Abstract: The present invention relates to field emission deices fabrication using carbon nanotube film as a cathode. The multi-wall carbon nanotubes film possesses low electron field emission and high emission current density, which is deposited by catalytic chemical vapor deposition at low temperature. The carbon nanotubes density can be controlled by tuning of the transition metal catalysts in the seed alloy layer. The film can be deposited onto the substrate uniformly with large area. The present invention is related to the fabrication of cold electron sources, florescent light, vacuum electronic devices, field emission displays and methods of making same.

Abstract: A substrate is coated with a hydrophobic coating system including diamond-like carbon (DLC) and at least one fluoro-alkyl silane (FAS) compound. In certain embodiments, the coating system includes an FAS inclusive layer provided over at least one DLC inclusive layer in order to increase the initial contact angle of the coated article. At least the FAS inclusive layer may be heated (i.e., thermally cured) to an extent sufficient to at least one of: (a) improve the initial contact angle &thgr; of the resulting coated article, (b) render the hydrophobic nature of the resulting coated article more stable when exposed to solution(s)/material(s) such as hexane and/or isopropyl alcohol, and/or (c) improve bonding characteristics of the FAS inclusive layer within itself and/or between the FAS inclusive layer and a layer immediately beneath it.

Abstract: The method for the manufacture of a functional ceramic layer (10) comprises the following two steps:

Abstract: A composition for application to a substrate to form a an electrically conductive coating thereon. The composition includes a sol-gel solution filled with a conductive powder. The coating may be conductive or resistive depending on the application. A process is provided for applying such a coating by mixing a sol-gel solution with up to about 90% by weight of the solution of a conductive powder selected from the group consisting of ceramics, inter-ceramics, semi-conductors and metals so as to provide a uniform stable dispersion. The stable dispersion is applied to a substrate and the coated substrate is fired at a temperature sufficient to remove organic constituents and to produce at least a partially conductive film on the substrate. A heating device is also provided which is a product of the above process.

Abstract: This invention relates to radioactively coated devices, preferably radioactively coated medical devices. These coated devices are characterized as having a low rate of leaching of the radioisotope from the surface of the coated device and a uniform radioactive coating, and are therefore suitable for use within biological systems. Methods for coating a device with a radioisotope comprising are also disclosed. One method comprises immersing the device within a solution containing a &Ugr;, &bgr;+, &agr;,&bgr;− For &egr; (electron capture) emitting radioisotope, then exposing the immersed substrate to tuned vibrational cavitation to produce a coated substrate. A second method involves coating a substrate using electroless plating, and yet a third method involves the use of electroplating a radioisotope onto a substrate of interest. With these methods, the coating procedures are followed by baking the coated substrate at a temperature below the recrystallization temperature of the substrate.

Abstract: A method of forming a multilayer sheet suitable for use as a mat for mounting a pollution control element or as a firestop. The method comprises providing one aqueous slurry and another aqueous slurry, each slurry containing inorganic materials suitable for making a mounting mat for a pollution control element or a firestop. The two aqueous slurries can be separated from one aqueous slurry. The method can also comprise depositing the one slurry onto a permeable substrate; partially removing water from the one slurry to form the one layer on the substrate; and depositing the other slurry onto the one layer. One layer is dried out of the one slurry and another layer is dried out of the other slurry so as to form the multilayer sheet.

Abstract: A process of coating a refractory turbine part with a protective coating which is ultimately diffusion bonded to the part. A slurry coating material is prepared from a mixture of a silicon alkyd paint and suspended particles of an aluminum or aluminum alloy powder. Parts may be dipped in the slurry and subsequently be heat treated in selected atmospheres and temperatures to diffuse the coating into the surface of the part.

Abstract: A Ti/TiN adhesion/barrier layer is formed on a substrate and annealed. The anneal step is performed at a temperature within a good morphology range of 100° C. above a base barrier anneal temperature that depends on the thickness of said barrier layer. The base barrier anneal temperature is about 700° C. for a barrier thickness of about 1000 Å and about 800° C. for a barrier thickness of about 3000 Å. The barrier layer is 800 Å thick or thicker. A first electrode is formed, followed by a BST dielectric layer and a second electrode. A bottom electrode structure in which a barrier layer of TiN is sandwiched between two layers of platinum is also disclosed. The process and structures also produce good results with other capacitor dielectrics, including ferroelectrics such as strontium bismuth tantalate.

