Abstract: The present invention relates to a polymer composition comprising polylactide and, based on the weight of this polymer, from 17 to 25 wt % of a chain modifier, from 30 to 55 wt % of an elastomeric polymer and from 20 to 45 wt % of a plasticizer. The invention also relates to the method of preparing said composition as well as to the method of manufacturing an article starting from said composition and the article per se.

Abstract: The invention relates to a cap for the neck of a container and to a method for producing one such cap. According to the invention, the skirt (12) of the cap (1) is provided with frangible bridge elements (44A, 44B) which break when the cap is first opened. In addition, on either side of the aforementioned frangible bridge elements, the skirt includes a non-removable part and a removable part provided with an outer biasing tab (24) that only extends along a peripheral portion (12A) of the skirt. In order to limit the biasing force of the tab, so as to release the removable skirt part, the radial dimension (e44A) of the bridges (44A) located in the skirt portion (12) associated with the tab is smaller than the radial dimension (e44B) of the bridges (44B) located outside said portion.

Abstract: Porous polymers having a plurality of openings or chambers that are highly convoluted, with each chamber being defined by multiple, thin, flat partitions are produced by a new gel enhanced phase separation technique. In a preferred embodiment, a second liquid is added to a polymer solution, the second liquid causing the solution to increase in viscosity. With sufficient polymer and second liquid present, the increase in viscosity can be up to that of a gel. The gel can then be shaped as needed. Subsequent solvent extraction leaves the porous polymeric body of defined shape. The porous polymers have utility as medical prostheses, the porosity permitting ingrowth of neighboring tissue. A second material may be incorporated into the chambers, thereby creating a microstructure filling the voids of the macrostructure.

Abstract: A microfluidic device includes at least two layers arranged one above the other, a membrane which is arranged between the at least two layers, a cavity in one of the at least two layers, and a channel in the other of the at least two layers. The membrane is arranged so as to be expandable between the cavity and the channel. The membrane is expandable into at least one specified displacement volume.

Abstract: A hinged closure lid made of plastic for placing onto a container, has a main part which has a dispenser opening, a lid which is mounted pivotably on the main part and, in a closure position resting on the main part, closes the dispenser opening, and an actuating part which is mounted on the main part so as to be adjustable between an inoperative position and an actuating position. The lid can be adjusted from the closure position in the direction of an open position when the actuating part is actuated. The actuating part here is connected to the lid via at least one flexible web serving as a predetermined breaking point. The web is destroyed when the actuating part is first adjusted into the actuating position.

Abstract: A process for producing a thermoplastic resin composition includes kneading a mixture obtained by combining a rubber component with a ground product, the ground product being formed by grinding a thermoplastic resin molded article having an alloy resin of a polycarbonate and an ABS, and then molding the mixture after kneading. The mixture has 0.5 wt % or more and 1.5 wt % or less of the rubber component based on 100 wt % of the mixture.

Abstract: The disclosure relates to compositions exhibiting a UV resistance of ?E ranging from more than 0 to less than or equal to 10 units after exposure to ultraviolet light for 300 hours, per ASTM D-4459 protocol. The compositions can include at least 15 wt % of a polyetherimide; at least 35 wt % of a polycarbonate; a polyetherimide siloxane; and optionally, at least one UV stabilizer. The disclosure also relates to methods of shaping such compositions and articles produced from such compositions.

Abstract: The invention relates to a photovoltaic system with a plastic support and a photovoltaic module for installation on roofs. The plastic support (1) may be mounted directly to a roof substructure, so that an additional roof covering can be dispensed with. The photovoltaic modules may be fixed on the plastic support (1) without screwing.

Abstract: A method of making a polymer composition comprising dispersed nanoparticles of an oxygen scavenging catalyst includes polymerizing one or more monomers or pre-polymers in the presence of a platinum group metal catalyst or precursor to obtain a polymer composition having dispersed nanoparticles of the platinum group metal. The oxygen scavenging catalyst is added during the polymerization as a solution of the platinum group metal or a compound thereof and a polyhydric alcohol (e.g., glycols). The food or beverage containers made from such polymer compositions exhibit high clarity and high oxygen scavenging properties.

Abstract: A hip spacer mold forming a spacer with a spacer stem connected to a spacer head has a stem portion for forming a spacer stem. The hip spacer mold also has a plurality of interchangeable head modules configured for alternatively forming spacer heads of a plurality of different predetermined sizes. The head modules are configured to be disposed adjacent the stem portion.

