Loose Particulate Mixture (i.e., Composition) Containing Metal Particles Patents (Class 75/255)
  • Patent number: 5876481
    Abstract: A steel powder consisting of a combination of purified steel and prealloyed manganese, chromium, molybdenum and nickel. The steel powder is used in the production of metal parts using powder metallurgy. The addition of the prealloyed elements results in a metal part having greater strength and hardness with a low oxygen content and good compressibility.
    Type: Grant
    Filed: June 14, 1996
    Date of Patent: March 2, 1999
    Assignee: Quebec Metal Powders Limited
    Inventors: Fran.cedilla.ois Chagnon, Yves Trudel
  • Patent number: 5876634
    Abstract: Tin oxide doped with an electrochromically effective amount of a metal, e.g. antimony or niobium, which provides a color change when the doped tin oxide is exposed to an electrochemical potential in the presence of mobile ions. Particles of electrochromic doped tin oxide, e.g. coated on a white or pastel pigment substrate, have a contrast ratio greater than 1.2, where contrast ratio is a measure of electrochromic functionality of a material and is the ratio of reflectance of the material in an oxidized state to the color of the material in a reduced state and where color is a photodiode measurement of the value of light reflected off the oxidized or reduced material from a constant source of light shining on the material. Such doped tin oxide-containing particles are useful as electrochromic material in display devices.
    Type: Grant
    Filed: December 23, 1996
    Date of Patent: March 2, 1999
    Assignee: Monsanto Company
    Inventor: James P. Coleman
  • Patent number: 5863618
    Abstract: A method for producing an atomized powder of chromium carbide particles dispersed in a nickel chromium matrix in which chromium in the powder is from 55 to 92 weight percent of the powder.
    Type: Grant
    Filed: October 3, 1996
    Date of Patent: January 26, 1999
    Assignee: Praxair St Technology, Inc.
    Inventors: William John Crim Jarosinski, Lewis Benton Temples, Calvin Henry Londry
  • Patent number: 5863870
    Abstract: An iron or copper based metal powder useful for plasma deposition of a coating that has a dry coefficient of friction 0.75 or less and readily conducts heat through the coating. The powder comprises (a) H.sub.2 O atomized and annealed particles consisting essentially of (by weight) carbon 0.15-0.85%, oxygen 0.1-0.45%, an air hardening agent selected from manganese and nickel of 0.1-06.5%, and the remainder iron or copper, with at least 90% of the particles having oxygen and iron or copper combined in the lowest atomic oxygen form for an oxide of such metal.A method of making anti-friction iron powder that is economical, selectively produces FeO and promotes fine flowable particles. The method comprises (a) steam atomization of a molten steel that excludes other oxygen, the steel containing carbon up to 0.4% by weight to produce a collection of comminuted particles, and (b) annealing the particles in an air atmosphere for a period of time of 0.25-2.0 hours in a temperature range of 800.degree.-1400.degree. F.
    Type: Grant
    Filed: August 18, 1997
    Date of Patent: January 26, 1999
    Assignee: Ford Global Technologies, Inc.
    Inventors: V. Durga Nageswar Rao, Robert Alan Rose, David Alan Yeager, Carlo Alberto Fucinari
  • Patent number: 5864071
    Abstract: Powdered ferrous metal compositions are disclosed which provide for increased corrosion resistance through the admixing of powder aluminum containing compositions with standard ferrous metal compositions prior to forming the powder metal parts. In a preferred embodiment, the aluminum ranges is admixed as an FeAl alloy powder with the standard ferrous metal composition. The present invention further includes a powder metal ferrous part formed from the composition produced by a method including the steps of (i) providing a ferrous powder metal composition, (ii) admixing a powder aluminum containing composition with the ferrous composition to form a blended mixture, and (iii) forming a powder metal part from at least a portion of the blended mixture.
    Type: Grant
    Filed: April 24, 1997
    Date of Patent: January 26, 1999
    Assignee: Keystone Powdered Metal Company
    Inventor: John C. Kosco
  • Patent number: 5850047
    Abstract: A method of producing copper powder having little variation in its particle size and an excellent monodispersion properties. A copper complex ion solution is prepared from a copper-containing solution and a complexing agent, then a reducing agent is added to the copper complex ion solution to precipitate metallic copper. The copper-containing solution herein contains copper sulfate, copper formate, copper pyrophosphate, copper chloride or copper carbonate and the complexing agent is at least one carboxylate or phosphate.
    Type: Grant
    Filed: March 11, 1997
    Date of Patent: December 15, 1998
    Assignee: Murata Manufacturing Co., Ltd.
    Inventors: Hiroji Tani, Naoaki Ogata
  • Patent number: 5846270
    Abstract: A magnetic-abrasive powder includes a magnetic component of a powder of a magnetic material, an abrasive component of a powder of an abrasive material, and an adhesive which adhesively connects particles of the magnetic material with particles of the abrasive material.
