Subsequent Working Patents (Class 419/28)
  • Patent number: 6132148
    Abstract: A machining tool and method of making same includes a blank that is formed to a shank and which is provided with machining faces. The machining faces are configured to expose material of a PCD or PCBN element that is formed in a recess in the blank and fused to the blank using material from the transition group of elements, such as cobalt. The recess has a configuration that is defined by side walls, a base wall, and end walls, so as to define a mold in which the PCD or PCBN material is formed into an element that becomes fused with the blank. Such fusing is achieved by leaching of the cobalt into the PCD or PCBN element during the application of heat. Thus, no additional fabrication process is required for joining the PCBN or PCD material to the blank.
    Type: Grant
    Filed: August 14, 1998
    Date of Patent: October 17, 2000
    Assignee: Habit Diamond Limited
    Inventor: Michael Frederick Thompson
  • Patent number: 6129890
    Abstract: It has been discovered that potassium retention in NS tungsten processing may be improved by double doping tungsten blue oxide (TBO) prior to reduction. The novel `double-doping` process consists of dry doping standard singly doped K--Al--Si TBO with potassium nitrate, KNO.sub.3, followed by the standard reduction, acid washing, sintering, rolling and drawing steps. In another aspect, the novel method includes an aqueous extraction of heteropolytungstate anion [SiW.sub.11 O.sub.39 ].sup.8- from a sample of the singly doped tungsten blue oxide to predict potassium retention.
    Type: Grant
    Filed: September 7, 1999
    Date of Patent: October 10, 2000
    Assignee: Osram Sylvania Inc.
    Inventors: Hans-Joachim Lunk, Henry J. Stevens, Thomas J. Patrician, Harry D. Martin, III
  • Patent number: 6110419
    Abstract: A method of densifying a sintered powder metal article by point contact.
    Type: Grant
    Filed: December 2, 1997
    Date of Patent: August 29, 2000
    Assignee: Stackpole Limited
    Inventors: Keith Buckley-Golder, Peter Jones, D. Sarafinchan
  • Patent number: 6110418
    Abstract: A method for manufacturing cutting knives, in particular granulator knives in which a mass of highly wear resistant material is bonded along one edge of a main body of a tougher, more ductile material, the cutting edge machined into the mass of wear resistant material, to increase the service life of the knife between sharpenings without subjecting the tool to breakage during heavy use in a granulator.
    Type: Grant
    Filed: November 9, 1998
    Date of Patent: August 29, 2000
    Inventor: David A. Jablonski
  • Patent number: 6074454
    Abstract: The invention relates to bullets having increased frangibility (or which can be easily fragmented) and to materials and processes for the manufacture of such bullets. The bullets of the present invention are typically made from copper or copper alloy powders (including brass, bronze and dispersion strengthened copper) which are pressed and then sintered under conditions so as to obtain bullets with the desired level of frangibility. In preferred embodiments of the invention, the bullets also contain several additives that increase or decrease their frangibility.
    Type: Grant
    Filed: July 11, 1996
    Date of Patent: June 13, 2000
    Assignee: Delta Frangible Ammunition, LLC
    Inventors: John T. Abrams, Anil V. Nadkarni, Roy Kelly
  • Patent number: 6059904
    Abstract: A method combining isothermal and high retained strain forging is described for Ni-base superalloys, particularly those which comprise a mixture of .gamma. and .gamma.' phases, and most particularly those which contain at least about 40 percent by volume of .gamma.'. The method permits the manufacture of forged articles having a fine grain size in the range of 20 .mu.m or less. The method comprises the selection of a fine-grained forging preform formed from a Ni-base superalloy, isothermal forging to develop the shape of the forged article, subsolvus forging to impart a sufficient level of retained strain to the forged article to promote subsequent recrystallization and avoid critical grain growth, and annealing to recrystallize the microstructure. The method permits the forging of relatively complex shapes and avoids the problem of critical grain growth. The method may also be used to produce location specific grain sizes and phase distributions within the forged article.
    Type: Grant
    Filed: May 23, 1997
    Date of Patent: May 9, 2000
    Assignee: General Electric Company
    Inventors: Mark Gilbert Benz, Michael Francis Henry, Charles Philip Blankenship, Jr., Aldo Enrique Murut
  • Patent number: 6042778
    Abstract: A sliding bearing which is multilayered, self-lubricating and maintenance-free includes a metallic supporting body; and a layer of sintered bronze which is provided on the metallic supporting body and which has pores filled with polytetrafluoroethylene (PTFE) to provide a PTFE-impregnated sintered bronze layer, the PTFE being uniformly distributed and serving as a solid lubricant, and the PTFE-impregnated sintered bronze layer having a sliding surface composed of the PTFE particles but no PTFE cover layer. The sliding bearing is made by a method including applying a layer of bronze powder onto the metallic supporting body, the bronze powder having different particle sizes, having a mean particle size of about 40 .mu.m, and having a particle shape which is dendritic; sintering the layer of bronze powder in a furnace at a temperature of about 800.degree. C.