Abstract: A corrosion-resistant member includes a substrate made of a ceramic material and having a diameter of at least 200 mm, and a film of chemically vapor deposited silicon carbide having a thickness of not less than 0.5 mm and covering at least such a portion of the surface of the substrate that is to contact a corrosive material. A process is disclosed for producing such a corrosion-resistant member, which process includes thermally treating the film at a temperature higher, by not less than 50° C. centigrade, than a film-forming temperature at which the film of silicon carbide is formed, after the formation of the silicon carbide film.

Abstract: The present invention provides surface coated phosphors useful in field emission displays and vacuum fluorescent displays. The surface coated phosphor comprises a thin coating of rare earth oxide, e.g., yttrium oxide, disposed on an uncoated phosphor such as a sulfide phosphor. The present invention further provides a process for preparing a surface coated phosphor comprising contacting the uncoated phosphor with a rare earth hydroxide gel solution to obtain a rare earth hydroxide gel coated phosphor, drying the gel coated phosphor to remove solvent residues, and heat treating the dried rare earth hydroxide gel coated phosphor. The surface coated phosphors of the present invention have improved cathodoluminescence efficiency, coulombic aging resistance, chemical, and/or oxidative stability.

Abstract: A method of producing a thin film of an inorganic solid electrolyte having a relatively high ionic conductance is provided. In the method, a thin film made of an inorganic solid electrolyte is formed, by a vapor deposition method, on a base member being heated. The thin film obtained through the heat treatment exhibits an ionic conductance higher than that of the thin film formed on the base member not being heated. The ionic conductance can also be increased through the steps of forming the thin film made of the inorganic solid electrolyte on the base member at room temperature or a temperature lower than 40° C. and then heating the thin film of the inorganic solid electrolyte.

Abstract: Low dielectric constant porous materials with improved elastic modulus and film hardness. The process of making such porous materials involves providing a porous dielectric material and plasma curing the porous dielectric material to produce a plasma cured porous dielectric material. Plasma curing of the porous dielectric material yields a material with improved modulus and hardness, but with a higher dielectric constant. The improvement in elastic modulus is typically greater than about 100%, and more typically greater than about 200%. The improvement in film hardness is typically greater than about 50%. The porous dielectric material is plasma cured for a time between about 15 and about 120 seconds at a temperature less than about 350° C. The plasma cured porous dielectric material can optionally be post-plasma treated.

Abstract: A concrete-based mortar is prepared for application on the exterior of a concrete building or other structure. The drying time of the concrete-based mortar is reduced by addition of an accelerant compound. After the concrete-based mortar sets on the building or other structure, an exterior skin of the concrete-based mortar is removed. This provides an even and attractive surface while reducing the amount of labor time required to complete the application.

Abstract: The invention provides a haze-resistant temperable coating which desirably includes an inner dielectric layer, a first silver layer; an intermediate dielectric stack a second silver layer, and an outer dielectric layer. The intermediate dielectric stack may have alternating layers of a first dielectric and a second dielectric, with each of the alternating layers having an optical thickness of no more than about 450 A or a physical thickness of no more than about 250 A. In a preferred coating, the first dielectric has an index of refraction between about 90% and 110% of that of the second dielectric and the first and second dielectric have different microstructures to limit crystal growth therebetween during tempering.

Abstract: The present invention provides a method for making a ceramic matrix composite comprising forming an infiltrated fiber reinforcement by infiltrating a plurality of plies of a fibrous material with a precursor polymer which decomposes to a substantially pure product selected from the group consisting of a refractory metal carbide and a refractory metal boride, and exposing the infiltrated fiber reinforcement to conditions effective to cure the precursor polymer and to decompose the precursor polymer to said substantially pure product.

Abstract: The present invention generally provides a method for depositing a low dielectric constant amorphous carbon film on a substrate or other workpiece using high density plasma chemical vapor deposition (HDP-CVD) techniques. Specifically, the present invention provides a method for forming an amorphous carbon film having a low dielectric constant of less than about 3.0 and a high thermal stability at a temperature of at least about 400° C. In a preferred embodiment, the film is deposited using methane (CH4) and argon in a HDP-CVD reactor. The amorphous carbon film formed according to the invention is useful for many applications in ultra large scale integration (ULSI) structures and devices, such as for example, an inter-metal dielectric material and an anti-reflective coating useful for patterning sub-micron interconnect features.

