Carbide Containing Patents (Class 419/14)
  • Patent number: 7163657
    Abstract: A sintered cemented carbide body (e.g., a cutting tool) and a method of making the same. The sintered cemented carbide body includes tungsten carbide, a binder phase of at least one metal of the iron group or an alloy thereof, and one or more solid solution phases. Each one of the solid solution phases has at least one of the carbides and carbonitrides of a combination of zirconium, niobium, and tungsten. The method includes the steps of providing a powder mixture that contains tungsten carbide, a binder metal powder comprising at least one metal of the iron group or an alloy thereof, and at least one of the carbides and carbonitrides of both zirconium and niobium including a powder of the carbides or carbonitrides of zirconium and niobium, forming a green compact of said powder mixture, and vacuum sintering or sinter-HIP said green compact at a temperature of from 1400 to 1560° C.
    Type: Grant
    Filed: December 3, 2003
    Date of Patent: January 16, 2007
    Assignee: Kennametal Inc.
    Inventors: Hans-Wilm Heinrich, Manfred Wolf, Dieter Schmidt
  • Patent number: 7097685
    Abstract: A cemented carbide comprises a binder phase consisting essentially of an iron family metal, a first hard phase consisting essentially of WC having a hexagonal crystal structure, and a second hard phase consisting essentially of one or more types of a compound of a metal or metals of group 4, 5 or 6 of the periodic table having an NaCl-type cubic crystal structure. The cemented carbide is formed by a surface region with a thickness of 2 to 50 ?m consisting of the binder phase and the first hard phase, and an inner region present underneath the surface region consisting of the binder phase, the first hard phase and the second hard phase. A ratio of an average grain size of the first hard phase in the surface region to an average grain size of the first hard phase in the inner region is 1 or less, and a ratio of an area of the binder phase in the surface region to an area of the binder phase in the inner region is greater than 1.
    Type: Grant
    Filed: August 25, 2004
    Date of Patent: August 29, 2006
    Assignee: Tungaloy Corporation
    Inventors: Hiroyuki Miura, Satoshi Kinoshita
  • Patent number: 7087202
    Abstract: This invention concerns particulate reinforced Al-based composites, and the near net shape forming process of their components. The average size of the reinforced particle in the invented composites is 0.1–3.5 ?m and the volume percentage is 10–40%, and a good interfacial bonding between the reinforced particulate and the matrix is formed with the reinforced particles uniformly distributed. The production method of its billet is to have the reinforced particles and Al-base alloy powder receive variable-speed high-energy ball-milling in the balling drum. Then, with addition of a liquid surfactant, the ball-mill proceeds to carry on ball-milling. After the ball-milling, the produced composite powder undergoes cold isostatic pressing and the subsequent vacuum sintering or vacuum hot-pressing to be shaped into a hot compressed billet, which in turn undergoes semisolid thixotropic forming and may be shaped into complex-shaped components. These components can be used in various fields.
    Type: Grant
    Filed: July 28, 2003
    Date of Patent: August 8, 2006
    Assignees: ASM Assembly Automation Ltd., General Research Institute for Non-Ferrous Metals
    Inventors: Deming Liu, Chou Kee Peter Liu, Jian Zhong Fan, Jun Xu, Tao Zuo, Zhao Zu Gao
  • Patent number: 7074247
    Abstract: There is provided a method of making a composite abrasive compact which comprises an abrasive compact bonded to a substrate. The abrasive compact will generally be a diamond compact and the substrate will generally be a cemented carbide substrate. The composite abrasive compact is made under known conditions of elevated temperature and pressure suitable for producing abrasive compacts. The method is characterised by the mass of abrasive particles from which the abrasive compact is made. This mass has three regions which are: (i) an inner region, adjacent the surface of the substrate on which the mass is provided, containing particles having at least four different average particle sizes; (ii) an outer region containing particles having at least three different average particle sizes; and (iii) an intermediate region between the first and second regions.
    Type: Grant
    Filed: October 15, 2001
    Date of Patent: July 11, 2006
    Inventors: Klaus Tank, Moosa Mahomed Adia, Roy Derrick Achilles, Paul Machael Daniel
  • Patent number: 6960319
    Abstract: Disclosed is a flow-softening tungsten alloy having the general formula: W100-pAiBjCkDe wherein W is tungsten; A is one or more elements selected from the group consisting of nickel, iron, chromium and cobalt; B is in or more elements selected from the group consisting of molybdenum, niobium and tantalum; C is one or more of the elements selected from the groups consisting of titanium and aluminum; D is one or more elements selected from the group consisting of boron, carbon, and silicon; i is from about 5 to about 8 weight percent; j is from 0 to about 4 weight percent; k is from about 0.1 to about 4 weight percent; 1 is from 0 to about 0.1 weight percent; and p is greater than or equal to about 7 weight percent and less than or equal to about 20 weight percent. In this alloy p is approximately equal to the sum of i, j, k and 1. A method of preparing this alloy and a kinetic energy penetrator manufactured from it are also disclosed.
