Aluminum Patents (Class 423/625)
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Patent number: 7531161Abstract: A modified polymer material is discloses, including a polymer base and boehmite particles provided in the polymer base, the boehmite particles are made up of mainly anisotropically shaped particles.Type: GrantFiled: March 12, 2007Date of Patent: May 12, 2009Assignee: Saint-Gobain Ceramics & Plastics, Inc.Inventors: Hui Tang, Christopher L. Mirley, Ralph Bauer
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Publication number: 20090111067Abstract: In the conventional alumina sintered bodies, a sintered body having high flexural strength, high toughness and high translucency in combination is not obtained, and a translucent alumina sintered body suitable for a dental material requiring both strength and sensuousness was not obtained. A translucent alumina sintered body having fracture toughness of 4.5 MPa·m0.5 or more, flexural strength of 350 MPa or more, and all light transmittance (sample thickness: 1 mm) to a visible light having a wavelength of 600 nm, of 60% or more is provided. The sintered body wherein sintered crystal grains are slender plate-like and/or columnar shape having an average aspect ratio of 1.5 or more and an average long axis length of 15 ?m or less is preferred.Type: ApplicationFiled: October 28, 2008Publication date: April 30, 2009Applicant: TOSOH CORPORATIONInventors: Koji Tsukuma, Isao Yamashita, Hitoshi Nagayama
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Nanocrystalline sintered bodies made from alpha aluminum oxide method for production and use thereof
Publication number: 20090098365Abstract: Nanocrystalline sintered bodies, and a method of making same, said sintered bodies based on a 95 to 100% content of alpha-aluminum oxide by weight, a Vickers hardness greater than or equal to 17.5 GPa, and a crystal structure where the average primary crystal size of the alpha-aluminum oxide is less than or equal to 100 nanometers.Type: ApplicationFiled: July 12, 2006Publication date: April 16, 2009Applicant: Center for Abrasives and Refractories Research & Developement C.A.R.R.D. GmbHInventor: Paul Moeltgen -
Patent number: 7504085Abstract: An alumina-based perovskite is formed by mixing a lanthanide source with a transitional alumina to form a dual-phase composition comprising in-situ formed LnAlO3 dispersed in alumina. The lanthanide content of the composition ranges from 6-35 wt. % to yield a high surface area composition which is useful as a catalyst or catalyst support such as for precious metals.Type: GrantFiled: May 12, 2005Date of Patent: March 17, 2009Assignee: BASF Catalysts LLCInventor: Xiaolin David Yang
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Publication number: 20090062556Abstract: A carrier for a catalyst useful for the epoxidation of an olefin which comprises an inert, refractory solid carrier is provided. The carrier has no or little absolute volume from small pores, of less than 1 micrometer, and large pores, of above 5 micrometer. By “no or little absolute volume from small pores of less than 1 micron” it is meant that the pore volume of such pores is less than 0.20 ml/g. By “no or little absolute volume from large pores of above 5 micron” it is meant that the pore volume of such pores is less than 0.20 ml/g. The invention further provides a catalyst useful for the epoxidation of an olefin supported on such a carrier and a process for the oxidation of an olefin, especially ethylene, to an olefin oxide, especially ethylene oxide.Type: ApplicationFiled: August 30, 2007Publication date: March 5, 2009Applicant: SD LIZENZVERWERTUNGSGESELLSCHAFT MBH & CO. KGInventor: Serguei Pak
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Publication number: 20090054224Abstract: A method of preparing a catalyst support is described comprising washing a precipitated metal oxide material with water and/or an aqueous solution of acid and/or base such that contaminant levels in said precipitated metal oxide are reduced. The method may be applied to precipitated alumina materials to reduce contaminants selected from sulphur, chlorine, Group 1 A and Group 2A metals. The catalyst supports may be used to prepare catalysts for the Fischer-Tropsch synthesis of hydrocarbons.Type: ApplicationFiled: March 21, 2006Publication date: February 26, 2009Applicant: Johnson Matthey PicInventors: John L. Casci, Elizabeth M. Holt, Adel F. Neale
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Publication number: 20090053482Abstract: A method of reducing dye fade of a printed inkjet image comprises the step of depositing a layer of Al2O3 over the image. Also contemplated is an inkjet printer that contains a depositable source of Al2O3.Type: ApplicationFiled: August 21, 2008Publication date: February 26, 2009Inventors: Julie Baker, Nicholas J. Dartnell