    Type: Grant
    Filed: April 6, 1998
    Date of Patent: December 8, 1998
    Inventors: Savva Feygin, Gennady Kremen, Leonid Igelstyn
  • Patent number: 5844153
    Abstract: A mixed metal powder for hard metal alloys comprising cobalt, 1 to 10 parts per weight tungsten and 1 to 10 parts by weight of aluminum and a hard metal alloy containing the mixed metal powder binder in an amount of from 2 to 12 parts by weight per about 100 parts by weight of a metal carbide for corrosion resistant hard metal tools.
    Type: Grant
    Filed: July 12, 1996
    Date of Patent: December 1, 1998
    Assignee: EMTEC Magnetics GmbH
    Inventors: Manfred Schlatter, Jurgen Koppe, Volker Eichhorst
  • Patent number: 5840166
    Abstract: A rare earth metal-nickel hydrogen storage alloy having a composition represented by the formula (1) (R.sub.1-x L.sub.x) (Ni.sub.1-y M.sub.y).sub.z . . . (1) (R: La, Ce, Pr, Nd; L: Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu, Y, Sc, Mg, Ca; M: Co, Al, Mn, Fe, Cu, Zr, Ti, Mo, Si, V, Cr, Nb, Hf, Ta, W, B, C; 0.05.ltoreq.x.ltoreq.0.4, 0.ltoreq.y.ltoreq.0.5, 3.0.ltoreq.z<4.5), the alloy including in an amount of not less than 30 volume % and less than 95 volume % thereof crystals each containing not less than 5 and less than 25 antiphase boundaries extending perpendicular to C-axis of a crystal grain of the alloy per 20 nm along the C-axis, not less than 60% and less than 95% of added amount of the element represented by L in the formula (1) being arranged in antiphase areas, and a method for producing the same.
    Type: Grant
    Filed: March 7, 1997
    Date of Patent: November 24, 1998
    Assignee: Santoku Metal Industry Co. Ltd.
    Inventor: Akihito Kaneko
  • Patent number: 5830257
    Abstract: A manufacturing method for an alumina-dispersed reinforced copper alloy according to the invention is an improved method which is capable of manufacturing efficiently alumina-dispersed reinforced copper having both good electro-conductivity used for wire-manufacturing-material and good mechanical property, the manufacturing method comprises the steps of obtaining powders constituted by particles having aluminum-contained copper alloy-oxide, allowing to mill aluminum-contained copper alloy powder within the air atmosphere by milling device with mechanical-alloying-operation due to shock compression, converting aluminum into aluminum-oxide by heat-treatment of the powders within inert atmosphere, implementing reduction-treatment of the converted member within the reducing atmosphere, and executing hot extrusion the reduction-treated-material.
    Type: Grant
    Filed: August 22, 1996
    Date of Patent: November 3, 1998
    Assignee: Yazaki Corporation
    Inventors: Hirohiko Fujimaki, Manabu Kiuchi, Tetsuya Takaai, deceased
  • Patent number: 5832360
    Abstract: A bond for a single layer metal bond abrasive tool can be easily chemically and electrochemically stripped from the metal core of a recovered used tool to facilitate reuse of the core. Relative to conventionally bonded tools, the speed of stripping the novel bond is quick, and the stripped core has a smooth, clean surface which needs only minimal mechanical repair prior to reuse. In one aspect, the novel bond consists essentially of a ternary bond composition of copper, tin and titanium, in which the copper and tin are pre-alloyed and the pre-alloy and titanium component are incorporated in the bond composition as fine particle size powders. In another aspect, the bond is a quaternary bond composition consisting essentially of copper, tin, titanium and silver. The powder components can be used dry or mixed with a fugitive liquid binder as a paste. The novel bond can be brazed at lower temperature than copper/tin/titanium bonds prepared otherwise.
    Type: Grant
    Filed: August 28, 1997
    Date of Patent: November 3, 1998
    Assignee: Norton Company
    Inventors: Richard M. Andrews, Bradley J. Miller, Marcus R. Skeem, Ren-Kae Shiue
  • Patent number: 5796018
    Abstract: Ferrous powder particles are coated with vaporized phosphorus in a fluid-bed reactor to obtain homogeneous coatings of phosphorus. The coated powders are useful feed for pressed structural parts, exhibiting improved green density, compressibility and sintered density thus improving magnetic and tensile properties.
    Type: Grant
    Filed: January 29, 1997
    Date of Patent: August 18, 1998
    Assignees: Procedyne Corp., Magna-Tech P/M Labs.
    Inventors: Kenneth H. Moyer, David J. Geveke, Thomas R. Parr, Robert B. Roaper
  • Patent number: 5785897
    Abstract: A coating solution for forming a transparent and electrically conductive film contains fine conductive metal or alloy particles dispersed in a polar solvent and having a diameter not exceeding 50 nm. The metal particles are of silver and at least one of palladium, copper and gold. The alloy particles are of an alloy of silver with at least one of palladium, copper and gold. The solution permits the use of a baking temperature which is as low as 150.degree.-450.degree. C.
    Type: Grant
    Filed: February 19, 1997
    Date of Patent: July 28, 1998
    Assignee: Sumitomo Metal Mining Co., Ltd.