    Type: Grant
    Filed: October 27, 1995
    Date of Patent: November 1, 2005
    Assignee: The United States of America as represented by the Secretary of the Army
    Inventor: Deepak Kapoor
  • Patent number: 6951579
    Abstract: A sintered alloy for valve seats is comprised of carbon at 1 to 2 percent by weight, chromium at 3.5 to 4.7 percent by weight, molybdenum at 4.5 to 6.5 percent by weight, tungsten at 5.2 to 7.0 percent by weight, vanadium at 1.5 to 3.2 percent by weight, and the remainder of iron and unavoidable impurities. Enstatite particles at 1 to 3 percent by weight, hard alloy particles (A) with a Vickers hardness of 500 to 900 at 15 to 25 percent by weight, and hard alloy particles (B) with a Vickers hardness of 1000 or more at 5 to 15 percent by weight (A+B=35 percent by weight or less) are dispersed in the matrix of the sintered alloy skeleton distributed with carbide. Copper or copper alloy at 15 to 20 percent by weight is infiltrated into pores of the skeleton.
    Type: Grant
    Filed: February 24, 2003
    Date of Patent: October 4, 2005
    Assignee: Teikoku Piston Ring Co., Ltd.
    Inventor: Yoshio Koyama
  • Patent number: 6946096
    Abstract: A method for making aerospace face seal rotors reinforced by rhenium metal, alloy, or composite in combination with silicon carbide or other ceramic. The resulting rotor also is disclosed. Ceramic grains, preferably silicon carbide (SiC), are mixed with powdered metallic (PM) binder that may be based on a refractory metal, preferably rhenium. The mixture is applied to a rotor substrate. The combined ceramic-metal powder mixture is heated to sintering temperature under pressure to enable fusion of the ceramic in the resulting metal-based substrate. A load may then be applied under an elevated temperature. The resulting coated rotor can exhibit high hot hardness, increased durability and/or high hot wear resistance, as well as high thermal conductivity.
    Type: Grant
    Filed: May 15, 2003
    Date of Patent: September 20, 2005
    Assignee: Honeywell International, Inc.
    Inventors: William L. Giesler, Robbie J. Adams
  • Patent number: 6921422
    Abstract: This invention relates to a ductile binder phase for use with AlMgB14 and other hard materials. The ductile binder phase, a cobalt-manganese alloy, is used in appropriate quantities to tailor good hardness and reasonable fracture toughness for hard materials so they can be used suitably in industrial machining and grinding applications.
    Type: Grant
    Filed: September 23, 2003
    Date of Patent: July 26, 2005
    Assignee: Iowa State University Research Foundation, Inc.
    Inventors: Bruce A. Cook, Alan Russell, Joel Harringa
  • Patent number: 6918943
    Abstract: A machining surface of a machining tool such as a drill is composed of a metal-rich section. A ceramics-rich section is formed centrally in the drill. Further, a gradient section is provided between the ceramics-rich section and the metal-rich section. In the gradient section, the composition ratio of metal is gradually increased from the ceramics-rich section to the metal-rich section. That is, the drill is composed of the gradient composite material in which the composition ratio of ceramics is increased and the composition ratio of metal is decreased inwardly from the machining surface.
    Type: Grant
    Filed: December 12, 2001
    Date of Patent: July 19, 2005
    Assignee: Honda Giken Kogyo Kabushiki Kaisha
    Inventors: Mitsuo Kuwabara, Masanori Ohtsuka
  • Patent number: 6916355
    Abstract: A composite material 5 in which a dispersing material 7 is dispersed in a matrix 6 is provided. The composite material 5 is producible by steps of filling said mixed material in a space forming region to be defined by at least two container elements when said at least two container elements are integrated into one body, and then infiltrating said aluminum (Al) being molten due to heat generated by said self-combustion reaction into pores inside said mixed material through at least one hole formed in an upper part of a reaction container formed by combining said at least two container elements in which said mixed material is filled in said space forming region in a state being fixed to a predetermined shape, thereby an aluminide intermetallic compound is formed by self-combustion reaction between said metal powder and said aluminum (Al), and a dispersing material is dispersed into said matrix.
    Type: Grant
    Filed: November 19, 2002
    Date of Patent: July 12, 2005
    Assignee: NGK Insulators, Ltd.
    Inventors: Masahiro Kida, Takahiro Ishikawa, Masayuki Shinkai, Takatoshi Ikematsu
  • Patent number: 6899844
    Abstract: A method of producing a fine TiC particle-dispersing type Al—Sn based aluminum alloy includes the steps of: preparing either Al mother-alloy or metallic raw materials of the Al alloy and a green compact, in which TiC is dispersed; melting the Al mother-alloy or the metallic raw materials of the Al alloy to form an Al alloy melt; bringing the Al alloy melt and the green compact, in which TiC is dispersed, into contact with one another, thereby dispersing the TiC in the Al-alloy melt; casting the Al alloy melt, in which TiC is dispersed, into an aluminum-alloy ingot, in which TiC is dispersed; and rolling the aluminum-alloy ingot.