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Patent number: 7491379Abstract: A method for producing nano-scale theta (?)-phase alumina microparticles is disclosed. The nano-scale ?-phase alumina microparticles are uniform in particle size and highly phase-pure. They are obtained by controlling the ratio of boehmite mixed with the ?-phase alumina initial powders, followed by at least one phase transformation. Therefore, the nano-scale ?-phase alumina microparticles produced by the present method have more uniform particle size and highly purer phase. As such for the production of nano-scale ?-phase alumina microparticles, the present method saves more process time and cost, and it provides an advantage such as the clean production.Type: GrantFiled: March 21, 2006Date of Patent: February 17, 2009Assignee: National Cheng Kung UniversityInventors: Fu-Su Yen, Rung-Je Yang
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Patent number: 7488464Abstract: Methods and systems for processing metal oxides from metal containing solutions. Metal containing solutions are mixed with heated aqueous oxidizing solutions and processed in a continuous process reactor or batch processing system. Combinations of temperature, pressure, molarity, Eh value, and pH value of the mixed solution are monitored and adjusted so as to maintain solution conditions within a desired stability area during processing. This results in metal oxides having high or increased pollutant loading capacities and/or oxidation states. These metal oxides may be processed according to the invention to produce co-precipitated oxides of two or more metals, metal oxides incorporating foreign cations, metal oxides precipitated on active and inactive substrates, or combinations of any or all of these forms.Type: GrantFiled: July 28, 2004Date of Patent: February 10, 2009Assignee: EnviroScrub Technologies CorporationInventors: Charles F. Hammel, Richard M. Boren
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Patent number: 7485282Abstract: A process is described for the synthesis of metal oxides in a nanometric particle form that cannot be easily obtained by conventional bulk synthesis techniques. The method makes use of Colloid Occluded Carbons (COC) and Colloid Imprinted Carbons (CIC) as reagents and as templating agents for the preparation of metal oxides in nanometric particle form. The nanometric particles are suitable useful in the field of chemical catalysis, particularly for petroleum refining when in porous form, and as sensors, optical wave guides, and coatings.Type: GrantFiled: March 23, 2005Date of Patent: February 3, 2009Assignee: Board of Trustees of Michigan State UniversityInventors: Thomas J. Pinnavaia, Seong-Su Kim
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Patent number: 7482382Abstract: The present invention is directed to novel sol-gel methods in which metal oxide precursor and an alcohol-based solution are mixed to form a reaction mixture that is then allowed to react to produce nanosized metal oxide particles. The methods of the present invention are more suitable for preparing nanosized metal oxide than are previously-described sol-gel methods. The present invention can provide for nanosized metal oxide particles more efficiently than the previously-described sol-gel methods by permitting higher concentrations of metal oxide precursor to be employed in the reaction mixture. The foregoing is provided by careful control of the pH conditions during synthesis and by ensuring that the pH is maintained at a value of about 7 or higher.Type: GrantFiled: May 19, 2004Date of Patent: January 27, 2009Assignees: The Texas A&M University System, Kaneka CorporationInventors: Yuntao Li, Hung-Jue Sue, Riichi Nishimura, Nobuo Miyatake
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Publication number: 20090013906Abstract: The invention relates to a metallic effect pigment, which metallic effect pigment has a substantially homogeneous chemical composition comprising at least one metal M and having an average content of oxygen of from 25 to 58 atomic percent, based on the total content of M and oxygen. The invention further relates to a method for the production of said metallic effect pigment.Type: ApplicationFiled: February 14, 2007Publication date: January 15, 2009Inventors: Martin Fischer, Wolfgang Herzing, Bernhard Geissler, Ralph Schneider
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Publication number: 20090016954Abstract: A method for the agglomeration of alumina particles, the method comprising the steps of comminuting a plurality of alumina particles having a soda content of less than approximately 0.4% by weight to a D50 of less than 12?, adding a quantity of pseudo-boehmite as an aqueous suspension having a pH of from about 2 to 6 to the plurality of alumina particles to form a mixture such that the quantity of pseudo-boehmite is between about 0.8 wt % and 5 wt % based on weight of the mixture, and spray drying the mixture to produce agglomerated granules.Type: ApplicationFiled: September 5, 2008Publication date: January 15, 2009Applicant: ALCOA WORLD ALUMINA LLCInventors: Barry James Robson, Ronald Gallagher