    Inventors: Atsushi Toufuku, Kenji Adachi
  • Patent number: 5782955
    Abstract: A metallurgical silicon or ferrosilicon in the form of granulates having an average size of less than 10 mm and in which the total oxygen concentration is less than 0.05% by weight, and a process for manufacture of this silicon or ferrosilicon consisting of a carbothermal reduction of silica in an electric oven, chlorine-based refining of the liquid metal, and granulation of the refined liquid metal in water under an inert atmosphere. The silicon may be used for silicone manufacture or as a constituent of an aluminum alloy, and the ferrosilicon, as a steel additive used to obtain magnetic sheet metals for electrical construction.
    Type: Grant
    Filed: January 11, 1996
    Date of Patent: July 21, 1998
    Assignee: Pechiney Electrometallurgie
    Inventors: Maurice Sales, Thomas Margaria
  • Patent number: 5776225
    Abstract: A clean refractory metal sponge fines product is made from refractory metal sponge fines free of refractory metal oxides, carbides, nitrides and binary iron alloys; silicon carbide, oils, greases and organic compounds; salt; dust; dirt; pieces of iron, iron alloy and tungsten carbide; and light contaminants. The sponge fines are vigorously washed and rinsed with a displacement wash to remove the bulk of the wash fluid and subject to a counter-current wash to yield clean refractory metal sponge fines. The clean sponge fines can be pressed into briquettes and sintered at elevated pressures, or mixed with an alkali metal refractory metal halide slat, pressed at elevated pressures into sponge fines/salt briquettes and dried or pressed into briquettes, dried and packaged, or pressed into briquettes and stored wet. The briquettes are non-pyrophoric.
    Type: Grant
    Filed: November 21, 1996
    Date of Patent: July 7, 1998
    Inventor: Joseph A. Megy
  • Patent number: 5766305
    Abstract: A metal powder composition for metallization is for use in forming a metallized film from a paste comprising Cu and Ti powder and consists essentially of about 95 to 99.5% Cu and 0.5 to less than 5% Ti by weight. The above-mentioned paste is then applied onto a substrate and then fired to provide a metallized substrate.
    Type: Grant
    Filed: September 12, 1996
    Date of Patent: June 16, 1998
    Assignee: Tokin Corporation
    Inventors: Youhei Watabe, Shinichi Iwata, Tomeji Ohno
  • Patent number: 5766304
    Abstract: An iron-base mixture and method for powder metallurgy containing iron-base powder, an alloy powder including at least copper, copper oxide or both, and an organic substance for bonding the alloy powder to the iron-base powder, wherein said copper powder or copper oxide powder has a particle size of agglomeration, when evaluated by the micro-track method, of about 5 .mu.m to 28 .mu.m, and wherein the particles of copper or copper oxide have a primary particle size which, when evaluated by the BET method, is about 0.2 .mu.m to 1.5 .mu.m.
    Type: Grant
    Filed: April 24, 1996
    Date of Patent: June 16, 1998
    Assignee: Kawasaki Steel Corporation
    Inventors: Satoshi Uenosono, Kuniaki Ogura
  • Patent number: 5759228
    Abstract: A nozzle for an electric dispersion reactor includes two coaxial cylindrical bodies, the inner one of the two delivering disperse phase fluid into a continuous phase fluid. A potential difference generated by a voltage source creates a dispersing electric field at the end of the inner electrode.
    Type: Grant
    Filed: January 16, 1996
    Date of Patent: June 2, 1998
    Assignee: Martin Marietta Energy Systems, Inc.
    Inventors: Warren G. Sisson, Michael T. Harris, Timothy C. Scott, Osman A. Basaran
  • Patent number: 5753005
    Abstract: A source powder for a wear-resistant sintered material, consisting essentially of, in weight percentages, Cr: 3.0 to 6.0%, 2 Mo+W: 10.0 to 20.0%, V: 1.0 to 8.0%, Co: 10.0% or below, C: 0.20% to {0.01(2 Mo+W)+0.24 V}%, Si: 0.1 to 1.0%, Mn: 0.1 to 1.0% and the balance being Fe and unavoidable impurities, or one prepared by adding 0.10 to 0.8% of S to the above composition. This powder can be compacted into a green compact having a high green density, which can further give a wear-resistant sintered material having a high sintered density, hardness and strength.
    Type: Grant
    Filed: January 10, 1997
    Date of Patent: May 19, 1998
    Assignees: Hitachi Powdered Metals Co., Ltd., Mitsubishi Steel Mfg. Co., Ltd.
    Inventors: Yoshimasa Aoki, Kei Ishii, Yukio Tokuyama, Yuji Soda
  • Patent number: 5736261
    Abstract: A conductive paste in which cracks do not occur even at boundaries between areas of different film thicknesses comprises spherical and flake-form silver powders, a low softening point glass frit, organic rhodium material and an organic vehicle; the proportion of the flake-form silver powder with respect to the total amount of silver powder is in the range 15 to 80 wt % and the proportion of the rhodium contained in the organic rhodium material with respect to the total amount of silver powder is 0.0001 wt % or less.
    Type: Grant
    Filed: November 22, 1995
    Date of Patent: April 7, 1998
    Assignee: Murata Manufacturing Co., Ltd.