    Type: Grant
    Filed: April 4, 2003
    Date of Patent: May 31, 2005
    Assignees: Taiho Kogyo Co., Ltd., Toyota Jidosha Kabushiki Kaisha
    Inventors: Toru Desaki, Soji Kamiya, Kazuaki Sato, Yukio Okouchi, Tetsuya Nukami
  • Patent number: 6872356
    Abstract: The residual stresses that are experienced in polycrystalline diamond cutters, which lead to cutter failure, can be effectively modified by selectively thinning the carbide substrate subsequent to high temperature, high pressure (sinter) processing, by selectively varying the material constituents of the carbide substrate, by subjecting the PDC cutter to an annealing process during sintering, by subjecting the formed PDC cutter to a post-process stress relief anneal, or a combination of those means.
    Type: Grant
    Filed: November 15, 2002
    Date of Patent: March 29, 2005
    Assignee: Baker Hughes Incorporated
    Inventors: Trent N. Butcher, Ralph M. Horton, Stephen R. Jurewicz, Danny E. Scott, Redd H. Smith
  • Patent number: 6852275
    Abstract: There is provided a process for producing an intermetallic compound-based composite material containing a reinforcing material and an intermetallic compound. The process includes infiltrating a metal powder into the gaps of a reinforcing material to form a preform and impregnating the preform with an Al melt to give rise to a spontaneous combustion reaction between the metal powder and the Al melt to convert the Al melt into an aluminide intermetallic compound. The Al melt and the metal powder are used in such amounts that they do not remain after the spontaneous combustion reaction. The process can produce an intermetallic compound-based composite material of large size and complicated shape in reduced steps.
    Type: Grant
    Filed: May 23, 2001
    Date of Patent: February 8, 2005
    Assignee: NGK Insulators, Ltd.
    Inventor: Masahiro Kida
  • Patent number: 6840978
    Abstract: A porous metal body having a foam structure of 500 ?m or less in average pore diameter, wherein the skeleton is composed of an alloy primarily including Fe and Cr, and Cr carbide or FeCr carbide is uniformly dispersed in the texture. The metal porous body is produced by preparing a slurry primarily containing an Fe oxide powder having an average particle diameter of 5 ?m or less, at least one powder selected from metallic Cr, Cr alloys, and Cr oxides, a thermosetting resin, and a diluent, applying a coating of this slurry to a resin core body having a foam structure, performing drying, and thereafter, performing firing in a non-oxidizing atmosphere so as to produce a metal porous body having the aforementioned skeleton structure.
    Type: Grant
    Filed: April 25, 2002
    Date of Patent: January 11, 2005
    Assignee: Sumitomo Electric Industries, Ltd.
    Inventors: Takahiro Matsuura, Keizo Harada
  • Publication number: 20040234407
    Abstract: The present invention concerns a powder metal composition for producing powder metal components comprising a Co-based pre-alloyed powder, with irregularly shaped particles comprising at least 15% by weight Cr and less than 0.3% by weight C, admixed with graphite.
    Type: Application
    Filed: March 17, 2004
    Publication date: November 25, 2004
    Applicant: HOGANAS AB
    Inventors: Christophe Szabo, Owe Mars
  • Patent number: 6814775
    Abstract: A sintered cubic boron nitride (cBN) compact for use in a tool is composed of between about 60 and 80 vol-% cBN having a volumetric mean particle size of between about 3 to 6 &mgr;m and between about 40 and 20 vol-% of a ceramic binder phase. The ceramic binder is composed of between about 20 and 60 vol-% of one or more of a carbide, nitride, or boride of a Group IVB or VIB metal, and between about 40 and 80 vol-% of one or more of carbides, nitrides, borides, or oxides of aluminum. The cBN compact additionally contains between about 3 and 15 wt-% tungsten. The cBN compacts are especially useful in machining iron and like chemically reactive parts, especially where such parts are powder metal parts.
    Type: Grant
    Filed: May 14, 2003
    Date of Patent: November 9, 2004
    Assignee: Diamond Innovations, Inc.
    Inventors: Robert Dean Scurlock, Stephen Lee Dole
  • Patent number: 6802883
    Abstract: An iron-based sintered alloy, which consists of from 0.5 to 5% of Ni, from 0.5 to 4% of Cr, from 0.5 to 2% of C, the balance being Fe and unavoidable impurities, and which has a micro-structure comprising an iron-based matrix containing Ni and a part of Cr as solutes and carbides containing the other part of Cr and dispersed in the matrix. The iron-based sintered alloy is appropriate for use as a valve seat of an internal combustion engine. Wear resistance is maintained at a moderate level while the additive amount of alloying elements is decreased to attain low cost.
    Type: Grant
    Filed: March 10, 2003
    Date of Patent: October 12, 2004
    Assignee: Kabushiki Kaisha Riken
    Inventors: Hiroji Henmi, Akiyoshi Ishibashi
  • Publication number: 20040194576
    Abstract: To provide a sintered alloy capable of showing wear resistance and a process for producing the same as well as a valve seat of good wear resistance.