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Patent number: 7476440Abstract: An alumina particle (1) of the present invention has an alumina body with a short axis length (b) of 1 to 10 nm, a long axis length (a) of 20 to 400 nm and an aspect ratio (a/b) of 5 to 80. The alumina body is expressed by a Formula I, and n is not less than 0. Al2O3.Type: GrantFiled: August 10, 2005Date of Patent: January 13, 2009Assignee: Nissan Motor Co., Ltd.Inventors: Takashi Oda, Yasuaki Kai, Tomohiro Ito
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Patent number: 7476272Abstract: The present invention relates to Aluminum trihydrate slurries comprising aluminum trihydrate particles, an acrylic dispersant, citric acid, synthetic hectorite clay, optionally a compound to adjust pH, a biocide and water. These slurries may be mixed with titanium dioxide slurries to produce a stable slurry blends useful in paper and paper-board applications.Type: GrantFiled: November 29, 2006Date of Patent: January 13, 2009Assignee: E.I. Du Pont de Nemours & CompanyInventors: Maureen A. Defeo, Glenn Richard Evers, Patrick F. McIntyre
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Publication number: 20080318760Abstract: The present invention is directed to a noise suppressor for electronic signals. The noise suppressor at least includes Aluminum Oxide (Al2O3) that is sintered under high temperature, resulting in ceramic Aluminum Oxide (Al2O3) for effectively absorbing or suppressing noise, and reshaping the waveform or filtering waveform glitch of the electronic signals.Type: ApplicationFiled: September 4, 2008Publication date: December 25, 2008Inventors: Cheng-Cheng Wu, Chien-Lung Chen, Cheng-Fu Wu
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Patent number: 7468169Abstract: This invention provides a production process, which can stably produce high-quality satin white (calcium trisulfoaluminate) having very small and homogeneous particulate shapes suitable for incorporation into coated paper for printing, and an apparatus for use in said process. In this process for producing calcium trisulfoaluminate, a calcium hydroxide suspension (A) is reacted with an aqueous aluminum sulfate solution (B) to produce calcium trisulfoaluminate (C). The aqueous aluminum sulfate solution (B) is added in plurality of stages to the calcium hydroxide suspension (A). At least any one stage of the plurality of stages addition, addition of the aqueous aluminum sulfate solution (B) to the calcium hydroxide suspension (A) is carried out in such a manner that the aqueous aluminum sulfate solution (B) is continuously added to the calcium hydroxide suspension (A) being continuously transferred.Type: GrantFiled: February 2, 2007Date of Patent: December 23, 2008Assignee: OJI Paper Co., Ltd.Inventors: Takayuki Kishida, Yuichi Ogawa, Yoshiki Kojima, Takuya Ono, Kenichi Mitsui, Tetsuya Hirabayashi, Masaki Nakano
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Publication number: 20080311031Abstract: The invention provides a method for the formation of small-size metal oxide particles, comprising the steps of a) preparing a starting aqueous solution comprising at least one of metallic ions and complexes thereof, at a concentration of at least 0.1 % w/w of the metal component; b) maintaining the solution at a temperature lower than 50° C. for a retention time in which hydrolysis takes place, the extent of the hydrolysis being sufficient to produce O.1 mmol protons per mmol of metal present in solution, wherein the time does not exceed 14 days, to form a system containing a retained solution; and c) adjusting the conditions in the system by at least one of the steps of: i) heating the retained solution to elevate the temperature thereof by at least 1° C.; ii) changing the pH of the retained solution by at least 0.1 units; and iii) diluting the retained solution by at least 20% whereby there are formed particles, wherein the majority of the particles formed are between about 2 nm and about 500 nm in size.Type: ApplicationFiled: December 21, 2006Publication date: December 18, 2008Applicant: JOMA INTERNATIONAL ASInventors: Asher Vitner, Aharon Eyal
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Publication number: 20080311032Abstract: A method of manufacturing aluminum oxide (Al2O3) substrate is disclosed. In this method, an aluminum planking is provided first, and then proceeding a chemical reaction is proceeded on the surface of the aluminum planking to form an Al2O3 layer, and finally, the aluminum oxide layer is separated from the aluminum planking by corroding the aluminum portion of the aluminum planking with chemical solution, grinding the aluminum portion or slicing the aluminum portion.Type: ApplicationFiled: October 25, 2007Publication date: December 18, 2008Inventor: Tsung-Ting Sun
