Carbide-, Nitride-, Or Sulfide-containing Layer Patents (Class 428/698)
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Patent number: 10287674Abstract: A medical, dental or surgical instrument comprising a substrate on at least part of the instrument with a rough surface structure and a layer which is applied to or deposited on the substrate in such a way that the rough surface structure of the substrate is at least not completely smoothed by the layer or the roughness is increased, wherein the layer applied to or deposited on the substrate is embodied as a glass-ceramic layer. In addition, for producing such an instrument or part thereof is described.Type: GrantFiled: February 8, 2016Date of Patent: May 14, 2019Assignee: W&H Dentalwerk Bürmoos GmbHInventor: Beate Wagner
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Patent number: 10265776Abstract: A cutting tool has a substrate. A surface of the substrate for the cutting tool is covered with a hard film. In the cutting tool, the hard film has a root-mean-square slope R?q in a surface of the hard film of 0.060° or less.Type: GrantFiled: April 22, 2015Date of Patent: April 23, 2019Assignee: Kobe Steel, Ltd.Inventors: Maiko Abe, Kenji Yamamoto
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Patent number: 10252379Abstract: A cutting tool including a cutting edge part made of cBN sintered material bonded through a brazing material for bonding and a cutting tool body made of WC-based cemented carbide is provided. In the cutting tool, the cutting edge part made of cBN sintered material and the cutting tool body made of WC-based cemented carbide are brazed by using a blazing material for bonding including: 35-40% of Ti in a mass ratio; 35-40% of Zr in a mass ratio; 5-15% of Ni in a mass ratio; and the Cu balance including inevitable impurities.Type: GrantFiled: December 22, 2014Date of Patent: April 9, 2019Assignee: MITSUBISHI MATERIALS CORPORATIONInventors: Makoto Igarashi, Tadakazu Ohashi, Kenji Yumoto, Hiroyasu Shimizu
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Patent number: 10184176Abstract: A cutting tool comprises a base including a hard alloy and a coating layer located on a surface of the base, wherein the coating layer comprises at least one TiCN layer, an Al2O3 layer and an outermost layer which are laminated in order from a side of the base, and a content of Cl at a thickness-center position of the TiCN layer is higher than a content of Cl at a thickness-center position of the outermost layer and the content of Cl at the thickness-center position of the outermost layer is higher than a content of Cl at a thickness-center position of the Al2O3 layer in a glow-discharge emission spectrometry (GDS analysis).Type: GrantFiled: December 25, 2014Date of Patent: January 22, 2019Assignee: KYOCERA CORPORATIONInventors: Hayato Kubo, Kou Ri
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Patent number: 10186630Abstract: Embodiments relate to fabricating a wafer including a thin, high-quality single crystal GaN layer serving as a template for formation of additional GaN material. A bulk ingot of GaN material is subjected to implantation to form a subsurface cleave region. The implanted bulk material is bonded to a substrate having lattice and/or Coefficient of Thermal Expansion (CTE) properties compatible with GaN. Examples of such substrate materials can include but are not limited to AlN and Mullite. The GaN seed layer is transferred by a controlled cleaving process from the implanted bulk material to the substrate surface. The resulting combination of the substrate and the GaN seed layer, can form a template for subsequent growth of overlying high quality GaN. Growth of high-quality GaN can take place utilizing techniques such as Liquid Phase Epitaxy (LPE) or gas phase epitaxy, e.g., Metallo-Organic Chemical Vapor Deposition (MOCVD) or Hydride Vapor Phase Epitaxy (HVPE).Type: GrantFiled: July 27, 2017Date of Patent: January 22, 2019Assignee: QMAT, INC.Inventor: Francois J. Henley
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Patent number: 10145779Abstract: Perturbed oscillatory kinetics electrochemistry methods include methods of determining an electrochemical response of a test coupon to a mechanical load. Such methods include applying a cell of electrolyte solution to a test region on a test coupon, contacting the electrolyte solution with a counter electrode, and applying a mechanical load to the test coupon to produce a deflection event. Additionally, methods include measuring a pre-event value of an electrical parameter of the test coupon, before applying the mechanical load, and measuring a post-event value of the electrical parameter, after applying the mechanical load. Methods include determining an electrochemical response of the test coupon to the mechanical load based on the post-event value and the pre-event value.Type: GrantFiled: January 26, 2016Date of Patent: December 4, 2018Assignee: The Boeing CompanyInventors: Erik David Sapper, Erica Nicole Bilodeau