    Type: Application
    Filed: May 5, 2004
    Publication date: October 7, 2004
    Inventors: Kimihiko Ando, Hiroyuki Murase, Noriyuki Tsuge, Kunihiko Endoh, Yukiharu Tomita, Naoshi Ishihara, Masahiro Hayakawa
  • Patent number: 6773482
    Abstract: A cold work steel alloy for the manufacture of parts, comprising the elements C, Si, Mn, Cr, W, Mo, V, Nb, Co, S, N, Ni and accompanying elements in the concentration ranges recited in claim 1 and having an oxygen content of less than 100 ppm and a content of nonmetallic inclusions corresponding to a K0 value of a maximum of 3 when tested according to DIN 50 602, as well as a method of making a part of said steel alloy by powder metallurgy.
    Type: Grant
    Filed: April 9, 2002
    Date of Patent: August 10, 2004
    Assignee: Bohler Edelstahl, GmbH
    Inventors: Werner Liebfahrt, Roland Rabitsch
  • Publication number: 20040103753
    Abstract: A hard particle having improved adhesion to a base material, a wear-resistant iron-base sintered alloy, a method of manufacturing the same, and a valve seat are provided. The hard particle comprises 20% to 70% Mo by mass, 0.2% to 3% C by mass, 1% to 15% Mn by mass, with the remainder being unavoidable impurities and Co. The sintered alloy comprises, as a whole, 4% to 35% Mo by mass, 0.2% to 3% C by mass, 0.5% to 8% Mn by mass, 3% to 40% Co by mass, with the remainder being unavoidable impurities and Fe. The alloy comprises a base material component comprising 0.2% to 5% C by mass, 0.1% to 10% Mn by mass, with the remainder being unavoidable impurities and Fe. The alloy further comprises a hard particle component comprising 20% to 70% Mo by mass, 0.2% to 3% C by mass, 1% to 15% Mn by mass, with the remainder being unavoidable impurities and Co. The hard particles are dispersed in the base material in an areal ratio of 10% to 60 %.
    Type: Application
    Filed: November 5, 2003
    Publication date: June 3, 2004
    Applicant: TOYOTA JIDOSHA KABUSHIKI KAISHA
    Inventor: Kimihiko Ando
  • Patent number: 6723279
    Abstract: Golf club structures, including club heads and shafts, composed of composites comprised of a matrix of metal, such as an aluminum alloy, or a plastic material and a fiber such as graphite or a ceramic, which may be whiskerized, and which may also be selectively weighted as in the toe and heel of a club head, with heavy particles such as tungsten metal. The club structure may also be surface hardened by applying a coating of fullerenes to a metal club structure and heat treating it to produce a hard coating of metal carbide, preferably by coating a titanium golf club structure with fullerenes and heat treating the coated structure to produce a titanium carbide surface.
    Type: Grant
    Filed: March 15, 1999
    Date of Patent: April 20, 2004
    Assignee: Materials and Electrochemical Research (MER) Corporation
    Inventors: James C. Withers, Raouf O. Loutfy, Sion M. Pickard, Kenneth J. Newell, William B. Kelly
  • Patent number: 6723387
    Abstract: A thermal spray method for the fabrication of ceramic/metal and ceramic/ceramic hardcoating for wear applications. The method makes use of feedstock powder, composed of micron-scale aggregates of hard phase material particles that are either mixed or coated with a readily fusible nano-scale binder phase material. Thus, during thermal spraying, the nanostructured material undergoes rapid melting while the aggregated material is heated but not necessarily melted. A dense coating is formed when the molten nano-material fills the available pore spaces between the heated and softened aggregates, providing a strong and tough matrix for the consolidated material. Optimal wear properties are achieved when the volume fraction of aggregated particles is high, typically in the range of 0.5-0.9. Aggregated material may be composed of one, two or more particles of difference sizes and/or compositions, with particle size distribution that gives high packing density for the hard phase.
    Type: Grant
    Filed: September 19, 2002
    Date of Patent: April 20, 2004
    Assignee: Rutgers University
    Inventors: Bernard H. Kear, Ganesh Skandan
  • Publication number: 20040067153
    Abstract: A carbon nano material is mixed with a metal material in a powder state. A resultant mixed material is compressed by a hot press and molded to granules. The metal in the granules are melted, blended and thus obtained composite material is injected into and fill a mold to form a composite metal product comprising the carbon nano material and the metal material. With the above process, it is possible to injection mold said granules to obtain the composite metal product to which the characteristics of the carbon nano material are applied.
    Type: Application
    Filed: August 21, 2003
    Publication date: April 8, 2004
    Inventors: Atsushi Koide, Kiyoto Takizawa, Yoshitoshi Yamagiwa, Masashi Suganuma, Mamoru Miyagawa
  • Publication number: 20040060390
    Abstract: A method of production of large Ingots of neutron attenuating composites using a vacuum-bellows system allows for large cross-sectional shapes to be extruded and rolled. This method uses a vacuum-bellows technology which allows the manufacturing of large 8-16 inch diameter ingots (50-450 lbs. each). A variety of primary metal matrix materials can be used in this technology. High specific strength and stiffness can be achieved because the technology allows for final densities of 99% and higher. The vacuum-bellows technology allows metals and ceramics to blend and mesh together at compression pressures of 800 tons with elevated temperatures. The controlled compression movement allows for any oxide layer, on the metal, to be broken up and consolidated with the chosen ceramic particulate. One application is to blend boron-rich ceramics and high purity (99.5-99.99%) aluminum particulates together and produce a large ingot using this vacuum-bellows technology.