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Publication number: 20080305025Abstract: The invention provides a method for the formation of small-size metal oxide particles, comprising the steps of: a) preparing a starting aqueous solution comprising at least one of metallic ion and complexes thereof, at a concentration of at least 0.1% w/w of the metal component; b) preparing a modifying aqueous solution having a temperature greater than 50° C.; c) contacting the modifying aqueous solution with the starting aqueous solution in a continuous mode in a mixing chamber to form a-modified system; d) removing the modified system from the mixing chamber in a plug-flow mode; wherein the method is characterized in that: i) the residence time in the mixing chamber is less than about 5 minutes; and iii) there are formed particles or aggregates thereof, wherein the majority of the particles formed are between about 2 nm and about 500 nm in size.Type: ApplicationFiled: December 21, 2006Publication date: December 11, 2008Applicant: Joma International ASInventors: Asher Vitner, Aharon Eyal
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Publication number: 20080305333Abstract: This invention relates to crystalline boehmitic aluminas the crystallites of which exhibit unusual dimensional differences in the space directions 020 and 120. This invention further relates to a method for preparing such aluminas and the follow-up products obtained therefrom by calcination.Type: ApplicationFiled: August 13, 2008Publication date: December 11, 2008Inventors: Klaus Noweck, Jurgen Schimanski, Jens Juhl, Frank Michael Bohnen, Reiner Glockler, Arnold Meyer
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Patent number: 7459104Abstract: A lead free, thick film heating element. Known thick film heating elements contain environmentally hazardous material such as lead. This is particularly problematic when manufacturing thick film heating elements, as lead is often used in thick film formulations to allow the glass-based thick film to be processed at low firing temperatures. Using composite sol gel technology, the present invention provides a method to produce a lightweight mica-based thick film heating element based on thick film materials that are free from lead or cadmium. This mica-based element is lightweight, has the performance advantages of a thick film heating element, and may be processed at a low temperature using thick film materials.Type: GrantFiled: July 18, 2006Date of Patent: December 2, 2008Assignee: Datec Coating CorporationInventors: Timothy Russell Olding, David Andrew Barrow, Mary Ann Ruggiero
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Publication number: 20080279761Abstract: A process for producing a low-soda alumina comprising calcining aluminum hydroxide in a calciner in the presence of a soda-removal agent, wherein the alumina dust produced in the calciner is sorted by particle size and collected in a dust collector and at least a portion of the collected alumina dust is subjected to a soda-removal process and is then returned to the calciner. An apparatus for producing a low-soda alumina, comprising a calciner for calcining aluminum hydroxide in the presence of a soda-removal agent, by which alumina dust is produced; a unit connected to the calciner for collecting, by particle size, the alumina dust; a unit for removing soda from a slurry containing at least a portion of the collected alumina dust; and a circuit for returning the soda-removed alumina dust back into the calciner.Type: ApplicationFiled: June 16, 2005Publication date: November 13, 2008Inventors: Kiichi Kimura, Takayoshi Komiya
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Publication number: 20080267852Abstract: Process for preparing pulverulent solids, in which one or more oxidizable and/or hydrolysable metal compounds are reacted in a high-temperature zone in the presence of oxygen and/or steam, the reaction mixture is cooled after the reaction, and the pulverulent solid is removed from gaseous substances, wherein at least one metal compound is introduced into the high-temperature zone in solid form and the evaporation temperature of the metal compound is below the temperature of the high-temperature zone.Type: ApplicationFiled: November 29, 2006Publication date: October 30, 2008Applicant: EVONIK DEGUSSA GmbHInventors: Kai Schumacher, Stefan Fiedler, Roland Schilling, Ronald Ihmig, Stipan Katusic
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Patent number: 7442361Abstract: The invention relates to a procedure for manufacturing alumina hydrates by precipitating aluminum salts in the presence of crystal nuclei of a specific size.Type: GrantFiled: July 5, 2000Date of Patent: October 28, 2008Assignee: Sasol Germany GmbHInventors: Rainer Gloeckler, Arnold Meyer