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Patent number: 10141582Abstract: A novel method to produce thin films spatially disposed on desired areas of workpieces is disclosed. Examples of include the formation of a yttria stabilized zirconia (YSZ) film formed on a desired portion of a stainless steel interconnect for solid oxide fuel cells by Atomic Layer Deposition (ALD). A number of methods to produce the spatially disposed YSZ film structures are described including polymeric and silicone rubber masks. The thin film structures have utility for preventing the reaction of glasses with metals, in particular alkali-earth containing glasses with ferritic stainless steels, allowing high temperature bonding of these materials.Type: GrantFiled: December 20, 2015Date of Patent: November 27, 2018Assignee: Sonata Scientific LLCInventors: Jeffrey F. Roeder, Peter C. Van Buskirk
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Patent number: 10128813Abstract: A bulk acoustic wave (BAW) resonator comprises: a first electrode; a second electrode comprising a plurality of sides, wherein at least one of the sides is a connection side; a piezoelectric layer disposed between the first and second electrodes, and an acoustic reflective element disposed beneath the first electrode, the second electrode and the piezoelectric layer, wherein an overlap of the reflective element, the first electrode, the second electrode, and the piezoelectric layer defines an active area of the acoustic resonator; a bridge adjacent to a termination of the active area of the BAW resonator; and a discontinuity disposed in the bridge.Type: GrantFiled: April 21, 2016Date of Patent: November 13, 2018Assignee: Avago Technologies International Sales Pte. LimitedInventors: Robert Thalhammer, Alexandre Shirakawa, Thomas Faust, Phil Nikkel
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Patent number: 10106881Abstract: A coating and a method for the production thereof. The coating includes at least one Mo—N-based layer of hard material which at least predominantly contains the hexagonal phase of the molybdenum nitride ?-MoN. The intensity ratio of the two peaks (?-MoN 220)/(?-MoN 200) are ?3, preferably ?10, especially preferably ?30.Type: GrantFiled: December 1, 2014Date of Patent: October 23, 2018Assignee: OERLIKON SURFACE SOLUTIONS AG, PFÄFFIKONInventors: Jurgen Ramm, Johann Karner
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Patent number: 10023952Abstract: A coated cutting tool and a hard and wear resistant coating for a body include at least one metal based nitride layer. The layer is (ZrxCrl-x-y-zAlyMez)Na with 0.55<x<0.85, 0.05<y<0.45, 0?z<0.20, 0.95<a<1.10, and Me is one or more of the elements: Y, Ti, V, Nb, Ta, Mo, W, Mn or Si. The layer can have a thickness between 0.5 ?m and 15 ?m and be comprisied of a single cubic phase or a single hexagonal phase or a mixture thereof. In an exemplary embodiment, the layer is a cubic phase of a sodium chloride structure. The layer can be deposited using cathodic arc evaporation and is useful for metal cutting applications generating high temperatures.Type: GrantFiled: September 5, 2013Date of Patent: July 17, 2018Assignee: SECO TOOLS ABInventors: Magnus Oden, Rikard Forsen, Mats Johansson-Joesaar, Syed Muhammad Bilal, Naureen Ghafoor
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Patent number: 10005696Abstract: An article includes a substrate and a coating on the substrate. The coating includes a compound of aluminum, boron and nitrogen in a continuous chemically bonded network having Al—N bonds and B—N bonds. Also disclosed is an article wherein the substrate is a plurality of fibers and the coating is a conformed coating of a compound of aluminum, boron and nitrogen having Al—N bonds and B—N bonds. The fibers are disposed in a matrix. Also disclosed is a method of protecting an article from environmental conditions. The method includes protecting a substrate that is susceptible to environmental chemical degradation using a coating that includes a compound of aluminum, boron and nitrogen having Al—N bonds and B—N bonds.Type: GrantFiled: August 25, 2014Date of Patent: June 26, 2018Assignee: United Technologies CorporationInventor: Wayde R. Schmidt
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Patent number: 10000420Abstract: A ceramic material includes of ?-sialon (Si(6-z)AlzOzN(8-z)), polytype 15R, an intergranular phase, and yttrium. The polytype 15R includes twin grains.Type: GrantFiled: November 13, 2015Date of Patent: June 19, 2018Assignee: TaeguTec, Ltd.Inventors: Sung Su Chun, Dae Yeop Lee, Geun Ho Park, Chang Hoon Hong