    Type: Application
    Filed: September 9, 2002
    Publication date: April 1, 2004
    Inventor: Robin A. Carden
  • Patent number: 6712871
    Abstract: A sintered alloy composition for automotive engine valve seats, and a method for producing the same, are described. An iron base sintered alloy composition comprising vanadium carbide particles, Fe—Co—Ni—Mo alloy particles, and Cr—W—Co—C alloy particles in which the composition is dispersed in a structure of sorbite is particularly suitable for use as materials of valve seats for automotive engines which requires excellent wear resistance, high-performance, high-rotation-speed, and low-fuel-consumption.
    Type: Grant
    Filed: August 29, 2002
    Date of Patent: March 30, 2004
    Assignee: Hyundai Motor Company
    Inventor: Jung Seok Oh
  • Publication number: 20040025631
    Abstract: An abrasive and wear resistant material comprises a mass of carbide particles, a mass of cubic boron nitride particles, and a bonding metal or alloy, bonded into a coherent, sintered form. The cubic boron nitride particle content of the material is from 10% to 18% inclusive by weight, the particle size of the cubic boron nitride is less than 20 micron or less, and the material is substantially free of hexagonal boron nitride. The abrasive material is of particular use in tool components or inserts for application in the abrading of wood and other lignocellulosic materials.
    Type: Application
    Filed: September 4, 2003
    Publication date: February 12, 2004
    Inventors: Robert Fries, Peter Michael Harden
  • Patent number: 6682579
    Abstract: Metallurgical powder compositions are provided that include silicon carbide to enhance the strength, ductility, and machine-ability of the compacted and sintered parts made therefrom. The compositions generally contain a metal powder, such as an iron-based powder, that constitutes the major portion of the composition. A silicon carbide-containing powder is blended with the metal powder, preferably in the form of a silicon carbide powder. Optionally, common alloying powders, lubricants, binding agents, and other powder metallurgy additives can be blended into the metallurgical composition. The metallurgical powder composition is used by compacting it in a die cavity to produce a “green” compact that is then sintered, preferably at relatively high temperatures.
    Type: Grant
    Filed: November 5, 2001
    Date of Patent: January 27, 2004
    Assignee: Hoeganaes Corporation
    Inventors: Kalathur S. Narasimhan, Nikhilesh Chawla
  • Publication number: 20040013556
    Abstract: The invention concerns a method for making thin films in metal/ceramic composite, characterised in that it consists in a) preparing a suspension (S) in an organic solvent from a substantially homogeneous mixture of ceramic reinforcements of metal particles, a binder, a plasticizing agent and an organic dispersant, the metal particles constituting at least 5 wt. % of the suspension; b) tape casting the suspension (S) to form a thing film (B), then climinating organic compounds contained in the binder and the plasticizing agent from said thin film; c) densifying the thin film from which said organic compounds have been removed in an oven.
    Type: Application
    Filed: June 4, 2003
    Publication date: January 22, 2004
    Inventors: Jean-Francois Silvain, Thierry Chartier, Pierre-Marie Geffroy
  • Publication number: 20040009088
    Abstract: A component is produced by powder metallurgy from hard metal. The alloy includes at least one grain growth-inhibiting additive from the group consisting of V, Cr, Ti, Ta and Nb with, at least locally, a graduated concentration profile. As a result, the mechanical properties also have a graduated profile. In the fabrication process, a dispersion or solution which contains the grain growth-inhibiting additive in finely distributed or dissolved form is applied to the surface of a green compact. Penetration of this dispersion or solution along open pores leads to a graduated distribution of the grain growth-inhibiting additive in the green compact. There is also described a process in which the grain growth-inhibiting additive in the form of a solution is distributed uniformly in the green compact and is then gradually broken down from edge regions by a heat treatment or a solvent.
    Type: Application
    Filed: April 17, 2003
    Publication date: January 15, 2004
    Inventors: Johannes Glatzle, Rolf Kosters, Wolfgang Glatzle
  • Patent number: 6676893
    Abstract: The presently claimed invention relates to a method of making a PcBN cutting tool insert. The method includes the following steps: mixing raw material powders, (e.g., cBN, hBN, TiC, TiN, Ti(C,N), WC, W, C, Co, Co2Al9, Al AlN, Al2O3) with a liquid (e.g., ethanol) and an agent (e.g., polyethylene glycol, PEG) to form a homogeneous slurry with the desired composition; forming spherical powder agglomerates, typically 100 &mgr;m in diameter, preferably by spray drying; pressing said agglomerates to form a body of desired dimensions and density using conventional tool pressing technology; removing the agent from the powder at a suitable temperature and atmosphere; raising the temperature to 1000-1350° C. in vacuum; solid state sintering the body at 1000-1350° C. in vacuum, for 1-90 minutes to form a body with 35-55 vol % porosity; optionally, adding 0.