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Publication number: 20080260612Abstract: Multi-step metal compound oxidation process to produce compounds and enhanced metal oxides from various source materials, e.g. metal sulfides, carbides, nitrides and other metal containing materials with metal oxides from secondary reaction steps being utilized as an oxidation agent in the first reactions.Type: ApplicationFiled: April 18, 2008Publication date: October 23, 2008Applicant: Orchard Material Technology, LLCInventor: Lawrence F. McHugh
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Patent number: 7438977Abstract: The present invention provides gibbsite type aluminum hydroxide particles having a primary particle diameter of from 0.01 ?m to 0.3 ?m and a DOP oil absorption of from 90 mL/100 g to 300 mL/100 g.Type: GrantFiled: November 21, 2006Date of Patent: October 21, 2008Assignee: Sumitomo Chemical Company, LimitedInventor: Kazuki Takemura
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Patent number: 7438882Abstract: A method of forming a gel and/or powder of a metallic oxide, metalloid oxide and/or a mixed oxide or resin thereof from one or more respective organometallic liquid precursor(s) and/or organometalloid liquid precursor(s) by oxidatively treating said liquid in a non-thermal equilibrium plasma discharge and/or an ionised gas stream resulting therefrom and collecting the resulting product. The non-thermal equilibrium plasma is preferably atmospheric plasma glow discharge, continuous low pressure glow discharge plasma, low pressure pulse plasma or direct barrier discharge. The metallic oxides this invention particularly relates to are those in columns 3a and 4a of the periodic table namely, aluminium, gallium, indium, tin and lead and the transition metals. The metalloids may be selected from boron, silicon, germanium, arsenic, antimony and tellurium.Type: GrantFiled: April 8, 2003Date of Patent: October 21, 2008Assignee: Dow Corning Ireland LimitedInventors: Andrew James Goodwin, Stuart Leadley, Pierre Chevalier, Bhukandas Parbhoo
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Publication number: 20080233030Abstract: Process for manufacturing an electrochemical device including a cathode, an anode and at least one electrolyte membrane disposed between the anode and the cathode, wherein at least one of the cathode, the anode and the electrolyte membrane, contains at least a ceramic material.Type: ApplicationFiled: March 30, 2004Publication date: September 25, 2008Applicant: PIRELLI & C.S.P.A.Inventors: Agustin Sin Xicola, A. Yuri Dubitsky, Enrico Albizzati, Evgeny Kopnin, Elena Roda
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Publication number: 20080226543Abstract: The invention describes a method for stripping alumina which is particularly suitable for removal of fluoride from alumina and comprises washing said alumina with an aqueous acid or alkali at elevated temperature. The method may be used for removal of unreacted radiofluoride such as [18F]fluoride from alumina following a radiofluorination reaction. Automated synthesis apparatus and cassettes therefor, which are adapted to perform the method are also claimed.Type: ApplicationFiled: March 21, 2006Publication date: September 18, 2008Inventors: Nigel John Osborn, Julian Grigg
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Patent number: 7422730Abstract: The present invention provides ?-alumina powders comprising ?-alumina particles of which at least 80% of the ?-alumina particles have a particle size of less than 100 nm. The invention also provides slurries, particularly aqueous slurries, which comprise ?-alumina powders of the invention. The invention further provides methods of manufacturing ?-alumina powders and ?-alumina slurries of the invention and methods of polishing using same.Type: GrantFiled: April 2, 2003Date of Patent: September 9, 2008Assignee: Saint-Gobain Ceramics & Plastics, Inc.Inventor: Yuhu Wang
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Publication number: 20080213123Abstract: The invention relates to an iridium alloy of at least 85% by weight iridium, at least 0.005% by weight molybdenum, 0.001 to 0.6% by weight hafnium and, if necessary, rhenium, the sum of molybdenum and hafnium being between 0.002 and 1.2% by weight, and to a process for the production of an iridium alloy, an IrMo and an IrHf master alloy, respectively, being produced in the electric arc and immersed into an iridium melt, if necessary together with Re.Type: ApplicationFiled: July 7, 2006Publication date: September 4, 2008Applicant: W.C. Heraeus GmbHInventors: Michael Koch, David Francis Lupton, Harald Manhardt, Tobias Mueller, Reinhold Weiland, Bernd Fischer