    Inventor: Haruhiko Kano
  • Patent number: 5733649
    Abstract: A matrix powder for formation along with an infiltrant into a matrix for use as a wear element or for use in retaining at least one discrete hard element. The matrix powder including macrocrystalline tungsten carbide particles, crushed sintered cemented macrocrystalline tungsten carbide particles, tungsten carbide, and an iron-based component.
    Type: Grant
    Filed: September 23, 1996
    Date of Patent: March 31, 1998
    Assignee: Kennametal Inc.
    Inventors: Harold E. Kelley, William E. Silvis, Charles J. Terry
  • Patent number: 5733664
    Abstract: A matrix powder for formation along with an infiltrant into a matrix for use as a wear element or for use in retaining at least one discrete hard element. The matrix powder includes crushed sintered cemented tungsten carbide particles. The composition of the crushed sintered cemented tungsten carbide comprises between about 6 weight percent and about 13 weight percent binder metal and between about 87 weight percent and about 94 weight percent tungsten carbide.
    Type: Grant
    Filed: December 18, 1995
    Date of Patent: March 31, 1998
    Assignee: Kennametal Inc.
    Inventors: Harold E. Kelley, William E. Silvis, Charles J. Terry, Gary R. Peterson
  • Patent number: 5702501
    Abstract: A clayish composition for producing a molded article of noble metal consists essentially of a noble metal powder, starch and a water-soluble cellulose resin as organic binder and water. The contents of the starch and the water-soluble cellulose resin each fall in the range of 0.02-3.0% by weight, based on the total amount of the organic binder and the noble metal powder. A method for producing the sintered article of noble metal consists essentially of a step for producing the clayish composition mentioned above, a step of molding the clayish composition in a desired shape, a step of drying the molded article and a step of sintering the dried molded article.
    Type: Grant
    Filed: September 10, 1996
    Date of Patent: December 30, 1997
    Assignee: Aida Chemical Industries Co., Ltd.
    Inventors: Yukio Osawa, Katsuhiko Shimamoto, Shinichi Ishigaki, Hitoshi Araki, Yukio Nakata, Atsushi Fujimaru
  • Patent number: 5698800
    Abstract: The present invention provides a mixed raw material which is capable of producing a porous metal sintered product having high porosity and fine and uniform pores. The mixed raw material for producing a porous metal sintered product is a composition including 0.05 to 10% of water-insoluble hydrocarbon organic solvent having 5 to 8 carbon atoms, 0.05 to 5% of surfactant, 0.5 to 20% of water-soluble resin binder, 5 to 80% of metallic powder having an average particle size of 0.5 to 500 .mu.m, optionally 0.1 to 40% of combustible agent for accelerating pore formation, and optionally, 0.1 to 15% of plasticizer consisting of at least one of polyhydric alcohols, oils and fats, ethers and esters, with a balance of water.
    Type: Grant
    Filed: August 2, 1996
    Date of Patent: December 16, 1997
    Assignee: Mitsubishi Materials Corporation
    Inventors: Koji Hoshino, Toru Kohno
  • Patent number: 5695861
    Abstract: Solder active braze compositions are disclosed which enable the formation of circuit traces having improved leach resistance during soldering operations so that it is not necessary to apply protective coatings onto the circuit traces. Additionally, the solder active braze compositions disclosed herein can be readily soldered to so that it is not necessary to separately apply a coating onto the circuit trace so that electrical connections can be made to the traces by soldering. Also disclosed are electronic assemblies comprising circuit traces formed from the particular solder active braze compositions, and methods of forming such electronic assemblies.
    Type: Grant
    Filed: October 18, 1995
    Date of Patent: December 9, 1997
    Assignee: CTS Corporation
    Inventor: Terry R. Bloom
  • Patent number: 5690716
    Abstract: A thermal spray powder for producing high hardness, low friction, wear resistant coatings on friction surfaces, comprising a blend of an agglomerated molybdenum/dimolybdenum carbide powder and a self-fluxing NiCrFeBSi alloy powder.
    Type: Grant
    Filed: February 17, 1995
    Date of Patent: November 25, 1997
    Assignee: Osram Sylvania Inc.
    Inventor: Sanjay Sampath
  • Patent number: 5678165
    Abstract: A plastically deformable aqueous mixture capable of being shaped into a body, the mixture being composed of any one or combination of ceramic, glass-ceramic, glass, molecular sieve, carbon, or metal powders, cellulose ether organic binder, water insoluble hydrophobic polymer co-binder having an average molecular weight of at least about 8,000, plasticizer, and water. A method of making a body which involves mixing the above components in a high shear mixer at a temperature of about 30.degree. C. to 70.degree. C. to form a homogeneous mixture, extruding the mixture at a temperature of about 30.degree. C. to 70.degree. C. into a green body, followed by drying and firing to produce the product body.