    Type: Grant
    Filed: April 25, 2002
    Date of Patent: January 13, 2004
    Assignee: Sandvik AB
    Inventors: Ulf Rolander, Gerold Weinl
  • Publication number: 20030230164
    Abstract: An iron-based sintered alloy, which consists of from 0.5 to 5% of Ni, from 0.5 to 4% of Cr, from 0.5 to 2% of C, the balance being Fe and unavoidable impurities, and which has a micro-structure comprising an iron-based matrix containing Ni and a part of Cr as solutes and carbides containing the other part of Cr and dispersed in the matrix. The iron-based sintered alloy is appropriate for use as a valve seat of an internal combustion engine. Wear resistance is maintained at a moderate level while the additive amount of alloying elements is decreased to attain low cost.
    Type: Application
    Filed: March 10, 2003
    Publication date: December 18, 2003
    Inventors: Hiroji Henmi, Akiyoshi Ishibashi
  • Patent number: 6652616
    Abstract: In accordance with the method according to the present invention, particles consisting of ferrotitanium, ferroniobium or ferrovanadium are dispersed and hot compacted in a metal matrix powder consisting of hardening steel or heat-resistant alloys. In so doing, titanium, niobium or vanadium carbide is obtained in situ by a solid-state reaction, i.e. without melting, from the carbon admixed or contained in the matrix powder and the ferroalloy particles. Carbon can also be absorbed from the gaseous phase and it may be substituted by nitrogen. This method permits a reasonably-priced introduction of hard particles into the composite material, the hard particles having a size that is necessary as a protection against scoring wear.
    Type: Grant
    Filed: May 28, 2002
    Date of Patent: November 25, 2003
    Assignee: Maschienfabrik Koppern GmbH & Co. KG
    Inventors: Hans Berns, Birgit Wewers
  • Patent number: 6641776
    Abstract: X-ray imageable articles, for instance surgical implements or parts therefore which are used in minimally invasive surgical procedures, may be prepared by a process including the steps of: (a) preparing a mixture composition comprising: i) radiolucent particulate material selected from ceramic materials, metallurgic materials, and combinations thereof and having a particulate size of no more than 40 microns, ii) radiopaque particulate material selected from ceramic materials, metallurgic materials, and combinations thereof and having a particulate size of no more than 40 microns, and (iii) at least one polymeric binder material; (b) injection molding the mixture composition into a preform; (c) optionally removing the binder material from the preform; and (d) sintering the preform.
    Type: Grant
    Filed: November 15, 2000
    Date of Patent: November 4, 2003
    Assignee: SciMed Life Systems, Inc.
    Inventors: Timothy J. Weaver, Dion Mraz
  • Patent number: 6638474
    Abstract: A coated cemented carbide tool, and a method for making the same, wherein the as-sintered substrate is formed by sintering in an atmosphere having at least a partial pressure and for a part of the time a nitrogen partial pressure.
    Type: Grant
    Filed: March 19, 2001
    Date of Patent: October 28, 2003
    Assignee: Kennametal Inc.
    Inventors: Yixiong Liu, Donald A. Botbyl, George P. Grab, Mark S. Greenfield
  • Patent number: 6635098
    Abstract: A low cost titanium, titanium alloy material, or Ti matrix composite comprising clean and divided titanium turnings that are blended with titanium, titanium alloy powder, and/or ceramic powder and consolidated is provided. A method of making the material is also provided. The low cost material is formed into preshapes, such as a billet, which is subsequently used as feedstock for extrusion, forging, casting, or rolling.
    Type: Grant
    Filed: February 12, 2002
    Date of Patent: October 21, 2003
    Assignee: Dynamet Technology, Inc.
    Inventors: Stanley Abkowitz, Susan M. Abkowitz, Harold L. Heussi, Kevin M. McCarthy
  • Patent number: 6630008
    Abstract: Objects comprising carbide particulate having pressure consolidated nanocrystalline coating material are formed. Oxides of the coating material, in particulate form, may become dispersed in the pressure consolidated object, thereby increasing its strength.
    Type: Grant
    Filed: September 18, 2000
    Date of Patent: October 7, 2003
    Assignee: Ceracon, Inc.
    Inventors: Henry S. Meeks, III, Marc S. Fleming
  • Publication number: 20030170137
    Abstract: Although MIM (metal injection molding) has received widespread application, aluminum has not been widely used for MIM in the prior art because of the tough oxide layer that grows on aluminum particles, thus preventing metal-metal bonding between the particles. The present invention solves this problem by adding a small amount of material that forms a eutectic mixture with aluminum oxide, and therefore aids sintering, to reduce the oxide, thereby allowing intimate contact between aluminum surfaces. The process includes the ability to mold and then sinter the feedstock into the form of compacted items of intricate shapes, small sizes (if needed), and densities of about 95% of bulk.
    Type: Application
    Filed: March 11, 2002
    Publication date: September 11, 2003
    Applicant: Advanced Materials Technologies Pte Ltd.
    Inventors: Chee-Tian Yeo, Lye-King Tan
  • Publication number: 20030155041
    Abstract: A method for densification of the surface layer of an optionally sintered powder metal component comprising the steps of: decarburizing the surface layer for softening the surface layer of the component; and densifying the surface layer of the component.
