Oxygen Containing Atmosphere Patents (Class 427/539)
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Publication number: 20130135712Abstract: The disclosure is directed to a method of making yttrium oxide, Y2O3, coatings on substrates suitable for use at infrared wavelengths, including use in the 2-12 ?m range. The coating method eliminates or substantially eliminates the absorptions peaks that typically appear at approximately 3.0 ?m, 6.6 ?m and 7.1 ?m. This is achieved by using Y metal as the yttrium source in combination with an oxygen-containing plasma to form the Y2O3, coating in place of the using Y2O3 as the coating material source The disclosure is further directed to optics suitable for use in the infrared that have such coatings. The transmission spectrum of the coated substrate made according to the method described herein is greater than the transmission spectrum of the uncoated substrate over the wavelength range of 4 ?m to 12 ?m.Type: ApplicationFiled: November 28, 2012Publication date: May 30, 2013Inventors: Horst Schreiber, Jue Wang, Scott J. Wilkinson
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Publication number: 20130119822Abstract: A Micro-Electro-Mechanical System (MEMS) device and its manufacturing method are provided. Said device comprises a MEMS component and said component comprises a main body (10) and a movable electrode (20). Said main body (10) contains a fixed electrode (110) and a cavity (30) and is covered by a first dielectric layer (400) which seals said cavity (30) into an enclosure. Said movable electrode (20) is connected with said main body (10) flexibly by a fixing piece and overhangs in said enclosure. Vias (405) are formed in said first dielectric layer (400) and filled with a second dielectric layer (500). The patent enables effective packaging for a MEMS device.Type: ApplicationFiled: December 13, 2010Publication date: May 16, 2013Applicant: Lexvu Opto Microelectronics Technology (Shanghai) Ltd.Inventors: Jianhong Mao, Fengqin Han, Deming Tang
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Publication number: 20130098764Abstract: A production method of the present invention is a method of producing a reaction instrument for electrophoresis (10), which is constituted by (i) a substrate (1) and (ii) an electrophoresis gel (3) which is immobilized on the substrate (1), including the steps of: (i) discharging a liquid to a surface of the substrate (1) on which surface the gel is to be immobilized, thereby forming a liquid pool (5); and thereafter (ii) discharging a gel solution to the liquid pool (5). This provides a method of producing a reaction instrument for electrophoresis, which method makes it possible to form a gel with high reliability in high yield.Type: ApplicationFiled: January 12, 2011Publication date: April 25, 2013Applicant: SHARP KABUSHIKI KAISHAInventors: Hiroshi Ohki, Yutaka Unuma, Yuji Maruo, Tsuyoshi Tanaka, Hiroshi Yamaki
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Publication number: 20130101752Abstract: Provided is a method of depositing a cyclic thin film that can provide excellent film properties and step coverage. The method includes the steps of depositing an insulating film by repeatedly performing a deposition step for depositing silicon on a substrate by injecting a silicon precursor into a chamber into which the substrate is loaded, a first purge step for removing a non-reacted silicon precursor and a reacted byproduct from the chamber, a reaction step for forming the deposited silicon as an insulating film including silicon by supplying a first reaction gas into the chamber and a second purge step for removing a non-reacted first reaction gas and a reacted byproduct from the chamber; and densifying the insulating film including silicon by supplying a plasma atmosphere into the chamber.Type: ApplicationFiled: August 1, 2011Publication date: April 25, 2013Applicant: EUGENE TECHNOLOGY CO., LTD.Inventors: Hai Won Kim, Sang Ho Woo
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Publication number: 20130095413Abstract: The present invention relates to a separator plate for a fuel cell and to a method for producing the same, and relates to an invention wherein a surface-modification layer is formed through the use of low temperature plasma processing such that it is possible to prevent the hydrophobic characteristics which occur during gasket forming and to have outstanding hydrophilic characteristics, and such that it is possible to obtain the advantageous effect of highly outstanding corrosion resistance and electrical conductivity not only initially but also even after long-term use in a fuel-cell operating environment, and also such that it is possible to maintain outstanding durability even when using a normal low-price stainless-steel sheet base material, and it is possible to reduce the unit cost of production of the separator plate for the fuel cell since surface processing can be carried out at low cost.Type: ApplicationFiled: June 24, 2010Publication date: April 18, 2013Applicant: HYUNDAI HYSCOInventors: Yoo-Taek Jeon, Eun-Young Kim, Man-Bean Moon
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Patent number: 8414987Abstract: A method for improving an adhesion of an adhesive to a cured silicon-containing surface is provided. The method comprises applying a primer composition to the surface before applying the adhesive; and subjecting the surface to a plasma treatment before or after the composition is applied thereto; wherein the primer composition comprises a polar organic solvent, an acrylic monomer, and an amino-containing silane.Type: GrantFiled: February 6, 2012Date of Patent: April 9, 2013Assignee: Great Eastern Resins Industrial Co., Ltd.Inventors: Shang-Hsin Guo, Wen-Ching Tsay, Bor-Kai Hsiung
