Patents Assigned to JEOL Ltd.
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Patent number: 10276342Abstract: An electron microscope includes a monochromator, an image acquiring portion for obtaining an electron microscope image containing interference fringes of the electron beam formed by an aperture located behind the monochromator, a line profile acquiring portion for obtaining a plurality of line profiles passing through the center of the aperture on the EM image, an energy dispersion direction identifying portion for identifying the direction of energy dispersion of the monochromator on the basis of the line profiles obtained by the line profile acquiring portion, and an optics controller for controlling an optical system on the basis of a line profile in the direction of energy dispersion to bring the focal plane for the electron beam exiting from the monochromator into coincidence with the achromatic plane.Type: GrantFiled: April 13, 2018Date of Patent: April 30, 2019Assignee: JEOL Ltd.Inventor: Masaki Mukai
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Patent number: 10269531Abstract: A scanning electron microscope having a charged particle device that processes a specimen using a charged particle beam, the scanning electron microscope includes: an electron source; a secondary-electron detector that detects secondary electrons generated from the specimen; a backscattered-electron detector that is disposed closer to the electron source than a detection surface of the secondary-electron detector to detect backscattered electrons generated from the specimen; a shielding plate for shielding a detection surface of the backscattered-electron detector; and a moving mechanism that moves the shielding plate. In a state where the shielding plate is moved by the moving mechanism so as to shield the detection surface of the backscattered-electron detector, the shielding plate is located between the detection surface of the backscattered-electron detector and the detection surface of the secondary-electron detector.Type: GrantFiled: March 7, 2018Date of Patent: April 23, 2019Assignee: JEOL Ltd.Inventors: Tatsuru Kuramoto, Yuichiro Ohori, Yoshinori Matsuda, Makoto Aoshima
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Patent number: 10269535Abstract: An information processing device includes a placement section that places a result display area within a display screen based on operation information, a setting section that sets at least one data processing method designated by the user to the result display area, and a data processing section that assigns measurement data to the result display area based on the operation information, performs data processing on the measurement data assigned to the result display area using the data processing method set to the result display area, and displays the data processing results within the result display area.Type: GrantFiled: September 16, 2015Date of Patent: April 23, 2019Assignee: JEOL Ltd.Inventor: Daisuke Shimamura
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Patent number: 10254302Abstract: An method is offered which can clean the nozzles of a reaction cuvette wash unit. A first detergent is put in first reagent containers located on a first reagent turntable. A computer controller drives a first reagent pipette to aspirate the detergent from the first reagent containers and to deliver the detergent into reaction cuvettes. The controller drives a reaction turntable to bring each reaction cuvette holding the detergent therein to the reaction cuvette wash unit. The controller drives the reaction cuvette wash unit to aspirate the detergent from inside the reaction cuvettes using reaction cuvette wash nozzles to thereby clean the wash nozzles. A second detergent is then used to clean the nozzles.Type: GrantFiled: October 19, 2016Date of Patent: April 9, 2019Assignee: JEOL Ltd.Inventor: Yoshiyuki Nakayama
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Patent number: 10254357Abstract: A sample rotor is placed in a sample chamber inside an inner container. An air bearing type rotation mechanism blows a refrigerant gas (composed of a bearing gas and a driving gas) onto the sample rotor, to rotate the sample rotor and simultaneously cool the same. The refrigerant gas discharged from the air bearing type rotation mechanism is filled in an internal space (such as the sample chamber and a detection circuit chamber) of the inner container. An upper airtight chamber is formed between an outer container and the inner container. A lower airtight chamber is formed below a sealing bulkhead within a bottom unit. The upper and lower airtight chambers are in vacuum states to thereby function as vacuum insulation spaces for the internal space of the inner container.Type: GrantFiled: January 28, 2016Date of Patent: April 9, 2019Assignees: Osaka University, JEOL Ltd.Inventors: Toshimichi Fujiwara, Yoh Matsuki, Shinji Nakamura