    Type: Application
    Filed: January 28, 2003
    Publication date: August 21, 2003
    Inventors: Sven Bengtsson, Yang Yu, Martin Svensson
  • Patent number: 6602314
    Abstract: The present invention provides an aluminum composite material having neutron absorbing power that improves the ability to absorb neutrons by increasing the content of B, while also being superior to materials of the prior art in terms of mechanical properties and workability. The aluminum composite material having neutron absorbing power contains in Al or an Al alloy matrix phase B or a B compound having neutron absorbing power in an amount such that the proportion of B is 1.5% by weight or more to 9% by weight or less, and the aluminum composite material has been pressure sintered.
    Type: Grant
    Filed: March 30, 2001
    Date of Patent: August 5, 2003
    Assignee: Mitsubishi Heavy Industries, Ltd.
    Inventors: Yasuhiro Sakaguchi, Tomikane Saida, Kazuo Murakami, Kazuhisa Shibue, Naoki Tokizane, Tatsumi Takahashi
  • Patent number: 6573210
    Abstract: A composite ceramic-metal material has an Al2O3 matrix interpenetrated by a network of a ductile metal phase with a higher meltin temperature than aluminum and which makes up 15 to 80 vol. % of its total volume. The Al2O3 matrix forms a coherent network that makes up 20 to 85 vol. %, and the material contains 0.1 to 20 atom % aluminide. To produce this composite material, a green body shaped by powder metallurgy and which contains a finely divided powdery mixture of Al2O3 and optionally other ceramic substances, as well as one or several metals or metal alloys different from aluminum and to which 0.1 to 20 atom % aluminum are added, in relation to the metal proportion, is sintered. The composition is selected in such a way that maximum 15 vol. % aluminide phase can be formed in the finished sintered body.
    Type: Grant
    Filed: November 11, 1998
    Date of Patent: June 3, 2003
    Inventors: Nils Claussen, Silvia Schicker, Daniel Garcia, Rolf Janssen
  • Patent number: 6562291
    Abstract: A process for the manufacture of compressed articles, particularly cemented-carbide cutting blade inserts, by compacting metallic powder and subsequently sintering the compact, particularly cemented-carbide reversible cutting blade inserts, which have a seating surface and at least one cutting edge extending approximately in parallel with the seating surface which is at a predetermined distance from the seating surface, by means of a press having a die-plate and a top ram and a bottom ram, comprising the steps of: Charging a predetermined volume of metallic powder into the die-plate bore with the bottom ram taking a predetermined charging position in the die-plate bore, Displacing the bottom ram and the top ram to predetermined first and second positions, Displacing the bottom ram and, if need be, the top ram more while simultaneously measuring the compressive force at least for the bottom ram with the shift of the bottom ram or top ram being effected along a predetermined curve desired for the compressive
    Type: Grant
    Filed: March 2, 2001
    Date of Patent: May 13, 2003
    Assignee: Wilhelm Fette GmbH
    Inventors: Jürgen Hinzpeter, Ulrich Zeuschner, Thomas Pannewitz, Ulf Hauschild, Klaus Peter Rüssmann
  • Patent number: 6551371
    Abstract: A titanium-based composite material according to the present invention is characterized in that it comprises: a matrix containing a titanium (Ti) alloy as a major component, and titanium compound particles and/or rare-earth element compound particles dispersed in the matrix, wherein the matrix contains 3.0-7.0% by weight of aluminum (Al), 2.0-6.0% by weight of tin (Sn), 2.0-6.0% by weight of zirconium (Zr), 0.1-0.4% by weight of silicon (Si) and 0.1-0.5% by weight of oxygen (O), the titanium compound particles occupy 1-10% by volume, and the rare-earth element compound particles occupy 3% by volume or less. With this arrangement, it is possible to obtain a titanium material, which is good in terms of the heat resistance, hot working property, specific strength, and so on.
    Type: Grant
    Filed: January 22, 2001
    Date of Patent: April 22, 2003
    Assignees: Kabushiki Kaisha Toyota Chuo Kenkyusho, Toyota Jidosha Kabushiki Kaisha
    Inventors: Tadahiko Furuta, Takashi Saito, Hiroyuki Takamiya, Toshiya Yamaguchi
  • Patent number: 6521013
    Abstract: A niobium sintered body for a capacitor, which exhibits an LC value of not larger than 300 &mgr;A/g as measured after an electrolytic oxide film is formed thereon. The sintered body preferably exhibits a product (CV) [i.e., a product of capacity (C) with electrolysis voltage (V)] of at least 40,000 &mgr;F·V/g. The sintered body is produced by sintering a niobium powder containing at least one niobium compound selected from niobium nitride, niobium carbide and niobium boride. A capacitor manufactured from the sintered body has a large capacity per unit weight and good leak current characteristics. Especially, a sintered body made of a niobium powder having a large average degree of roundness has a relatively large porosity and a good packed density, and a capacitor manufactured from this sintered body has a large capacity and good withstand voltage characteristics.