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Patent number: 9995169Abstract: A process of forming a calcium-magnesium-aluminosilicate (CMAS) penetration resistant coating, and a CMAS penetration resistant coating are disclosed. The process includes providing a thermal barrier coating having a dopant, and exposing the thermal barrier coating to calcium-magnesium-aluminosilicate and gas turbine operating conditions. The exposing forming a calcium-magnesium-aluminosilicate penetration resistant layer. The coating includes a thermal barrier coating composition comprising a dopant selected from the group consisting of rare earth elements, non-rare earth element solutes, and combinations thereof. Additional or alternatively, the coating includes a thermal barrier coating and an impermeable barrier layer or a washable sacrificial layer positioned on an outer surface of the thermal barrier coating.Type: GrantFiled: March 13, 2013Date of Patent: June 12, 2018Assignee: General Electric CompanyInventors: Jon Conrad Schaeffer, Surinder Singh Pabla, Paul Stephen Dimascio, Krishnamurthy Anand, Joshua Lee Margolies, Padmaja Parakala
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Patent number: 9994717Abstract: A CVD-coated article has a substrate with a substrate surface and a CVD coating scheme on the substrate surface. The coating scheme includes a coating layer of Ti1-xMex nitride wherein Me is selected from the group of zirconium or hafnium or a mixture of zirconium and hafnium, and x equals between about 0.1 and about 0.9. The coating layer of Ti1-xMex nitride has a microhardness equal to between about 2300 HV0.05 and about 2600 HV0.05, a face centered cubic crystal structure, and a lattice constant equal to between about 0.427 nanometers and about 0.453 nanometers.Type: GrantFiled: April 13, 2015Date of Patent: June 12, 2018Assignee: KENNAMETAL INC.Inventors: Volkmar Sottke, Hartmut Westphal, Karl H. Wendt, Peter R. Leicht, Rodrigo A. Cooper, Yixiong Liu
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Patent number: 9994958Abstract: A coating is formed from one layer or two or more layers, at least one of the layers includes a multi-layer structure in which a first unit layer composed of TiN and a second unit layer composed of Ti1-xAlxN are alternately stacked, the first unit layer has an fcc crystal structure, and the second unit layer has an fcc crystal structure, X in Ti1-xAlxN being not smaller than 0.6 and not greater than 0.9.Type: GrantFiled: January 20, 2016Date of Patent: June 12, 2018Assignee: SUMITOMO ELECTRIC HARDMETAL CORP.Inventors: Anongsack Paseuth, Hideaki Kanaoka, Susumu Okuno
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Patent number: 9987687Abstract: A coated cutting tool for chip forming machining of metals includes a substrate having a surface coated with a chemical vapour deposition (CVD) coating. The coating has a layer of ?-Al2O3, wherein the ?-Al2O3 layer exhibits a texture coefficient TC(0 0 12)?7.2 and wherein the ratio of I(0 0 12)/I(0 1 14) is ?1.Type: GrantFiled: December 18, 2015Date of Patent: June 5, 2018Assignee: SANDVIK INTELLECTUAL PROPERTY ABInventors: Erik Lindahl, Jan Engqvist
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Patent number: 9962771Abstract: A surface-coated tool includes a substrate and a coating film formed on the substrate. The coating film includes an alternate layer in which one or more A layers and one or more B layers are alternately stacked. The A layer and the B layer each have a thickness not smaller than 2 nm and not greater than 100 nm. An average composition of the A layer is expressed as TiaAlbSicN (0.5<a<0.8, 0.2<b<0.4, 0.01<c<0.1, a+b+c=1), an average composition of the B layer is expressed as TidAleSifN (0.4<d<0.6, 0.3<e<0.7, 0.01<f<0.1, d+e+f=1), and a condition of 0.05<A?D?0.2 AND 0.05<E?B?0.2 is satisfied.Type: GrantFiled: May 19, 2015Date of Patent: May 8, 2018Assignee: Sumitomo Electric Hardmetal Corp.Inventors: Keizo Tanaka, Hiroki Takeshita, Kazuhiro Hirose, Haruyo Fukui
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Patent number: 9950960Abstract: A composite sintered body includes a first phase and a second phase. The first phase is a diamond phase, and the second phase is a phase formed of one or more types of elements or compounds or both thereof and applying strain to the first phase. A contained amount of the second phase is larger than 0 ppm and not larger than 1000 ppm. As a result, there is provided a high wear-resistant, high local wear-resistant, and high chipping-resistant diamond-containing composite sintered body.Type: GrantFiled: March 16, 2015Date of Patent: April 24, 2018Assignee: Sumitomo Electric Industries, Ltd.Inventors: Takeshi Satoh, Hitoshi Sumiya
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Patent number: 9919286Abstract: A method is described for preparing a sorbent including the steps of: (i) mixing together an inert particulate support material and one or more binders to form a support mixture, (ii) shaping the support mixture by granulation in a granulator to form agglomerates, (iii) coating the agglomerates with a coating mixture powder including a particulate copper sulphide and one or more binders to form a coated agglomerate, and (iv) drying the coated agglomerate to form a dried sorbent.Type: GrantFiled: December 4, 2014Date of Patent: March 20, 2018Assignee: Johnson Matthey Public Limited CompanyInventors: Matthew James Evans, Matthew David Gwydion Lunn, Martin Graham Partridge, Christopher John Young