Abstract: Glassy coatings that isolate metal surfaces from carbon particles, and a method of applying the coatings. The coatings composed of essentially K2O, SiO2, and Al2O3, and has a CTE of at least 80×10−7/° C. These glassy coatings, which adhere well to metals, employ a potassium-silicate glass composition in three forms: a pure glass, a glass loaded with inert filler having a CTE higher than the glass itself, and a precursor frit that when “reactive-cerammed” produces a predominantly leucite crystalline phase and forms the glassy coating in-situ on the metal surface, creating a protective layer between the exposed metal surface and corrosive chemical-processing environments.

Abstract: A method of making an electrode structure, an electrode structure, and a double layer capacitor including the electrode structure, the method includes the steps of: applying a first slurry including conducting carbon powder and a binder to a current collector plate; curing the applied first slurry to form a primary coating; applying a second slurry that includes activated carbon powder, a solvent and a binder to the primary coating; and curing the applied second slurry to form a secondary coating, thereby forming a first electrode. In variations, additional primary and secondary coatings may be formed on both sides of the collector plate.

Abstract: A method for producing an insulator film for use as an interlayer dielectric film in a semiconductor device having a multi-level interconnection structure is disclosed. An inert plasma producing gas, such as argon, is introduced into a vacuum vessel along with a thin film deposition gas, such as a compound gas containing fluorine and carbon. Activation of the plasma producing gas activates the thin film producing gas, resulting in a thin fluorine containing carbon insulator film on the semiconductor device. In order to thermally stabilize the insulator layer, the semiconductor device is annealed.

Abstract: A method for providing a protective coating on a metal-based substrate is disclosed. The method involves the application of an aluminum-rich mixture to the substrate to form a discontinuous layer of aluminum-rich particles, followed by the application of a second coating over the discontinuous layer of aluminum-rich particles. Aluminum diffuses from the aluminum-rich layer into the substrate, and into any bond coat layer which is subsequently applied. Related articles are also described.

Abstract: A conductively coated panel for inclusion in a transparent interactive input device useful with an electro-optic display includes a transparent substrate having a transparent, conductive layer on at least one surface. The conductive layer is applied in a predetermined pattern with at least one area having a conductive layer thereon and a second area without a conductive layer. A transparent layer of a metal oxide such as silicon dioxide overlies both areas whereby visible contrast between the areas is reduced and light transmission through the coated panel is increased. An interactive device, and a method for forming an interactive device with the conductively coated panel, are also disclosed.

Abstract: A thick film fuse assembly for high voltage, high amperage, high reliability applications. In a first embodiment the fuse assembly consists of an insulative substrate on which a parallel array of low mass thick film fusible elements are disposed. Thick film contact pads permit attachment of lead wires in electrical contact with the fusible elements. The fusible array is covered with a coating of arc suppressant glass. In a second embodiment of the fuse assembly, the fusible elements comprise thick film end portions and upstanding conductive wires which are positioned above and away from the insulative substrate. The arc suppressant glass surrounds each of the upstanding wires which permits higher amperage capacity.

Abstract: The present invention provides a method of decorating a ceramic article including: providing an ink composition including a metallic soap, the ink composition being a viscous oil or waxy solid at about 25° C.; heating the ink composition to reduce its viscosity to less than about 40 centipoise; depositing micro-droplets of the heated ink composition upon the ceramic article; and firing the ceramic article in an oxidizing atmosphere. In the most preferred embodiment of the invention, the ink composition is substantially solvent-free.

Abstract: A multilayer ceramic substrate contains a ceramic coating which is different in composition than the main body of the multilayer ceramic substrate to control camber of the multilayer ceramic substrate during sintering. The primary component of the ceramic coating is a secondary component of the main body of the multilayer ceramic substrate.