    Type: Grant
    Filed: December 12, 1997
    Date of Patent: March 28, 2000
    Assignee: Federal-Mogul Deva GmbH
    Inventors: Erik Kraft, Udo Roos, Hubert Schwarze, Thomas Piesch
  • Patent number: 6042779
    Abstract: The invention relates to a method for forming high performance metal alloys using powder metallurgy. Alloys are extruded under controlled temperature conditions through an extrusion die containing non-metal bearing inserts. This allows the extrusion of hypereutectic alloys without excessive wear of the extrusion die.
    Type: Grant
    Filed: July 30, 1998
    Date of Patent: March 28, 2000
    Assignee: Reynolds Metals Company
    Inventors: Edward L. Oschmann, Thomas G. Haynes
  • Patent number: 6038461
    Abstract: There are disclosed a high temperature superconductive material which can be plastically deformed, processed optionally into predetermined configurations and industrially mass produced and a method of manufacturing a formed body of the high temperature superconductive material. Mixed is a powder raw material which is mainly composed of: 10 to 50 mol % of at least one amide or nitride of alkali metal of Li, Na or K; 10 to 60 mol % of cyanide containing at least one metal selected from aluminum, copper, silver or gold; 5 to 50 mol % of at least one pure metal selected from aluminum, copper, silver or gold; and 10 mol % or less of at least one alkaline earth metal selected from Be, Mg, Ca, Sr or Ba. The powder raw material is pressed, and heated and sintered at the temperature of 673 K to 1553 K. In this manner, obtained is the plastically deformable high temperature superconductive material which can be optionally processed through forging, rolling and the like.
    Type: Grant
    Filed: April 24, 1998
    Date of Patent: March 14, 2000
    Inventors: Yoshifumi Sakai, Itsuko Sakai
  • Patent number: 6030577
    Abstract: The invention relates to a method for manufacturing thin-walled pipes, which are made of a heat-resistant and wear-resistant aluminum-based material. The method comprises the providing of a billet or a tube blank made of a hypereutectic aluminum-silicon AlSi material, possibly a subsequent averaging annealing, the extruding of the billet or of the tube blank to a thick-walled pipe, and the hot deformation of this pipe to a thin-walled pipe. Such a method is in particular suited for the production of cylinder liners of internal combustion engines, since the produced liners exhibit the required properties in regard to wear resistance, heat resistance and reduction of pollutant emission.
    Type: Grant
    Filed: February 27, 1998
    Date of Patent: February 29, 2000
    Assignee: Erbsloh Aktiengesellschaft
    Inventors: Bernhard Commandeur, Rolf Schattevoy, Klaus Hummert
  • Patent number: 6030472
    Abstract: A powder metallurgical process of preparing a sheet from a powder having an intermetallic alloy composition such as an iron, nickel or titanium aluminide. The sheet can be manufactured into electrical resistance heating elements having improved room temperature ductility, electrical resistivity, cyclic fatigue resistance, high temperature oxidation resistance, low and high temperature strength, and/or resistance to high temperature sagging. The iron aluminide has an entirely ferritic microstructure which is free of austenite and can include, in weight %, 4 to 32% Al, and optional additions such as .ltoreq.1% Cr, .gtoreq.0.05% Zr.ltoreq.2% Ti, .ltoreq.2% Mo, .ltoreq.1% Ni, .ltoreq.0.75% C, .ltoreq.0.1% B, .ltoreq.1% submicron oxide particles and/or electrically insulating or electrically conductive covalent ceramic particles, .ltoreq.1% rare earth metal, and/or .ltoreq.3% Cu.
    Type: Grant
    Filed: December 4, 1997
    Date of Patent: February 29, 2000
    Assignee: Philip Morris Incorporated
    Inventors: Mohammad R. Hajaligol, Clive Scorey, Vinod K. Sikka, Seetharama C. Deevi, Grier Fleischhauer, A. Clifton Lilly, Jr., Randall M. German
  • Patent number: 6021174
    Abstract: An explosive forming process provides an anode (10) suitable for use in a high energy x-ray tube. The process includes applying a shaped charge (54, 80, 90, 92) to a refractory material which has been formed in the general shape of the anode. The configuration of the charge is calculated to provide a target area (16) on the anode of uniform, high density which does not tend to outgas in the high vacuum conditions of the x-ray tube. The explosive process is capable of forming anodes with much larger diameters than is possible with conventional forging techniques.
    Type: Grant
    Filed: October 26, 1998
    Date of Patent: February 1, 2000
    Assignee: Picker International, Inc.
    Inventor: Robert B. Campbell
  • Patent number: 6017489
    Abstract: A method of densifying the wall of an opening in a powder metal preform includes forcibly extending a densification tool through the opening having a plurality of radially enlarged forming portions arranged in axially spaced succession from smallest to largest which act to enlarge and densify the preform material and impart beneficial compressive stresses. The space between successive forming portions enables the preform material to recover elastically between adjacent forming sections to maximize induced compressive stresses.