Abstract: Valves (110) and other apparatus, methods of moulding and moulds (112) are provided for the moulding of materials such as injection or injection-compression moulding of molten thermoplastic materials. The valve includes a valve element/piston (126) that is orientated at 60 degrees relative to the mould's bounding wall (116) and that can reciprocate in a barrel (122) and that can rotate. The piston (126) h a leading face (128) that is also orientated at 60 degrees, so that the flow passage/melt channel (118) extends past the leading face (128) when the valve (110) is open and the leading face (128) forms part of the bounding wall of the mould cavity (114) when the valve is closed. The piston (126) is advanced or retracted a very short distance and is rotated through 180 degrees, to open and close the valve (110).

Abstract: A cartridge for implantation of a deformable intraocular lens (IOL) through a small incision in the eye, including a body portion including a first section including a first lens delivery passageway configured to contain an IOL readied for implantation, and a second section including a second lens delivery passageway connected to the first passageway, configured to fold the IOL when the IOL is pushed through the second passageway, and a nozzle portion extending from the body portion, the nozzle portion including a third passageway and a tip for insertion through the incision in the eye, the second passageway extending to the third passageway, the third passageway configured to transfer the folded IOL into an incision in an eye when the folded IOL is pushed through the nozzle. Related apparatus and methods are also described.

Abstract: A durable, injection moldable, thermoplastic elastomer that has the favorable resilience, feel, spin, barrier, and UV stability performance attributes is disclosed herein. An OBC grafted with silane provides a good cover shear durability (cut/tear/abrasion resistance). This invention combines the benefits of OBCs and silane crosslinking technology to yield a golf ball cover with a desirable combination of properties.

Abstract: This invention relates to a composition and method of modifying the surface of a polymeric to produce a film or article with a reduced coefficient of friction (COF) and improved release properties. The reduced coefficient of friction improves both the slip and anti-blocking properties of the material as well aiding in processing of the polymeric material. Additionally, the invention improves demolding and release of the polymeric c material from other polymeric surfaces or adhesives as well as metal molding surfaces.

Abstract: A piston has a one-piece body having a first portion and a second portion. The second portion is integrally formed with the first portion, is flexibly movable between a first position and a second position relative to the first portion, and is biased toward the first position. The first portion has an orifice, and the second portion has a seal member. When the second portion is disposed in the first position, the seal member is disposed in a sealed arrangement with the orifice, and when the second portion is disposed in the second position, the seal member is disposed in an unsealed arrangement with the orifice.

Abstract: A shield device helps prevent selected surface areas from being painted by a paint material. The shield device includes a sheet member; and a handle member pivotable in a plane defined by the sheet member. The shield device is arranged between a folded configuration where the handle member is positioned generally parallel to an attachment edge of the sheet member, and an unfolded configuration, and an unfolded position.

Abstract: Topographical features, such as projections or recesses, having a maximum dimension which is less than 3 ?m, with the features being separated by a distance which is less than 10 ?m are transferred to polyetheretherketone, on an industrial scale, by injection moulding relatively low viscosity PEEK, using a mould in which is arranged a master structure which carries the desired topography. The topographical features increase the water contact angle of a surface which includes them and such a modified surface has been shown to influence cell attachment and differentiation. Parts which incorporate the topographical features may be used in medical devices such as implantable medical devices for cardiology or for neuromodulation.

Abstract: Disclosed herein are compositions and methods for the manufacture of polycarbonate blend compositions containing recycle for improvement in surface aesthetics. The resulting compositions, can be used in the manufacture of articles while still retaining the advantageous physical properties of polycarbonate blend reference compositions that do not contain recycle material. This abstract is intended as a scanning tool for purposes of searching in the particular art and is not intended to be limiting of the present invention.

Abstract: An airway device for human or animal use comprising an airway tube having a distal end and a proximal end, the distal and of which is surrounded by a laryngeal cuff, adapted to fit anatomically over the laryngeal structure of a patient, wherein the device optionally further comprises a buccal cavity stabilizer located on or around the airway tube between the laryngeal cuff and the proximal end of the tube, said buccal cavity stabilizer being adapted to nest with the anterior aspect of the patient's tongue, the size, shape and configuration of the buccal stabilizer being adapted to prevent rotational or side-to-side movement of the airway device in use.

