Abstract: The present invention relates to a method for preparing an optic material by depositing on a substrate at least two layers of inorganic polymeric material, each of these layers containing at least one metal oxide or metalloid oxide, the deposited layers being densified cross-linked by exposure to ultraviolet rays. The invention also concerns the optic material which may be prepared using this method. The optic materials which may be prepared using said method are in particular multilayer materials such as antireflective materials and reflective materials.

Abstract: This invention is directed toward methods for fabricating polycrystalline thin films. More particularly, the invention is directed toward optimized solid phase crystallization of plasma enhanced chemical vapor deposited amorphous silicon thin films as a means for obtaining, with a low thermal budget, polycrystalline silicon thin films comprising larger grain sizes and smother surfaces. The process of plasma enhanced chemical vapor deposition is quantified for silane containing various types of dilutants, thereby allowing deposition temperature, type of dilutant, type of plasma and other parameters to be controlled to yield the desired crystallization grain size at the desired thermal budget. Methods of annealing, annealing temperature, and pre-annealment treatments are also quantified such that grain size and thermal budget can be controlled in the fabrication of polycrystalline silicon thin films.

Abstract: A UV-curable coating for use with golf balls and other substrates includes one or more low viscosity polyether acrylate, a functional carbodiimide resin, one or more low viscosity aliphatic urethane polyacrylate oligomer, and a photoinitiator selected from one or more of mono-aryl ketones, trimethylbenzoyldiphenyl phosphinates, and/or phosphine oxides. In addition, a method of curing a UV-curable coating is disclosed. The method includes the steps of spraying the formulation onto the exterior of a substrate, surrounding the substrate in an inert gas enviromnent, and irradiating the substrate with ultraviolet radiation from a doped medium pressure mercury vapor lamp.

Abstract: A method for manufacturing a color filter comprises a step for charging an ink comprising a thermosetting resin composition onto an opening of a black matrix provided on a transparent substrate and a step for curing the ink by heat treatment. The thermosetting resin composition comprises either a coloring agent, a multifunctional epoxide having at least two glycidyl groups and a compound crosslinked by the multifunctional epoxide; or a coloring agent, a cellulose-reactive compound and a compound crosslinked by the cellulose-reactive compound.

Abstract: A method of preparing a coated substrate comprising: providing a radiation curable composition comprising a resin component including an unsaturated monomer and an unsaturated oligomer, binder or mixture of oligomer and binder; applying the radiation curable composition at a temperature in the range of from 35 to 150.degree. C. to the substrate; and subjecting the applied coating to radiation to thereby cure the coating. The invention also provides a composition for application of pigmented finishes and a method of coating in which a radiation curable composition is applied to a wet substrate.

Abstract: A pretreatment method for use in manufacturing an improved optical component comprises (i) providing a polymeric optical substrate; and (ii) exposing the polymeric optical substrate to electromagnetic energy having a wavelength of about 30 nm to about 350 nm. The exposure of the polymeric optical substrate to the electromagnetic energy substantially improves adhesion between the substrate and an optical coating deposited onto the substrate following pretreatment. The invention addresses the significant need for coated plastic optics by providing a method to achieve reliable adhesion of optical coatings placed on polymeric optical substrates. Specifically, this invention enables improved adhesion for even highly curved or shaped parts which have been historically more difficult to coat. The pretreatment method is particularly useful for molded substrates such as molded polymethylmethacrylate.

Abstract: Display elements of computer screens and other information displays are printed using conservative printing techniques. Contemplated electronic components that can be conservatively printed at the display element level include switches, transistors, capacitors, memory elements, and actuators. Contemplated light path components that can be conservatively printed at the display element level include light pipes or other optical wave guides, mirrors, light emitting diodes, liquid crystals, and actuators. The conservatively printed components may advantageously be produced by a process that includes depositing a precursor onto the substrate in a desired pattern, depositing an appropriate ligand onto the substrate, and applying sufficient energy to transfer electrons from the ligand to the precursor, thereby decomposing the precursor to form a precipitate. In an especially preferred class of embodiments, light emission at individual display elements is controlled by a conservatively printed moving actuator.

Abstract: Coating and filler materials for localized thermal processing of glazed ceramics and other brittle and low thermal conductivity materials. The coating materials include oxide compositions that exhibit coefficients of thermal expansion which are less than about 8.times.10.sup.-6 /.degree. C. and glass transition temperatures which are less than about 400.degree. C. The filler materials include particulate oxide materials which do not substantially react during localized thermal processing of glazed ceramics and other brittle and low thermal conductivity materials. The coating and filler materials are useable together as a composite material for repairing cavities having depths greater than about 2 mm.

Abstract: A method of improving the breakdown strength of polymer multi-layer (PML) capacitors is provided and of providing a window in food packaging is provided. The method comprises patterning the aluminum coating, either by selective removal of deposited aluminum or by preventing deposition of the aluminum on selected areas of the underlying polymer film. Apparatus is also provided for patterning metal deposition on polymer films comprising masking for defining regions in which metal is deposited. The apparatus comprises: (a) a rotating drum; (b) a monomer evaporator for depositing a monomer film on the rotating drum; (c) a radiation curing element for curing the monomer film to form a cross-linked polymer film; and (d) a resistive evaporator for depositing a metal film on the cross-linked polymer film. The foregoing elements are enclosed in a vacuum chamber.