    Type: Grant
    Filed: December 6, 1995
    Date of Patent: October 14, 1997
    Assignee: Corning Incorporated
    Inventor: Shy-Hsien Wu
  • Patent number: 5667554
    Abstract: Base metal resistors based on a new approach to alloy formation of nickel and chromium metals are presented that are rugged and offer excellent stability. Fine particle size nickel and chromium powders together with fluxing agents are blended together in a preselected ratio with a glass fret and screening agent. The composition is subsequently printed and fired in a nitrogen furnace at approximately 900.degree. C. to 930.degree. C. These resistors are compatible with other prior art base metal conductors, resistors and dielectrics.
    Type: Grant
    Filed: April 19, 1996
    Date of Patent: September 16, 1997
    Assignee: CTS Corporation
    Inventor: Charles C. Y. Kuo
  • Patent number: 5666634
    Abstract: The invention has for its object the provision alloy steel powders for Cr-based high strength sintered bodies having high tensile strength, fatigue strength and toughness which are adapted for use in parts for motor vehicles and parts for OA apparatus.The composition of the alloy steel powder comprises, by wt %, not larger than 0.1% of C, not larger than 0.08% of Mn, 0.5-3% of Cr, 0.1-2% of Mo, not larger than 0.01% of S, not larger than 0.01% of P, not larger than 0.2% of O, optionally one or more of 0.2.about.2.5% Ni, 0.5.about.2.5% Cu and the balance being inevitable impurities and Fe. The sintered body has substantially the same composition provided that the content of C alone is limited to 0.2-1.2%.The manufacturing method comprises molding the above alloy steel powder, sintering the resulting green compact at a temperature of 1100.degree.-1300.degree. C. and immediately cooling at a cooling rate of 10.degree.-200.degree. C./minute.
    Type: Grant
    Filed: December 23, 1994
    Date of Patent: September 9, 1997
    Assignee: Kawasaki Steel Corporation
    Inventors: Shigeru Unami, Osamu Furukimi
  • Patent number: 5663124
    Abstract: An iron or copper based metal powder useful for plasma deposition of a coating that has a dry coefficient of friction 0.75 or less and readily conducts heat through the coating. The powder comprises (a) H.sub.2 O atomized and annealed particles consisting essentially of (by weight) carbon 0.15-85%, oxygen 0.1-0.45%, an air hardening agent selected from manganese and nickel of 0.1-6.5%, and the remainder iron or copper, with at least 90% of the particles having oxygen and iron or copper combined in the lowest atomic oxygen form for an oxide of such metal.A method of making anti-friction iron powder that is economical, selectively produces FeO and promotes fine flowable particles. The method comprises (a) steam atomization of a molten steel that excludes other oxygen, the steel containing carbon up to 0.4% by weight to produce a collection of comminuted particles, and (b) annealing the particles in an air atmosphere for a period of time of 0.25-2.0 hours in a temperature range of 800.degree.-1400.degree. F.
    Type: Grant
    Filed: December 9, 1994
    Date of Patent: September 2, 1997
    Assignee: Ford Global Technologies, Inc.
    Inventors: V. Durga Nageswar Rao, Robert Alan Rose, David Alan Yeager, Carlo Alberto Fucinari
  • Patent number: 5656787
    Abstract: A process of forming a sintered article for powder metal comprising blending carbon and ferro alloys and lubricant with compressible elemental iron powder, pressing said blended mixture to form sintering said article, and then high temperature sintering said article in a reducing atmosphere to produce a sintered article having a high density from a single compression.
    Type: Grant
    Filed: November 21, 1995
    Date of Patent: August 12, 1997
    Assignee: Stackpole Limited
    Inventors: Rohith Shivanath, Peter Jones, Danny Thien Duc Thieu
  • Patent number: 5649994
    Abstract: A wear resistant coating includes a mixture or compound of Cobalt and Phosphorous either alone or mixed with one or more alloys to provide a coating for metallic surfaces rendering the metallic surfaces more resistant to wear. A preferred combination of Cobalt and Phosphorous utilized in the present invention consists of 89%, by weight, Cobalt and 11%, by weight, Phosphorous, which combination is at approximately the "eutectic" ratio, that is, that combination of Cobalt and Phosphorous exhibiting the lowest melting point. The 89Co-11P alloy is mixed with a second alloy including, by weight, about 61.1%Co, 8%Cr, 2.5%Si, 0.04%C, and 28%Mo. Preferred environments of application of the inventive coating include surgical blades, files and burrs, guide slots, drills and drill guides, surgical instruments and medical prostheses and for abrasive particles. The subject coatings have achieved a micro-hardness of 1500 DPH (Diamond Pyramid Hardness), approximately equal to the Rockwell C75 hardness.
    Type: Grant
    Filed: October 24, 1994
    Date of Patent: July 22, 1997
    Inventor: Kenneth Henry Holko
  • Patent number: 5649277
    Abstract: An apparatus and process for the free-forming manufacture of three-dimensal components. A powder-binder mixture, or a material with a high melting point, is plasticized or made molten, by raising the temperature inside a process chamber. The resulting molten material is discharged under pressure through a nozzle which is arranged at the end of the process chamber. The material inside the process chamber is deposited in layers. The processing direction and processing speed of the nozzle are programmed. An embodiment of the invention is disclosed in which a non-molten powder is deposited and supported by the deposition of a second powder alongside the non-molten powder.