Abstract: Methods and compositions useful for increasing water resistance of a surface associated with a concrete, masonry or wood building material as disclosed herein. The method comprises the steps of applying a selected amount of an aqueous treating solution to the surface, wherein the aqueous treating solution includes a hydrophobic anion salt dissolved in water; allowing a portion of the aqueous treating solution to absorb into the surface; and evaporating the water to yield a treated surface having increased water resistance. The composition comprises a major amount of cement and a minor amount of a hydrophobic anion salt. The major amount of cement may be Portland cement, and the minor amount of hydrophobic anion salt may be potassium stearate, sodium stearate, as well as combinations thereof.

Abstract: Improved articles of manufacture are disclosed, together with methods for preparing such articles, whereby the surface of a graphite or comparable substrate is first densified with carbon to reduce surface porosity while still retaining sufficient surface texture to enhance the adherence of a subsequently applied boron coating.

Abstract: A suspension application apparatus for applying a suspension containing powder particles of an oxide dispersed in a liquid to a plate for magnet sintering, the oxide having a specific gravity greater than the liquid. The apparatus includes: a container for storing the suspension; a stirrer for stirring the suspension stored in the container; a transport path through which the suspension is transported from the container to the plate; and a homogenizer for homogenizing the suspension by applying a mechanical force to at least part of the suspension flowing through the transport path.

Abstract: The invention describes a method for applying an electrocatalytic or a protective coating to a metal substrate or repairing a damaged area of the same, consisting in a thermal treatment of a precursor of said catalytic coating by means of a hot air jet from a blower. The temperature of the substrate is locally controlled by means of surface temperature sensors or by an infrared measuring system. The metal substrate may be an exhausted electrode structure, in which case the reactivation is easily carried out at the plant site without any need of sending the structure to the producer. The method of the invention is particularly useful for reactivating anodes for oxygen evolution as it permits to avoid the risky procedure of detaching the anode from the current conductor.

Abstract: A method for providing the surface of base bodies of displacement or angle measuring systems with magnetizable material. Hard ferrite powder or materials comprising rare earths are preferred components of the magnetizable coating material. The composition of the material is changed during application of the coating such that the percentage of the ferrite or rare earth compound is increased.

Abstract: Polishing pads used in the manufacturing of microelectronic devices, and apparatuses and methods for making and using such polishing pads. In one aspect of the invention, a polishing pad for planarizing microelectronic-device substrate assemblies has a backing member including a first surface and a second surface, a plurality of pattern elements distributed over the first surface of the backing member, and a hard cover layer over the pattern elements. The pattern elements define a plurality of contour surfaces projecting away from the first surface of the backing member. The cover layer at least substantially conforms to the contour surfaces of the pattern elements to form a plurality of hard nodules projecting away from the first surface of the backing member. The hard nodules define abrasive elements to contact and abrade material from a microelectronic-device substrate assembly. As such, the cover layer defines at least a portion of a planarizing surface of the polishing pad.

Abstract: Purpose: The object of the present invention is to provide an anti-thrombogenic material and a manufacturing method therefor permitting to surely treat a blood contact surface of complex shapes, and moreover, permitting to suppress not only generation of fibrin induced by a blood coagulation factor such as fibrinogen on the blood contact surface but also both of the adhesion and activation of platelets.

Abstract: A halogen gas plasma-resistant member to be exposed to a halogen gas plasma, includes a main body of said member, and a corrosion-resistant film formed at least a surface of said main body, wherein a peeling resistance of the corrosive film to said main body is not less than 15 MPa.

Abstract: The present invention aims at providing a material for a diamond sintered compact tool, which has a high strength and is available as a material for a cutting tool. Accordingly, the present invention is concerned with a diamond sintered compact comprising a WC-Co type cemented carbide substrate having slight undulation and a diamond sintered compact bonded to one surface of the substrate by sintering during a step of sintering at an ultra-high pressure and high temperature, which has a plate thickness is 0.5 mm to 5 mm and an outer diameter is at least 20 mm and whose diamond sintered compact layer has at least 50% of a thickness area within a range of 0.05 mm to 0.4 mm and contains Co diffusing from the cemented carbide substrate.

Abstract: A method for nitriding a metallic base material at low temperatures in a salt bath containing electrolyzed titanium metal. A nitride coating of exceptional depth and hardness is obtained in a very short operating time due to the rapid nitriding process. The method is applicable to steel, titanium, aluminum and alloys thereof.

