Abstract: The invention provides for a cermet powder containing 75-90% by weight of at least one hard material powder, from 10 to 25% by weight of one or more matrix metal powders and up to 3% by weight of at least one modifier, wherein the matrix metal powder or powders contain from 0 to 38% by weight of cobalt, from 0 to 38% by weight of nickel, from 0 to 20% by weight of aluminum, from 0 to 90% by weight of iron and from 10 to 35% by weight of chromium and the sum of the contents of iron and chromium is in the range from 10 to 95% by weight and the sum of the contents of cobalt, nickel and iron is in the range from 65 to 95% by weight. The invention also relates to a cermet and a process to make the cermet containing the cermet powder and shaped article coated with the cermet powder and a process to make the shaped article.
Type:
Grant
Filed:
September 21, 2007
Date of Patent:
January 2, 2018
Assignee:
H. C. Starck GmbH
Inventors:
Jürgen Fischer, Aloys Eiling, Frank Schrumpf, Stefan Zimmermann, Peter Thienel, Roland Scholl
Abstract: The invention is directed at sputter targets including 50 atomic % or more molybdenum, a second metal element of titanium, and a third metal element of chromium or tantalum, and deposited films prepared by the sputter targets. In a preferred aspect of the invention, the sputter target includes a phase that is rich in molybdenum, a phase that is rich in titanium, and a phase that is rich in the third metal element.
Type:
Grant
Filed:
July 30, 2015
Date of Patent:
December 5, 2017
Assignee:
H.C. STARCK INC.
Inventors:
Gary Alan Rozak, Mark E. Gaydos, Patrick Alan Hogan, Shuwei Sun
Abstract: In various embodiments, a metal alloy resistant to aqueous corrosion consists essentially of or consists of niobium with additions of tungsten, molybdenum, and one or both of ruthenium and palladium.
Abstract: A method for producing a composite material includes providing a composition comprising at least one hardness carrier and a base binder alloy, and sintering the composition. The base binder alloy comprises from 66 to 93 wt.-% of nickel, from 7 to 34 wt.-% of iron, and from 0 to 9 wt.-% of cobalt, wherein the wt.-% proportions of the base binder alloy add up to 100 wt.-%.
Abstract: In various embodiments, a sputtering target initially formed by ingot metallurgy or powder metallurgy and rejuvenated by, e.g., cold spray, is utilized in sputtering processes to produce metallic thin films.
Type:
Grant
Filed:
September 10, 2014
Date of Patent:
October 10, 2017
Assignees:
H.C. Starck Inc., H.C. Starck GmbH
Inventors:
Steven A. Miller, Prabhat Kumar, Richard Wu, Shuwei Sun, Stefan Zimmermann, Olaf Schmidt-Park
Abstract: A refractory metal plate is provided. The plate has a center, a thickness, an edge, a top surface and a bottom surface, and has a crystallographic texture (as characterized by through thickness gradient, banding severity; and variation across the plate, for each of the texture components 100//ND and 111//ND, which is substantially uniform throughout the plate.
Abstract: A tantalum or tantalum alloy which contains pure or substantially pure tantalum and at least one metal element selected from the group consisting of Ru, Rh, Pd, Os, Jr, Pt, Mo, W and Re to form a tantalum alloy that is resistant to aqueous corrosion. The invention also relates to the process of preparing the tantalum alloy.
Abstract: A niobium or niobium alloy which contains pure or substantially pure niobium and at least one metal element selected from the group consisting of Ru, Rh, Pd, Os, Ir, Pt, Mo, W and Re to form a niobium alloy that is resistant to aqueous corrosion. The invention also relates to the process of preparing the niobium alloy.
Abstract: A cermet powder includes a) from 50 to 90 wt-% of at least one hard material, and b) from 10 to 50 wt-% of a matrix metal composition. The wt.-% for a) and b) are based on a total weight of the cermet powder. The matrix metal composition comprises i) from 40 to 75 wt-% of iron and nickel, ii) from 18 to 35 wt-% of chromium, iii) from 3 to 20 wt.-% of molybdenum, and iv) from 0.5 to 4 wt-% of copper. The wt-% for i) to iv) are based in each case on a total weight of the matrix metal composition. A weight ratio of iron to nickel is from 3:1 to 1:3.
Abstract: A valve metal powder having a particle shape factor mean value f, as determined by SEM image analysis, of 0.65?f?1, said powder has an average agglomerate particle size D50 value, as determined with a MasterSizer in accordance with ASTM B 822, of 40 to 200 ?m and wherein the valve metal powder is niobium.
