Abstract: The invention is directed to a process for the continuous preparation of ammonium paratungstate hydrate by back reextraction of a tungsten-laden organic phase with an ammonia-containing aqueous solution in a mixer-settler apparatus. The reextraction is carried out at an NH3:W molar ratio of from 0.83 to 1.30, and a volume feed ratio of the tungsten-laden organic phase to the ammonia-containing aqueous solution of from 5 to 25. The above crystalline is in high purity and in high yield. The production method can be carried out in a simple and energy-efficient manner.
Type:
Grant
Filed:
January 29, 2008
Date of Patent:
July 10, 2012
Assignee:
H.C. Starck GmbH
Inventors:
Viktor Stoller, Michael Erb, Juliane Meese-Marktscheffel, Michael Lohse, Klaus-Jürgen Marschall, Frank Schrumpf
Abstract: In various embodiments, sputter-target formation includes application of a layer having an intermediate coefficient of thermal expansion between the backing plate and the target material.
Type:
Grant
Filed:
November 8, 2007
Date of Patent:
June 12, 2012
Assignees:
H.C. Starck GmbH, H.C. Starck Inc.
Inventors:
Steven A. Miller, Olaf Schmidt-Park, Prabhat Kumar, Richard Wu, Shuwei Sun, Stefan Zimmermann
Abstract: Disclosed is a niobium suboxide powder for the manufacture of capacitors with higher break down voltages, higher temperatures of operation and elongated lifetimes. The powder is doped with nitrogen which is at least partly present in the form homogeneously distributed, x-ray detectable Nb2N-crystal domains. The niobium suboxide powder contains niobium suboxide particles having a bulk nitrogen content of between 500 to 20,000 ppm.
Type:
Grant
Filed:
May 31, 2006
Date of Patent:
May 29, 2012
Assignee:
H. C. Starck GmbH
Inventors:
Christoph Schnitter, Holger Brumm, Christine Rawohl, Colin McCracken
Abstract: In accordance with various embodiments, plates are formed via a plurality of upset-forging and forging-back cycles followed by a plurality of rolling passes.
Abstract: The invention is directed to a method for the production of ammonium paratungstate tetrahydrate by thermal treatment of ammonium paratungstate decahydrate in an aqueous suspension. The ammonium paratungstate tetrahydrate can be produced with high purity and high yield. The production method may furthermore be carried out in a simple and energy-efficient manner.
Type:
Grant
Filed:
January 29, 2008
Date of Patent:
May 1, 2012
Assignee:
H.C. Starck GmbH
Inventors:
Viktor Stoller, Michael Erb, Juliane Meese-Marktscheffel, Michael Lohse, Wolfgang Mathy
Abstract: The present invention relates to coatings comprising electrically conductive polymers and flavones, their production and use, and dispersions for the production of such coatings.
Abstract: The invention relates to a process for the production of electrolyte capacitors having a low equivalent series resistance and low residual current, electrolyte capacitors produced by this process and the use of such electrolyte capacitors.
Type:
Application
Filed:
October 6, 2011
Publication date:
March 29, 2012
Applicant:
H.C. Starck GmbH
Inventors:
Udo Merker, Wilfried Lövenich, Klaus Wussow, Ralph Tillmann
Abstract: The invention relates to a process for producing electrolytic capacitors with low equivalent series resistance, low residual current and high thermal stability, which consist of a solid electrolyte and an outer layer comprising conjugated polymers, to electrolytic capacitors produced by this process and to the use of such electrolytic capacitors.
Type:
Application
Filed:
February 4, 2010
Publication date:
March 8, 2012
Applicant:
H.C. Starck Clevios GmbH
Inventors:
Matthias Intelmann, Klaus Wussow, Udo Merker
Abstract: Process for the production of a powdered spherical tungstic acid by acidification of an aqueous alkaline tungstate solution with mineral acid at elevated temperature, preferably in a continuous stirred tank or a cascade of at least 2 continuous stirred tanks, and tungstic acid obtainable in this way, which is characterised by a high bulk density and spherical morphology.
Type:
Application
Filed:
September 23, 2011
Publication date:
February 23, 2012
Applicant:
H.C. Starck GmbH
Inventors:
Sven Albrecht, Armin Olbrich, Michael Reib, Frank Schrumpf, Juliane Meese-Marktscheffel, Uwe Kutzler
Abstract: A crucible for producing a silicon suitable for producing a semiconductor includes a plurality of components and at least one unclosed joint gap.
Abstract: In various embodiments, a metallic structure includes first and second clad structures each comprising a protective layer disposed over a steel layer, a joint joining the steel layers of first and second clad structures, and, directly connecting the protective layers of the first and second clad structures, a layer of metal powder disposed in contact with (i) the joint, (ii) the protective layers of the first and second clad structures, and (iii) a portion of at least one of the steel layers proximate the joint.
Type:
Grant
Filed:
July 18, 2011
Date of Patent:
February 14, 2012
Assignee:
H.C. Starck, Inc.