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Publication number: 20080193759Abstract: The present invention relates to surface-modified nanoparticulate metal oxides where the metal is chosen from the group consisting of aluminum, cerium, iron, titanium, zinc and zirconium, wherein the surface modification comprises a coating with a copolymer P comprising, as monomers, A) 1 to 99 mol % of a N-vinylamide N-vinylpyrrolidone and B) 99 to 1 mol % of a monomer comprising, per molecule, a free-radically polymerizable ?,?-ethylenically unsaturated double bond and an anionogenic and/or anionic group, with the proviso that the copolymer P must comprise no further monomers chosen from the group consisting of C8-C30-alkyl esters of monoethylenically unsaturated C3-C8-carboxylic acids, N-alkyl- or N,N-dialkyl-substituted amides of acrylic acid or of methacrylic acid with C8-C18-alkyl radicals, or vinyl esters of aliphatic C8-C30-carboxylic acids.Type: ApplicationFiled: May 30, 2006Publication date: August 14, 2008Applicant: BASF AKTIENGESELLSCHAFTInventors: Jens Rieger, Jutta Kissel, Valerie Andre, Nathalie Bouillo
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Publication number: 20080193760Abstract: Disclosed is a method of manufacturing a metal oxide nano powder comprising preparing a first dispersed solution by adding a nano-sized metal powder to water and dispersing the metal powder within the water, performing a hydration reaction of the first dispersed solution at a temperature of about 30 to about 70° C. to generate a precipitation, and filtering and drying the precipitation to prepare a metal oxide powder. Also, disclosed is a metal oxide nano powder manufactured by the method described above, and having any one of a bar-form, a cube-form, and a fiber-form.Type: ApplicationFiled: November 6, 2007Publication date: August 14, 2008Inventors: Chang Kyu Rhee, Min Ku Lee, Young Rang Uhm, Jin Ju Park, Byung Sun Han, Hi Min Lee, Seung-Hee Woo
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Patent number: 7402612Abstract: This invention relates to methods for making a stabilized transition alumina of enhanced hydrothermal stability, which include the introduction of at least one structural stabilizer; a steaming step before or after the introduction step, wherein steaming is effective in transforming a transition alumina at least partially to boehmite and/or pseudoboehmite; and a calcining step to create a stabilized transition alumina. The combination of the structural stabilizer and the steaming step is believed to impart high hydrothermal stability to the alumina crystal lattice. Particularly preferred structural stabilizers include boron, cobalt, and zirconium. The stabilized transition alumina is useful as a catalyst support for high water partial pressure environments, and is particularly useful for making a catalyst having improved hydrothermal stability. The invention more specifically discloses Fischer-Tropsch catalysts and processes for the production of hydrocarbons from synthesis gas.Type: GrantFiled: October 16, 2003Date of Patent: July 22, 2008Assignee: ConocoPhillips CompanyInventors: Yaming Jin, Rafael L. Espinoza, Nithya Srinivasan, Olga P. Ionkina
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Patent number: 7399459Abstract: A mesoporous alumina molecular sieve and a method of manufacturing a mesoporous alumina mesoporous alumina molecular sieve of the invention is produced without using traditionally used additives. Also, because the size and distribution of the pores can be controlled, the molecular sieve can be produced simply and economically, producing molecular sieve with high surface area and thermal stability. Further, a method of manufacturing an alumina nanotube by using a surfactant and a use of the alumina nanotube as a hydrogen storage material are provided.Type: GrantFiled: October 18, 2002Date of Patent: July 15, 2008Assignee: Postech FoundationInventors: Jae Sung Lee, Kyung Hee Lee, Hae Jin Kim, Hyun Chul Lee, Dae Hyun Choo
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Publication number: 20080138622Abstract: In a particular embodiment, a particulate material includes alumina hydrate. The particulate material has a 500 psi Compaction Volume Ratio of at least about 4.0 cc/cc.Type: ApplicationFiled: November 29, 2007Publication date: June 12, 2008Applicant: SAINT-GOBAIN CERAMICS & PLASTICS, INC.Inventors: Olivier Guiselin, Nathalie Pluta, Yves Boussant-Roux, Doruk O. Yener
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Publication number: 20080121584Abstract: Methods of making unique water treatment compositions are provided. In one embodiment, a method of making a doped metal oxide or hydroxide for treating water comprises: disposing a metal precursor solution and a dopant precursor solution in a reaction vessel comprising water to form a slurry; and precipitating the doped metal oxide or hydroxide from the slurry.Type: ApplicationFiled: June 14, 2007Publication date: May 29, 2008Applicants: INFRAMAT CORPORATION, UNIVERSITY OF HOUSTONInventors: Huimin Chen, Dennis A. Clifford