Abstract: The present disclosure provides a polyester polymer product which contains partially or fully cobalt-neutralized organic sulphonic acid component and which is substantially free of ether and its preparation. The present disclosure also provides an oxygen scavenging composition made from a mixture of the polyester polymer product of the present disclosure, an organic oxidizable polymeric component and optionally at least one additional polyester component. The present disclosure further provides a packaging article defined by walls having an oxygen transmission rate (OTR) less than 0.2 cc·m?2 day?1 at 0.28 mm thickness and its preparation.

Abstract: Propylene impact copolymers (ICPs) are provided which comprise: (a) a matrix phase which comprises from 60 to 95 weight % of a polypropylene polymer containing from 0 to 6 mole % of units derived from one or more alpha-olefins other than propylene, and (b) a dispersed phase which comprises from 5 to 40 weight % of a copolymer derived from a first comonomer which can be either propylene or ethylene together with a second alpha-olefin comonomer. The ICP is further characterized by having a beta/alpha ratio less than or equal to 1.1. The ICPs of the present invention are particularly well suited for applications requiring clear, tough polymers such as thin walled injection molded articles for frozen food packaging applications.

Abstract: An expandable material is shaped to form a part that can provide functional attributes such as reinforcement to a structure of article of manufacture such as an automotive vehicle.

Abstract: Embodiments of the invention relate to injection mold components, assemblies, and molding system that include superhard materials. Such injection mold components, assemblies, and systems may decrease wear of certain injection mold components, which may result in improved productivity of the injection mold and molding systems that utilize such components.

Abstract: The invention relates to a composition comprising, relative to the total weight of the composition: between 25% and 52% by weight of at least one semi-crystalline or amorphous polyamide, having an amine chain-end content of less than 0.040 meq/g, between 24% and 40% by weight of at least one reinforcer, and between 24% and 35% by weight of at least one metal salt, optionally contained in a polymer, chosen from a metal salt of phosphinic acid, a metal salt of diphosphinic acid, and a mixture thereof. The invention also relates to the process for preparing this composition and its use.

Abstract: Disclosed herein are compositions including a cross-linked polycarbonate. The cross-linked polycarbonate may be derived from a polycarbonate having about 0.5 mol % to about 5 mol % endcap groups derived from a monohydroxybenzophenone. A plaque including the composition can achieve a UL94 5VA rating. Also disclosed herein are articles including the compositions, methods of using the compositions, and processes for preparing the compositions.

Abstract: The invention relates to a fastening member for fastening of elements, which fastening member has at least a first side and a second side, wherein the first side of the fastening member has at least two transversal extensions. The fastening member has at least one longitudinal extension, and at least two holes, in the longitudinal axis of the fastening member. The invention further relates to a system and a method for manufacturing a fastening member used for fastening of elements, and an arrangement and a use for fastening elements.

Abstract: An apparatus of the present invention presents a housing for engaging a mold device that includes a top plate having a top mold and a bottom plate having a bottom mold. The top plate presents side edges presenting a plurality of male elements extending therefrom. A top portion of the housing presents a safety and locking device (the device) to secure the top plate. The device presents several plates movable relative one another to secure the top plate. In case of a power outage, an actuator cooperably connected with the device prevents a shaft, connected to one of the plates, to move back to its idle position thereby locking the top plate within the device to prevent disengagement of the top plate from the device.

Abstract: Mold 2 includes a pair of mold halves (upper mold half 4 and lower mold half 6). A spherical cavity is formed by mating upper mold half 4 and lower mold half 6. A large number of pimples 10 are provided on the cavity face of the upper mold half 4 and lower mold half 6. The upper mold half 4 and the lower mold half 6 have flat plane 14, protrusion 16 and recess 18, respectively. The protrusion 16 projects from the equator Eq. The recess 18 is depressed from the equator Eq. The protrusion 16 includes a part of the pimple 10. The proportion P1 of the number of the protrusion 16 that is adjacent to other protrusion 16 belonging to other mold half distinct from the mold half to which itself belongs, to the total number of the protrusions 16 is equal to or greater than 50%. The proportion Pw of the sum total of the widths of the protrusions 16 measured along the equator, to the entire length of the equator is equal to or greater than 35%.