Inventors:
Steven A. Miller, Leonid N. Shekhter, Stefan Zimmerman
Abstract: A process for producing a solid electrolyte capacitor with an anode comprising a sintered fine NbOx powder, where 0.5<x<1.7, includes providing a green anode body. The green anode body is sintered so as to provide a sintered anode body. The sintered anode body is formed so as to provide a formed anode body, wherein the forming is essentially performed without applying a pressure. The formed anode body is provided with a cathode so as to provide the solid electrolyte capacitor.
Abstract: A process for the production of a valve metal oxide powder, in particular an Nb2O5 or Ta2O5 powder by continuous reaction of a fluoride-containing valve metal compound with a base in the presence of water and calcination of the resultant product, wherein the reaction is performed in just one reaction vessel and at a temperature of at least 45° C. Valve metal oxide powders obtainable in said manner which exhibit a spherical morphology, a D50 value of 10 to 80 ?m and an elevated BET surface area.
Type:
Grant
Filed:
August 18, 2009
Date of Patent:
January 24, 2012
Assignee:
H.C. Starck GmbH
Inventors:
Karsten Beck, Hady Seyeda, Klaus Lerch, Bianca Agnes Balan
Abstract: The invention is directed at sputter targets including 50 atomic % or more molybdenum, a second metal element of niobium or vanadium, and a third metal element selected from the group consisting of titanium, chromium, niobium, vanadium, and tantalum, wherein the third metal element is different from the second metal element, and deposited films prepared by the sputter targets. In a preferred aspect of the invention, the sputter target includes a phase that is rich in molybdenum, a phase that is rich in the second metal element, and a phase that is rich in the third metal element.
Type:
Application
Filed:
June 30, 2010
Publication date:
January 5, 2012
Applicant:
H.C. STARCK, INC.
Inventors:
Gary Alan Rozak, Mark E. Gaydos, Patrick Alan Hogan, Shuwei Sun
Abstract: Molybdenum, sputtering targets and sintering characterized as having no or minimal texture banding or through thickness gradient. The molybdenum sputtering targets having a fine, uniform grain size as well as uniform texture, are high purity and can be micro-alloyed to improved performance. The sputtering targets can be round discs, square, rectangular or tubular and can be sputtered to form thin films on substrates. By using a segment-forming method, the size of the sputtering target can be up to 6 m×5.5 m. The thin films can be used in electronic components such as Thin Film Transistor-Liquid Crystal Displays, Plasma Display Panels, Organic Light Emitting Diodes, Inorganic Light Emitting Diode Displays, Field Emitting Displays, solar cells, sensors, semiconductor devices, and gate device for CMOS (complementary metal oxide semiconductor) with tunable work functions.
Type:
Grant
Filed:
August 29, 2005
Date of Patent:
January 3, 2012
Assignee:
H.C. Starck Inc.
Inventors:
Brad Lemon, Joseph Hirt, Timothy Welling, James G. Daily, III, David Meendering, Gary Rozak, Jerome O'Grady, Peter R. Jepson, Prabhat Kumar, Steven A. Miller, Richard Wu, Davd G. Schwarz
Abstract: The invention relates to a device and a method for the production of compounds by precipitation of solids from solutions, the physical and chemical properties of the solid particles formed on precipitation being flexible and can be independently fixable. Custom products can thus be produced with very high space-time yields and a particulate nickel/cobalt mixed hydroxide of formula NixCo1-x(OH)2, with a BET surface area of 20 m2/g and a tap density of greater than 2.4 g/cm3.
Type:
Application
Filed:
March 20, 2007
Publication date:
December 8, 2011
Applicant:
H.C. STARCK GMBH
Inventors:
Armin Olbrich, Juliane Meese-Marktscheffel, Matthias Jahn, Rüdiger Zertani, Gerd Maikowske, Sven Albrecht, Stefan Malcus, Josef Schmoll, Gabriele Christine Schmoll, Christian Peter Schmoll, Wolfgang Josef Schmoll, Volker Schmoll, Georg Wilhelm Schmoll, Michael Kruft
Abstract: Computer-implemented processes for making refractory metal pots, including: cutting an a refractory metal ingot into a first workpiece; subjecting the first workpiece to multiple upset forgings, annealings in a vacuum or inert gas to a temperature sufficiently high to cause at least partial recrystallization, forging-backs, and rollings to form a plate; wherein the forged, annealed workpiece undergoes a reduction in thickness after at least one rolling pass and is turned between at least one pass, to form the plate; and deep drawing the plate to form a pot; wherein dimensions of at least one workpiece or plate suitable for processing into a pot are pre-determined with a computer-implemented finite element modeling assessment method.
Abstract: The invention relates to a process for the production of electrolyte capacitors having a low equivalent series resistance and low residual current, electrolyte capacitors produced by this process and the use of such electrolyte capacitors.
Type:
Grant
Filed:
September 13, 2006
Date of Patent:
November 15, 2011
Assignee:
H. C. Starck GmbH
Inventors:
Udo Merker, Wilfried Lövenich, Klaus Wussow, Ralph Tillmann