    Type: Grant
    Filed: February 17, 1999
    Date of Patent: January 25, 2000
    Assignee: Federal-Mogul World Wide, Inc.
    Inventors: Richard Mark Woolf, Rajesh Parameswaran
  • Patent number: 6012392
    Abstract: Shaped charge liners are formed from an alloy of nickel, tin, and copper, which is first formed into a powder, and then pressed into strips. The pressed strips of powdered alloy are next sintered and then cold rolled. Thereafter, the powdered, pressed, and sintered alloy strips are formed into shaped charge liners, for example, by stamping. The shaped charge liners may be heat treated either before or after the forming step.
    Type: Grant
    Filed: May 10, 1997
    Date of Patent: January 11, 2000
    Assignees: Arrow Metals division of Reliance Steel and Aluminum Co., Owen Oil Tool, Inc.
    Inventors: Kimball J. Norman, Dan W. Pratt
  • Patent number: 5997805
    Abstract: A manufacturing method is provided for the production of high density, high carbon, sintered powder metal steels. The composition consists of iron based powder, graphite, lubricant, and possibly at least one alloying element from the group of chromium, copper, manganese, molybdenum, nickel, niobium or vanadium. The composition is compacted in rigid tools, sintered and during cooling an isothermal or slow cooling treatment is introduced between 650.degree. C. and 750.degree. C. The isothermal or slow cooling treatment may alternatively be applied during a heat treatment cycle that is carried out after a conventional sintering cycle. The material processed as described may then be formed to high density. Forming to high density is not practical with high carbon materials that have been processed by conventional methods. The high density article is then heat treated in a manner to suit specific product requirements.
    Type: Grant
    Filed: June 19, 1997
    Date of Patent: December 7, 1999
    Assignee: Stackpole Limited
    Inventors: Roger Lawcock, Peter Jones
  • Patent number: 5997605
    Abstract: The present invention concerns a method of producing powder-metallurgical compacted components, which during subsequent processing are split into individual parts mating in pairs, sintered and optionally heat-treated and remated. According to the process, an iron-based powder is compacted, the obtained green body is fracture-split into at least two parts, which are subsequently sintered and optionally heat-treated. The obtained sintered parts are then remated.
    Type: Grant
    Filed: March 31, 1999
    Date of Patent: December 7, 1999
    Assignee: Hoganas AB
    Inventors: Nils Carlbaum, Bjorn Johansson
  • Patent number: 5976214
    Abstract: A slide member of a sintered aluminum alloy includes a matrix (1) formed of an aluminum alloy powder, and aluminum nitride films (2) dispersed along old, i.e. former original, powder grain boundaries of this matrix. When a state in which the aluminum nitride films (2) completely continuously enclose the peripheries of the old powder grain boundaries is defined as a dispersion ratio of 100%, the present aluminum nitride films (2) are discontinuously dispersed at a dispersion ratio of not more than 80%. A powder compact consisting of rapidly solidified aluminum alloy powder is heated and held in a nitrogen gas atmosphere, thereby facilitating reaction between aluminum and nitrogen through an exothermic phenomenon following deposition of elements solidly dissolved in the aluminum alloy, for forming aluminum nitride films dispersed on the aluminum alloy powder grain surfaces.
    Type: Grant
    Filed: December 13, 1995
    Date of Patent: November 2, 1999
    Assignee: Sumitomo Electric Industries, Ltd.
    Inventors: Katsuyoshi Kondoh, Yoshishige Takano
  • Patent number: 5976458
    Abstract: The invention relates generally to aluminum containing iron-base alloys useful as electrical resistance heating elements. The aluminum containing iron-base alloys have improved room temperature ductility, electrical resistivity, cyclic fatigue resistance, high temperature oxidation resistance, low and high temperature strength, and/or resistance to high temperature sagging. The alloy has an entirely ferritic microstructure which is free of austenite and includes, in weight %, over 4% Al, .ltoreq.1% Cr and either .gtoreq.0.05% Zr or ZrO.sub.2 stringers extending perpendicular to an exposed surface of the heating element or .gtoreq.0.1% oxide dispersoid particles. The alloy can contain 14-32% Al, .ltoreq.2% Ti, .ltoreq.2% Mo, .ltoreq.1% Zr, .ltoreq.1% C, .ltoreq.0.1% B, .ltoreq.30% oxide dispersoid and/or electrically insulating or electrically conductive covalent ceramic particles, .ltoreq.1% rare earth metal, .ltoreq.1% oxygen, .ltoreq.3% Cu, balance Fe.
    Type: Grant
    Filed: January 3, 1996
    Date of Patent: November 2, 1999
    Assignee: Philip Morris Incorporated
    Inventors: Vinod K. Sikka, Seetharama C. Deevi, Grier S. Fleischhauer, Mohammad R. Hajaligol, A. Clifton Lilly, Jr.