Abstract: A process for forming a product by injection molding.

Abstract: An in-mold shutter (140) for embedding in an injection mold (100, 200, 300) is described herein. The in-mold shutter (140, 240, 340, 440, 540) includes a shutter actuator (148, 548) that is configured to selectively engage a first mold shoe (130) of the injection mold (100, 200, 300) with a platen of a mold clamping assembly (996) to hold the first mold shoe (130) in an extended position (E), along a mold-stroke axis (X), during a step of molding a first molded article (102A) in the injection mold (100, 200, 300). Also described herein is a molded article transfer device (150, 250) for use with the injection mold (100, 200, 300). The molded article transfer device (150, 250) includes a shuttle (154) that is slidably arranged, in use, within the injection mold (100, 200, 300).

Abstract: A rotary knob assembly and methods for forming and controlling friction effecting features of the knob assembly are disclosed. The knob assembly includes a mounting structure and a knob. The knob is rotatably coupled to a bezel of the mounting structure. The knob includes a stabilizer, a guide member, and a retainer having a patterned surface. At least a portion of the stabilizer is disposed between the bezel and the retainer to maintain an axial position and a radial position of the knob. A detent formed on the guide member cooperates with a patterned surface of the retainer to provide a haptic feedback to a user.

Abstract: Processes for improving melt flow properties of molten compositions with polyoxymethylene polymers and polymer/polyol additives having a certain core-link-arm structure, which include: obtaining melt viscosity stability while improving notched Izod, decreasing relative apparent capillary melt viscosity, and increasing elongation at break relative to molten compositions of polyoxymethylene polymers without the polymer/polyol additives.

Abstract: A motor vehicle assembly unit having a connector, in particular a quick connector, and having a motor vehicle fluid line, wherein the connector includes an insertion end for inserting the fluid line, wherein there is a securing spike on the insertion end, which is encompassed by an outer sleeve. An annular insertion space for the fluid line or a fluid line end of the fluid line is disposed between the securing spike and the outer sleeve. The outer sleeve is connected to the securing spike by means of at least one break-away element, that breaks when the fluid line is inserted in the annular insertion space, such that the outer sleeve can be slid onto the securing spike, or further slid onto the securing spike from, or with, the fluid line.

Abstract: Embodiments relate to injection mold assemblies that include superhard materials, such as polycrystalline diamond compacts (“PDCs”), and related injection mold presses, components, and methods. The superhard materials are positioned to define at least a portion of a mold cavity for injection molding. Superhard materials may be fully or partially encapsulated by a substrate and the superhard materials and substrate may be secured to the injection mold. Superhard materials may be formed or otherwise separated from a substrate and secured to the injection mold without support of a substrate. Superhard materials may also be attachable to an injection mold to define only a portion of a mold cavity. In an embodiment, an injection mold insert includes a superhard material for insertion into a generic cavity within an injection mold assembly.

Abstract: A process for homogenizing and pelletizing a polyethylene composition comprising the steps of a) providing a polyethylene composition having a density of from 0.90 g/cm3 to 0.97 g/cm3 and a melt flow rate MFR21.6 at 190° C. under a load of 21.6 kg of from 1 g/10 min to 80 g/10 min, b) melting the polyethylene composition; c) passing the melt through a combination of screens consisting of screens having a mesh opening of at least 205 ?m and comprising at least two screens having a mesh opening of from 205 ?m to 350 ?m; and e) pelletizing the molten polyethylene composition, the use of a polyethylene composition obtained by such a process for the preparation of films, fibers, pipes, blow-molded articles, injection-molded articles, compression-molded articles or rotomolded articles and films, fibers, pipes, blow-molded articles, injection-molded articles, compression-molded articles or rotomolded articles prepared from a polyethylene composition obtained by such a process.

Abstract: A method of molding a boot for a constant velocity joint includes: molding a compact by injection molding; raising split dies of an inner die so as to separate the split dies from a set ring; raising a core shaft of the inner die so as to separate the core shaft from the split dies; separating each of the split dies from the compact; introducing a lower end portion of the separated split die into the set ring along an engaging surface; and inserting a lower end portion of the core shaft through the set ring from above the set ring, and pressing upper end portions of the split dies downward by a protruding portion at an upper end portion of the core shaft so that the lower end portions of the split dies are engaged with the engaging surface and the split dies are brought into close contact.