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Patent number: 9884790Abstract: A cutting tool includes a base material and a coating formed on the base material. The base material is a sintered body containing 30 to 80% by volume of cubic boron nitride, and a binder. The surface in contact with the coating, of the base material, has a plurality of convex portions made of the cubic boron nitride and a plurality of concave portions made of the binder. A surface roughness Rsub of the surface in contact with the base material, is 0.1 to 0.4 ?m. A surface roughness Rsurf of an outermost surface of the coating is 0 to 0.15 ?m. A surface roughness Rasurf of the outermost surface of the coating is 0 to 0.1 ?m. The surface roughness Rsub of the surface in contact with the coating, of the base material, is greater than the surface roughness Rsurf of the outermost surface of the coating.Type: GrantFiled: November 25, 2014Date of Patent: February 6, 2018Assignee: Sumitomo Electric Hardmetal Corp.Inventors: Nozomi Tsukihara, Makoto Setoyama, Katsumi Okamura
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Patent number: 9863927Abstract: A method of inspecting and forming sapphire structures. The method of inspecting a sapphire structure may include providing an annealed sapphire structure, and measuring a profile of at least a portion of the annealed sapphire structure. The profile of at least the portion of the annealed sapphire structure may be measured using a non-x-ray based measuring device. Additionally, the method of inspecting may include identifying a defect within at least a portion of the measured profile of the annealed sapphire structure.Type: GrantFiled: February 7, 2014Date of Patent: January 9, 2018Assignee: APPLE INC.Inventors: Dale N. Memering, Matthew S. Rogers, Scott A. Myers
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Patent number: 9828254Abstract: A surface-coated cutting tool according to the present invention includes a coating. The coating has an ?-Al2O3 layer. The ?-Al2O3 layer includes a lower layer portion and an upper layer portion. When respective crystal orientations of crystal grains of ?-Al2O3 are specified by performing EBSD analyses with an FE-SEM on a cross-section obtained when the ?-Al2O3 layer is cut along a plane including a normal line of a surface of the ?-Al2O3 layer and a color map is prepared based on the crystal orientations, in the color map, an area in the upper layer portion occupied by the crystal grains of which normal direction of a (001) plane is within ±10° with respect to a normal direction of the surface of the ?-Al2O3 layer is equal to or more than 90%, and such an area in the lower layer portion is equal to or less than 50%.Type: GrantFiled: August 28, 2015Date of Patent: November 28, 2017Assignee: Sumitomo Electric Hardmetal Corp.Inventors: Shinya Imamura, Anongsack Paseuth, Takanori Detani, Hideaki Kanaoka
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Patent number: 9777239Abstract: An element with at least one slide surface with a coating for use on an internal combustion engine may include a base of a metallic alloy and at least one inner surface provided with a hard ceramic coating generated by physical vapor deposition. The element may include a porosity with a rate lower than 2 percent by volume, a Vickers hardness ranging from 1500 to 3000HV, and a compressive inner tension lower than 500 MPa.Type: GrantFiled: May 28, 2012Date of Patent: October 3, 2017Assignees: MAHLE Metal Leve S.A., MAHLE International GmbHInventors: Paulo Jose Da Rocha Mordente, Robert R. Banfield, Jose V. Sarabanda
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Patent number: 9758859Abstract: The present disclosure relates to a coated cutting tool including a substrate and a coating disposed on the substrate, wherein the coating includes a layer of TixZryAl(1-x-y)N, where 0<x?0.3, 0.2?y?0.8 and 0.1?(1-x-y)?0.7. The disclosure further relates to a method of producing such a coated cutting tool, and to a cutting insert forming a coated cutting tool.Type: GrantFiled: July 27, 2015Date of Patent: September 12, 2017Assignee: SANDVIK INTELLECTUAL PROPERTYInventors: Lars Johnson, Robert Pilemalm, Lina Rogstrom
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Patent number: 9761763Abstract: Techniques for fabricating and using arrays of violet-emitting LEDs coated with densely-packed-luminescent-material layers together with apparatus and method embodiments thereto are disclosed.Type: GrantFiled: December 19, 2013Date of Patent: September 12, 2017Assignee: Soraa, Inc.Inventors: Frank M. Steranka, Rafael Aldaz, Seshasayee Ankireddi, Troy Trottier, Rohit Modi, Rajarshi Saha
