Aluminum Patents (Class 423/625)
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Publication number: 20100147689Abstract: The invention provides a method for modifying a surface of aluminum oxide. Aluminum oxide is contacted with a hydrogen peroxide aqueous solution having 5-70 volume % of hydrogen peroxide for 20 minutes to 3 hours. The invention also provides an electroosmosis pump and electric power generator having a porous aluminum oxide membrane modified by the above method.Type: ApplicationFiled: May 27, 2009Publication date: June 17, 2010Applicant: INDUSTRIAL TECHNOLOGY RESEARCH INSTITUTEInventors: Yu-Feng Chen, Yen-I Chou
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Patent number: 7727500Abstract: Disclosed are adhesive coating compositions containing a metal peroxide for producing clear colorless adhesive coatings on substrates, particularly micro particulate substrates. In one preferred embodiment the nanoparticle coatings are chemically active and function at a high level of efficiency due to the high total surface area of the micro particulate substrate. Also disclosed are coated substrates and compositions having nanoparticles bound to a substrate by the coating compositions.Type: GrantFiled: March 8, 2007Date of Patent: June 1, 2010Assignee: PURETI, Inc.Inventor: John W. Andrews
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Patent number: 7727301Abstract: A method and an assembly for treating minerals using microwave energy are disclosed. The method includes exposing a moving bed, preferably a mixed moving bed, of mineral particles to pulsed high energy microwave energy so that at least substantially all particles receive at least some exposure to microwave energy.Type: GrantFiled: September 30, 2005Date of Patent: June 1, 2010Assignee: Technological Resources Pty. LimitedInventor: Raymond Walter Shaw
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Patent number: 7708975Abstract: There is described a process for preparing metal oxide particles which are substantially free of coarse tail from an oxidizing agent and a vaporous metal reactant in a flow reactor; comprising, (a) directing a flow of the metal reactant into a contacting region of the flow reactor; comprising (a) passing a flow of oxidizing agent through a high temperature zone of the flow reactor to form a flow of hot oxidizing agent and directing the flow of the hot oxidizing agent onto the contacting region of the flow reactor at a flow condition sufficient to form a reaction stream comprising a flow of hot oxidizing agent, a flow of metal reactant and a diffusive flow of the hot oxidizing agent and the metal reactant, the temperature of the hot oxidizing agent being at least sufficient to initiate oxidation of the metal reactant in the diffusive flow; (c) passing the reaction stream into a reaction zone of the flow reactor, while simultaneously introducing a flow of an upper cooling fluid substantially coaxially with theType: GrantFiled: July 18, 2005Date of Patent: May 4, 2010Assignee: E.I. du Pont de Nemours and CompanyInventors: Juergen Kurt Plischke, Stephan Claude de la Veaux, Scott Rickbeil Frerichs, Jodi Lynn Witt, Christian Normand
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Patent number: 7704471Abstract: A Bayer process comprises grinding and then digestion of bauxite by bringing it into contact with a sodium aluminate liquor. Digestion consists of forming a slurry that is then treated to separate insoluble residues from the sodium aluminate liquor. The liquor is then crystallized and recycled back to green liquor after having been separated from the alumina trihydrate precipitated during crystallization. The process comprises a predesilication treatment during which the ground bauxite, before digestion, is brought into contact with an aqueous sodic solution that has a content of carbonates, sulphates and possibly chlorides which, expressed as a percentage related to the caustic concentration, has less than half of the corresponding impurities content of the spent liquor. Preferably, the pure caustic soda used to compensate for caustic soda losses in the Bayer circuit, previously injected just after evaporation, is now added in the aqueous sodic solution for the predesilication treatment.Type: GrantFiled: May 11, 2005Date of Patent: April 27, 2010Assignee: Aluminium PechineyInventors: Eric Tizon, Clotilde Fryns
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Publication number: 20100098780Abstract: The present invention has an object to provide a flaky particulate material giving skin an excellent smoothness, which is free from whitening problem upon use thereof owing to its high transparency. The present invention also has another object to provide a cosmetic composition containing the flaky particulate material. The present invention relates to flaky particulate material, which has an average coefficient of friction is not more than 0.50, and a total light transmittance is not less than 85%. A particle in the flaky particulate material comprises a substrate particle made of one material selected from the group consisting of mica, a synthetic mica, sericite, talc, barium sulfate and aluminum oxide. The present invention provides a flaky particulate material that gives skin excellent smoothness, a natural tone, and a matt appearance. The flaky particulate material of the present invention gives a cosmetic composition which provides great comfort of use, and an excellent appearance.Type: ApplicationFiled: February 13, 2007Publication date: April 22, 2010Applicant: SAKAI CHEMICAL INDUSTRY CO., LTD.Inventors: Keiji Ono, Takuro Ashida, Hiroyuki Izumikawa, Hirobumi Yoshida