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Publication number: 20080118428Abstract: A method for manufacturing a cathode active material for a lithium rechargeable battery, including: selecting a first metal compound from a group consisting of a halide, a phosphate, a hydrogen phosphate and a sulfate of Mg or Al; selecting a second metal compound from a group consisting of an oxide, a hydroxide and a carbonate of Mg or Al; combining the first metal compound and the second metal compound to obtain a metal compound, the metal compound containing either Mg or Al atoms; mixing a lithium compound, a transition metal compound and the metal compound to obtain a mixture; and sintering the mixture.Type: ApplicationFiled: November 16, 2007Publication date: May 22, 2008Applicant: Nippon Chemical Industrial Co., Ltd.Inventors: Hidekazu Awano, Minoru Fukuchi, Yuuki Anbe
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Publication number: 20080099734Abstract: Solid battery components are provided. A block copolymeric electrolyte is non-crosslinked and non-glassy through the entire range of typical battery service temperatures, that is, through the entire range of at least from about 0° C. to about 70° C. The chains of which the copolymer is made each include at least one ionically-conductive block and at least one second block immiscible with the ionically-conductive block. The chains form an amorphous association and are arranged in an ordered nanostructure including a continuous matrix of amorphous ionically-conductive domains and amorphous second domains that are immiscible with the ionically-conductive domains. A compound is provided that has a formula of LixMyNzO2. M and N are each metal atoms or a main group elements, and x, y and z are each numbers from about 0 to about 1. y and z are chosen such that a formal charge on the MyNportion of the compound is (4?x). In certain embodiments, these compounds are used in the cathodes of rechargeable batteries.Type: ApplicationFiled: April 2, 2007Publication date: May 1, 2008Applicant: Massachusetts Institute of TechnologyInventors: Yet-Ming Chiang, Donald R. Sadoway, Young-Il Jang, Biying Huang
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Patent number: 7357910Abstract: Method for producing metal oxide nanoparticles. The method includes generating an aerosol of solid metallic microparticles, generating plasma with a plasma hot zone at a temperature sufficiently high to vaporize the microparticles into metal vapor, and directing the aerosol into the hot zone of the plasma. The microparticles vaporize in the hot zone into metal vapor. The metal vapor is directed away from the hot zone and into the cooler plasma afterglow where it oxidizes, cools and condenses to form solid metal oxide nanoparticles.Type: GrantFiled: July 15, 2002Date of Patent: April 15, 2008Assignee: Los Alamos National Security, LLCInventors: Jonathan Phillips, Daniel Mendoza, Chun-Ku Chen
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Patent number: 7351393Abstract: This invention is directed to star shaped alumina extrudates with a pore volume in the pores of a diameter over 1000 nm, as determined by mercury porosity, of at least 0.05 ml/g and a total pore volume between 0.5-0.75 ml/g. The extrudates have a length of between 2-8 mm, a length to diameter ratio of between 1-3, a side crushing strength of at least 50 N and a bulk crushing strength of at least 1 MPa.Type: GrantFiled: November 4, 1999Date of Patent: April 1, 2008Assignee: Engelhard CorporationInventors: Cornelis Roeland Bayense, Durk Ykema
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Patent number: 7351394Abstract: A method for producing an ?-alumina powder is described. The method for producing an ?-alumina powder comprises a step of calcining an aluminum salt in the presence of a seed crystal at 600-890° C.Type: GrantFiled: February 24, 2004Date of Patent: April 1, 2008Assignee: Sumitomo Chemical Company, LimitedInventors: Hajime Maki, Yoshiaki Takeuchi
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Publication number: 20080075649Abstract: Disclosed are methods for making ultrafine particles. These methods include (a) introducing a plurality of precursors to a high temperature chamber, the precursors including a first precursor and a second precursor different from the first precursor and comprising an alkali metal dopant; (b) heating the plurality of precursors in the high temperature chamber, yielding a gaseous product stream; (c) quenching the gaseous product stream, thereby producing ultrafine particles; and (d) collecting the ultrafine particles. Also disclosed are apparatus for the production of ultrafine particles, ultrafine particles produced from a plurality of precursors and coating compositions and coated substrates that include ultrafine particles.Type: ApplicationFiled: September 22, 2006Publication date: March 27, 2008Applicant: PPG INDUSTRIES OHIO, INC.Inventors: Cheng-Hung Hung, Noel R. Vanier