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Patent number: 9739675Abstract: A surface acoustic wave (SAW) sensor includes a surface acoustic wave material and a comb-teeth electrode. The surface acoustic wave material is to be arranged at a place where the surface acoustic wave material is distorted by physical quantity such as stress. The comb-teeth electrode is arranged on the surface of the surface acoustic wave material to excite a surface acoustic wave to the surface acoustic wave material. The surface acoustic wave material has a sapphire board and a ScAlN film arranged on a surface of the sapphire board.Type: GrantFiled: May 27, 2015Date of Patent: August 22, 2017Assignees: DENSO CORPORATION, TOHOKU UNIVERSITY, National University Corporation Chiba UniversityInventors: Akihiko Teshigahara, Toshihiko Takahata, Takao Iwaki, Shuji Tanaka, Masayoshi Esashi, Kenya Hashimoto
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Patent number: 9724804Abstract: Methods of forming a cutting element include disposing a volume of polycrystalline material adjacent a liquid electrolytic solution and applying an electrical between the polycrystalline material and a cathode in contact with the liquid electrolytic solution to increase an oxidation state of the metal catalyst material. The polycrystalline material includes interbonded grains of hard material and metal catalyst particles in the interstitial spaces between adjacent grains of hard material. Some methods include forming a barrier over a portion of a surface of a volume of polycrystalline material.Type: GrantFiled: January 9, 2015Date of Patent: August 8, 2017Assignee: Baker Hughes IncorporatedInventor: Oleg A. Mazyar
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Patent number: 9719164Abstract: An amount of nitrogen in a compound film is controlled. A method of manufacturing compound film comprising forming films laminated on a substrate placed at a film forming chamber is provided. According to the method of manufacturing compound film, a first compound layer including one or more elements selected from metal elements and semimetal elements and oxygen element and a second compound layer including one or more elements and nitrogen element are laminated alternately. The first compound layer is formed by a Filtered Arc Ion Plating method and the second compound layer is formed by a sputtering method.Type: GrantFiled: October 29, 2015Date of Patent: August 1, 2017Assignee: NIKON CORPORATIONInventors: Tsukasa Kishiume, Koichiro Iwahori
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Patent number: 9680056Abstract: A heteroepitaxy strain-management structure for a light emitting device includes: a substrate or template; an epitaxial layer to be epitaxially formed over the substrate or template, wherein a calculated in-plane compressive strain to be exerted by the substrate or template to the epitaxial layer is equal to or larger than 1%; and a heavily doped interlayer inserted in-between the epitaxial layer and the substrate or template; wherein the heavily doped interlayer is of substantially the same material composition as that of the epitaxial layer, with a thickness of 40-400 nm, and doped at a doping level in the range of 5×1019 to 5×1020 cm?3. Also provided is an ultraviolet light emitting device having a heteroepitaxy strain-management structure.Type: GrantFiled: July 8, 2016Date of Patent: June 13, 2017Assignee: BOLB INC.Inventors: Jianping Zhang, Ling Zhou
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Patent number: 9670575Abstract: The present invention is a laminated coating film such that at least one of each of the below mentioned coating film (Q) and coating film (R) are laminated in alternation on a substrate. [Coating film Q] At least one coating film selected from the group consisting of: a coating film having a compositional formula of Ti1-a-b-cBaCbNc and satisfying the atom ratios of each element being 0.2?a?0.7, 0?b?0.35, and 0?c?0.35; a coating film having a compositional formula of Si1-d-eCdNe and satisfying the atom ratios of each element being 0.2?d?0.50 and 0?e?0.3; and a coating film having a compositional formula of B1-f-gCfNg and satisfying the atom ratios of each element being 0.03?f?0.25 and 0?g?0.5. [Coating film R] A coating film having a compositional formula of L(BxCyN1-x-y) (where L is at least one element selected from the group consisting of W, Mo, and V) and satisfying the atom ratios of each element being 0?x?0.15 and 0?y?0.5.Type: GrantFiled: March 14, 2014Date of Patent: June 6, 2017Assignee: Kobe Steel, Ltd.Inventors: Kenji Yamamoto, Maiko Abe, Mamoru Hosokawa
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Patent number: 9666685Abstract: A radio frequency (RF) power transistor includes a semiconductor heterostructure, a gate electrode, a drain electrode and a source electrode. The drain electrode includes an ohmic contact and a Schottky contact extending from the ohmic contact toward the gate electrode, spaced apart from the gate electrode (4) by a distance (LGD), and having a length (LEXT) being not less than 2 ?m and not greater than 4 ?m. A ratio of the length (LEXT) to a sum of the length (LEXT) and a distance (LGD) is greater than 0.83 and less than 0.98.Type: GrantFiled: April 1, 2016Date of Patent: May 30, 2017Assignee: NATIONAL TSING HUA UNIVERSITYInventors: Shuo-Hung Hsu, Chuan-Wei Tsou, Yi-Wei Lien