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Publication number: 20100092762Abstract: A dispersion containing a high-surface-area, pyrogenically-produced aluminium oxide with a surface area and BET of more than 115 m2/g and a Sears number of more than 8 ml/2 g, is produced by mixing a high-surface-area, pyrogenically-produced aluminium oxide having a BET specific surface area of more than 115 m2/g and a Sears number of more than 8 ml/2 g, with water, setting a pH value of 2 to 11 (preferably 3 to 8) and dispersing the mixture by the introduction of controlled shearing forces. It can be used for the production of Inkjet media, digital imaging products and other printing medium.Type: ApplicationFiled: July 10, 2009Publication date: April 15, 2010Inventors: Heinz Lach, Gerrit Schneider, Thomas Scharfe
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Patent number: 7691362Abstract: A method for producing an ?-alumina powder is provided. T method for producing an ?-alumina powder comprising steps of: (1) pulverizing a metal compound having a full width at half maximum (Ho) of a main peak in XRD pattern to obtain a seed crystal having a full width at half maximum (H) of the main peak in XRD pattern in the presence of pulverizing agent, (2) mixing the obtained seed crystal with an aluminum salt, (3) calcining the mixture, and wherein a ratio of H/Ho is 1.06 or more.Type: GrantFiled: August 26, 2005Date of Patent: April 6, 2010Assignee: Sumitomo Chemical Company, LimitedInventors: Hajime Maki, Yoshiaki Takeuchi, Kazuhisa Kajihara
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Publication number: 20100075055Abstract: A process to deposit an Alpha Alumina (?-Al2O3) crystalline coating on a substrate surface, wherein the process includes hydrothermal synthesis of the ?-Al2O3 crystalline coating.Type: ApplicationFiled: September 4, 2009Publication date: March 25, 2010Applicant: Sawyer Technical Materials LLCInventor: Wojciech L. Suchanek
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Patent number: 7674525Abstract: The present invention provides a process for producing fine ?-alumina particles, which comprises sintering a mixture of ?-alumina precursor particles and seed crystal particles, wherein a center particle diameter of the seed crystal particles is 40 nm or less, and a ratio of the number of coarse particles having a particle diameter greater than 100 nm to the number of the total particles is 1% or less.Type: GrantFiled: March 15, 2006Date of Patent: March 9, 2010Assignee: Sumitomo Chemical Company, LimitedInventors: Hajime Maki, Yoshiaki Takeuchi, Yuzuru Saitou
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Publication number: 20100056816Abstract: This invention relates to shaped porous bodies of alpha-alumina platelets which are useful as catalyst carriers, filters, membrane reactors, and preformed bodies for composites. This invention also relates to processes of making such shaped bodies and processes for modifying the surface composition of alpha-alumina.Type: ApplicationFiled: July 20, 2007Publication date: March 4, 2010Inventors: Sten A. Wallin, Juliana G. Serafin, Madan M. Bhasin, Steven R. Lakso
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Publication number: 20100051855Abstract: Herein disclosed is alumina powder incorporated into a composition which should have excellent heat conduction and used as a heat-radiating member and for sealing a semiconductor. The spherical ?-alumina powder has an average sphericity of not less than 0.93 and a content of ?-crystalline form is not less than 95% and the spherical ?-alumina powder is prepared according to the method, which comprises the steps of: (1) softening metallic aluminum powder or alumina powder through the treatment with a flame; (2) solidifying the softened powder by passing the same through a zone maintained at a temperature ranging from 800 to 500° C.; (3) increasing the content of ?-phase by passing the solidified powder through a zone maintained at a temperature ranging from 950 to 1,500° C.; and (4) collecting the resulting powdery product while cooling the same.Type: ApplicationFiled: October 31, 2006Publication date: March 4, 2010Applicant: Denki Kagaku Kogyo Kabushiki KaishaInventors: Osamu Kunitomo, Takaaki Tanaka
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Patent number: 7669658Abstract: A method for making hollow spheres of alumina or aluminate comprises: coating polymeric beads with an aqueous solution of an alumoxane, drying the beads so as to form an alumoxane coating on the beads; heating the beads to a first temperature that is sufficient to convert the alumoxane coating to an amorphous alumina or aluminate coating and is not sufficient to decompose the polymeric beads; dissolving the polymeric bead in a solvent; removing the dissolved polymer from the amorphous alumina or aluminate coating; and heating the amorphous alumina or aluminate coating to a second temperature that is sufficient to form a hollow ceramic sphere of desired porosity and strength. The hollow spheres can be used as proppants or can be incorporated in porous membranes.Type: GrantFiled: December 18, 2006Date of Patent: March 2, 2010Assignee: William Marsh Rice UniversityInventors: Andrew R. Barron, Kimberly A. DeFriend