  • Patent number: 5972069
    Abstract: A primary product comprising tungsten or molybdenum accommodated in a container 1 is heated at 500.degree. C. with 1000 atmospheric pressure in an Ar gas atmosphere and retained for 1 hour. According to the present invention, the crystal orientation in the (110) face can be 99% or more, and thus a material with a good electron radiation characteristic can be obtained.
    Type: Grant
    Filed: July 22, 1998
    Date of Patent: October 26, 1999
    Assignee: Mitsubishi Denki Kabushiki Kaisha
    Inventors: Shigeki Maekawa, Megumi Takemoto
  • Patent number: 5972132
    Abstract: Inner or outer cylindrical worked surfaces of powder metal components are bearingized by orbiting tapered rollers against them using a tapered mandrel having points for impacting the rollers against the worked surface.
    Type: Grant
    Filed: February 10, 1999
    Date of Patent: October 26, 1999
    Assignee: Zenith Sintered Products, Inc.
    Inventor: Terry M. Cadle
  • Patent number: 5966581
    Abstract: A method for manufacturing metal by a cold worked powdered metal forging process is disclosed. A certain amount of a powdered metal is measured out and then compacted into a briquette or other compact. The briquette is then sintered to form a preform. After sintering, the preform is then cold worked to increase its strength. After cold working, the preform is forged to form the desired part. The resultant part has improved fatigue life, surface finish, and metallurgical characteristics.
    Type: Grant
    Filed: August 30, 1996
    Date of Patent: October 12, 1999
    Assignee: Borg-Warner Automotive, Inc.
    Inventors: Jack E. Pederson, Hayward P. Summers
  • Patent number: 5950064
    Abstract: There is provided a lead-free projectile, such as a bullet or a ballistic shot, formed by liquid phase sintering or liquid phase bonding of a first particulate having a density greater than lead, a second, ductile, particulate having a melting temperature in excess of 400.degree. C. and a binder having a fluidity temperature that is less than the melting temperature of the second particulate. Unlike solid phase sintering that tends to produce articles having a porosity of about 20%, by volume, liquid phase sintering and liquid phase bonding achieve close to 0% porosity. Reducing the porosity level decreases the amount of high density, first particulate, required to achieve a density close to that of lead. Since the high density particulate tends to be the most expensive component of the projectile, this significantly reduces the cost of the projectile. The reduced porosity also allows for an increase in the amount of the second, ductile, component.
    Type: Grant
    Filed: January 17, 1997
    Date of Patent: September 7, 1999
    Assignee: Olin Corporation
    Inventors: Peter W. Robinson, Brian Mravic, Derek E. Tyler
  • Patent number: 5940675
    Abstract: Powder metallurgy production of T222 alloy affording properties comparable to melt derived T222, but at higher yields and lower costs, is enabled by blending component powders of minus 325 mesh and sintering at 2,400.degree. C. in three sinter steps and utilizing a slow ramp up in the first sinter step and cold isostatic pressing prior to the first sinter step and isostatic press densification in conjunction with at least the first sinter step.
    Type: Grant
    Filed: December 24, 1997
    Date of Patent: August 17, 1999
    Assignee: H. C. Starck, Inc.
    Inventors: Robert W. Balliett, Trung Luong
  • Patent number: 5936169
    Abstract: A high vanadium, powder metallurgy cold work tool steel article and method for production. The nickel, chromium, vanadium, and carbon plus nitrogen contents of the steel are controlled during production to achieve a desired combination of corrosion resistance, metal to metal wear resistance, and hardenability.
    Type: Grant
    Filed: October 16, 1997
    Date of Patent: August 10, 1999
    Assignee: Crucible Materials Corporation
    Inventors: Kenneth E. Pinnow, William Stasko, John Hauser
  • Patent number: 5933699
    Abstract: Methods of making gas turbine structures with cooling channels, such as, for example, combustor/transition pieces for gas turbines having a double wall with a plurality of cooling channels, having axially and/or circumferential cross-flow passages positioned between the structure's inner member and the outer member to provide cooling air thereto, are disclosed.
    Type: Grant
    Filed: June 24, 1996
    Date of Patent: August 3, 1999
    Assignee: General Electric Company
    Inventors: Ann Melinda Ritter, Melvin Robert Jackson, Nesim Abuaf, Robert Patrick Campbell, Ronald Scott Bunker
  • Patent number: 5915160
    Abstract: High strength gold wire for use in microelectronics and a method of producing the same are disclosed. In the methods of the present invention, a gold alloy having gold and a dilute rare earth (RE) element is produced. Next, the gold alloy is atomized into a powder. The dilute RE element is at least partially oxidized during atomization. Then, the powder is consolidated into an oxide dispersion strengthened gold billet. Finally, gold wire is formed from the oxide dispersion strengthened gold billet. The high strength gold wire can be drawn to a diameter less than conventional gold wire, while still maintaining mechanical and electrical properties, thereby facilitating microelectronics miniaturization.