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Patent number: 8404302Abstract: A solution process is provided for forming a textured transparent conductive oxide (TCO) film. The process provides a substrate, and forms a first layer on the substrate of metal oxide nanoparticles such as ZnO, In2O3, or SnO2. The metal oxide nanoparticles have a faceted structure with an average size greater than 100 nanometers (nm). Voids between the metal oxide nanoparticles have a size about equal to the size of the metal oxide nanoparticles. Then, a second layer is formed overlaying the first layer, filling the voids between the nanoparticles of the first layer, and completely covering the substrate. The result is a continuous TCO film having an average surface roughness that is created by the combination of first and second layers.Type: GrantFiled: July 14, 2010Date of Patent: March 26, 2013Assignee: Sharp Laboratories of America, Inc.Inventors: Jer-shen Maa, Gregory S. Herman, Apostolos T. Voutsas
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Publication number: 20130059091Abstract: A method for forming carbon nanotubes includes preparing a target object having a surface on which one or more openings are formed, each of the openings having a catalyst metal layer on a bottom thereof; performing an oxygen plasma process on the catalyst metal layers; and activating the surfaces of the catalyst metal layers by performing a hydrogen plasma process on the metal catalyst layers subjected to the oxygen plasma process. The method further includes filling carbon nanotubes in the openings on the target object by providing an electrode member having a plurality of through holes above the target object in a processing chamber, and then growing the carbon nanotubes by plasma CVD on the activated catalyst metal layer by diffusing active species in a plasma generated above the electrode member toward the target object through the through holes while applying a DC voltage to the electrode member.Type: ApplicationFiled: October 31, 2012Publication date: March 7, 2013Applicant: TOKYO ELECTRON LIMITEDInventor: Tokyo Electron Limited
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Patent number: 8361565Abstract: A method for plasma treatment and painting of a surface, the surface including a plurality of different materials includes blasting the surface with a carbon dioxide snow so as to activate the surface to improve an adhesive strength; and treating the surface with a plasma treatment using at least one plasma nozzle following the blasting step, the treating including guiding the at least one plasma nozzle at a distance of not more than 15 mm from the surface at a feed rate of not more than 50 m/min.Type: GrantFiled: February 12, 2010Date of Patent: January 29, 2013Assignee: Airbus Operations GmbHInventors: Birgit Kuhlenschmidt, Daniel Lahidjanian, Dirk Bausen, Karl Hausmann, Bettina Kroeger-Kallies
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Patent number: 8359106Abstract: Adhesiveless direct bonding between polymeric tubular members assembled with an interference fit using an oxidative cold gas plasma treatment, and implantable medical leads manufactured in part using a cold gas plasma bonding process are disclosed. An illustrative method includes subjecting a number of polymeric tubular members to an oxidative cold gas plasma, creating an oxygen rich layer on each of the tubular members. The treated surfaces of the tubular members are assembled together, forming a direct bond along an overlapping region between the tubular members when in conformal contact with each other.Type: GrantFiled: September 10, 2009Date of Patent: January 22, 2013Assignee: Cardiac Pacemakers, Inc.Inventors: Kalpana Viswanathan, Paul E. Zarembo
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Publication number: 20120308737Abstract: The invention concerns a method for antiseptic processing of the surface of a product made of organosilicon rubbers with molecular weight 2·105?6·105, said method consisting in a two stages formation of an antiseptic coating on said surface of said product: (a) at a first stage said surface is modified by treatment in low-temperature oxygen plasma at high-frequency electromagnetic radiation; and (b) at a second stage the modified surface is processed applying on it an antiseptic preparation containing: a biocide, which is a nanodispersed powder of bentonite intercalated by ions of silver or/and copper; a fluoroacrylic polymeric binding agent, wherein said binding agent is dissolved in a mixture of fluoroalkylethers. The method provides the formation of a coating having effective antiseptic and operational properties especially when the coating is applied on the surface of small orthopedic devices such as foot-correctors, insoles, heel pads, etc.Type: ApplicationFiled: December 14, 2010Publication date: December 6, 2012Inventors: Ara Arshavirovich Abramyan, Mikhail Mefodievich Afanasyev, Viacheslav Ivanovich Beklemyshev, Igor Ivanovich Makhonin, Umberto Orazio Giuseppe Maugeri, Vladimir Aleksandrovich Solodovnikov
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Patent number: 8318264Abstract: Process for surface functionalization of a glass reinforcement, characterized in that the said reinforcements are chemically modified by means of surface treatment by the action of a homogeneous plasma at atmospheric or sub-atmospheric pressure in a controlled, oxidizing or nitriding gas atmosphere, and in that the said surface portion is contacted with an aqueous impregnating solution of an organic or inorganic matrix, or directly with the matrix.Type: GrantFiled: March 30, 2007Date of Patent: November 27, 2012Assignee: Saint-Gobain AdforsInventors: Patrick Moireau, Maxime Duran, Jean-Baptiste Denis
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Publication number: 20120275059Abstract: According to one embodiment, a magnetic recording medium includes a substrate, an auxiliary layer formed on the substrate, and at least one perpendicular magnetic recording layer formed on the auxiliary layer. The perpendicular magnetic recording layer includes a magnetic dot pattern. The perpendicular magnetic recording layer is made of an alloy material containing one element selected from iron and cobalt, and one element selected from platinum and palladium. This alloy material has the L10 structure, and is (001)-oriented. The auxiliary layer includes a dot-like first region covered with the magnetic dot pattern, and a second region not covered with the magnetic dot pattern. The first region is made of one metal selected from (100)-oriented nickel and (100)-oriented iron. The second region contains an oxide of the metal used in the first region.Type: ApplicationFiled: January 16, 2012Publication date: November 1, 2012Applicant: KABUSHIKI KAISHA TOSHIBAInventors: Tomoyuki Maeda, Yousuke Isowaki, Akira Watanabe