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Publication number: 20100047157Abstract: There is provided a process for the preparation of a alumina precursor powder from aluminum hydroxide powder obtained by hydrolysis of aluminum alkoxide which precursor enables to provide alumina powder with a high volumetric efficiency. Such process comprises mixing aluminum hydroxide powder obtained by hydrolysis of an aluminum alkoxide with the following aqueous medium so as to obtain an aluminum hydroxide mixed slurry and then drying the aluminum hydroxide mixed slurry: aqueous medium: water or a medium mixture of water and a water-soluble alcohol wherein a water content in said medium mixture is not less than 15 parts by weight to 100 parts by weight of the medium mixture.Type: ApplicationFiled: August 25, 2009Publication date: February 25, 2010Applicant: SUMITOMO CHEMICAL COMPANY, LIMITEDInventors: Noriaki FUJITA, Shinji FUJIWARA
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Publication number: 20100040536Abstract: A method for producing boehmite particles includes subjecting powder of aluminum hydroxide to hydrothermal reaction together with a nucleation agent, thereby obtaining boehmite particles having an average primary particle size of 0.6 ?m or less and including primary particles each having a hexahedral shape. A method for producing alumina particles includes: drying the boehmite particles produced by the above described method; calcining the boehmite particles, which have been dried, to obtain alumina particles; and disintegrating the obtained alumina particles.Type: ApplicationFiled: August 18, 2009Publication date: February 18, 2010Applicant: FUJIMI INCORPORATEDInventors: Hitoshi Morinaga, Muneaki Tahara, Keiji Ashitaka
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Publication number: 20100040535Abstract: ?-Alumina powder having a purity of at least 99.99% by weight, a specific surface area of from 0.1 to 2.0 m2/g, a relative density of from 55 to 90%, and a closed porosity of 4% or less, wherein in a weight-based particle size distribution obtained by the dry sieving test according to JIS K0069 (1992), an amount of particles having a particle size of less than 75 ?m is 5% by weight or less; an amount of particles having a particle size exceeding 2.8 mm is 15% by weight or less; and at least one frequency maximum peak appears in a particle size range of 100 ?m or more and to less than 850 ?m. This ?-alumina powder can be charged in a crucible at a high bulk density, from which sapphire having a few voids can be produced without causing the oxidation of a crucible in a heat melting step.Type: ApplicationFiled: September 18, 2007Publication date: February 18, 2010Applicant: SUMITOMO CHEMICAL COMPANY, LIMITEDInventors: Norifumi Azima, Shinji Fujiwara
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Patent number: 7658907Abstract: Titanium-aluminium mixed oxide powder with a proportion of aluminium oxide of less than 1 wt. % or a proportion of titanium dioxide of less than 5 wt. %, wherein the sum of the proportions of titanium dioxide and aluminium oxide is at least 99.7 wt. %. It is produced by transferring a vaporous starting compound of the quantitatively greater component of the mixed oxide into a mixing chamber by means of primary air and a vaporous starting compound of the quantitatively smaller component of the mixed oxide by means of an inert gas, and burning the mixture mixed with hydrogen in a mixing chamber into a reaction chamber. It can be used as a catalyst support.Type: GrantFiled: December 20, 2005Date of Patent: February 9, 2010Assignee: Degussa GmbHInventors: Kai Schumacher, Roland Schilling, Harald Alff, Helmut Roth
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Patent number: 7658896Abstract: Process for the treatment of bauxite (10) by alkaline digestion, typically using the Bayer process in order to obtain alumina hydrate, characterized in that ground bauxite (11, 15) is added directly into an alkaline solution (21a) that is drawn off and that will be reinserted into the Bayer aluminate liquor circuit (20), the said alkaline solution (21a) being heated at a temperature such that after the said ground bauxite (11, 15) and the said alkaline solution have been brought into contact, the temperature of the slurry resulting from this mix is greater than a temperature close to the boiling temperature at atmospheric pressure, in other words typically greater than 95° C. and preferably greater than or equal to the boiling temperature at atmospheric pressure.Type: GrantFiled: October 21, 2003Date of Patent: February 9, 2010Assignee: Pechiney RhenaluInventors: Nicolas Mugnier, Patrick Leizour
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Publication number: 20100028674Abstract: Nanofibers and methods for making the nanofibers are described. Porous metal oxide nanofibers and porous metal oxide nanofibers comprising metal nanoparticles made via electrospinning methods are also described.Type: ApplicationFiled: July 31, 2008Publication date: February 4, 2010Inventor: Fredrick O Ochanda