Abstract: A coating composition comprising at least a stimulable phosphor, a binder, and a mixed solvent is prepared. The mixed solvent comprises a low boiling temperature solvent having a viscosity of at most 0.6 mPa·s and a high boiling temperature solvent having a viscosity higher than 0.6 mPa·s, boiling temperatures of the low boiling temperature solvent and the high boiling temperature solvent being different by at least 10° C. from each other. The coating composition is applied onto a substrate and dried, and a stimulable phosphor layer is thereby formed on the substrate. The boiling temperature of the low boiling temperature solvent may be at most 110° C., and the boiling temperature of the high boiling temperature solvent may fall within the range of 110° C. to 220° C. The thus formed stimulable phosphor layer has uniform stimulable phosphor density, and a radiation image storage panel exhibiting little nonuniformity in light emission is capable of being produced.

Abstract: An article includes a substrate and an adhesion layer overlying the substrate. The adhesion layer includes a first phase including particles, and a second phase including braze alloy that bonds the particles to the substrate. The article further includes a ceramic layer overlying the adhesion layer. In one embodiment, the ceramic layer is a thermal barrier coating (TBC), formed of stabilized zirconia (ZrO2).

Abstract: A substrate is coated with a hydrophobic coating system including diamond-like carbon (DLC) and at least one fluoro-alkyl silane (FAS) compound. In certain embodiments, the coating system includes an FAS inclusive layer provided over at least one DLC inclusive layer in order to increase the initial contact angle of the coated article. At least the FAS inclusive layer may be heated (i.e., thermally cured) to an extent sufficient to at least one of: (a) improve the initial contact angle &thgr; of the resulting coated article, (b) render the hydrophobic nature of the resulting coated article more stable when exposed to solution(s)/material(s) such as hexane and/or isopropyl alcohol, and/or (c) improve bonding characteristics of the FAS inclusive layer within itself and/or between the FAS inclusive layer and a layer immediately beneath it.

Abstract: A luminescent nanophase binder is provided for use in UV and VUV applications. The binder promotes adherence of phosphor coatings to lamp envelopes and emits visible light under UV and VUV excitation. In a preferred embodiment, the binder comprises SiO2 nanoparticles doped with terbium or terbium and yttrium. Preferably, the nanoparticles have a particle size of less than 50 nm.

Abstract: A dendritic sponge which is directionally-grown on a substrate material has a high surface to volume ratio and is suitable for forming anodes for highly efficient capacitors. A dielectric film is formed on the sponge surface by oxidizing the surface. In a preferred embodiment, the dielectric is grown on titanium sponge and is doped with oxides of Ca, Mg, Sr, Be, or Ba to improve the film's dielectric constant or with higher valent cations, such as Cr6+, V5+, Ta5+, Mo6+, Nb5+, W6+, and P5+, to reduce the oxygen vacancy concentration and leakage current of the dielectric film. A capacitor formed from the sponge includes a cathode electrolyte which serves as an electrical conductor and to repair the dielectric film by re-oxidizing the anode surface at areas of local breakdown. Sponges of titanium, tantalum, and aluminum form efficient dielectric films. In another embodiment, sponges of elements which do not form efficient dielectric films are coated with a dielectric material.

Abstract: The object is to provide a laminated radiation member and a power semiconductor apparatus in which no cracks occur due to thermal stress caused by cooling and thermal cycle and which are low in thermal resistance.

Abstract: A method for producing an oxide cathode including a sleeve containing a heater coil, a cathode substrate provided on one end of the sleeve, and an emissive material layer formed by thermally decomposing an alkaline earth metal carbonate layer adhered onto the cathode substrate, which method includes adhering the alkaline earth metal carbonate onto the cathode substrate so that it has a bulk density of 0.5 to 0.8 g/cm3, then pressing it so that the bulk density becomes not more than 0.9 g/cm3, and then thermally decomposing it in vacuum. Accordingly, an oxide cathode in which the current density distribution of emission electrons is smooth and an electron emission characteristic is not deteriorated when operated for a long time is realized, and a method for producing a cathode-ray tube with high resolution in which moire is invisible is provided.

Abstract: A method for forming a resistor on a roughened surface for use in process fluids employed in the semiconductor-processing industry as part of a clean, particle-free, nonreactive, non-trapping, ultra-pure, thermally tolerant, sealed system. In one arrangement, the method for forming the resistor includes the steps of selecting a coating for the roughened surface from among the group of resistive materials, roughening a surface to promote mechanical adherence of the coating to the selection of a coating comprising resistive material, roughening a surface for promoting mechanical adherence of the resistive material thereto, and electroplating the resistive material onto the roughened surface to provide a uniformly controllable resistance in the coating.