    Type: Grant
    Filed: February 5, 2001
    Date of Patent: February 18, 2003
    Assignee: Showa Denko Kabushiki Kaisha
    Inventors: Kazumi Naito, Atsushi Shimojima
  • Patent number: 6506226
    Abstract: The invention relates to a hard metal or cermet body with a hard material phase consisting of WC and/or at least one carbide, nitride, carbonitride and/or oxicarbonitride of at least one of the elements from group IVa, Va, or VIa of the periodic table and a binding metal phase consisting of Fe, Co and/or Ni, said binding metal phase making up 3 to 25 mass %. In particular, WC crystallites should protrude beyond the hard metal or cermet surface of the by 2 to 20 &mgr;m in order to improve the adhesion of surface layers that are applied.
    Type: Grant
    Filed: November 3, 2000
    Date of Patent: January 14, 2003
    Assignee: Widia GmbH
    Inventors: Limin Chen, Walter Lengauer, Hans Werner Daub, Klaus Dreyer, Dieter Kassel, José Garcia, Georg Korb
  • Publication number: 20020178862
    Abstract: A process of making an article of a tungsten-carbide-cobalt alloy with or without an additive of one or more of tantalum, cobalt-nickel, nickel-tantalum, tantalum-carbide, titanium-carbide, niobium-carbide, chromium-carbide, titanium-nitride and diamond dust. The method includes forming a homogeneous mixture of polygonal-shaped powder tungsten- carbide-cobalt and a polygonal-shaped powder additive and a binder including wax and a high molecular weight polyolefin polymer and injecting the mixture under heat and pressure into a metal injection mold to form a green preform of the article. The green preform is immersed in a linear hydrocarbon or a halogenated hydrocarbon or mixtures to dissolve and remove the wax and convert the green preform into a brown preform which is sintered to remove the remainder of the binder and to densify the brown preform into an article having a density not less than 98%. Various tungsten-carbide articles are disclosed.
    Type: Application
    Filed: April 18, 2002
    Publication date: December 5, 2002
    Inventors: David J. Smith, Thomas B. Shappie, Robert A. Sanford, Richard J. Liesz
  • Patent number: 6440358
    Abstract: The present invention relates to a method of forming a powder rod core comprising injecting a powder mix material into a mold, moving the mold to a curing station, and injecting material into a second mold.
    Type: Grant
    Filed: November 9, 2001
    Date of Patent: August 27, 2002
    Assignee: Schlumberger Technology Corporation
    Inventors: Harold A. Sreshta, Eric F. Drake
  • Publication number: 20020110474
    Abstract: The present invention relates to a method of forming a powder rod core comprising injecting a powder mix material into a mold, moving the mold to a curing station, and injecting material into a second mold.
    Type: Application
    Filed: November 9, 2001
    Publication date: August 15, 2002
    Inventors: Harold A. Sreshta, Eric F. Drake
  • Patent number: 6432150
    Abstract: A superabrasive containing layered composite is provided which comprises a substrate block consisting of either ceramic material and metallic or several metallic materials, and a superabrasive containing body adjacent said substrate block. The superabrasive contains superabrasive particles, and a metallic ingredient which is distributed in the superabrasive containing layer, including a working surface. The superabrasive material may be formed using a compression cell wherein the compression cell comprises a die defined by a vertical wall and a flat closed bottom. Placed in the die, in order from bottom upward, comprises a formed pallet of single body or layers of mixed powder forming a refractory compound, a material mass of a working layer containing diamond particles, a mass of ignition material comprising an SHS composition, and an electrical heating element.
    Type: Grant
    Filed: May 12, 2000
    Date of Patent: August 13, 2002
    Assignees: The Ishizuka Research Institute, Ltd., Moscow Steel and Alloys Institute, SHS-Center
    Inventors: Evgeny Alexandrovich Levashov, Alexander Sergeevich Rogatchov, Boris Vladmirovich Spitsin, Mitsue Koizumi, Manshi Ohyanagi, Satoru Hosomi
  • Patent number: 6428596
    Abstract: A multiplex powder composite for use in a cored wire electrode to be deployed in a thermal spray or welding apparatus. The composite comprises micron-sized particles and sub-micron-sized particles, including nano-scale particles, the particles mechanically cooperating to promote smooth powder flow, which facilitates compaction of the cored wire electrode.
    Type: Grant
    Filed: November 13, 2000
    Date of Patent: August 6, 2002
    Assignee: Concept Alloys, L.L.C.
    Inventors: David John Urevich, Joseph Paul Hughes
  • Patent number: 6402802
    Abstract: Embodiments include a method for fabricating a nanograined component from a nanograined powder composition. A compact is formed from the nanograined powder composition and sufficient heat is applied to the compact to generate at least one exothermic reaction while the compact is at a temperature lower than its eutectic temperature. Pressure is applied to the powder compact during the heating operation to consolidate the powder compact. The application of heat and pressure are controlled to inhibit grain growth and form a component having a nanograined microstructure that is at least 98 percent dense at a temperature lower than the eutectic temperature.
    Type: Grant
    Filed: October 28, 1999
    Date of Patent: June 11, 2002
    Assignee: The Penn State Research Foundation
    Inventor: Ram B. Bhagat