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Publication number: 20120269987Abstract: An integrated system for processing a substrate in controlled environment to enable deposition of a thin copper seed layer on a surface of a metallic barrier layer of a copper interconnect is provided. The system includes a lab-ambient transfer chamber, a vacuum transfer chamber, a vacuum process module for cleaning an exposed surface of a metal oxide of a underlying metal, a vacuum process module for depositing the metallic barrier layer, and a controlled-ambient transfer chamber filled with an inert gas, wherein at least one controlled-ambient process module is coupled to the controlled-ambient transfer chamber. In addition, the system includes an electroless copper deposition process module used to deposit the thin layer of copper seed layer on the surface of the metallic barrier layer.Type: ApplicationFiled: June 27, 2012Publication date: October 25, 2012Applicant: Lam Research CorporationInventors: Yezdi Dordi, John Boyd, Tiruchirapalli Arunagiri, Hyungsuk Alexander Yoon, Fritz C. Redeker, William Thie, Arthur M. Howald
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Publication number: 20120247180Abstract: Device for the selective detection of benzene gas, which comprises, on a base substrate, a combination of at least one functionalised multi- or single-wall carbon nanotube sensor decorated with rhodium clusters, and at least one functionalised multi- or single-wall carbon nanotube sensor decorated with metal clusters selected from gold, palladium, nickel and titanium, and/or undecorated, where said substrate additionally comprises means for measuring the variation in the resistance of said sensors. The device is useful at ambient temperature in the presence or absence of oxygen and easy to handle. It also relates to a method for the manufacturing thereof and for detecting the gas in the chemical industry, the petrochemical industry, petrol stations, or household, aeronautical or research applications.Type: ApplicationFiled: November 2, 2010Publication date: October 4, 2012Inventors: Eduard Llobet Valero, Radouane Leghrib, Marc Delgado Olivella, Jean-Jacques Pireaux, Alexandre Felten, Jérôme Guillot, Henri-Nöel Migeon, Ali Mansour, François Amand Baudouin Reniers, Nicolas Yves Claessens, Frédéric Gilbert Michel Demoisson
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Patent number: 8263190Abstract: The present invention aims to provide a method of producing a magnetic recording medium which is a method of producing a magnetic recording medium having a magnetically-separated magnetic recording pattern, the method including: forming a magnetic layer on a non-magnetic substrate; then exposing a surface of the magnetic layer partially to reactive plasma, or a reactive ion generated in the plasma to amorphize the portion of the magnetic layer.Type: GrantFiled: June 17, 2008Date of Patent: September 11, 2012Assignee: Showa Denko K.K.Inventors: Masato Fukushima, Akira Sakawaki, Yasumasa Sasaki
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Publication number: 20120219724Abstract: In a method for forming a metal oxide film, by which excellent adhesion between the film and Cu can be provided, a gas containing an organometallic compound is supplied to a base, and the metal oxide film is formed on the base. After forming the metal oxide film on the base by supplying the organometallic compound to the base, the metal oxide film is exposed to the oxygen-containing gas or oxygen-containing plasma in the final step of the process of forming the metal oxide film.Type: ApplicationFiled: September 17, 2010Publication date: August 30, 2012Applicants: TOHOKU UNIVERSITY, TOKYO ELECTRON LIMITEDInventors: Koji Neishi, Junichi Koike, Kenji Matsumoto
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Publication number: 20120201973Abstract: A method for improving an adhesion of an adhesive to a cured silicon-containing surface is provided. The method comprises applying a primer composition to the surface before applying the adhesive; and subjecting the surface to a plasma treatment before or after the composition is applied thereto; wherein the primer composition comprises a polar organic solvent, an acrylic monomer, and an amino-containing silane.Type: ApplicationFiled: February 6, 2012Publication date: August 9, 2012Applicant: GREAT EASTERN RESINS INDUSTRIAL CO., LTD.Inventors: Shang-Hsin GUO, Wen-Ching TSAY, Bor-Kai HSIUNG
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Patent number: 8206794Abstract: A method for applying an abrasion-resistant coating to a substrate including the steps of generating an atmospheric plasma, introducing a precursor to the atmospheric plasma, the precursor being selected to form the abrasion-resistant coating, and positioning the substrate relative to the atmospheric plasma such that the atmospheric plasma deposits the abrasion-resistant coating onto the substrate.Type: GrantFiled: May 4, 2009Date of Patent: June 26, 2012Assignee: The Boeing CompanyInventors: Liam S. C. Pingree, Vasan S. Sundaram, Michael R. Sirkis, Shawn M. Pare