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Publication number: 20100021374Abstract: Provided is a process for producing a high-purity ?-alumina in which an Si content, an Fe content, a Ca content, and an Na content are simultaneously removed. The high-purity ?-alumina is produced by burning aluminum hydroxide having an Na content of 0.11 mass % or less, an Fe content of 6 ppm or less, a Ca content of 1.5 ppm or less, and an Si content of 10 ppm or less as impurities in terms of alumina respectively, and having an average particle diameter of 55 ?m or less at a burning temperature of 1,100 to 1,500° C. by using a burning vessel containing Al2O3 in a range of 85 to 93 wt % and SiO2 in a range of 7 to l4 wt % and subjecting the obtained ?-alumina to wash treatment.Type: ApplicationFiled: December 4, 2007Publication date: January 28, 2010Applicant: NIPPON LIGHT METAL COMPANY, LTD.Inventors: Jun Mizuno, Toshihiro Matsuba, Shigeo Yamamoto, Takashi Yamada
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Patent number: 7651676Abstract: There is provided a process for preparing aluminium chloride comprising: leaching aluminium dross residues with HCl so as to obtain a mixture comprising a solid and a liquid; and hydrochlorinating the liquid obtained from the mixture, so as to form a precipitate comprising aluminium chloride. Such a sequence can also be used for preparing alumina. In such a case, the process can further comprise the step of converting the so-obtained aluminium chloride into alumina. In the processes previously defined, the solid so-obtained can also be leached with H2SO4, thereby generating a leachate. The leachate can also eventually be hydrochlorinated so as to increase the yield of the desired product obtained i.e. alumina or aluminium chloride.Type: GrantFiled: November 23, 2007Date of Patent: January 26, 2010Assignee: Groupe Conseil Procd Inc.Inventors: Martin Beaulieu, Stéphane Chabot, Yves Charest, Jean-François Savard
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Publication number: 20100003203Abstract: The present invention relates to methods of producing surface-modified nanoparticulate particles at least of one metal oxide, metal hydroxide and/or metal oxide hydroxide, and aqueous suspensions of these particles. The invention further relates to the surface-modified nanoparticulate particles, obtainable by these methods, at least of one metal oxide, metal hydroxide and/or metal oxide hydroxide and aqueous suspensions of these particles, and to their use for cosmetic sunscreen preparations, as stabilizer in plastics and as antimicrobial active ingredient.Type: ApplicationFiled: October 10, 2007Publication date: January 7, 2010Applicant: BASF SEInventors: Andrey Karpov, Hartmut Hibst, Jutta Kissel, Bernd Bechtloff, Hartwig Voss, Kerstin Schierle-Arndt, Valerie Andre
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Patent number: 7638105Abstract: The present invention provides ?-alumina powders comprising ?-alumina particles of which at least 80% of the ?-alumina particles have a particle size of less than 100 nm. The invention also provides slurries, particularly aqueous slurries, which comprise ?-alumina powders of the invention. The invention further provides methods of manufacturing ?-alumina powders and ?-alumina slurries of the invention and methods of polishing using same.Type: GrantFiled: August 13, 2008Date of Patent: December 29, 2009Assignee: Saint-Gobain Ceramics & Plastics, Inc.Inventor: Yuhu Wang
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Patent number: 7638455Abstract: A process for the preparation of a catalyst, which process comprises the steps of: i) mixing an alumina precursor with combustible carbon-containing fibers with a diameter in the range of from 0.5 to 5 ?m and a length of no greater than 100 ?m in an amount in the range of from 20 to 40 wt % based on the total dry mixture; ii) adding nitric acid and water to form an extrudable mass; iii) extruding the mixture to form shaped particles; iv) drying the shaped particles; v) heating the particles in an atmosphere comprising no more than 5 vol % oxygen at a temperature in the range of from 350 to 600° C.; and vi) then heating the particles in a gas mixture comprising at least 12 vol % oxygen at a temperature in the range of from 450 to 600° C.Type: GrantFiled: March 8, 2007Date of Patent: December 29, 2009Assignee: Shell Oil CompanyInventors: Peter Birke, Frank Heinz Goerlitz, Wigbert Gerhard Himmel, Jürgen Hunold, Hans-Heino John
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Patent number: 7638112Abstract: A method for making zinc aluminate nano-material, the method comprises the following steps. Firstly, providing a growing substrate and a growing device, and the growing device comprising a heating apparatus and a reacting room. Secondly, placing the growing substrate and a quantity of reacting materials into the reaction room, and the reacting materials comprising zinc and aluminum. Thirdly, introducing an oxygen-containing gas into the reaction room. Lastly, heating the reaction room to a temperature of 660˜1100° C.Type: GrantFiled: November 6, 2008Date of Patent: December 29, 2009Assignees: Tsinghua University, Hon Hai Precision Industry Co., Ltd.Inventors: Hai-Lin Sun, Kai-Li Jiang, Qun-Qing Li, Shou-Shan Fan