    Type: Grant
    Filed: February 17, 1998
    Date of Patent: June 22, 1999
    Assignee: Rockwell International
    Inventors: Phillip D. Krotz, David D. Hillman, Nicole L. DeBlieck Cavanah
  • Patent number: 5905939
    Abstract: There is provided a connecting rod including a connecting rod body and a cap having excellent alignment properties, and a method of producing such a connecting rod. A connecting rod body and a cap are produced through the steps of molding green compacts respectively corresponding to the connecting rod body and the cap; sintering and unifying both the green compacts; forging the resultant sintered product in a mold; and fracturing the resultant forged product. The green compact corresponding to the cap and/or the green compact corresponding to the connecting rod body includes opposite circumferential end faces formed with one or more projection. A clearance c is formed between both circumferential end faces of the sintered product due to the projection. With this clearance c, both the circumferential end faces are formed with recesses and projections which are fitted to each other during the forging process and which are relatively large and thus have large biting amounts.
    Type: Grant
    Filed: July 3, 1997
    Date of Patent: May 18, 1999
    Assignees: Hitachi Powdered Metals Co., Ltd, Honda Giken Kogyo Kabushiki Kaisha
    Inventors: Zenzo Ishijima, Junichi Ichikawa, Syuji Sasaki, Jun Sakai, Hideo Shikata, Hideo Urata
  • Patent number: 5903813
    Abstract: A flat section with density not less than 25% from theoretical value is sintered from the powder of low ductile reactive alloy, welded by diffusion welding with cover foils made from ductile reactive metal that seal hermetically inner and surface pores, and assembled with two heat resistant sheets in the laminated package. Cover foils are made from metal that belongs to the same metal system as said sintered powder. The package is encapsulated in a capsule made from reactive alloy that belongs also to the same metal system as said sintered powder. An anti-adhesive release agent such as Y.sub.2 O.sub.3, A1.sub.2 O.sub.3, or CaF.sub.2 is deposited on both sides of the laminated package and between cover foils and heat resistant sheets. A portion of metal powder such as Mn, Ti, Nb, Cr, or other metals, having a high affinity to oxygen, inserts into said capsule for absorbtion of oxygen during the heating and forming. After outgassing vacuum heating at 1100-1500.degree. F.
    Type: Grant
    Filed: July 24, 1998
    Date of Patent: May 11, 1999
    Assignee: Advanced Materials Products, Inc.
    Inventors: Vladimir S. Moxson, Aleksandr E. Shapiro
  • Patent number: 5900560
    Abstract: A high vanadium, powder metallurgy cold work tool steel article and method for production. The nickel, chromium, vanadium, and carbon plus nitrogen contents of the steel are controlled during production to achieve a desired combination of corrosion resistance, metal to metal wear resistance, and hardenability.
    Type: Grant
    Filed: July 29, 1998
    Date of Patent: May 4, 1999
    Assignee: Crucible Materials Corporation
    Inventors: Kenneth E. Pinnow, William Stasko, John Hauser
  • Patent number: 5881354
    Abstract: A method of making a sintered article of powder metal having a carbon composition in the range of about 0.8% to 2.0% by weight, then spheroidizing the sintered article and then warm forming the sintered article at a temperature between 250.degree. and 700.degree. C. for a time duration selected to form the article to a final shape.
    Type: Grant
    Filed: May 3, 1996
    Date of Patent: March 9, 1999
    Assignee: Stackpole Limited
    Inventors: Rohith Shivanath, Peter Jones
  • Patent number: 5878323
    Abstract: A plurality of blanks divided at a division end face 5 or a blank-bonded product comprising a plurality of blanks sintered and bonded together are or is compressed in the same mold, so that they are plastically deformed until the division end faces 5 are cohered. Thereafter, a load is applied to the plastically worked product in a direction of breaking of the division end faces 5 to break the division end faces 5 and divide the plastically worked product into a plurality of members. In this manner, a split type mechanical part having irregularities meshed with each other on mating faces and easily positionable relative to each other can be produced with a good dimentional accuracy.
    Type: Grant
    Filed: August 10, 1995
    Date of Patent: March 2, 1999
    Assignee: Honda Giken Kogyo Kabushiki Kaisha
    Inventors: Jun Sakai, Junichi Ichikawa, Zenzo Ishijima, Shuji Sasaki, Hideo Shikata, Katsuhiko Ueda, Hideo Urata
  • Patent number: 5850591
    Abstract: A method of manufacturing a porous metal sheet having pores forming a pattern, comprising the steps of supplying metal powders to a peripheral surface, of at least one pattern roller of a pair of rollers, on which a pattern including a large number of concaves is formed; dropping metal powders to the concaves and accumulating metal powders on the peripheral surface of the pattern roller except the concaves; and rolling directly the metal powders accumulated on the peripheral surface of the pattern roller by rotating a pair of the rollers. It is preferable to laminate porous metal sheets or solid metal sheets manufactured by a method other than the above-described method on the metal sheet manufactured by the above-described method.
    Type: Grant
    Filed: April 18, 1997
    Date of Patent: December 15, 1998
    Assignee: Katayama Special Industries, Ltd.
