter. The specialized filter implements a linear ramp function, a windowing function, and/or a polynomial function. The 3D image is back-projected from the filtered two-dimensional images, yielding a 3D image that has improved visual distinction of overlapping anatomic structures and reduced blurring.
    Type: Grant
    Filed: June 1, 2004
    Date of Patent: December 18, 2007
    Assignee: General Electric Co.
    Inventors: Baojun Li, Steven W. Metz, John Michael Sabol, Gopal B. Avinash, Jiang Hsieh
  • Patent number: 7289598
    Abstract: The change in the sample size and a change in background intensity due to the coexisting element are measured in real time to thereby automatically change a measurement time, the detection lower limit is kept constant, so that a fluorescent X-ray apparatus is provided that is capable of measuring every time in the same detection lower limit even in a case where there have existed a change in size of a sample, a change in sensitivity due to a difference in main ingredient, and a change of a magnitude in background due to an influence of a coexisting element.
    Type: Grant
    Filed: November 1, 2005
    Date of Patent: October 30, 2007
    Assignee: SII Nano Technology Inc.
    Inventor: Yoshiki Matoba
  • Patent number: 7258485
    Abstract: An X-ray thin film inspection apparatus including a sample table on which an inspection target such as a product wafer or the like is mounted, a positioning mechanism for moving the sample table, a goniometer having first and second swing arms, at least one X-ray irradiation unit that are mounted on the first swing arm and containing an X-ray tube and an X-ray optical element in a shield tube, an X-ray detector mounted on a second swing arm, and an optical camera for subjecting the inspection target disposed on the sample table to pattern recognition.
    Type: Grant
    Filed: October 26, 2005
    Date of Patent: August 21, 2007
    Assignee: Rigaku Corporation
    Inventors: Asao Nakano, Takao Kinefuchi, Hiroshi Motono, Atsunori Kiku
  • Patent number: 7220964
    Abstract: In various embodiments, techniques are described for combining an X-ray detector (e.g., for providing EPMA) and an electron detector (e.g., for providing AES) to provide a tool for determining film compositions and thicknesses on a specimen, such as a semiconductor structure or wafer. In one embodiment, a system includes a beam generator configurable to direct an electron beam towards a specimen. The electron beam may generate Auger electrons and X-rays. The system may also include at least one electron detector disposed adjacent to (e.g., above) the specimen to detect electrons and measure their energies emanating from a top layer of the specimen. One or more X-ray detectors may be disposed adjacent to the specimen to detect X-rays.
    Type: Grant
    Filed: May 18, 2005
    Date of Patent: May 22, 2007
    Assignee: KLA-Tencor Technologies Corporation
    Inventors: Ying Gao, Gary Janik
  • Patent number: 7187751
    Abstract: A calculating device 10 for calculating the concentration of elements contained in a sample 13 based on the FP method is provided. The calculating device 10 is operable to assume a concentration of unmeasured elements as far as unmeasured elements, of which fluorescent X-rays are not measured, are concerned, and, also, to utilize, in place of the secondary X-rays emanating from the unmeasured elements contained in the sample, scattered X-rays of the primary X-rays at least equal in number to the number of the unmeasured elements, of which concentrations are assumed, and including scattered X-rays of different wavelengths before they are scattered from the sample.
    Type: Grant
    Filed: May 11, 2006
    Date of Patent: March 6, 2007
    Assignee: Rigaku Industrial Corporation
    Inventors: Naoki Kawahara, Shinya Hara, Makoto Doi
  • Patent number: 7184517
    Abstract: An analytical method for determining crystallographic phases of a measuring sample comprises the steps of acquiring a diffraction pattern of the measuring sample and qualitative phase analysis of the measured diffraction pattern, acquiring an element spectrum of the measuring sample and determining concentrations of chemical elements in the measuring sample from the acquired element spectrum, and carrying out a quantitative phase analysis of the measuring sample on the basis of the measured intensities of the acquired diffraction pattern thereby taking into consideration determined element concentrations as a boundary condition, wherein differences between calculated and measured intensities of the diffraction pattern and between calculated and determined element concentrations are simultaneously minimized in an iterative process. The inventive method permits quantitative phase determination with high reliability.
    Type: Grant
    Filed: September 30, 2004
    Date of Patent: February 27, 2007
    Assignee: Bruker AXS GmbH
    Inventor: Arnt Kern
  • Patent number: 7166838
    Abstract: An x-ray metrology system includes an e-beam generator to cause a test sample to emit x-rays, x-ray optics for focusing the x-rays, and an x-ray imager to generate an image of the test sample from the focused x-rays. Because the x-ray imager provides a direct representation of the x-ray emission characteristics of the test sample, the resolution of a measurement taken using such a sensor is limited only by the resolution of the sensor (and any focusing optics), rather than by the amount of e-beam spread in the thin film. The x-ray imaging can be performed for object planes at the test sample that are not parallel to the test sample, thereby allowing vertical dimension data to be accurately generated by the x-ray imaging system.