    Type: Grant
    Filed: June 13, 1994
    Date of Patent: July 15, 1997
    Assignee: Fraunhofer-Gesellschaft Zur Foerderung Der Angewandten Forschung E.V.
    Inventors: Mathias Greul, Ewald Staskewitsch, Wilhelm Steger, Theo Pintat, Martin Geiger, Klaus Melchior
  • Patent number: 5643352
    Abstract: The present invention features a new iron material for use in situ with a hydrogen-air fuel cell, to generate the hydrogen to fuel the fuel cell. The iron material is made up of freshly-ground particles of iron, ranging in diameter size from approximately 25 to 1,200 .mu.m, with an average-sized distribution having at least twenty per cent (20%) of the particles less than about 300 .mu.m in diameter, and having an average particle density approximately ranging from about 1 to 7.8 g/cc, and a surface area greater than approximately 0.001 meters.sup.2 /g. The particles are in a freshly ground state, in situ, for enhancing their reactivity in producing hydrogen for the fuel cell.
    Type: Grant
    Filed: June 7, 1995
    Date of Patent: July 1, 1997
    Assignee: H Power Corporation
    Inventor: John Werth
  • Patent number: 5641580
    Abstract: A molybdenum-based composite powder for thermal spray applications. The composite powder includes a molybdenum-chromium, molybdenum-tungsten, or molybdenum-tungsten-chromium alloy dispersion strengthened with molybdenum carbide (Mo.sub.2 C). The molybdenum-based composite powder may be combined with a nickel-based or cobalt-based alloy to form a two-phase powder blend. The coatings from such powders are made up of molybdenum-based alloy lamellae and, in the two-phase embodiments, nickel-based or cobalt-based alloy lamellae. The coatings exhibit improved corrosion resistance and strength while retaining good sprayability.
    Type: Grant
    Filed: October 3, 1995
    Date of Patent: June 24, 1997
    Assignee: Osram Sylvania Inc.
    Inventors: Sanjay Sampath, Jack E. Vanderpool
  • Patent number: 5641920
    Abstract: Provided is a powder and binder system for manufacturing sintered parts from particulate material, and a method of injection molding parts for sintering. The particulate material includes ceramic, metallic and intermetallic powders. Preferably, selected powder particles are coated with one or more additives depending on their shape and surface chemistry to create a powder system. The additives may include antioxidants, coupling agents, surfactants, elasticizing agents, dispersants, plasticizer/compatibilizers and lubricants. The surface active additives are designed to improve the interface between the powder and the binder. The powder system may be mixed or compounded with a binder system in an inert atmosphere to form a powder and binder system, or feedstock, for powder molding. The binder system, may contain one or more components which are removed prior to the sintering the powder. The powder and binder system may also be molded about an expendable core which is extracted prior to sintering.
    Type: Grant
    Filed: September 7, 1995
    Date of Patent: June 24, 1997
    Assignee: Thermat Precision Technology, Inc.
    Inventors: Karl Frank Hens, Joseph A. Grohowski, Jr.
  • Patent number: 5640666
    Abstract: A method of producing a composite powder by providing particles of (I) tungsten, niobium, zirconium, titanium or mixtures thereof, (II) silicon and (III) carbon in a proportion relative to each other so as to possess an overall chemical composition in that segment of the ternary diagram of FIGS. 2(a), 2(b), 2(c) and 2(d) designated A, and subjecting the particles to a mechanical alloying process under conditions and for a time sufficient to produce the composite powder. Also disclosed is a method of forming a substantially oxygen-free composition of matter comprising a matrix substance of WSi.sub.2, NbSi.sub.2, ZrSi.sub.2, TiSi.sub.2 or alloys thereof having SiC dispersed therein, the method comprising consolidating the above-described composite powder. Also disclosed is a method of forming oxidation- and wear-resistant coatings by subjecting the composite powder whose composition lies in segment A to a metallurgical process such as plasma spraying.
    Type: Grant
    Filed: October 2, 1995
    Date of Patent: June 17, 1997
    Assignee: University of Florida
    Inventors: S. Jayashankar, Michael J. Kaufman
  • Patent number: 5637132
    Abstract: Lead-free metallurgy powder for use in manufacturing a shaped bronze part by powder metallurgy techniques which consists essentially of a substantially homogeneous blend of metal powders having about 90 parts copper, about 10 parts tin and an amount of bismuth in the range from an amount effective to improve the machinability of the shaped bronze part up to about 5% weight are disclosed. Lead-free metallurgy powder for use in manufacturing a shaped brass part by powder metallurgy techniques which consists essentially of a substantially homogeneous blend of metal powders about 70-90 parts copper, about 10-30 parts zinc and an amount of bismuth in the range from an amount effective to improve the machinability of the shaped brass part up to about 5% weight are also disclosed.
    Type: Grant
    Filed: May 15, 1995
    Date of Patent: June 10, 1997
    Assignee: United States Bronze Powders, Inc.