    Inventor: Hirofumi Sugikawa
  • Patent number: 5846288
    Abstract: Electrical contact material made from intimate mixtures of silver powder and a powder of a second phase material is shown in which the powder of the second phase material is milled to produce a selected grain distribution of approximately 90% less than 7-10 microns, approximately 50% between 2 and 5 microns and approximately 10% less than 0.8 to 1.0 microns. The powder of the second phase material is added to a silver salt solution, ammonium hydroxide and hydrazine hydrate to form a precipitate of second phase material particles covered with silver. For applications in which the particles need to be free flowing the particles are compacted together without any binder, broken into chunks and milled to provide granules. In one embodiment homogeneously doped tin oxide particles are disclosed in which tin oxide and the oxide of the dopant are dissolved in nitric acid to produce finely dispersed tin oxide and dopant oxide. The oxides are calcined and ground to the selected grain size distribution.
    Type: Grant
    Filed: November 26, 1996
    Date of Patent: December 8, 1998
    Assignee: Chemet Corporation
    Inventors: Ernest M. Jost, Kirk McNeilly
  • Patent number: 5841044
    Abstract: Silver-iron materials for electrical switching contacts with properties which come very close to those of silver-nickel materials formed of 0.5 to 4.5% by weight iron and 0.05 to 2% by weight of one or more of the oxides magnesium oxide, calcium oxide, yttrium oxide, lanthanum oxide, titanium oxide, zirconium oxide, hafnium oxide, cerium oxide, niobium oxide, tantalum oxide, chromium oxide, manganese oxide, iron oxide, zinc oxide, aluminum oxide, indium oxide, silicon oxide, and tin oxide, the balance being silver.
    Type: Grant
    Filed: November 19, 1996
    Date of Patent: November 24, 1998
    Assignee: Degussa Aktiengesellschaft
    Inventors: Wolfgang Weise, Willi Malikowski, Roger Wolmer, Peter Braumann, Andreas Koffler
  • Patent number: 5824923
    Abstract: A sintered friction material includes a copper alloy base and hard particles. The copper alloy base includes copper and at least one of, and preferably both, Zn and Ni within a total range of 5 to 40 wt % of the copper alloy base. The hard particles are uniformly dispersed in a matrix formed by the original composite copper alloy powder constituting the base, in a content amount within a range of 10 to 30 wt % of the friction material.
    Type: Grant
    Filed: September 28, 1995
    Date of Patent: October 20, 1998
    Assignee: Sumitomo Electric Industries, Ltd.
    Inventors: Katsuyoshi Kondoh, Yoshishige Takano
  • Patent number: 5815790
    Abstract: The invention relates to a method for the manufacturing of a composite metal product. More particularly, the invention relates to a method for the manufacturing of a composite product consisting of at least two stainless steel materials having different chemical compositions, particularly a composite stainless product on which decorative patterns can or has been produced by etching.It is significant feature of the invention that at least two stainless steel materials having different chemical compositions are bonded together through hot isostatic compaction at a pressure exceeding 600 bar and a temperature exceeding 1000.degree. C., at least one of said materials consisting of powder, for the achievement of a consolidated body.
    Type: Grant
    Filed: December 4, 1996
    Date of Patent: September 29, 1998
    Assignee: Soderfors Powder Aktiebolag
    Inventors: Per Billgren, Kaj Embretsen
  • Patent number: 5798468
    Abstract: An electrical contact material for switching rated currents between 20 and 100 Ampere having improved operational life made of 3.2 to 19.9 wt-% tin oxide and 0.05 to 0.4 wt-%, in each case, of indium oxide and bismuth oxide, the remainder being silver. In the course of the manufacture of the material by powder metallurgy more than 60 wt-% of the tin oxide should exhibit a particle size of more than 1 .mu.m.
    Type: Grant
    Filed: January 31, 1996
    Date of Patent: August 25, 1998
    Assignee: Degussa Aktiengesellschaft
    Inventors: Wolfgang Weise, Roger Wolmer, Peter Braumann
  • Patent number: 5799238
    Abstract: A method making a titanium ceramic composite involves forming a hot pressed powder body having a microstructure comprising at least one titanium metal or alloy layer and at least one ceramic particulate reinforced titanium metal or alloy layer and hot forging the hot pressed body follwed by hot rolling to substantially reduce a thickness dimension and substantially increase a lateral dimension thereof to form a composite plate or sheet that retains in the microstructure at least one titanium based layer and at least one ceramic reinforced titanium based layer in the thickness direction of the composite plate or sheet.
    Type: Grant
    Filed: June 14, 1995
    Date of Patent: August 25, 1998
    Assignee: The United States of America as represented by the United States Department of Energy
    Inventors: George T. Fisher, II, Jeffrey S. Hansen, Laurance L. Oden, Paul C. Turner, Thomas L. Ochs
  • Patent number: 5773734
    Abstract: A powdered metal piston ring includes a structure of predominantly pearlite with a dispersion of metallic particles having an element with a high affinity for nitrogen. The ring is nitrided to form a hard surface layer at an outer periphery of the ring. The layer includes a first iron nitrided region and an adjacent region having greater hardness because of a reaction between the metallic particles and nitrogen. Preferred metallic particles include a high chromium steel alloy which forms part of the original powder metal of the piston ring.