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Publication number: 20120107851Abstract: The present invention is directed to a lateral flow assay device for the monitoring and measuring of coagulation and method thereof. Ideally, the invention is directed to a lateral capillary flow device for the monitoring and/or measurement of coagulation in a liquid sample wherein the device comprises a non-porous substrate with a zone for receiving a sample and a defined flow path zone wherein a clotting agent is deposited on at least part of the defined flow path zone to accelerate the coagulation of the liquid sample, enable the formation of an evenly distributed clot along the defined flow path zone and to result in the change in flow rate or cessation of flow of the liquid sample along the defined flow path zone.Type: ApplicationFiled: April 23, 2010Publication date: May 3, 2012Inventors: Anthony Joseph Killard, Magdalena Maria Dudek, Brian MacCraith, Ib Mendel-Hartvig, Ove Öhman
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Publication number: 20120107607Abstract: A multilayered material is provided which includes a substrate and a silicon-containing film formed on the substrate, wherein the silicon-containing film has a nitrogen-rich area including silicon atoms and nitrogen atoms, or silicon atoms, nitrogen atoms, and an oxygen atoms and the nitrogen-rich area is formed by irradiating a polysilazane film formed on the substrate with an energy beam in an atmosphere not substantially including oxygen or water vapor and denaturing at least a part of the polysilazane film. A method of producing the multilayered material is also provided.Type: ApplicationFiled: July 12, 2010Publication date: May 3, 2012Applicant: MITSUI CHEMICALS, INC.Inventors: Toshihiko Takaki, Haruhiko Fukumoto
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Patent number: 8163358Abstract: A method of increasing the hydrophilicity of a polymer surface, such as a contact lens surface, includes exposing the polymer substrate to a first plasma under conditions selected to generate free radicals on the surface of the polymer substrate. The method also includes reacting an organic compound with the free radicals on the surface of the polymer substrate to thereby form an organic coating. The method further includes exposing the organic coating to a second plasma under conditions selected to oxidize the organic coating to thereby form a hydrophilic layer at the substrate surface. The hydrophilic layer can have a contact angle with respect to water that is less than about 50°.Type: GrantFiled: February 18, 2010Date of Patent: April 24, 2012Assignee: Synergeyes, Inc.Inventors: Ramazan Benrashid, Ivan Sabath, Jenny Xuan Huynh
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Patent number: 8163357Abstract: A scratch-resistant coating comprising a polymer including a functionalized polysilsesquioxane. The scratch-resistant coating is exposed to oxidizing conditions (e.g., ozone or ultraviolet light) that modify the surface chemistry of the coating to enhance adhesion to inorganic thin film coatings, such as antireflective coatings.Type: GrantFiled: March 26, 2009Date of Patent: April 24, 2012Assignee: Signet Armorlite, Inc.Inventors: Thomas J. Engardio, Geoffrey Yuxin Hu, Dae Ki Kang, Erick S. Rorye
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Patent number: 8153188Abstract: The present invention relates to a method for manufacturing a magnetoresistive element having a magnetization pinned layer, a magnetization free layer, and a spacer layer including an insulating layer provided between the magnetization pinned layer and the magnetization free layer and current paths penetrating into the insulating layer. A process of forming the spacer layer in the method includes depositing a first metal layer forming the metal paths, depositing a second metal layer on the first metal layer, performing a pretreatment of irradiating the second metal layer with an ion beam or a RF plasma of a rare gas, and converting the second metal layer into the insulating layer by means of supplying an oxidation gas or a nitriding gas.Type: GrantFiled: October 9, 2008Date of Patent: April 10, 2012Assignee: Kabushiki Kaisha ToshibaInventors: Hideaki Fukuzawa, Katsuhiko Koui, Hiromi Yuasa, Susumu Hashimoto, Hitoshi Iwasaki
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Patent number: 8137763Abstract: Processes for preparing catalyst structures, include forming a layer of a catalytic material on a substrate, and separating the layer of the catalytic material into droplet-shaped bodies of the catalytic material adhered to the substrate.Type: GrantFiled: February 7, 2005Date of Patent: March 20, 2012Assignee: Commissariat a l'Energie AtomiqueInventors: Jean Dijon, Francoise Geffraye
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Publication number: 20120034423Abstract: The present invention provides; a method for forming a metal oxide film which has both a surface irregularity and a predetermined pattern or either and has few unevenness of surface specific resistance, light transmittance and the like, and such the metal oxide film. The method for forming a metal oxide film having both a surface irregularity and a predetermined pattern or either on a substrate, wherein, the method comprises a first process in which a liquid material containing a metal salt is applied on the substrate to form a metal salt film, a second process in which a surface irregularity or a predetermined pattern is formed to the metal salt film, and a third process in which the metal salt film is converted to a metal oxide film by thermal oxidation treatment or plasma oxidation treatment.Type: ApplicationFiled: March 23, 2010Publication date: February 9, 2012Applicant: LINTEC CORPORATIONInventors: Satoshi Naganawa, Takeshi Kondo
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Publication number: 20120021138Abstract: A NanoLayer Deposition (NLD) process for depositing composite films of tertiary, quaternary, pentanary, and hexary stoichiometric films is provided. The inventive deposition process is a cyclic process consisting of a sequence of thin film deposition and treatment steps to obtain a desired film stoichiometry. The deposition steps are not self-limiting as in atomic layer deposition. In one embodiment for depositing a compound oxide film, the deposition process comprises a first deposition, followed by a hydrogen-containing plasma treatment, a second deposition followed by a hydrogen-containing plasma treatment, and then a third deposition followed by a hydrogen-containing plasma and then an oxygen-containing plasma treatment to produce a stoichiometric quaternary film. The cyclic process is repeated until the desired overall film thickness is achieved. The inventive process is used to fabricate high k dielectric films, ferroelectric films, piezoelectric films, and other complex oxides.Type: ApplicationFiled: September 19, 2011Publication date: January 26, 2012Applicant: TEGAL CORPORATIONInventors: Robert Anthony Ditizio, Tue Nguyen, Tai Dung Nguyen