    Inventors: Paul Matthews, Thomas Pelletier, II
  • Patent number: 5635255
    Abstract: Erosion and wear resistant iron alloy, comprising: Cr 20.0-36.0% by weight, B 2.5-5.0% by weight, Mn 0.5-3.2% by weight, Si 0.05-0.6 by weight, Mo 0.3-2.5% by weight, V 0.05-0.3% by weight, Nb 0.03-0.3% by weight, P 0.5% by weight or less, C 0.05-0.3% by weight, and a trace of unavoidable impurities, which confers superior corrosion and wear resistance upon abraded or corroded portions by coating or molding.
    Type: Grant
    Filed: November 28, 1995
    Date of Patent: June 3, 1997
    Assignee: Samsung Heavy Industries Co., Ltd.
    Inventors: Kwang W. Kwon, Kang H. Kim
  • Patent number: 5628814
    Abstract: A nickel-base superalloy article has a coating having a composition, in weight percent, of from about 10 to about 20 percent cobalt, from about 14 to about 25 percent chromium, from about 2 to about 12 percent aluminum, from 0 to about 0.2 percent yttrium, from about 0.001 to about 3 percent boron, from about 1 to about 10 percent silicon, balance nickel and incidental impurities. The coating is preferably applied by mixing together two powders, one with a higher solidus temperature and one with a lower solidus temperature, whose net composition is that of the coating. The powder mixture is compacted with a binder, applied to a surface of the article, and heated to a temperature above the lower solidus temperature.
    Type: Grant
    Filed: November 22, 1995
    Date of Patent: May 13, 1997
    Assignee: General Electric Company
    Inventors: Jim D. Reeves, David E. Budinger, Robert A. Anderson
  • Patent number: 5607780
    Abstract: Disclosed are a target material for magneto-optical recording medium having a structure formed by sintering of an RE-TM phase (A) having a composition with an RE content higher than that of the composition of an intermetallic compound represented by the chemical formula TM.sub.2 RE, and a TM-RE phase (B) having a composition with an RE content equal to or lower than that of the composition of an intermetallic compound represented by the chemical formula TM.sub.2 E, wherein RE denotes at least one rare earth element selected from the group of elements consisting of Nd, Gd, Tb, Dy, Ho and Er, and TM denotes at least one element selected from the group of metals of the iron group which consists of Fe, Co and Ni; and a process for producing the same.
    Type: Grant
    Filed: May 20, 1994
    Date of Patent: March 4, 1997
    Assignee: Hitachi Metals, Ltd.
    Inventors: Kaoru Masuda, Takashi Meguro
  • Patent number: 5605561
    Abstract: Tantalum powder obtained by adding magnesium powder to tantalum powder which is prepared by reducing potassium tantalum fluoride with sodium metal, without conventional heat-treatment for agglomeration, to remove oxygen present in the tantalum powder, then washing with an acid and drying; an anode body for electrolytic capacitors produced by sintering the tantalum powder; and, an electrolytic capacitor which comprises the anode body incorporated therein. The tantalum powder has a large specific surface area and accordingly, the electrolytic capacitor in which the anode body produced from the tantalum powder is incorporated has an extra high capacity, i.e., a CV ranging from 70000 to 80000. The probability of causing ignition during the production process is substantially reduced and thus the tantalum powder can be handled with safety.
    Type: Grant
    Filed: September 6, 1995
    Date of Patent: February 25, 1997
    Assignee: Starck Vtech Ltd.
    Inventors: Katsuo Iwabuchi, Tadashi Komeya, Hiroshi Oki, Dieter Behrens
  • Patent number: 5605559
    Abstract: Alloy steel powders capable of obtaining high strength in a sintered state and having excellent compacting compressibility and methods of manufacturing a sintered body. The alloy steel powder comprises, by wt %, about 0.5-2% of Cr, not greater than about 0.08% of Mn, about 0.1-0.6% of Mo, about 0.05-0.5% of V, not greater than about 0.015 of S, not greater than about 0.2% of O, and the balance being Fe and incidental impurities. The alloy steel powder is compacted and sintered at a temperature of about 1100.degree.-1300.degree. C. and then cooled at a cooling rate no higher than about 1.degree. C./s in a temperature range of from about 800.degree. C. to 400.degree. C. The alloy steel powder can contain Nb and/or Ti and one or more of Co, W and B. Additionally, Ni powder and/or Cu powder may be adhered and dispersed onto the surface of the alloy steel powder.
    Type: Grant
    Filed: February 22, 1995
    Date of Patent: February 25, 1997
    Assignee: Kawasaki Steel Corporation
    Inventors: Shigeru Unami, Satoshi Uenosono
  • Patent number: 5597401
    Abstract: A clean refractory metal SWARF particle product is made from refractory metal SWARF. The SWARF particles are produced with coolant at a temperature less than 650.degree. C. to prevent formation of refractory metal oxides and nitrides. The SWARF particles are comminuted to reduce the particle size of the SWARF slivers and to liberate residual coolant The comminuted SWARF slivers are washed with a displacement wash to remove the bulk of the coolant and subject to a counter current wash to remove substantially all of the coolant components to produce to clean SWARF particles. The clean SWARF particles can be pressed into briquettes and sintered at elevated pressures or mixed with an alkali metal refractory metal halide salt, pressed at elevated pressures into SWARF/soft briquettes and dried. The briquettes are non-pyrophoric.