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Patent number: 10241064Abstract: A probe head in a nuclear magnetic resonance measurement apparatus includes a rotating mechanism. In the probe head, an exhaust gas having a high temperature or a low temperature is discharged from a discharge port of the rotating mechanism. An additive gas having room temperature is introduced into the probe head through a plurality of ejection holes. The additive gas is mixed with the exhaust gas, and, as a result, an exhaust gas mixture having a temperature closer to room temperature than is the temperature of the sample is produced. A deflector regulates the direction in which the exhaust gas flows.Type: GrantFiled: December 20, 2016Date of Patent: March 26, 2019Assignee: JEOL Ltd.Inventors: Yuki Endo, Masahide Nishiyama
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Patent number: 10241063Abstract: In an embodiment of the invention inductive coupling of an idler coil to a parent coil is used to provide a double resonance circuit without the disadvantages of capacitive coupling to the parent coil. In an embodiment of the invention, an inductive coupling coil can be used to achieve a double-tuned circuit. In an embodiment of the invention, a circuit uses inductive coupling to achieve a double resonance circuit for 1H, 19F, and 13C experiments where one of the three nuclei are observed and the other two are decoupled. In an embodiment of the invention a pivot or a shunt can be used to couple and decouple the idler coil and the parent coil.Type: GrantFiled: April 8, 2016Date of Patent: March 26, 2019Assignee: JEOL LTD.Inventor: Albert Zens
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Patent number: 10241165Abstract: In various embodiments of the invention, inductive coupling can be to a secondary coil rather than a primary coil in order to optimize the topology of the NMR probe. In addition, by coupling to a secondary coil using a detection coil located below the lower insulator the RF homogeneity and signal to noise can be improved together with the NMR probe topology. By effecting inductive coupling to an inductor in a multiple resonance circuit, rather than to the sample inductor parameters associated with the NMR, probe construction can be arranged to increase RF homogeneity and signal to noise, while reducing space utilization constraints. In various embodiments of the invention, the primary mode in a secondary coil can be split into two modes with a resonator with inductive coupling to the secondary coil.Type: GrantFiled: March 14, 2017Date of Patent: March 26, 2019Assignee: JEOL LTDInventor: Albert Zens
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Patent number: 10224173Abstract: There is provided an objective lens capable of reducing the effects of magnetic fields on a sample. The objective lens includes a first lens and a second lens. The lenses are arranged so that the component of the magnetic field of the first lens lying along the optical axis and the component of the magnetic field of the second lens lying along the optical axis cancel out each other at a sample placement surface. The first and second lenses each include an inner polepiece and an outer polepiece. The inner polepieces have front end portions, respectively. The outer polepieces have front end portions, respectively, which jut out toward the optical axis. The distances of the front end portions of the outer polepieces, respectively, from the sample placement surface are less than the distances of the front end portions of the inner polepieces, respectively, from the sample placement surface.Type: GrantFiled: September 20, 2017Date of Patent: March 5, 2019Assignee: JEOL Ltd.Inventors: Tatsuo Naruse, Yuji Kohno
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Patent number: 10224176Abstract: There is provided an electron microscope capable of producing good images by reducing contrast nonuniformity.Type: GrantFiled: July 28, 2017Date of Patent: March 5, 2019Assignee: JEOL Ltd.Inventor: Takashi Suzuki
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Publication number: 20190004128Abstract: In various embodiments of the invention, inductive coupling can be to a secondary coil rather than a primary coil in order to optimize the topology of the NMR probe. In addition, by coupling to a secondary coil using a detection coil located below the lower insulator the RF homogeneity and signal to noise can be improved together with the NMR probe topology. By effecting inductive coupling to an inductor in a multiple resonance circuit, rather than to the sample inductor parameters associated with the NMR, probe construction can be arranged to increase RF homogeneity and signal to noise, while reducing space utilization constraints. In various embodiments of the invention, the primary mode in a secondary coil can be split into two modes with a resonator with inductive coupling to the secondary coil.Type: ApplicationFiled: August 3, 2018Publication date: January 3, 2019Applicant: JEOL LTD.Inventor: ALBERT ZENS