    Type: Grant
    Filed: May 23, 2005
    Date of Patent: January 23, 2007
    Assignee: KLA-Tencor Technologies Corporation
    Inventor: Gary R. Janik
  • Patent number: 7095822
    Abstract: This invention pertains to an x-ray microprobe that can be placed very close the sample surface. A practical implementation is an x-ray target material integrated to an atomic force microscope (AFM) tip and an electron beam is focused to the target materials to generate x-ray emission. This microprobe can be combined with energy-resolved detector or a fluorescence imaging system for material analysis applications.
    Type: Grant
    Filed: July 28, 2005
    Date of Patent: August 22, 2006
    Assignee: Xradia, Inc.
    Inventor: Wenbing Yun
  • Patent number: 7049590
    Abstract: A method of reducing atom ejection from a sample during electron beam bombardment. An electron beam is directed through a low pressure environment toward a surface of the sample. The electron beam thereby impinges on the sample at a target location, and thereby causes characteristic x-ray emission from the target location of the sample. A capping precursor is introduced into the low pressure environment, where the capping precursor forms a capping layer on the surface of the sample at the target location when contacted by the electron beam. The capping layer thereby reduces atom ejection from the sample at the target location, while not appreciably impeding and confounding the characteristic x-ray emission from the target location of the sample.
    Type: Grant
    Filed: October 28, 2004
    Date of Patent: May 23, 2006
    Assignee: KLA-Tencor Technologies Corporation
    Inventor: David Aitan Soltz
  • Patent number: 6975894
    Abstract: The invention provides method, system and device for determining trabecular bone structure and strength by digital topological analysis, and offers, for the first time, a demonstration of superior associations between vertebral deformity and a number of architectural indices measured in the distal radius, thus permitting reliable and noninvasive detection and determination of the pathogenesis of osteoporosis. A preferred embodiment provides imaging in three dimension of a region of trabecular bone, after which the 3D image is converted into a skeletonized surface representation. Digital topological analysis is applied to the converted image, and each image voxel is identified and classified as a curve, a surface, or a junction; and then associated with microarchitectural indices of trabecular bone to quantitatively characterize the trabecular bone network. The invention is applicable in vivo, particularly on human subjects, or ex vivo.
    Type: Grant
    Filed: April 11, 2002
    Date of Patent: December 13, 2005
    Assignee: Trustees of the University of Pennsylvania
    Inventors: Felix W. Wehrli, Punam K. Saha, Bryon Roos Gomberg
  • Patent number: 6885727
    Abstract: An apparatus determines the thickness and composition of a multi-layered sample comprised of at least a copper layer and a tin-copper alloy plating layer disposed on the copper layer. The sample is irradiated with primary X-rays and an energy-dispersive X-ray detector detects fluorescent X-rays and diffracted X-rays emitted from the sample. An X-ray spectrum of the detected fluorescent X-rays and diffracted X-rays is generated. The concentration of copper in the tin-copper alloy plating layer of the sample is determined utilizing peak intensities of the diffracted X-rays in the X-ray spectrum. The thickness of the tin-copper alloy plating layer of the sample is determined utilizing peak intensities of the fluorescent X-rays in the X-ray spectrum and the determined copper concentration.
    Type: Grant
    Filed: August 6, 2002
    Date of Patent: April 26, 2005
    Assignee: SII NanoTechnology Inc.
    Inventor: Koichi Tamura
  • Patent number: 6858148
    Abstract: The method for screening binding between a target binder and potential pharmaceutical chemicals involves sending a solution (preferably an aqueous solution) of the target binder through a conduit to a size exclusion filter, the target binder being too large to pass through the size exclusion filter, and then sending a solution of one or more potential pharmaceutical chemicals (preferably an aqueous solution) through the same conduit to the size exclusion filter after target binder has collected on the filter. The potential pharmaceutical chemicals are small enough to pass through the filter. Afterwards, x-rays are sent from an x-ray source to the size exclusion filter, and if the potential pharmaceutical chemicals form a complex with the target binder, the complex produces an x-ray fluorescence signal having an intensity that indicates that a complex has formed.
    Type: Grant
    Filed: July 16, 2003
    Date of Patent: February 22, 2005
    Assignee: The Regents of the University of California
    Inventors: Benjamin P. Warner, George J. Havrilla, Thomasin C. Miller, Cyndi A. Wells
  • Patent number: 6856827
    Abstract: A system for surgical imaging and display of tissue structures of a patient, including a display and an image processor for displaying such images in coordination with a tool image to facilitate manipulation of the tool during the surgical procedure. The system is configured for use with a fluoroscope such that at least one image in the display is derived from the fluoroscope at the time of surgery. A fixture is affixed to an imaging side of the fluoroscope for providing patterns of an of array markers that are imaged in each fluoroscope image. A tracking assembly having a plurality of tracking elements is operative to determine positions of said fixture and the patient. One of the tracking elements is secured against motion with respect to the fixture so that determining a position of the tracking element determines a position of all the markers in a single measurement.