    Type: Grant
    Filed: November 15, 1994
    Date of Patent: January 28, 1997
    Inventor: Joseph A. Megy
  • Patent number: 5595608
    Abstract: A permanent magnet which contains R, T and B as main ingredients wherein R is Y or a rare earth element and T is Fe or Fe and Co and has a primary phase of R.sub.2 T.sub.14 B is produced by compacting a mixture of 60 to 95 wt % of a primary phase-forming master alloy and a grain boundary phase-forming master alloy both in powder form and sintering the compact. The primary phase-forming master alloy has columnar crystal grains of R.sub.2 T.sub.14 B with a mean grain size of 3-50 .mu.m and grain boundaries of an R rich phase and contains 26-32 wt % of R. The grain boundary phase-forming master alloy is a crystalline alloy consisting essentially of 32-60 wt % of R and the balance of Co or Co and Fe. In anther form, a permanent magnet which contains R, T and B as main ingredients wherein R is yttrium or a rare earth element, T is Fe or Fe+Co/Ni and has a primary phase of R.sub.2 T.sub.
    Type: Grant
    Filed: November 2, 1994
    Date of Patent: January 21, 1997
    Assignee: TDK Corporation
    Inventors: Katashi Takebuchi, Shinya Fujito, Shinya Hashimoto, Koichi Yajima
  • Patent number: 5580367
    Abstract: An improved flaked tantalum powder and process for making the flaked powder are disclosed. The powder is characterized by having a Scott density greater than about 13 g/in.sup.3 and preferably at least about 90% of the flake particles having no dimension greater than about 55 micrometers. Agglomerates of the flaked tantalum powder, provide improved flowability, green strength and pressing characteristics compared to conventional flaked tantalum powders. The improved flaked tantalum powder can be made by preparing a flaked tantalum and then reducing the flake size until a Scott density greater than about 18 g/in.sup.3 is achieved. The invention also provides pellets and capacitors prepared from the above-described flaked tantalum powder.
    Type: Grant
    Filed: April 17, 1995
    Date of Patent: December 3, 1996
    Assignee: Cabot Corporation
    Inventor: James A. Fife
  • Patent number: 5577546
    Abstract: Particles of metal alloys and composites have been developed that are particularly suitable for use in producing thixotropic alloys and in the injection molding of such alloys. The particulate material comprises particles of metal alloy or composite, wherein a substantial proportion of the particles is shaped such that the ratio of the length of the largest dimension of a particle to the effective diameter of the particle is in the range of 1.0 to 4.0 and the substantial proportion of particles has a particle size wherein the largest dimension of the particles lies within the range of 0.5 to 5.0 mm. This allows convenient handling of the particles whilst also avoiding binding or clogging of the screw, in the case where a screw extruder is used.
    Type: Grant
    Filed: April 24, 1995
    Date of Patent: November 26, 1996
    Assignee: Comalco Aluminium Limited
    Inventors: Anthony R. Kjar, Ronald G. Iacocca, Randall M. German, John L. Mihelich
  • Patent number: 5571305
    Abstract: Atomized steel powder having excellent machinability, containing about S 0.005 wt % to 0.3 wt %, Cr 0.03 wt % to 0.3 wt %, Mn 0.03 wt % to 0.5 wt %, O 0.30 wt % or less, and the balance Fe and incidental impurities, and sintered steel that can be manufactured therefrom. In particular, each of specific components is limited to a preferred range so that atomized steel powder exhibiting excellent machinability, dimensional accuracy and wear resistance and sintered steel that can be manufactured therefrom are provided.
    Type: Grant
    Filed: August 31, 1994
    Date of Patent: November 5, 1996
    Assignee: Kawasaki Steel Corporation
    Inventors: Satoshi Uenosono, Hiroyuki Ishikawa, Kuniaki Ogura
  • Patent number: 5560761
    Abstract: Tantalum powder used as an anode material for an electrolytic capacitor comprising usual tantalum powder (having an average particle size ranging from 1.0 to 5.0 .mu.m) mixed with tantalum powder having an average particle size on the order of nanometers (ranging from 10 to 500 nm) in an amount ranging from 1 to 25 parts by weight per 100 parts by weight of the former; an anode body for use in an electrolytic capacitor which is produced by sintering the tantalum powder; an electrolytic capacitor in which the anode body is incorporated.
    Type: Grant
    Filed: September 6, 1995
    Date of Patent: October 1, 1996
    Assignee: Starck Vtech Ltd.
    Inventor: Hiroo Naito
  • Patent number: 5556446
    Abstract: Brass powder metallurgy compositions for use in manufacturing a brass part by powder metallurgy techniques. The compositions comprise from about 70-90% wt. copper, 10-30% wt. zinc, and from about 0.1-1.5% wt. graphite as an addition to improve the machinability of the resultant compacted brass part. The compositions preferably contain less than 2% wt. lead.
    Type: Grant
    Filed: May 19, 1995
    Date of Patent: September 17, 1996
    Assignee: United States Bronze Powders
    Inventors: Paul E. Matthews, Thomas W. Pelletiers, II