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Publication number: 20090305040Abstract: The present invention relates to a method for producing a metal oxide by heating a porous metal-organic framework material, the framework material comprising at least one at least bidentate organic compound bound to at least one metal ion by coordination, and the metal ion being selected from the metals comprising groups to 4 and 13 of the Periodic Table of the Elements, above the complete decomposition temperature of the framework material, and also to metal oxides obtainable by this method, and to the use thereof.Type: ApplicationFiled: April 12, 2007Publication date: December 10, 2009Inventors: Markus Schubert, Ulrich Müller, Natalia Trukhan
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Publication number: 20090301350Abstract: Use of pyrogenic metal oxide for the manufacture of a selfcompacting composition comprising hydraulic binders and having high early strength, the composition comprising at least one hydraulic binder and water as further constituents and the product of the BET surface area, in m2/g, of the pyrogenic metal oxide and the proportion by weight of the pyrogenic metal oxide based on the hydraulic binder being 20 to 200 m2/100 g of hydraulic binder.Type: ApplicationFiled: March 12, 2007Publication date: December 10, 2009Applicant: Evonik Degussa GmbhInventors: Christoph Tontrup, Reinhard Trettin, Michael Geyer
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Publication number: 20090297433Abstract: The invention relates to a method for obtaining ?-alumina crystals or fibers using the vapor-liquid-solid (VLS) mechanism, by controlling the slightly oxidizing atmospheres in systems that contain metal Al and SiO2. The inventive method consists of growing ?-alumina fibers using the growth of alumina fibers via VLS from Al and SiO2, and controlling the partial pressure of the different oxidizing agents, in the area known as active oxidation of Al with formation of corundum fume and active oxidation of Si with formation of silica fume in accordance with the respective Si—SiO2 and Al—Al2O3 volatility diagrams.Type: ApplicationFiled: December 22, 2006Publication date: December 3, 2009Inventors: Carmen Cerecedo Fernandez, Victor Andres Valcarcel Juárez, Francisco Guitián
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Publication number: 20090283761Abstract: A method of dividing single crystals, particularly of plates of parts thereof, is proposed, which can comprise: pre-adjusting the crystallographic cleavage plane (2?) relative to the cleavage device, setting a tensional intensity (K) by means of tensional fields (3?, 4?), determining an energy release rate G(?) in dependence from a possible deflection angle (?) from the cleavage plane (2?) upon crack propagation, controlling the tensional fields (3?, 4?) such that the crack further propagates in the single crystal, wherein G(0)?2?e(0) and simultaneously at least one of the following conditions is satisfied: ? ? G ? ? ? ? = 0 ? 2 ? ? e h ? ? if ? ? ? 2 ? G ? ? 2 ? 0 ? ? or ( 2.1 ) ? ? G ? ? ? ? 2 ? ? e h ? ? ? ? : ? ? 1 < ? < ? 2 , ( 2.Type: ApplicationFiled: November 14, 2008Publication date: November 19, 2009Inventors: Ralf HAMMER, Manfred Jurisch
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Adsorbents for Radioisotopes, Preparation Method Thereof, and Radioisotope Generators Using the Same
Publication number: 20090277828Abstract: Disclosed is a novel adsorbent for use in a 99Mo/99mTc generator, which is a medical diagnostic radioisotope generator, and in a 188W/188Re generator, which is a therapeutic radioisotope generator. The adsorbent composed of sulfated alumina or alumina-sulfated zirconia exhibits adsorption capacity superior to that of conventional adsorbents, and is stable and is thus loaded in a dry state in an adsorption column so that the radioisotope 99Mo or 188W can be adsorbed. Thus, it is possible to miniaturize the column, and such a miniaturized column is small, convenient to use, and highly efficient, and extracts a radioisotope satisfying the requirements for pharmaceuticals, and thus can be useful for radioisotope generators extracting 99mTc or 188Re.Type: ApplicationFiled: May 8, 2008Publication date: November 12, 2009Applicant: KOREA ATOMIC ENERGY RESEARCH INSTITUTEInventors: Jun Sig LEE, Hyon Soo HAN, Ul Jae PARK, Kwang Jae SON, Hyeon Young SHIN, Soon Bog HONG, Kang Duk JANG, Jong Sub LEE -
Patent number: 7615577Abstract: Aqueous dispersion containing transition aluminium oxide as only solid and a dispersant, in which—the transition aluminium oxide is present in the form of aggregates of primary particles, the content of transition aluminium oxide in the dispersion is from 40 to 65% by weight, the aggregates in the dispersion have a mean aggregate diameter of less than 100 nm,—the dispersant contains polyaluminium hydroxychloride, polyaluminium hydroxynitrate and/or polyaluminium hydroxysulphate, the dispersion has a pH of from 3 to 5.Type: GrantFiled: December 7, 2006Date of Patent: November 10, 2009Assignee: Evonik Degussa GmbHInventors: Wolfgang Lortz, Heinz Lach, Joachim Von Seyerl