Abstract: Various devices, systems and methods for knotless suturing of tissue are disclosed. These devices allow sutures to be anchored to bone, and more specifically provide a suture anchor which eliminates the need for knotting the suture. Thus, damaged tissue may be re-attached to a substrate tissue. The anchors have a minimum of moving parts may be suited to being a single molded polymer construction. The anchors will find particular utility in hip and shoulder arthroscopy, e.g. labral re-attachment and similar procedures.

Abstract: A process of manufacturing an overlapping formliner is disclosed. The process includes applying a formliner material to a mold, the mold having pocket molds for producing formliner pockets and a lattice of ridge molds for producing formliner ridges, then forming the overlapping formliner, the overlapping formliner having a varied ridge width being configured to be positioned to overlap an adjacent formliner, and then demolding the formliner from the mold to produce the formliner having the formliner pockets and the formliner ridges.

Abstract: Provided are an acrylic resin composition, an acrylic resin sheet, and an acrylic resin laminate that exhibit superior transparency and impact resistance. The acrylic resin composition contains 100 parts by mass of an acrylic polymer (A) having 50 to 100% by mass of a methyl methacrylate unit and 0.002 to 0.7 parts by mass of an olefin-alkyl (meth)acrylate copolymer (B). The copolymer (B) is preferably an ethylene-alkyl acrylate copolymer (B-2). The acrylic resin sheet contains this acrylic resin composition. The acrylic resin sheet has a haze value of 0.5% or less based on JIS K 7136, a 50% impact-puncture height of at least 350 mm or more in a falling ball test based on JIS K 7211 under the described conditions, and a sheet thickness of 2 mm or less. The acrylic resin laminate has a cured layer laminated on at least one surface of the acrylic resin sheet.

Abstract: A process of manufacturing a formliner is disclosed. The process includes applying a formliner material to a mold, the mold having pocket molds for producing formliner pockets and a lattice of ridge molds for producing formliner ridges, then forming the formliner, and then demolding the formliner from the mold to produce the formliner having the formliner pockets and the formliner ridges. The lattice of the ridge molds have texture for producing texture in the formliner ridges and/or the mold includes a rigid high-density urethane closed cell foam or a rigid polyisocyanurate foam.

Abstract: A system for mounting an injection molding system actuator to a manifold and a clamp plate comprising: a mount comprised of a thermally conductive material having first and second thermally conductive surfaces, the actuator being mounted to the first thermally conductive surface in thermal communication with the second thermally conductive surface, the clamp plate being mounted in thermal communication with the second thermally conductive surface, the actuator being mounted in thermal communication with the heated manifold; wherein the clamp plate, manifold and mold are assembled together with the actuator and the mount in an assembled operating arrangement such that the second thermally conductive surface is in compressed contact with the clamp plate under a spring force.

Abstract: A circuit package for housing semiconductor or other integrated circuit devices (“die”) includes a high-copper flange, one or more high-copper leads and a liquid crystal polymer frame molded to the flange and the leads. The flange includes a dovetail-shaped groove or other frame retention feature that mechanically interlocks with the molded frame. During molding, a portion of the frame forms a key that freezes in or around the frame retention feature. The leads include one or more lead retention features to mechanically interlock with the frame. During molding, a portion of the frame freezes in or adjacent these lead retention features. The frame includes compounds to prevent moisture infiltration and match its coefficient of thermal expansion (CTE) to the CTE of the leads and flange. The is frame is formulated to withstand die-attach temperatures. A lid is ultrasonically welded to the frame after a die is attached to the flange.

Abstract: The present invention discloses a needle guard (100) for protecting a needle (210) from accidental contact, comprising; a spring loaded needle shield (110) being pivotable from an open position in which the needle shield (110) is separated from the needle (210) to a closed position in which the needle shield (110) is enclosing and protecting the needle (210); and a mounting base (140) having a constant spatial relationship with the needle (210) when the needle guard (100) is being used, the mounting base (140) being movably connected to the needle shield (110) for enabling movement between the open and the closed position; wherein the needle shield (110) is having a passive state and an active state, the needle shield (110) being urged towards the closed position when in the active state. Methods of manufacturing the needle guard (100) and a needle guard assembly comprising the needle guard (100), are also disclosed.