    Type: Grant
    Filed: December 21, 1995
    Date of Patent: June 30, 1998
    Assignee: Dana Corporation
    Inventor: William B. Young
  • Patent number: 5768678
    Abstract: Disclosed is a metal sulfide composition for use as a machining aid comprising 55.0% to 65.0% by weight of manganese, 29.0% to 36.0% by weight of sulfur, and greater than 2.0% to 10% by weight of iron. Also disclosed is a method of making the metal sulfide composition comprising mixing manganese, sulfur, and iron; initiating an exothermic reaction between the manganese and sulfur, wherein the iron component moderates and cools the exothermic reaction; forming a solid mass of manganese sulfide composition containing a portion of the iron suspended therein; and recovering the solid manganese sulfide composition. A method of using the manganese sulfide composition according to the present invention as a machining aid comprises mixing into a blend a desired metal powder with the manganese sulfide composition; spreading the blend into a metal part die; compacting the blend into the die; sintering the compacted part; and machining the sintered part.
    Type: Grant
    Filed: May 8, 1996
    Date of Patent: June 16, 1998
    Assignee: Pyron Corporation
    Inventors: Kuldip Chopra, Stephen F. Claeys, G. Russell Lewis, Ralph A. Casciani
  • Patent number: 5765096
    Abstract: A method for producing a space shuttle or nuclear reprocessing structural material of an intermetallic compound having a formula NiAl+xMoRe+cB, wherein the atomic ratio of Ni:Al is 56.5:43.5, the atomic ratio of Mo:Re is 1:1, or 1:0.5, x is between 0.1 and 1 at. %, and c is from 0 to 0.2 at. %, including the steps of:mixing Ni and Al powders in the atomic ratio of 56.5:43.5 in an inert gasadding thereto between 0.1 and 1 at. % total of Mo and Re powders in an atomic ratio of 1:1 or 1:0.5 and from 0 to 0.2 at. % of B and mixing to obtain a uniform powder mixture,packing the mixture in a steel capsule to obtain a packed mixture, and Hot Isostatically Pressing the packed mixture at a temperature from 1000.degree. to 1200.degree. C. with 200 MPA pressure to obtain a pressed material, swaging the pressed material to at least 90% theoretical reduction, and obtaining the material having a uniform and refined structure.
    Type: Grant
    Filed: May 29, 1997
    Date of Patent: June 9, 1998
    Assignee: Japan Atomic Energy Research Institute
    Inventor: Shintaro Ishiyama
  • Patent number: 5759305
    Abstract: A method for forming nickel base superalloy articles of manufacture by a combination of hot die forging, isothermal forging and heat treatment below and above the solvus.
    Type: Grant
    Filed: February 7, 1996
    Date of Patent: June 2, 1998
    Assignee: General Electric Company
    Inventors: Mark Gilbert Benz, Edward Lee Raymond, Robert Donald Kissinger, Eric Scott Huron, Charles Philip Blankenship, Jr., Michael Francis Henry
  • Patent number: 5742891
    Abstract: A wire for fabrication of a vibration resistant filament for an incandescent lamp. The wire includes about 0.05-1.00 weight percent lanthanum oxide dispersed in a tungsten matrix and has a microstructure including stringers of fine particles of lanthanum oxide extending parallel to the wire axis. During primary recrystallization of a vibration resistant lamp filament from the filament wire, the stringers produce a microstructure in the filament exhibiting sufficient grain boundary segments extending generally axially along the length of the filament to render the filament resistant to vibration. A method for producing a vibration resistant filament for an incandescent lamp is also disclosed.
    Type: Grant
    Filed: April 4, 1996
    Date of Patent: April 21, 1998
    Assignee: Osram Sylvania Inc.
    Inventors: Thomas J. Patrician, Harry D. Martin, III
  • Patent number: 5740516
    Abstract: A firearm bolt prepared from an alloy of tungsten, nickel and iron having a density of about from 14.1 g/cc to 18.0 g/cc. The alloy preferably also contains at least one of molybdenum, cobalt, rhenium, tantalum and gold. The alloy is preferably manufactured by standard powder metallurgical techniques followed by a liquid phase sinter and vacuum anneal. The bolt can also be manufactured using solid state sintering. The bolt can also be manufactured by mechanically working the material after sintering, after annealing, or after both sintering and annealing.
    Type: Grant
    Filed: December 31, 1996
    Date of Patent: April 14, 1998
    Assignee: Remington Arms Company, Inc.