Abstract: In various embodiments, an electrode has a shaft extending from an electrode head and a cooling passage extending from an open end disposed at an attachment end of the shaft to a closed end disposed within the electrode head. The electrode head has an approximately teardrop shape with a smoothly rounded outer contour.
Abstract: A refractory metal compound agglomerate powder having a product of a BET surface area in m2/g and a sliding coefficient of ? of 0.33 to 0.95, wherein the refractory metal compound agglomerate powder is selected from niobium agglomerate powder, niobium suboxide agglomerate powder, and tantalum agglomerate powder.
Abstract: In various embodiments, a precursor powder is pressed into an intermediate volume and chemically reduced, via sintering, to form a metallic shaped article.
Abstract: In various embodiments, etchants featuring (i) mixtures of hydrochloric acid, methanesulfonic acid, and nitric acid, or (ii) mixtures of phosphoric acid, methanesulfonic acid, and nitric acid, are utilized to etch metallic bilayers while minimizing resulting etch discontinuities between the layers of the bilayer.
Type:
Grant
Filed:
March 3, 2015
Date of Patent:
September 27, 2016
Assignees:
H.C. Starck, Inc., Daetec, LLC
Inventors:
Patrick Hogan, John Moore, Alex Brewer, Jared Pettit
Abstract: A sintered spray powder includes from 5 to 50 wt.-% of a metallic matrix, from 50 to 95 wt.-% of a hard material, and from 0 to 10 wt.-% of a wear-modifying oxide, each based on the total weight of the sintered spray powder. The metallic matrix comprises from 0 to 20 wt.-% of molybdenum based on the total weight of the metallic matrix. The hard material comprises at least 70 wt.-% of molybdenum carbide based on the total weight of the hard material. An average particle diameter of the molybdenum carbide in the sintered spray powder is <10 ?m, determined in accordance with ASTM E112.
Abstract: In various embodiments, joined sputtering targets are formed at least in part by spray deposition of the sputtering material and/or welding.
Type:
Grant
Filed:
September 27, 2012
Date of Patent:
August 9, 2016
Assignee:
H.C. Starck, Inc.
Inventors:
Francois-Charles Dary, Mark Gaydos, William Loewenthal, Steven A. Miller, Gary Rozak, Scott Jeffrey Volchko, Stefan Zimmermann, Michael Thomas Stawovy
Abstract: A process for producing an anode for an electrolytic capacitor includes pressing a tantalum powder around a tantalum wire, a tantalum ribbon, or a tantalum sheet to form a pressed body. The pressed body is sintered to form a porous sintered body. The porous sintered body is cooled to form a cooled porous sintered body. The cooled porous sintered body is treated with at least one oxidant comprising at least one of a gaseous oxidant and a liquid oxidant to form a treated sintered body. The treated sintered body is anodically oxidized in an electrolyte to form a dielectric layer.
Type:
Grant
Filed:
August 8, 2012
Date of Patent:
June 28, 2016
Assignee:
H.C. STARCK GMBH
Inventors:
Helmut Haas, Marcel Hagymasi, Holger Brumm, Christoph Schnitter
Abstract: The invention is directed to a process for preparing a pulverulent compound of the formula NiaM1bM2cOx(OH)y where M1 is Fe, Co, Zn, Cu or mixtures thereof, M2 is Mn, Al, Cr, B, Mg, Ca, Sr, Ba, Si or mixtures thereof, having the following steps: a) providing at least a first starting solution and a second starting solution, b) combining of at least the first starting solution and the second starting solution in a reactor and producing a homogeneously mixed reaction zone having a specific mechanical power input of at least 2 watt/liter and producing a product suspension containing insoluble product and a mother liquor which is supersaturated by setting of an excess of alkali and has a pH of 10-12, c) partial separating the mother liquor from the precipitated product to set solids contents of at least 150 g/l in the suspension.
Abstract: A sputtering target that includes at least two consolidated blocks, each block including an alloy including molybdenum in an amount greater than about 30 percent by weight and at least one additional alloying ingredient; and a joint between the at least two consolidated blocks, the joint being free of any microstructure due to an added bonding agent (e.g., powder, foil or otherwise), and being essentially free of any visible joint line the target that is greater than about 200 ?m width (e.g., less than about 50 ?m width). A process for making the target includes hot isostatically pressing, below a temperature of 1080° C., consolidated perform blocks that may be surface prepared (e.g., roughened to a predetermined roughness value) prior to pressing.