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Patent number: 10147590Abstract: A mass spectrometry data processing apparatus includes a data analysis unit that processes a mass spectrum of each of analysis-target areas within a two-dimensional range set on a sample. The data analysis unit obtains a plurality of mass spectra each associated with position information of a corresponding one of the analysis-target areas; creates an average mass spectrum that is an average of the plurality of obtained mass spectra; extracts, for each mass range, a highest peak by comparing the plurality of obtained mass spectra with one another, and creates a maximum mass spectrum constituted by the extracted highest peaks; creates an intensity ratio spectrum indicating an intensity ratio of the average mass spectrum to the maximum mass spectrum; and selects a peak in a range of a threshold set for the intensity ratio spectrum and specifies a mass range including the peak.Type: GrantFiled: January 13, 2016Date of Patent: December 4, 2018Assignee: JEOL Ltd.Inventors: Takuhiro Hizume, Takaya Satou
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Patent number: 10132761Abstract: A method capable of constructing an accurate three-dimensional image is offered. The method comprises the step (S10) of obtaining a first series of tilted images which are constituted by electron microscope images or elemental mapping images of a sample (S) at different tilt angles and which have been obtained by tilting the sample in angular increments, the step (S14) of obtaining a second series of tilted images which are constituted by electron microscope images or elemental mapping images of the sample at different tilt angles and which have been obtained by rotating the sample about an axis (P) perpendicular to a surface (Sf) of the sample and then tilting the sample in angular increments, and the step (S16) of constructing the three-dimensional image on the basis of the first and second series of tilted images.Type: GrantFiled: August 26, 2015Date of Patent: November 20, 2018Assignee: JEOL Ltd.Inventor: Yoshitaka Aoyama
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Patent number: 10134561Abstract: There is provided an electron microscope in which a crossover position can be kept constant. The electron microscope (100) includes: an electron source (110) for emitting an electron beam; an acceleration tube (170) having acceleration electrodes (170a-170f) and operative to accelerate the electron beam; a first electrode (160) operative such that a lens action is produced between this first electrode (160) and the initial stage of acceleration electrode (170a); an accelerating voltage supply (112) for supplying an accelerating voltage to the acceleration tube (170); a first electrode voltage supply (162) for supplying a voltage to the first electrode (160); and a controller (109b) for controlling the first electrode voltage supply (162). The lens action produced between the first electrode (160) and the initial stage of acceleration electrode (170a) forms a crossover (CO2) of the electron beam.Type: GrantFiled: May 10, 2017Date of Patent: November 20, 2018Assignee: JEOL Ltd.Inventor: Masaki Mukai
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Patent number: 10132896Abstract: In a magnetic resonance measurement apparatus, a plurality of transmission signals are combined to generate a digital combined signal. The digital combined signal is converted into an analog combined signal by a D/A converter. The signal includes, for example, a first pulse of a rectangular shape and a second pulse of a mountain shape. During measurement, an operation of a dynamic variable attenuator is changed immediately after the first pulse. With this process, the second pulse is suppressed, and a suppressed second pulse is generated.Type: GrantFiled: July 22, 2015Date of Patent: November 20, 2018Assignee: JEOL Ltd.Inventors: Kenichi Hachitani, Kenya Izumi, Takeshi Tsukada
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Patent number: 10121630Abstract: A control device that controls a spectrometer includes: a specimen image display control section that performs a control process that displays a specimen image acquired by the spectrometer on a display section; and an spectrometer control section that performs a control process that causes the spectrometer to start analysis based on designation of an analysis position within the specimen image that has been performed by a pointing device, and performs a control process that causes the spectrometer to stop the analysis based on cancellation of the designation of the analysis position that has been performed by the pointing device.Type: GrantFiled: April 25, 2016Date of Patent: November 6, 2018Assignee: JEOL Ltd.Inventors: Kazuhiro Tachibana, Hisashi Zaimoku, Akira Abe