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Publication number: 20120015147Abstract: A solution process is provided for forming a textured transparent conductive oxide (TCO) film. The process provides a substrate, and forms a first layer on the substrate of metal oxide nanoparticles such as ZnO, In2O3, or SnO2. The metal oxide nanoparticles have a faceted structure with an average size greater than 100 nanometers (nm). Voids between the metal oxide nanoparticles have a size about equal to the size of the metal oxide nanoparticles. Then, a second layer is formed overlaying the first layer, filling the voids between the nanoparticles of the first layer, and completely covering the substrate. The result is a continuous TCO film having an average surface roughness that is created by the combination of first and second layers.Type: ApplicationFiled: July 14, 2010Publication date: January 19, 2012Inventors: Jer-shen Maa, Gregory S. Herman, Apostolos T. Voutsas
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Publication number: 20110312176Abstract: Accordingly, the present invention provides a method of forming an electrode having reduced corrosion and water decomposition on a surface thereof. A substrate which has a conductive layer disposed thereon is provided and the conductive layer has an oxide layer with an exposed surface. The exposed surface of the oxide layer contacts a solution of an organic surface active compound in an organic solvent to form a protective layer of the organic surface active compound over the oxide layer. The protective layer has a thickness of from about 0.5 nm to about 5 nm and ranges therebetween depending on a chemical structure of the surface active compound.Type: ApplicationFiled: June 22, 2010Publication date: December 22, 2011Applicant: INTERNATIONAL BUSINESS MACHINES CORPORATIONInventors: Ali Afzali-Ardakani, Shafaat Ahmed, Hariklia Deligianni, Dario L. Goldfarb, Stefan Harrer, Binquan Luan, Glenn J. Martyna, Hongbo Peng, Stanislav Polonsky, Stephen Rossnagel, Xiaoyan Shao, Gustavo A. Stolovitzky
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Publication number: 20110312164Abstract: The present invention provides a method of forming an electrode having reduced corrosion and water decomposition on a surface thereof. A conductive layer is deposited on a substrate. The conductive layer is partially oxidized by an oxygen plasma process to convert a portion thereof to an oxide layer thereby forming the electrode. The oxide layer is free of surface defects and the thickness of the oxide layer is from about 0.09 nm to about 10 nm and ranges therebetween, controllable with 0.2 nm precision.Type: ApplicationFiled: June 22, 2010Publication date: December 22, 2011Applicant: INTERNATIONAL BUSINESS MACHINES CORPORATIONInventors: Ali Afzali-Azdakani, Shafaat Ahmed, Hariklia Deligianni, Dario L. Goldfarb, Stefan Harrer, Hongbo Peng, Stanislav Polonsky, Stephen Rossnagel, Xiaoyan Shao, Gustavo A. Stolovitzky
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Publication number: 20110305874Abstract: The invention relates to a process for obtaining a hydrophobic coating on a substrate, preferably consisting of a glass material, a ceramic or a glass-ceramic, said process being characterized in that it comprises: a) a first deposition step, consisting in applying a primer first layer essentially consisting of the silicon oxycarbide SiOxCy type on said substrate, said primer layer having an RMS surface roughness of greater than 4 nm; b) an activation step, in which said SiOxCy primer layer is activated by a plasma of a gas chosen from the noble gases of the Ar or He type and the gases N2, O2 or H2O or by a plasma of a mixture of these gases; and c) a second deposition step, in which a hydrophobic coating comprising at least one fluorocompound, preferably a fluoroalkylsilane, is deposited on said first layer. The invention also relates to hydrophobic glazing comprising or formed by a substrate as defined above, this glazing being in particular used as glazing for transport vehicles or for buildings.Type: ApplicationFiled: January 6, 2010Publication date: December 15, 2011Applicant: SAINT-GOBAIN GLASS FRANCEInventors: Claire Thoumazet, Bernard Nghiem, Bruno Cordier
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Publication number: 20110298869Abstract: A method of providing a printhead assembly having a hydrophilic ink pathway and a hydrophobic ink ejection face. The method includes the steps of: providing a printhead assembly comprising a printhead attached to an ink supply manifold, the printhead comprising a nozzle plate having a hydrophobic coating and a protective metal film disposed on the hydrophobic coating; treating surfaces of an ink pathway in the printhead assembly with a solution comprising an alkoxylated polyethyleneimine; drying the surfaces; and removing the protective metal film so as to reveal the hydrophobic coating.Type: ApplicationFiled: October 18, 2010Publication date: December 8, 2011Inventors: Simon Fielder, Lewis Matich, Kia Silverbrook, Gregory John McAvoy, R+e,acu o+ee n+e,acu a+ee n P+e,acu a+ee draig Se+e,acu a+ee n O'Reilly, Emma Rose Kerr