Abstract: The present invention relates to a novel polyamide synthesized from biosourced monomers. The novel polyamide comprises the repeating unit of formula I below: in which A represents a covalent bond or a divalent hydrocarbon-based group chosen from saturated or unsaturated aliphatics, saturated or unsaturated cycloaliphatics, aromatics comprising at least 5 carbon atoms, arylaliphatics and alkylaromatics; X represents a divalent group of formula II or III below: The present invention also relates to the process for preparing the said polyamide, to its uses, and to articles and compositions comprising the said polyamide.

Abstract: A transparent polyamide elastomer of the general structure (I), where R1 is a polyamide segment formed from a) 10-100 mol % of alkyl-substituted bis(aminocyclohexyl)methane or bis(aminocyclohexyl)propane and 0-90 mol % of other cycloaliphatic, aliphatic or aromatic C6-C36 diamines, based on the total amount of diamine in the polyamide segment, and b) aliphatic C4-C36 dicarboxylic acids, cycloaliphatic or aromatic C8-C36 dicarboxylic acids, and c) optionally lactams or aminocarboxylic acids C6-C12, R2 being selected from the group of the divalent radicals: linear or branched C2-C5 polyoxyalkylene, polyolefin, polysiloxane with a number-average molar mass in the range of 200-3000 g/mol, C2-C36 alkylene, C6-C36 cycloalkylene, C6-C20 aryl, polycaprolactone, polyesters based on aliphatic or cycloaliphatic dicarboxylic acids and diols, aliphatic polycarbonate, and also copolymers of or mixtures of these elements, and X1 and X2 independently of one another being amide (CONH) or ester (COO) bonds.

Abstract: An injection mold for an intake hose and an intake hose production method utilizes a main core removably dualized to automatically extract a molding-completed intake hose from the main core after injection molding is completed and an air supplying member supplying compressed air between the main core and the molding-completed intake hose is configured in the main core to automatically extract the intake hose from the main core without an additional extraction equipment, thereby reducing an entire manufacturing process and saving a manufacturing cost.

Abstract: A preferred method of the invention introduces organosilicon polymer into the reservoir of a mold with trenches defining a negative mold impression of a feature that has a high aspect ratio in fluid communication with the micro-dimensioned reservoir. The mold is preferably coated with a low-stiction coating. The polymer is moved via capillary action into the negative mold from the reservoir. The polymer is cured. The polymer is then released from the mold. Preferably, the polymer is soaked in a releasing solution prior to release. Preferably, the polymer is released by gripping cured polymer in the reservoir and gently peeling the cured micropolymer from the mold. In preferred embodiments, the polymer is poly-dimethyl-siloxane (PDMS). A preferred structure formed by methods of the invention is polymer microbeam in a liquid having a length of one to a few millimeters and a stiffness of k<0.1 pN/?m. Aerodynamic features can be created along with the beam.

Abstract: A boot unit may comprise a boot that includes a small diameter portion formed at one side, a large diameter portion form at the other side, and a wrinkle portion formed between the small diameter portion and the large diameter portion, a bushing that is integrally formed with an interior circumference or an exterior circumference in a circumferential direction and having a predetermined thickness, and a band that is formed in the bushing along the circumferential direction of the bushing and has substantially a ring shape.

Abstract: The present invention relates to components of mobile electronic devices made of an amorphous polyamide composition characterized by excellent mechanical properties, low moisture uptake, low distortion and very good aesthetical properties. The amorphous polyamide has recurring units derived from the polycondensation of a mixture of monomers of aromatic dicarboxylic acid(s), cycloaliphatic diamine(s) with 6 to 12 carbon atoms, and a third monomer with 10 to 16 carbon atoms.

Abstract: Process for the preparation of a nitrile rubber comprising: —subjecting at least one ?,?-unsaturated nitrile, at least one conjugated diene and, optionally, one or more further copolymerizable monomers, to emulsion polymerization, in the presence of at least one alkyl thiol containing from 12 to 16 carbon atoms and at least three tertiary carbon atoms and having the sulfur bound to one of said tertiary carbon atoms, at a pH ranging from 7 to 10, preferably from 8 to 9, obtaining a latex; —subjecting said latex to coagulation, in the presence of at least one metal sulfate selected from magnesium, sodium, potassium, preferably magnesium, at a temperature higher than or equal to 30° C., preferably ranging from 40° C. to 60° C.