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Patent number: 9649746Abstract: A cutting tool formed by a coating layer on a substrate has cutting edges that feature serrations. The linear dimensions of the serrations may vary from a few nanometers up to 10 microns. The serrations result in a smoother cut edge on the workpiece, particularly when the workpiece is formed of certain materials that are seen as particularly difficult to cut, such as hardened steels.Type: GrantFiled: May 29, 2012Date of Patent: May 16, 2017Assignee: NanoMech, Inc.Inventors: Ajay P. Malshe, Wenping Jiang
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Patent number: 9623468Abstract: The present invention relates to a coating for high-temperature applications with tribological stress. The coating comprises a multi-layer system and a top lubrication layer, the top lubricant layer containing, as a main component, molybdenum.Type: GrantFiled: November 11, 2013Date of Patent: April 18, 2017Assignee: OERLIKON SURFACE SOLUTIONS AG, PFÄFFIKONInventors: Matthias Lukas Sobiech, Jurgen Ramm
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Patent number: 9608049Abstract: An organic light emitting diode (OLED) display includes a flexible substrate, a barrier layer disposed on the flexible substrate, and an organic light emitting diode disposed on the barrier layer. The barrier layer includes a plurality of metal layers and a plurality of insulation layers in which the metal layers and the insulation layers are alternatively stacked with each other on the flexible substrate.Type: GrantFiled: October 1, 2014Date of Patent: March 28, 2017Assignee: SAMSUNG DISPLAY CO., LTD.Inventor: Jusuck Lee
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Patent number: 9551062Abstract: A tool hard film that is to be disposed as coating on a surface of a tool, the tool hard film being a TiCrMoWV oxycarbide, oxynitride, or oxycarbonitride having a phase with a NaCl-type crystal structure as a main phase, the oxycarbide, oxynitride, or oxycarbonitride having fine crystals due to introduction of oxygen.Type: GrantFiled: March 28, 2013Date of Patent: January 24, 2017Assignees: OSG CORPORATION, NATIONAL UNIVERSITY CORPORATION TOHOKU UNIVERSITYInventors: Masatoshi Sakurai, Mei Wang, Toshihiro Ohchi, Yuji Sutou, Junichi Koike, Shoko Komiyama
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Patent number: 9528180Abstract: The present invention relates to a coating for sliding parts that allows using diamond like carbon (DLC) or DLC-comprising coatings in combination with Molybdenum- and/or Zinc-comprising lubricants in such a manner that enhanced reduction of wear and friction in comparison to the state of the art is attained. The coating system according to the present invention comprises at least a metal-comprising carbon layer of the type Me-C/a)-C:X, whose element composition can be expressed as (MeaC1-a)1-bXb with 0.3?a?0.6 and 0<b?0.3, where Me is a metal or a combination of different metals and X is an element different from Me and different from C or X is a mixture of elements different from Me and which doesn't contain C. Me can be preferably Chromium (Cr) or Molybdenum (Mo) and X can be preferably hydrogen (H) or a mixture of silicon and hydrogen (Si+H).Type: GrantFiled: March 1, 2012Date of Patent: December 27, 2016Assignee: OERLIKON SURFACE SOLUTIONS AG, PFAFFIKONInventors: Jürgen Becker, Martin Grischke, Astrid Gies
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Patent number: 9523145Abstract: A cutting tool insert having a cemented carbide substrate and a coating including a layer of NbN, wherein the cemented carbide substrate includes 11-12.5 wt % cobalt, 0.2-1.2 wt % chromium, and 86.3-88.4 wt % wolfram carbide.Type: GrantFiled: June 20, 2013Date of Patent: December 20, 2016Assignee: SECO TOOLS ABInventors: Tommy Larsson, Peter Lofroth, Hanna Kallerhult, Hindrik Engstrom, Jan Qvick
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Patent number: 9520597Abstract: A cathode material for a solid oxide fuel cell comprises a complex oxide having a perovskite structure expressed by the general formula ABO3, a content amount of P included in the complex oxide being at least 1 ppm and no more than 50 ppm, a content amount of Cr in the complex oxide being at least 1 ppm and no more than 500 ppm, and a content amount of B in the complex oxide being at least 1 ppm and no more than 50 ppm in a weight ratio relative to a total weight of the complex oxide.Type: GrantFiled: September 14, 2012Date of Patent: December 13, 2016Assignee: NGK INSULATORS, LTD.Inventors: Makoto Ohmori, Ayano Kobayashi, Shinji Fujisaki