    Inventors: Marlin R. Jiranek, II, Michael D. Keeney
  • Patent number: 5734960
    Abstract: A process for producing potassium and silicon doped molybdenum (KS molybdenum). The process involves mixing an aqueous ammonium molybdate solution and a dilute aqueous potassium silicate solution. The molybdate solution has a pH and a specific gravity sufficient to promote formation of diammonium molybdate crystals in the mixture. Preferably, the pH is about 8.8-11.0 and the specific gravity is about 1.20-1.32. The amount of potassium silicate and the amount of potassium silicate solution are selected to provide predetermined amounts of potassium and silicon in the mixture, preferably about 800-1300 ppm potassium and about 500-1100 ppm silicon, both amounts based on the amount of molybdenum. The mixture is heated to aid dissolution of the potassium silicate and ammonium molybdate in said mixture and to produce a homogeneous solution of ammonium molybdate, potassium, and silicon.
    Type: Grant
    Filed: August 29, 1994
    Date of Patent: March 31, 1998
    Assignee: Osram Sylvania Inc.
    Inventors: Thomas J. Patrician, Michael J. Miller, James N. Christini, Michael J. Cheresnowsky, Vernon L. Carr, Jr.
  • Patent number: 5729822
    Abstract: A powder metal gear wheel having a core density of at least 7.3 g/cc, and in one embodiment 7.4 to 7.6 g/cc and a hardened carburized surface. A method of manufacturing transmission gears comprises, sintering a powder metal blank to produce a core density of between 7.4 to 7.6 g/cc, rolling the surface of the gear blank to densify the surface, and then heating the rolled sintered part and carburizing in a vacuum furnace.
    Type: Grant
    Filed: May 24, 1996
    Date of Patent: March 17, 1998
    Assignee: Stackpole Limited
    Inventors: Rohith Shivanath, Peter Jones
  • Patent number: 5722033
    Abstract: A method of extruding a boron carbide-aluminum alloy metal matrix composite includes heating the ingots of the composite to temperatures of about 570.degree. C., holding the ingots at about 570.degree. C. to soften the ingots, placing the ingots in a heated extrusion chamber, and extruding the softened ingots at pressures about 15% to 20% higher than typical pressures used to extrude aluminum alloys. A method of casting a boron carbide-aluminum alloy metal matrix composite includes heating ingots of the composite to about 700.degree. C. to melt the ingots, gently stirring the melt, removing dross from the melt, vigorously stirring the melt with an impeller without creating a vortex, degassing the melt with an argon diffuser wand, and continuously removing froth formed during degassing until the rate of froth formation is reduced and the melt gently bubbles.
    Type: Grant
    Filed: July 1, 1996
    Date of Patent: February 24, 1998
    Assignee: Alyn Corporation
    Inventor: Robin A. Carden
  • Patent number: 5722035
    Abstract: A hunting projectile with a hollow point is produced with a only few working steps, and in particular a hollow point construction is formed out only in one working step. For this purpose the whole projectile is made of a metal powder by a powder-metallurgical process and then calibrated and during the powder pressing, the hollow tip construction is brought in so that during the calibration it is deformed to produce a final projectile tip.
    Type: Grant
    Filed: June 13, 1995
    Date of Patent: February 24, 1998
    Assignee: Wilhelm Brenneke GmbH & Co. KG
    Inventors: Peter Matysik, Heinz Wiechmann
  • Patent number: 5718778
    Abstract: A chromium target is disclosed for use in the formation of chromium films or sheets of reduced thickness by means of sputtering. The target has a recrystallized structure represented by the equation, A/B.ltoreq.0.6, where A is the diffraction intensity of the (110) planes as determined by X-ray diffraction of a sputtered surface, and B is the diffraction intensity as determined from the sum of the (110), (200) and (211) planes. The target preferably has a deflective strength of above 500 MPa and an average crystal grain of below 50 .mu.m. The chromium target is produced by subjecting a starting chromium material to at least one stage of plastic working at a temperature of not higher than 1,000.degree. C., and subsequently by heat-treating the resulting chromium material for recrystallization at a temperature of higher than the recrystallization temperature of the chromium material but not higher than 1,200.degree. C.
    Type: Grant
    Filed: March 29, 1996
    Date of Patent: February 17, 1998
    Assignee: Hitachi Metals, Ltd.
    Inventors: Hideo Murata, Shigeru Taniguchi
  • Patent number: 5701574
    Abstract: A method of producing a sliding sleeve for a synchronizer of a speed-changing gear, the sliding sleeve being comprised of a sintered powder metal compact having a claw extending along an inner periphery of the sleeve, and the claw consisting of teeth having opposite end faces and a cross-section between the end faces which is reduced relative to an undercut portion at at least one of the end faces, which method comprises the steps of sintering the powder metal compact having the claw consisting of the teeth having the opposite end faces and the reduced cross-section extending between the end faces, and then applying solely an axial upsetting force to the one end face to form the undercut portion thereat while leaving the reduced cross-section unchanged.
    Type: Grant
    Filed: February 6, 1996
    Date of Patent: December 23, 1997
    Assignee: Miba Sintermetall Aktiengesellschaft
    Inventors: Karl Derflinger, Herbert Schmid, Johann Dickinger