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Patent number: 7615201Abstract: By using a halogen-free siloxane and an organometallic compound containing at least one metal other than silicon as feed stocks, and simultaneously atomizing and burning them in a flame, spherical particles of silica-containing compound oxide are prepared which are substantially halogen-free, consist of 0.5-99% by weight of metal oxides and the balance of silica, and have a particle size of 10 nm to 3 ?m. The particles are useful as a filler in epoxy resin base semiconductor sealants, a refractive index modifier or the like.Type: GrantFiled: July 23, 2002Date of Patent: November 10, 2009Assignee: Shin-Etsu Chemical Co., Ltd.Inventors: Yoshiharu Konya, Koichiro Watanabe, Susumu Ueno
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Publication number: 20090267024Abstract: The present invention relates to a novel inorganic sulfate ion scavenger that is environmentally friendly and has high performance. With regard to the inorganic sulfate ion scavenger of the present invention, the amount of ionic impurities leaching out in pure water is no greater than 500 ppm and the amount of sulfate ion leaching out in pure water is no greater than 30 ppm. Furthermore, the present invention relates to an inorganic scavenging composition comprising the inorganic scavenger, and to an electronic component-sealing resin composition, an electronic component-sealing material, an electronic component, a varnish, an adhesive, a paste, and a product employing the inorganic scavenger or the inorganic scavenging composition.Type: ApplicationFiled: December 25, 2006Publication date: October 29, 2009Inventor: Yasuharu Ono
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Patent number: 7601324Abstract: The method for synthesizing metal oxide nanopowder produces powders of nanoparticle size from metals having relatively low boiling temperatures, such as zinc, tellurium, bismuth, and strontium by vapor-phase oxidation using a conventional 2.45 GHz microwave oven. The energy that initiates the combustion comes from the microwave through a susceptor tube that absorbs radiant microwave energy and transfers it to the metal, which evaporates to small particles inside the susceptor tube and then combusts in air to form nanosize powder. The susceptor is made of silicon carbide composite material.Type: GrantFiled: July 11, 2008Date of Patent: October 13, 2009Assignee: King Fahd University of Petroleum and MineralsInventor: Saleh I. Al-Quraishi
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Publication number: 20090232726Abstract: A method for manufacturing alumina particles having a size on the order of nanometers and an excellent heat resistance at about 1000° C. comprises providing a liquid medium containing particles made of ?-alumina or boehmite alumina hydrate and a metal component such as La, Ba, Mg or the like, and thermally treated the alumina and the metal component in the liquid medium in a pressurized condition. The thermally treated particles are dried and sintered at a temperature of from 900° C. to lower than 1200° C. to provide alumina particles which has a metal aluminate crystal phase thereon. The metal component is formed as a solid solution as a surface layer of individual alumina particles by subjecting the alumina particles and the metal component to the thermal treatment prior to sintering, so that the metal aluminate crystal phase can be formed by sintering at temperatures lower than ordinary sintering temperatures.Type: ApplicationFiled: March 12, 2009Publication date: September 17, 2009Applicant: DENSO CORPORATIONInventors: Hiroaki Yotou, Miho Itoh, Tomoya Itakura
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Patent number: 7582277Abstract: A boehmite particulate material is disclosed. The material is formed by a process that includes providing a boehmite precursor and boehmite seeds in a suspension, and heat treating the suspension to convert the boehmite precursor into boehmite particulate material. The boehmite particulate material has an aspect ratio of not less than 3:1.Type: GrantFiled: August 6, 2007Date of Patent: September 1, 2009Assignee: Saint-Gobain Ceramics & Plastics, Inc.Inventors: Ralph Bauer, Margaret L. Skowron, Martin Barnes, Doruk O. Yener
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Publication number: 20090213591Abstract: The present invention relates to a reflective member (7). The reflective member (7) includes a reflective layer 61 (7) formed to be porous using an inorganic material. The reflective layer 61 (7) has a porosity of 15-43%. Such reflective layer 61 (7) is formed by partly combining a plurality of inorganic particles with each other.Type: ApplicationFiled: March 25, 2006Publication date: August 27, 2009Applicant: KYOCERA CORPORATIONInventors: Kousuke Katabe, Yuki Mori
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Patent number: 7579014Abstract: The present invention encompasses novel mesoporous compositions comprising vitamin E and alumina, and methods for their synthesis. The mesoporous compositions of the present invention have applications as drug-delivery vehicles.Type: GrantFiled: December 27, 2006Date of Patent: August 25, 2009Assignee: Board of Regents the University of Texas SystemInventors: Ying Ma, Kenneth J. Balkus, Jr.