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Publication number: 20080075941Abstract: A method and apparatus for the production of C-plane single crystal sapphire is disclosed. The method and apparatus may use edge defined film-fed growth techniques for the production of single crystal material exhibiting low polycrystallinity and/or low dislocation density.Type: ApplicationFiled: September 21, 2007Publication date: March 27, 2008Inventors: Vitali Tatartchenko, Christopher D. Jones, Steven Anthony Zanella, John W. Locher, Fery Pranadi
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Patent number: 7344988Abstract: Methods of manufacturing alumina abrasive for use in chemical mechanical polishing are described, wherein the abrasive is in a slurry having gamma alumina formed in a low temperature fuming process, water, an acid sufficient to maintain the pH below about 7, wherein the slurry does not settle appreciably in an 8 to 24 hour period. Advantageously, the alumina is wet-milled without the use of wet-milling salt additives.Type: GrantFiled: October 26, 2004Date of Patent: March 18, 2008Assignee: DuPont Air Products Nanomaterials LLCInventor: Philippe H. Chelle
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Publication number: 20080064770Abstract: A catalyst for use in a Fischer-Tropsch synthesis reaction which comprises cobalt supported on alumina, in which: the catalyst average particle size is in the range 20 to 100 ?m; the specific surface area of the impregnated and calcined catalyst particles is greater than 80 m2/g; the average pore size of the impregnated and calcined catalyst is at least 90 ? (9 nm); and the pore volume of the impregnated and calcined catalyst is greater than 0.35 cm3g.Type: ApplicationFiled: November 10, 2003Publication date: March 13, 2008Inventors: Erling Rytter, Sigrid Eri, Dag Schanke
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Publication number: 20080038176Abstract: The invention relates to unsymmetrical nanoscale or mesoscopic particles, and to a method for preparing the same. Said particles are characterized by a surface F1 and the zone Z2 carries groups F2 different from the groups F1, the zone Z1 being free of groups F2 and the zone Z2 being free of groups F1. The method of preparation comprises the following steps: 1) the zone Z2 of the surface of the initial particles is masked by fixing a polymer nodule thereto; 2) the masked particles obtained at the end of step 1) are treated in order to modify the nonmasked surface zone Z1 thereof; 3) the polymer nodule is removed after modifying the zone Z1; 4) optionally, the surface of the zone Z2 of the particles is modified following the demasking process.Type: ApplicationFiled: November 4, 2004Publication date: February 14, 2008Applicants: Centre National De La Recherche Scientifique, Cpe Lyon Formation Continue Et Recherche, Universite Paul Sabatier, Universite Des Sciences Et TechnologiesInventors: Etienne Duguet, Celine Poncet-Legrand, Serge Ravaine, Elodie Bourgeat-Lami, Stephane Reculusa, Christophe Mingotaud, Marie-Helene Delville, Franck Pereira
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Patent number: 7326398Abstract: A method for preparation for mesoporous oxide comprising a non silica oxide having a hexagonal pore structure periodicity and an average maximum pore length of from 2 nm to 5 nm, characterized by comprising blending 0.003 mol to 0.01 mol of TaCl5, NbCl5 or a mixture thereof and Al isopropoxide comprising 10 g of an aliphatic linear alcohol and 1 g of a template compound to prepare a mixture for forming a sol solution, adding 5 mol to 35 mol (based on the metal compounds) of water or an aqueous inorganic acid solution to the mixture followed by hydrolysis and polycondensation to give a sol solution, transferring the sol into an oxygen containing atmosphere followed by again at 40° C. to 100° C. to form a gel, and then calcinating the gel in an oxygen containing atmosphere at 350° C. to 550° C.; and the mesoporous oxide obtained by the method.Type: GrantFiled: November 11, 2002Date of Patent: February 5, 2008Assignee: Japan Science and Technology AgencyInventors: Kazunari Domen, Junko Nomura, Tokumitsu Kato
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Publication number: 20080015299Abstract: Acicular boehmite having a BET specific surface area of at 20 to 80 m2/g, a dioctyl phthalate oil absorption of 200 to 600 cm3/100 g, a minor axis length of 30 to 300 nm and an aspect ratio of 5 to 50, which may be produced by hydrothermally reacting aluminum hydroxide powder at a temperature of 160 to 250° C. in an aqueous solution having pH of 4 to 6 and containing 0.1 to 5 mol/L of a salt of a metal ion selected from magnesium ion, manganese ion and zinc ion and an anion selected from carboxylate ion, nitrate ion and sulfate ion.Type: ApplicationFiled: July 13, 2007Publication date: January 17, 2008Inventors: Kazuki Takemura, Yusuke Kawamura, Katsuhisa Kitano