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Patent number: 8067065Abstract: A fibrillar, nanotextured coating is deposited on a substrate by contacting the substrate with a reaction mixture comprising a reagent which is hydrolyzable to produced a cross-linked reaction product, and a first solvent which solvates the reagent and the reaction product. The reagent is hydrolyzed so as to provide a cross-linked reaction product which is bonded to the substrate. The substrate is then contacted with a second solvent which is a non-solvent for the reaction product so as to cause nanoscopic phase separation of the reaction product, resulting in the formation of a fibrillar nanotextured coating which is bonded to the substrate. The thus produced coating may be subjected to further chemical modification. The method may be utilized to produce superhydrophobic coatings. Also disclosed are coatings made by the method of the present invention.Type: GrantFiled: July 5, 2006Date of Patent: November 29, 2011Assignee: Toyota Motor Engineering & Manufacturing North America, Inc.Inventors: Thomas J. McCarthy, Lichao Gao
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Publication number: 20110279979Abstract: Some embodiments include methods of forming rutile-type titanium oxide. A monolayer of titanium nitride may be formed. The monolayer of titanium nitride may then be oxidized at a temperature less than or equal to about 550° C. to convert it into a monolayer of rutile-type titanium oxide. Some embodiments include methods of forming capacitors that have rutile-type titanium oxide dielectric, and that have at least one electrode comprising titanium nitride. Some embodiments include thermally conductive stacks that contain titanium nitride and rutile-type titanium oxide, and some embodiments include methods of forming such stacks.Type: ApplicationFiled: May 12, 2010Publication date: November 17, 2011Inventors: Nik Mirin, Tsai-Yu Huang, Vishwanath Bhat, Chris Carlson, Vassil Antonov
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Patent number: 8012529Abstract: According to the invention, an insulating or semi-insulating barrier layer which has a thickness where a tunnel current can flow through is provided between a hole injection electrode and an organic compound layer with hole transport characteristics (a hole injection layer or a hole transport layer). Specifically, a thin insulating or semi-insulating barrier layer which contains silicon or silicon oxide; silicon or silicon oxide and a light transmitting conductive oxide material; or silicon or silicon oxide, a light transmitting conductive oxide material, and carbon may be provided between a light transmitting conductive oxide film formed of a light transmitting conductive oxide material, such as ITO and a hole injection layer containing an organic compound.Type: GrantFiled: July 18, 2007Date of Patent: September 6, 2011Assignee: Semiconductor Energy Laboratory Co., Ltd.Inventors: Junichiro Sakata, Masakazu Murakami, Koji Moriya, Yoshiaki Oikawa, Taketomi Asami, Hisashi Ohtani
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Patent number: 8007916Abstract: A composite part is produced by a process in which at least one of components a) and b) of said composite part is treated with an Openair plasma on a contact surface between said components a) and b) prior to production of the composite part, followed by molding-on of the other component; wherein said components are as follows: a) a part which entirely or to some extent comprises a molding composition comprising at least 40% by weight of a polyamide whose monomer units contain an average of at least 8 carbon atoms, and b) a part comprising another molding composition.Type: GrantFiled: January 30, 2006Date of Patent: August 30, 2011Assignee: Evonik Degussa GmbHInventors: Karl Kuhmann, Klaus Hülsmann, Martin Wielpütz, Walter-Konrad Mertens, Ursula Schaub, Kirsten Alting, Simon Amesöder, Leo Hoffmann
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Publication number: 20110205669Abstract: According to one embodiment, a method for manufacturing a magneto-resistance effect element is disclosed. The element has first and second magnetic layers, and an intermediate layer provided between the first and second magnetic layers. The intermediate layer has an insulating layer and a conductive portion penetrating through the insulating layer. The method can include forming a structure body having the insulating layer and the conductive portion, performing a first treatment including irradiating the structure body with at least one of ion including at least one selected from the group consisting of argon, xenon, helium, neon and krypton and a plasma including at least one selected from the group, and performing a second treatment including at least one of exposure to gas containing oxygen or nitrogen, irradiation of ion beam containing oxygen or nitrogen, irradiation of plasma containing oxygen or nitrogen, to the structure body submitted to the first treatment.Type: ApplicationFiled: September 14, 2010Publication date: August 25, 2011Applicants: Kabushiki Kaisha Toshiba, TDK CORPORATIONInventors: Shuichi Murakami, Hiromi Yuasa, Michiko Hara, Yoshihiko Fuji, Hideaki Fukuzawa, Kunliang Zhang, Min Li
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Publication number: 20110206578Abstract: Methods for activating and/or reactivating a metal oxide surface for deposition, immobilizing, and/or growing a biological sample (e.g., an oligonucleotide, a polynucleotide, functionalized particle, a polymer, etc.) thereon are disclosed. The metal oxide surface (e.g., zirconium oxide) can be activated and/or reactivated by exposing the metal oxide surface to various activation and/or treatment protocols capable of enhancing a slide's activity relative to the activity of an untreated slide. The activation and/or treatment protocol can include subjecting the slide (or at least the metal oxide layer) to an oxygen plasma treatment and/or a peroxide solution for an amount of time sufficient to activate and/or reactivate the metal oxide surface. Activated sequencing slides capable of incorporation, for example, into various embodiments of a flow cell for use in NGS platforms are also disclosed herein.Type: ApplicationFiled: February 23, 2011Publication date: August 25, 2011Applicant: LIFE TECHNOLOGIES CORPORATIONInventors: Evan Foster, Jessica Reed, Heather Shepherd, Christina Inman, Scott Benson