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Patent number: 7575736Abstract: A process for producing plate-like alumina particles with a high aspect ratio is described. Nano-sized particles of an aluminium precursor compound, optionally formed by milling, are mixed with a sufficient volume fraction of a diluent and heat treated to form substantially discrete plate-like alpha alumina particles dispersed in the diluent. A mineraliser may be added to lower the effective melting point of the system. Substantially discrete plate-like particles may be formed without agitation when the heat treatment is conducted below the melting point of the diluent.Type: GrantFiled: January 6, 2004Date of Patent: August 18, 2009Assignee: Advanced Nano Technologies Pty. Ltd.Inventors: John Sydney Robinson, Lara Michelle Heatley, Takuya Tsuzuki, David Andrew Lee, Paul Gerard McCormick
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Patent number: 7576035Abstract: A pillar-shaped honeycomb structure has a plurality of cells longitudinally placed in parallel with one another with a wall portion therebetween, wherein the honeycomb structure mainly includes inorganic fibers which form the honeycomb structure without lamination interfaces.Type: GrantFiled: April 7, 2008Date of Patent: August 18, 2009Assignee: Ibiden Co., Ltd.Inventors: Kazushige Ohno, Tomokazu Oya
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Publication number: 20090202427Abstract: Process for preparing mixed metal oxide powders Abstract Process for preparing a mixed metal oxide powder, in which oxidizable starting materials are evaporated in an evaporation zone of a reactor and oxidized in the vaporous state in an oxidation zone of this reactor, the reaction mixture is cooled after the reaction and the pulverulent solids are removed from gaseous substances, wherein at least one pulverulent metal, together with one or more combustion gases, is fed to the evaporation zone, the metal is evaporated completely in the evaporation zone under nonoxidizing conditions, an oxygen-containing gas and at least one metal compound are fed, separately or together, in the oxidation zone to the mixture flowing out of the evaporation zone, the oxygen content of the oxygen-containing gas being at least sufficient to oxidize the metal, the metal compound and the combustion gas completely.Type: ApplicationFiled: May 16, 2007Publication date: August 13, 2009Applicant: EVONIK DEGUSSA GMBHInventors: Stipan Katusic, Guido Zimmermann, Michael Krämer, Horst Miess, Edwin Staab
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Patent number: 7572423Abstract: The invention provides a process for producing fumed metal oxide particles comprising providing a stream of a liquid feedstock comprising a volatizable, non-halogenated metal oxide precursor, providing a stream of a combustion gas having a linear velocity sufficient to atomize and combust or pyrolyze the liquid feedstock, and injecting the stream of the liquid feedstock into the stream of combustion gas to form a reaction mixture such that the liquid feedstock is atomized and subjected to a sufficient temperature and residence time in the combination gas stream for fumed metal oxide particles to form before the combustion gas temperature is reduced below the solidifying temperature of the metal oxide particle. The invention further provides fumed silica particles having a relatively small aggregate size and/or narrow aggregate size distribution.Type: GrantFiled: November 24, 2003Date of Patent: August 11, 2009Assignee: Cabot CorporationInventor: Yakov E. Kutsovsky
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Patent number: 7553474Abstract: It is an object to provide a method for producing stable alkaline metal oxide sols having a uniform particle size distribution. The method comprises the steps of: heating a metal compound at a temperature of 60° C. to 110° C. in an aqueous medium that contains a carbonate of quaternary ammonium; and carrying out hydrothermal processing at a temperature of 110° C. to 250° C. The carbonate of quaternary ammonium is (NR4)2CO3 or NR4HCO3 in which R represents a hydrocarbon group, or a mixture thereof. The metal compound is one, or two or more metal compounds selected from a group of compounds based on a metal having a valence that is bivalent, trivalent, or tetravalent.Type: GrantFiled: August 8, 2005Date of Patent: June 30, 2009Assignee: Nissan Chemical Industries, Ltd.Inventors: Yutaka Ohmori, Hirokazu Kato, Yoshinari Koyama, Kenji Yamaguchi