Abstract: Systems and methods are described for environmental exchange control for a polymer on a wafer surface. An apparatus for controlling an exchange between an environment and a polymer on a surface of a wafer located in the environment includes: a chamber adapted to hold the wafer, define the environment, and maintain the polymer in an adjacent relationship with the environment; and a heater coupled to the chamber. A method for improving performance of a spin-on material includes: forming the spin-on material on a surface of a wafer; then locating the spin-on material in an environment so that said environment is adjacent said spin-on material; and then controlling an exchange between the spin-on material and said environment. The systems and methods provide advantages because inappropriate deprotection is mitigated by careful control of the environmental temperature and environmental species partial pressures (e.g. relative humidity).

Abstract: There is provided a method for adhering precious metal to vitreous substances or bodies. Precious metal (including but not limited to, gold, palladium or platinum) is deposited or applied to the surface of the vitreous body. After such initial application, which may include a preheating step, the outer skin or membrane of the glass is made plastic and sticky by superheating. This change in viscosity allows the glass to bond to the deposited precious metal. The superheating process is completed quickly before distortion of the contour of the vitreous object and unwanted vaporization of the deposited metal take place. After the superheating process is completed, the object is annealed conventionally to room temperature.

Abstract: A metal article, in particular a component for a thermal cracking furnace, and a method of protecting the metal from exposure to carbon, the article having a protective coating that has a glass-ceramic surface and an interior having a CTE between that of the glass-ceramic and the metal.

Abstract: A coated article suitable for use at elevated temperature is formed of a substrate made from metal or a ceramic, a diffuse reflective barrier coating overlying the substrate, and a low-emissivity top coat covering the diffuse reflective barrier coating. The diffuse reflective barrier coating includes a transmissive medium having a transmissive-medium index of refraction, and a plurality of radiation-scattering centers distributed in the transmissive medium, the radiation-scattering centers having a scattering-center index of refraction different from the transmissive-medium index of refraction. The radiation scattering centers may be voids or second ceramic particles. The diffuse reflective barrier coating has a surface roughness of less than about 150 microinches RMS.

Abstract: A process for the production of insulator-coated black particles, which comprises the steps of (1-a) dispersing particles of silica or a metal oxide in an alcohol-based solvent consisting mainly of an intermediate alcohol to obtain a dispersion of the above particles, (1-c) forming a titanium oxide coating of TiO2 on the surface of each of the particles whose surfaces have been activated in the above step, to obtain titanium oxide-coated particles, (1-d) calcining the titanium oxide-coated particles obtained in the above step in a reducing and/or nitriding atmosphere and thereby blackening the above titanium oxide coatings to obtain black particles, and (1-e) forming an electrical insulator coating on a surface of each of the black particles obtained in the above step, to obtain insulator-coated black particles; characerized in that the process includes a step of (1-b) adding an alkaline aqueous solution to the dispersion obtained instep (1-a) to activate a surface of each of the particles of a metal oxi

Abstract: A porcelain enamel coating suitable for use on high-carbon content, heat-rolled sheet steel is provided. The coating includes a ground coat layer for coating directly onto the steel and a cover coat layer. The ground coat layer includes a soft ground coat frit having nickelous oxide dispersed substantially uniformly throughout. The resulting porcelain enamel coating provides good resistance to boiling defects, such as pinholes.

Abstract: A process for the coating of glass microspheres with an aluminium hydroxide, which involves the hydrothermal treatment of a suspension of complexed Al3+-ions with glass microspheres. The aluminium hydroxide coated glass microspheres can be applied in the production of light weight glass-reinforced plastic materials, e.g., for use in mass transportation.

Abstract: Excellent adhesion of vitreous enamel to steel can be achieved via an intermediate layer formed on the steel by bringing it into contact with a liquid composition that contains water and a component of solute selected from the group consisting of dissolved silicates and dissolved borates and, optionally, surfactant. The modification of the steel surface achieved by treating it with silicates and/or borates is also effective for improving the adhesion of steel to other protective type coatings such as paint.