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Publication number: 20110198313Abstract: The invention relates to a controlled graphene film growth process characterized in that it comprises the following steps: the production on the surface of a substrate (S1) of a layer of a metal having with carbon a phase diagram such that above a molar concentration threshold ratio CM/CM+CC, where CM is the molar metal concentration in a metal/carbon mixture and CC is the molar carbon concentration in said mixture, a homogeneous solid solution is obtained; the exposure of the metal layer to a controlled flux of carbon atoms or carbon-containing radicals or carbon-containing ions at a temperature such that the molar concentration ratio obtained is greater than the threshold ratio so as to obtain a solid solution of carbon in the metal; and an operation for modifying the phase of the mixture into two phases, a metal phase and a graphite phase respectively, leading to the formation of at least a lower graphene film (31) located at the (metal layer incorporating carbon atoms)/substrate interface and an upperType: ApplicationFiled: October 16, 2009Publication date: August 18, 2011Applicants: ECOLE POLYTECHNIQUE, CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUEInventors: Laurent Baraton, Costel-Sorin Cojocaru, Didier Pribat
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Publication number: 20110198334Abstract: The subject of the invention is a method of obtaining a heated window, comprising depositing a continuous thin film of a transparent electronically conductive oxide, having a sheet resistance that is uniform over the entire area of the film, on a glass sheet; and subjecting the thin film to a plasma treatment in which a device that emits excited species of an oxygen plasma is placed facing a region of the thin film, and then a relative movement is created between the thin film and the device in order to treat differentially the various regions of the thin film, so that after the thin film has been treated it has regions with different sheet resistances.Type: ApplicationFiled: February 17, 2011Publication date: August 18, 2011Applicant: SAINT - GOBAIN GLASS FRANCEInventors: Georges Zagdoun, Pierre Chaussade, Vincent Legois
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Publication number: 20110168544Abstract: [Object]To provide a manufacturing method of an optical filter having favorable film quality by removing a foreign substance adhered onto a surface of a substrate by cleaning before a thin film is formed. [Solution] By performing a cleaning step P1 for cleaning a substrate S by means of a solution including water, a pre-treatment step P3 for plasma-treating a surface of the substrate S cleaned in the cleaning step P1 by plasma of an oxygen gas, and a thin film formation step (P4, P5) for forming the thin film on the surface of the substrate S plasma-treated in the pre-treatment step P3, the foreign substance adhered onto the surface of the substrate can be effectively removed. In the pre-treatment step P3, only the oxygen gas is introduced to an area where the plasma is generated, and a flow rate of the oxygen gas to be introduced is greater than a flow rate of the oxygen gas introduced in the thin film formation step.Type: ApplicationFiled: September 14, 2009Publication date: July 14, 2011Applicant: Shincron Co., LTDInventors: Ichiro Shiono, Toshihiko Sato, Yasuhisa Togashi, Yousong Jiang, Takuya Sugawara
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Publication number: 20110159299Abstract: A hydrophobic coating and method of preparing a hydrophobic coating with an adhesion promoting layer formed from an adhesion promoting composition and a hydrophobic layer, is disclosed. The adhesion promoting composition may comprise an adhesion promoting compound having an amine group and at least one of a silane functional group and/or a germanium functional group. The hydrophobic layer forming composition may comprise a hydrophobic layer forming compound having a hydrophobic aliphatic group and at least one of a silane functional group and/or a germanium functional group.Type: ApplicationFiled: July 16, 2010Publication date: June 30, 2011Inventors: Mattew R. Linforf, Gaurav Saini
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Publication number: 20110159204Abstract: A method of radical-enhanced atomic layer deposition (REALD) involves alternating exposure of a substrate to a first precursor gas and to radicals, such as monatomic oxygen radicals (O•), generated from an oxygen-containing second precursor gas, while maintaining spatial or temporal separation of the radicals and the first precursor gas. Simplified reactor designs and process control are possible when the first and second precursor gases are nonreactive under normal processing conditions and can therefore be allowed to mix after the radicals recombine or otherwise abate. In some embodiments, the second precursor gas is an oxygen-containing compound, such as carbon dioxide (CO2) or nitrous oxide (N2O) for example, or a mixture of such oxygen-containing compounds, and does not contain significant amounts of normal oxygen (O2).Type: ApplicationFiled: December 28, 2010Publication date: June 30, 2011Applicant: Lotus Applied Technology, LLCInventors: Eric R. Dickey, William A. Barrow
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Publication number: 20110151136Abstract: Methods for depositing high-K dielectrics are described, including depositing a first electrode on a substrate, wherein the first electrode is chosen from the group consisting of platinum and ruthenium, applying an oxygen plasma treatment to the exposed metal to reduce the contact angle of a surface of the metal, and depositing a titanium oxide layer on the exposed metal using at least one of a chemical vapor deposition process and an atomic layer deposition process, wherein the titanium oxide layer comprises at least a portion rutile titanium oxide.Type: ApplicationFiled: March 3, 2011Publication date: June 23, 2011Inventors: Xiangxin Rui, Sunil Shanker, Sandra Malhotra, Imran Hashim, Edward Haywood