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Patent number: 7553465Abstract: Cerium oxide powder having carbonate groups and made of crystalline primary particles containing cerium oxide and having carbonate groups on the surface and in a region close to the surface, and having a BET surface area of from 25 to 150 m2/g, a mean diameter of from 5 to 50 nm, a carbonate concentration in the region close to the surface decreasing inwardly from the surface, a carbon content due to carbonate groups on the surface of from 5 to 50% by area, a carbon content due to carbonate groups at a depth of about 5 nm in a region close to the surface of from 0 to 30% by area, a content of cerium oxide calculated as CeO2 and based on the powder of at least 99.5% by weight and a content of organic and inorganic carbon of from 0.01 to 0.3% by weight. A dispersion containing this powder.Type: GrantFiled: August 11, 2006Date of Patent: June 30, 2009Assignee: Degussa AGInventors: Stipan Katusic, Michael Kroell, Michael Kraemer, Stefan Heberer, Edwin Staab, Guenther Michael
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Patent number: 7547431Abstract: A method of producing high purity nanoscale powders in which the purity of powders produced by the method exceeds 99.99%. Fine powders produced are of size preferably less than 1 micron, and more preferably less than 100 nanometers. Methods for producing such powders in high volume, low-cost, and reproducible quality are also outlined. The fine powders are envisioned to be useful in various applications such as biomedical, sensor, electronic, electrical, photonic, thermal, piezo, magnetic, catalytic and electrochemical products.Type: GrantFiled: December 10, 2002Date of Patent: June 16, 2009Assignee: PPG Industries Ohio, Inc.Inventors: Tapesh Yadav, Karl Pfaffenbach
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Publication number: 20090136757Abstract: A method of fractionating a dispersion of oxidic nanoparticles wherein at least one step of the method is a membrane crossflow filtration step, the flow of the dispersion over the membrane being brought about by means of driven rotating parts; and dispersions of oxidic nanoparticles that are obtainable by the method.Type: ApplicationFiled: November 14, 2008Publication date: May 28, 2009Applicant: EVONIK DEGUSSA GmbHInventors: Roland WURSCHE, Goetz Baumgarten, Wolfgang Lortz, Michael Kroell
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Patent number: 7534415Abstract: Mesoporous crystalline alumina compositions and process for the preparation thereof are described. The compositions are useful as catalysts and absorbents.Type: GrantFiled: December 28, 2005Date of Patent: May 19, 2009Assignee: Board of Trustees of Michigan State UniversityInventors: Thomas J. Pinnavaia, Zhaorong Zhang, Randall Hicks
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Publication number: 20090123362Abstract: A process is claimed for producing nanocrystalline ?-Al2O3 that is characterized in that nuclei are added to aluminum chlorohydrate, which is subjected to thermal treatment within less than 30 minutes, the resultant agglomerates being comminuted.Type: ApplicationFiled: July 13, 2006Publication date: May 14, 2009Inventor: Norbert Roesch
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Publication number: 20090123363Abstract: The present invention provides a method for producing an ?-alumina powder. The method for producing an ?-alumina powder comprises steps of: (1) pulverizing a metal compound having a full width at half maximum (Ho) of a main peak in XRD pattern to obtain a seed crystal having a full width at half maximum (H) of the main peak in XRD pattern, (2) mixing the obtained seed crystal with an aluminum compound, (3) calcining the mixture, and wherein a ratio of H/Ho is 1.06 or more.Type: ApplicationFiled: January 2, 2009Publication date: May 14, 2009Applicant: Sumitomo Chemical Company, LimitedInventors: Shinobu Maruno, Hajime Maki, Yoshiaki Takeuchi
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Publication number: 20090123354Abstract: A solid material is presented for the partial oxidation of natural gas. The solid material includes a solid oxygen carrying agent and a hydrocarbon activation agent. The material precludes the need for gaseous oxygen for the partial oxidation and provides better control over the reaction.Type: ApplicationFiled: November 14, 2007Publication date: May 14, 2009Inventors: Deng-Yang Jan, Joel T. Walenga, Kurt M. Vanden Bussche, Joseph A. Kocal, Lisa M. King