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Patent number: 9493871Abstract: A surface-coated cutting tool includes a hard coating layer vapor-deposited on a surface of a tool body, in which a composition of the hard coating layer is expressed by a composition formula of (AlxTi1-x)N (0.5?x?0.8), the average layer thickness of the hard coating layer is 0.5 ?m to 7.0 ?m, the hard coating layer is formed of crystal grains having an average grain size of 5 nm to 50 nm, the hard coating layer have a mixed structure including cubic crystal grains having a rock-salt structure, and hexagonal crystal grains having a wurtzite structure, and {200} planes of the cubic crystal grains and {11-20} planes of the hexagonal crystal grains are oriented so as to be perpendicular to the surface of the tool body.Type: GrantFiled: November 29, 2013Date of Patent: November 15, 2016Assignee: MITSUBISHI MATERIALS CORPORATIONInventors: Koichi Tanaka, Masakuni Takahashi
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Patent number: 9487403Abstract: Provided are titanium oxynitride having a titanium deficiency-type halite structure (Ti1-xO1-yNy, wherein x and y are real numbers), in which x representing a deficiency degree of titanium is greater than 0 and less than 1, and y representing an introduction degree of nitrogen is greater than 0 and less than 1, and a method of preparing the same. The titanium oxynitride having the titanium deficiency-type halite structure with an improved photocatalyst property in the visible wavelength region may be provided.Type: GrantFiled: November 20, 2012Date of Patent: November 8, 2016Assignee: TMC Co., LTD.Inventors: Young Soo Lim, Won-Seon Seo
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Patent number: 9415446Abstract: A coated tool with a hard coating layer, which has an excellent hardness and heat insulating effect; and exhibits an excellent chipping resistance and an excellent fracturing resistance for a long-term usage, is provided. The hard coating layer included in the coated tool has a chemically vapor deposited alternate laminated structure, which is made of: a region A layer and a region B layer, each of which is expressed by the composition formula of (Ti1-xAlx)(CyN1-y); and has the average total layer thickness of 1-10 ?m. In the region A layer, relationships, 0.70?x?0.80 and 0.0005?y?0.005, are satisfied; the average grain width W is 0.1 ?m or less; and the average grain length L is 0.1 ?m or less. In the region B layer, relationships, 0.85?x?0.95 and 0.0005?y?0.005, are satisfied; the average grain width W is 0.1-2.0 ?m; and the average grain length L is 0.5-5.0 ?m.Type: GrantFiled: August 28, 2013Date of Patent: August 16, 2016Assignee: Mitsubishi Materials CorporationInventors: Sho Tatsuoka, Naoyuki Iwasaki, Kenji Yamaguchi, Akira Osada
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Patent number: 9409823Abstract: This invention provides a hybrid material that exhibits strength, stiffness and ability to resist high temperatures. This hybrid material essentially consists of component A and component B. Component A is selected from the group consisting of inorganic compounds, oxides, carbides, nitrides, borides, and combinations thereof. Component B is selected from the group comprising elemental carbon, inorganic compounds, oxides, carbides, nitrides, borides, and combinations thereof. Component B comprises a plurality of units, each of the units substantially exhibiting a shape, such that this shape substantially exhibits a long dimension and a short dimension, with the short dimension being in a direction that is essentially perpendicular to the direction of the long dimension and the short dimension being in the range from 0.1 nm to 0.5 ?m. Each of the units of component B is substantially in contact with and substantially bonded to at least one of the units of component A.Type: GrantFiled: February 15, 2013Date of Patent: August 9, 2016Inventors: Deborah Duen Ling Chung, Xiaoqin Gao
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Patent number: 9371797Abstract: To provide a high-thermal-conductivity piston ring having excellent scuffing resistance and wear resistance, which can be used in a high-heat-load environment in engines, a TiN coating as thick as 10-60 ?m, in which the texture coefficient of a (220) plane is 1.1-1.8 in X-ray diffraction on the coating surface, larger than those of (111) and (200) planes, is formed under the optimized ion plating conditions on a peripheral surface of the piston ring. Also, to obtain excellent sliding characteristics with low friction without losing excellent thermal conductivity of TiN, a hard amorphous carbon coating is formed on the TiN coating.Type: GrantFiled: June 21, 2012Date of Patent: June 21, 2016Assignee: KABUSHIKI KAISHA RIKENInventors: Takuma Sekiya, Yuuichi Murayama, Masayuki Sato, Yuji Shima, Junya Takahashi, Masaki Moronuki
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Patent number: 9347559Abstract: A high-thermal-conductivity piston ring having excellent scuffing resistance and wear resistance, which can be used in a high-heat-load environment in engines is provided. Also, to provide a piston ring with low friction for contributing to the improvement of fuel efficiency, a TiN coating as thick as 10-60 ?m, in which the texture coefficient of a (111) plane is 1.2-1.65 in X-ray diffraction on the coating surface, with the texture coefficient of a (111) plane>the texture coefficient of a (220) plane>the texture coefficient of a (200) plane, is formed under the optimized ion plating conditions on a peripheral surface of the piston ring. Further, to obtain excellent sliding characteristics with low friction without losing excellent thermal conductivity of TiN, a hard amorphous carbon coating is formed on the TiN coating.Type: GrantFiled: June 21, 2012Date of Patent: May 24, 2016Assignee: KABUSHIKI KAISHA RIKENInventors: Takuma Sekiya, Yuuichi Murayama, Masayuki Sato, Yuji Shima, Junya Takahashi, Masaki Moronuki