    Type: Grant
    Filed: December 2, 2002
    Date of Patent: February 15, 2005
    Assignee: GE Medical Systems Global Technology Company, LLC
    Inventors: Teresa Seeley, Faith Lin, Tina Kapur, Gene Gregerson
  • Patent number: 6856826
    Abstract: A method for surgical imaging and display including (i.) positioning a defined set of markers disposed in a pattern so as to be imaged in each pose or view of an imaging assembly, the set of markers being fixed in pre-determined positions in a rigid carrier, (ii.) securing a first tracking element against motion with respect to the rigid carrier so that determining a position of the first tracking element in a single measurement determines positions of all the markers of the set, and (iii.) identifying images of at least a subset of the markers in a first view.
    Type: Grant
    Filed: November 15, 2002
    Date of Patent: February 15, 2005
    Assignee: GE Medical Systems Global Technology Company, LLC
    Inventors: Teresa Seeley, Faith Lin, Tina Kapur, Gene Gregerson
  • Patent number: 6798863
    Abstract: In order to provide a single, small apparatus capable of elemental and structural analysis of inorganic matter by utilizing X-rays having non-obstructive and non-contact characteristics there is provided a small, energy distribution type X-ray detector for detecting X-ray fluorescence and subjecting the X-ray fluorescence to elemental and quantative analysis, and a CCD line sensor for performing structural analysis. An X-ray tube target structure that is a Cu layer on an Mo layer is adopted. When excitation is performed using a low accelerating voltage, this is made monochromatic by using a Cu filter to filter the Cu—K lines and the continuous X-rays generated, with the radiation quality (Cu—K lines) thus generated then being utilized in X-ray diffraction.
    Type: Grant
    Filed: May 16, 2002
    Date of Patent: September 28, 2004
    Assignee: SII NanoTechnology Inc.
    Inventor: Masao Sato
  • Patent number: 6765986
    Abstract: An x-ray fluorescence analyzer and method. The analyzer and method use a single radio-active source, such as, 241Am to determine the composition of a metal alloy or precious metal. The method compensates for Rayleigh scattering by first determining a scaling factor using a particular energy line in the spectrum of the test material and comparing that line to the same energy line for a pure metal. Based on the scaling factor the energy spectrum for the pure is compensated and then subtracted from the energy spectrum of the test material at discrete points.
    Type: Grant
    Filed: February 4, 2002
    Date of Patent: July 20, 2004
    Assignee: Niton Corporation
    Inventors: Lee Grodzins, Hal Grodzins
  • Publication number: 20040052330
    Abstract: The present invention relates to the calibration and alignment of an X-ray reflectometry (“XRR”) system for measuring thin films. An aspect of the present invention describes a method for accurately determining C0 for each sample placement and for finding the incident X-ray intensity corresponding to each pixel of a detector array and thus permitting an amplitude calibration of the reflectometer system. Another aspect of the present invention relates to a method for aligning an angle-resolved X-ray reflectometer that uses a focusing optic, which may preferably be a Johansson crystal. Another aspect of the present invention is to validate the focusing optic. Another aspect of the present invention relates to the alignment of the focusing optic with the X-ray source. Another aspect of the present invention concerns the correction of measurements errors caused by the tilt or slope of the sample.
    Type: Application
    Filed: August 19, 2003
    Publication date: March 18, 2004
    Inventors: Louis N. Koppel, Craig E. Uhrich, Jon Opsal
  • Patent number: 6670200
    Abstract: Methods and apparatus are disclosed for detecting a thickness of a surficial layer (e.g., metal or insulating layer) on a workpiece (e.g., semiconductor wafer) during a process for planarizing the layer, so as to stop the process when a suitable process endpoint is reached. Layer thickness is detected based on a spectral-characteristic signal of reflected or transmitted signal light, obtained by directing a probe light onto the surface of the workpiece. Example spectral characteristics are local maxima and minima of signal-light waveform, differences or quotients of the same, a dispersion of the signal-light waveform, a component of a Fourier transform of the signal waveform, a cross-correlation function of the signal waveform. Alternatively, the zeroth order of signal light is selected for measurement, or a spatial coherence length of the probe light is compared with the degree of fineness of the pattern on the surface illuminated with the probe light.
    Type: Grant
    Filed: June 13, 2001
    Date of Patent: December 30, 2003
    Assignee: Nikon Corporation
    Inventors: Yoshijiro Ushio, Takehiko Ueda
  • Patent number: 6646263
    Abstract: Samples such as semiconductor wafers may be subjected to an elementary analysis by irradiation by means of electrons and measurement of the X-rays 30 generated in the sample. In order to achieve a high spatial resolution, two adjacent holes 6, 8 are formed in the sample surface, leaving a very thin separating wall 10 between said holes and hence limiting the dimension of the interaction volume 24. However, electrons pass through the wall, thus generating disturbing X-rays in the walls of the hole 8 behind the wall. According to the invention the hole 8 behind the separating wall 10 is provided with a stopping material 12 of an elementary composition which deviates from that of the wall 10. If the wall to be analyzed contains silicon, the stopping material 12 should preferably be platinum or carbon.
    Type: Grant
    Filed: April 16, 2002
    Date of Patent: November 11, 2003
    Assignee: FEI Company
    Inventors: Laurens Franz Taemsz Kwakman, Kars Zege Troost