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Publication number: 20110143101Abstract: Provided are a graphene structure and a method for producing the same in which graphene can be patterned with high precision, and thereby microfabrication of electronic device elements and electronic devices using graphene is possible and the manufacturing cost can be notably reduced. A resist film is precisely patterned on a substrate, hydrophilized films are formed in openings of the resist film, and then GO is selectively fixed on the portions of the hydrophilized films by a chemical bond utilizing the hydrophilicity of the GO, and the GO is reduced to obtain a graphene structure in which graphene is selectively fixed to only the portions of the hydrophilized films. Thus, the graphene structure is constituted by disposing graphene on a substrate and forming a bond, by hydrophilization treatment, between the hydrophilized portion of the substrate and the graphene and/or between the unhydrophobized portion of the substrate and the graphene.Type: ApplicationFiled: December 21, 2009Publication date: June 16, 2011Inventor: Adarsh Sandhu
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Publication number: 20110128643Abstract: A method for manufacturing a color filter includes obtaining a color filter, treating the color filter with oxygen plasma, treating the color filter with fluorine plasma and forming one or more color conversion layers. The color filter is obtained by forming on a transparent substrate, multiple color filter layers having respective colors, and banks. The color filter layers are composed of polysiloxane and pigments. The banks are composed of resin and formed at boundaries between color filter layers of different colors. The color conversion layers have respective colors and are formed on the color filter layers by an inkjet method.Type: ApplicationFiled: February 16, 2009Publication date: June 2, 2011Applicant: FUJI ELECTRIC HOLDING CO., LTD.Inventor: Yuko Nakamata
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Publication number: 20110123413Abstract: The present invention generally relates to coating materials, including photoactive coating materials. In some aspects of the invention, a sol-gel is provided that can be formed as a coating on a microfluidic channel. One or more portions of the sol-gel can be reacted to alter its hydrophobicity, in some cases. For instance, in one set of embodiments, a portion of the sol-gel may be exposed to light, such as ultraviolet light, which can be used to induce a chemical reaction in the sol-gel that alters its hydrophobicity. In one set of embodiments, the sol-gel can include a photoinitiator, that upon exposure to light, produces radicals. Optionally, the photoinitiator may be conjugated to a silane or other material within the sol-gel. The radicals so produced may be used to cause a polymerization reaction to occur on the surface of the sol-gel, thus altering the hydrophobicity of the surface. In some cases, various portions may be reacted or left unreacted, e.g.Type: ApplicationFiled: February 11, 2009Publication date: May 26, 2011Applicant: PRESIDENT AND FELLOWS OF HARVARD COLLEGEInventors: Adam R. Abate, Amber T. Krummel, David A. Weitz
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Publication number: 20110111367Abstract: Disclosed is nanocoupling of a polymer onto a surface of a metal substrate for improving coating adhesion of the polymer on the metal substrate, and in vivo stability and durability of the polymer. In accordance with the present invention, the polymers can be grafted via a chemical bonding on the surface of the metal substrate by the nanocoupling, by which adhesion, biocompatibility and durability of a polymer-coated layer which is to be formed later on the metal substrate were remarkably improved; therefore, the nanocoupling according to the present invention can be applied to surface modification of a metal implant, such as stents, mechanical valves, and an articular, a spinal, a dental and an orthopedic implants.Type: ApplicationFiled: October 27, 2010Publication date: May 12, 2011Inventors: Dong Keun HAN, Kwi Deok PARK, Jae-Jin KIM, Chul Ho PARK, Seong Bae CHO
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Publication number: 20110064887Abstract: A process for manufacturing workpiece whose surface is to be plated by means of electroless plating includes an ozone-processing step, and a superficial-layer removing step. In the ozone-processing step, a workpiece body including resin and having a surface is processed by means of an ozone treatment by brining the workpiece body into contact with a solution including ozone. Thus, a modified layer is formed on the surface of the workpiece body. Then, in the superficial-layer removing step, a superficial layer is removed from the resultant modified layer by applying energy onto the modified layer.Type: ApplicationFiled: September 16, 2010Publication date: March 17, 2011Applicants: KABUSHIKI KAISHA TOYOTA JIDOSHOKKI, TOYOTA JIDOSHA KABUSHIKI KAISHAInventors: Manabu OSAMURA, Toshihisa Shimo, Isami Kato, Takashi Yoshida, Takeshi Bessho
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Publication number: 20110064886Abstract: A method for improving an optical sensor is disclosed, which includes the following steps: providing an optical sensor; acid-treating the surface of the optical sensor; forming a thin metal film on the acid-treated surface of the optical sensor; and plasma-modifying the thin metal film on the optical sensor. The aforesaid method is to clean the surface of the optical sensor and then to improve the hydrophilicity thereof by acid treatment. The thin metal film subsequently formed has good flatness and improved adhesion to the optical sensor. Once the optical sensor has the improved hydrophilicity, the plasma modification is performed to further improve optical performance of the optical sensor.Type: ApplicationFiled: February 18, 2010Publication date: March 17, 2011Applicant: Forward Electronics Co., Ltd.Inventors: Yu-Chia Tsao, Min-Tzu Chao, Woo-Hu Tsai, Shu-Ting Chang, Hsiao-Ling Yeh