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Patent number: 10114089Abstract: A sample tube is arranged in a sample temperature adjusting pipe, and a temperature adjustment gas is supplied. A vacuum vessel is formed with the sample temperature adjusting pipe and an outer wall body, and a detection coil and the like to be placed in a cooling state are arranged in the vacuum vessel. A sealed section between the sample temperature adjusting pipe and the outer wall body is sealed by a sealing structure. The sealing structure includes a high-vacuum O-ring and a low-temperature O-ring. The high-vacuum O-ring has characteristics for sealing the sealed section in a regular temperature region. The regular temperature region is a temperature region excluding a low temperature region, and the low temperature region is a temperature region including a lower limit in a possible temperature adjustment range of the temperature adjustment gas. The low-temperature O-ring has characteristics for sealing the sealed section in the low temperature region.Type: GrantFiled: January 11, 2017Date of Patent: October 30, 2018Assignee: JEOL Ltd.Inventors: Katsuyuki Toshima, Shinji Nakamura, Shigenori Tsuji
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Patent number: 10088538Abstract: An inner container including a tube body is provided in an outer container. With this structure, the inside of the outer container is separated into a primary airtight chamber and a sub airtight chamber (upper airtight chamber and lower airtight chamber). A detection circuit is placed in the primary airtight chamber. The detection circuit is a tuning and matching circuit having a transmission and reception coil serving as an NMR detection element and a variable capacitor. An additional member including an additional element such as a capacitor is inserted into the upper airtight chamber, and the additional member is set on a top terminal mounting member and a bottom terminal mounting member. With this structure, the additional element is electrically connected to the detection circuit and a characteristic of the detection circuit is changed.Type: GrantFiled: February 3, 2016Date of Patent: October 2, 2018Assignee: JEOL Ltd.Inventors: Takashi Mizuno, Kiyonori Takegoshi, Koji Fujioka
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Publication number: 20180267118Abstract: In various embodiments of the invention, inductive coupling can be to a secondary coil rather than a primary coil in order to optimize the topology of the NMR probe. In addition, by coupling to a secondary coil using a detection coil located below the lower insulator the RF homogeneity and signal to noise can be improved together with the NMR probe topology. By effecting inductive coupling to an inductor in a multiple resonance circuit, rather than to the sample inductor parameters associated with the NMR, probe construction can be arranged to increase RF homogeneity and signal to noise, while reducing space utilization constraints. In various embodiments of the invention, the primary mode in a secondary coil can be split into two modes with a resonator with inductive coupling to the secondary coil.Type: ApplicationFiled: March 14, 2017Publication date: September 20, 2018Applicant: JEOL LTD.Inventor: ALBERT ZENS
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Patent number: 10073153Abstract: A device for attaching and detaching a cryogenic probe to and from a nuclear magnetic resonance (NMR) spectrometer. The device permits the probe to be loaded in the spectrometer in a shortened time and achieves high measurement throughput. The device has loading platforms (11-1, 11-2) on which cryogenic probes (P1, P2) are loaded. Each loading platform has a horizontal drive mechanism, a vertical drive mechanism, and a spacing mechanism. The device further includes probe cooling devices (14-1, 14-2) for circulating a refrigerant to and from the cryogenic probes (P1, P2) via transfer tubes (12-1, 12-2) made of a flexible material, thus cooling the probes (P1, P2). A temperature-controlled gas feeder (18) supplies a temperature variable gas for temperature adjustment to the probes (P1, P2). A vacuum pumping system (15) evacuates the interiors of the probes (P1, P2) via vacuum pipes (17-1, 17-2) made of a flexible material.Type: GrantFiled: November 18, 2014Date of Patent: September 11, 2018Assignee: JEOL Ltd.Inventors: Masanori Hirose, Yoshiaki Yamakoshi, Masahide Nishiyama, Shinji Nakamura, Katsuyuki Toshima, Fumio Hobo, Terumasa Okada, Shigenori Tsuji, Ryoji Tanaka, Hiroto Suematsu