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Patent number: 9324913Abstract: A nitride semiconductor structure includes: a plurality of crystal growth seed regions formed of a nitride semiconductor, of which the principal surface is an m-plane and which extends to a range that defines an angle of not less than 0 degrees and not more than 10 degrees with respect to an a-axis; and a laterally grown region formed of a nitride semiconductor which has extended in a c-axis direction from each of the plurality of crystal growth seed regions. An S width that is the spacing between adjacent ones of the plurality of crystal growth seed regions is at least 20 ?m.Type: GrantFiled: June 2, 2014Date of Patent: April 26, 2016Assignee: Panasonic Intellectual Property Management Co., Ltd.Inventors: Songbaek Choe, Shunji Yoshida, Toshiya Yokogawa
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Patent number: 9309120Abstract: There is provided a method for efficiently producing a high-purity alkali metal nitride or alkaline earth metal nitride by simple processes. Specifically provided is a method for producing an alkali metal nitride, an alkaline earth metal nitride, or a composite thereof, the method including thermally decomposing one or more alkali metal amides or alkaline earth metal amides.Type: GrantFiled: November 11, 2010Date of Patent: April 12, 2016Assignee: TAIHEIYO CEMENT CORPORATIONInventors: Shoji Suzuki, Kazuhiko Tokoyoda, Tsutomu Suzuki
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Patent number: 9297054Abstract: The present invention relates to a cemented carbide article comprising a core of metal carbide grains and a binder selected from cobalt, nickel, iron and alloys containing one or more of these metals and a surface layer defining an outer surface for the article, the surface layer comprising 5 to 25 weight percent of tungsten and 0.1 to 5 weight percent carbon, the balance of the surface layer comprising a metal or alloy selected from the binder metals and alloys and the surface layer being substantially free of carbide grains as determined by optical microscopy or SEM. A method for the production of a cemented carbide article is also provided.Type: GrantFiled: January 17, 2012Date of Patent: March 29, 2016Assignee: Element Six GmbHInventors: Igor Yurievich Konyashin, Bernd Heinrich Ries, Christina Lachmann
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Patent number: 9273931Abstract: Amorphous alloy armor made of at least one thin layer of bulk-solidifying amorphous alloys and methods of forming such armor are provided. Forming the armor in accordance with the current invention provides ruggedness, a lightweight structure, excellent resistance to chemical and environmental effects, and low-cost manufacturing.Type: GrantFiled: November 9, 2009Date of Patent: March 1, 2016Assignee: Crucible Intellectual Property, LLCInventor: Gerald A. Croopnick
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Patent number: 9254506Abstract: A barrier film having a substrate, a base polymer layer applied to the substrate, an oxide layer applied to the base polymer layer, and a top coat polymer layer applied to the oxide layer. An optional inorganic layer can be applied over the top coat polymer layer. The top coat polymer includes a silane and an acrylate co-deposited to form the top coat layer. The use of a silane co-deposited with an acrylate to form the top coat layer of the barrier films provide for enhanced resistance to moisture and improved peel strength adhesion of the top coat layer to the underlying barrier stack layers.Type: GrantFiled: July 2, 2010Date of Patent: February 9, 2016Assignee: 3M INNOVATIVE PROPERTIES COMPANYInventors: Mark A. Roehrig, Alan K. Nachtigal, Mark D. Weigel
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Patent number: 9255342Abstract: The present invention discloses a semi-insulating wafer of GaxAlyIn1-x-yN (0?x?1, 0?x+y?1) which is doped with bismuth (Bi). The semi-insulating wafer has the resistivity of 104 ohm-cm or more. Although it is very difficult to obtain a single crystal ingot of group III nitride, the ammonothermal method can grow highly-oriented poly or single crystal ingot of group III nitride having the density of dislocations/grain boundaries less than 105 cm?2. The invention also disclose the method of fabricating the semi-insulating group III nitride bulk crystals and wafers.Type: GrantFiled: February 28, 2013Date of Patent: February 9, 2016Assignees: SixPoint Materials, Inc., Seoul Semiconductor Co., Ltd.Inventors: Tadao Hashimoto, Edward Letts, Sierra Hoff