Abstract: A method is proposed with which chemically defined bodies can be deposited on a substrate. Therefor, the bodies are fixed with a predetermined orientation on a stamping means which is then approached to the substrate whereby the bodies are deposited. While releasing the stamping means the bodies remain on the substrate keeping their orientation.

Abstract: A magnetic disk having improved tribological characteristics in the data zone of the disk surface while retaining a low sliding stiction in the landing zone is disclosed. It contains the conventional elements of a substrate, a magnetic recording layer, a protective overcoat, and a lubricant layer on the protective overcoat. However, the lubricant layer is UV irradiated under a photo mask to cause a radially inner zone and a radially outer zone. The photo mask is designed so that the radially outer zone of the lubricant layer has a ratio of bonded/unbonded lubricant molecules greater than that in the radially inner zone. The reduced proportion of mobile lubricant molecules in the data zone prevents the lubricant molecules from being collected by the magnetic head. On the other hand, a large proportion of the lubricant molecules in the landing zone remained mobile. This allowed the sliding stiction in the landing zone to stay at the desiredly low value.

Abstract: A process for forming a coating of a thermoplastic polymer on a hollow object formed of a low electrically conductive material is described, characterized in that the thermoplastic polymer has its maximum IR absorption between 1300 and 1900 nm and/or 2800 and 3000 nm, is applied electrostatically as a powder to the object while the objet is held at a temperature below the melting point of the thermoplastic polymer, and thereafter the object is heated by IR radiation to form the coating.

Abstract: The present invention provides a surface modification method that provides beneficial changes in surface properties, can modify a surface to a greater depth than previous methods, and that is suitable for industrial application. The present method comprises applying a thin-film coating to a surface of a substrate, then subjecting the coated surface to an ion beam. The ion beam power pulse heats the coated surface, leading to alloying between the material in the coating and the material of the substrate. Rapid cooling of the alloyed layer after an ion beam pulse can lead to formation of metastable alloys and microstructures not accessible by conventional alloying methods or intense ion beam treatment of the substrate alone.

Abstract: The object of the present invention is to provide a treatment method to remove lattice defects and non-diamond elements that exist in a diamond or a diamond thin film.The treatment method whereby the aforementioned object is achieved is to have the diamond or the diamond thin film irradiated by ultra-violet light or heated in an oxygen ambient.According to said treatment method, it has become possible to obtain a diamond or a diamond thin film that is free from the adverse effects of lattice defects and non-diamond elements.

Abstract: Paint or varnish is applied to the exterior of elongate elements such as pencils, by passing the pencils(3) through a receptacle(12) containing the paint or varnish(13), causing the pencils(3) to leave the receptacle(12) through a washer(17) which permits the pencils to leave the receptacle with a coating of paint or varnish on the exterior thereof, and subsequently passing the pencils through a light box(23) adapted to apply light to each point on the exterior of each pencil(3), the paint or varnish(13) comprising a resin which has the property that curing of the resin is initiated in response to the application of the light.

Abstract: A surface-decorated article by noble metal having a decorating matter of noble metal fused to the surface of a ceramic article. The decorating matter has a dual layer structure of a frit layer and an insulating noble metal film layer, which film layer comprising golden components of 60-90% Au, 3-15% Si, 2-11% In and 2-14% Ca. The noble metal decorating matter is not damaged on exposure to an electronic range, superior in chemical stability and abrasion resistance.

Abstract: Disclosed is a method for the formation of a silica-based coating film of a relatively large thickness in the manufacturing process of semiconductor devices and liquid crystal display panels by repeating the sequence consisting of coating of the surface with a coating solution containing a partial hydrolysis-condensation product of a trialkoxy silane compound followed by drying until a desired overall thickness of the coating film is obtained prior to a final baking treatment at 350 to 500.degree. C . The invention provides an improvement obtained by an ultraviolet irradiation treatment of the coating film intervening between a sequence of coating and drying and the next sequence of coating and drying so that the adhesion between the coating layers formed by repeating the sequence of coating and drying can be improved along with an advantage of absence of pinholes in the coating film.

Abstract: The invention concerns a method of treating surfaces and surface-adjacent layers of dental components in particular. A series of several different plasma treatments produces high adhesion between the plasma-treated surface and a layer of plastic applied thereto. The invention also concerns a method of sealing the surface of work by treating it with plasma and covering it with a layer that contains silicate.

Abstract: A combined business form/identification card includes a sheet of cellulosic stock material having a barrier coating on a first portion of the sheet with an overlay of laser-printable varnish on the barrier coat. Lines of weakness are provided in the sheet in the area of the barrier coat and varnish to produce an identification card detachable from the sheet. A second portion of the sheet has indicia imaged thereon.

Abstract: A method for producing a laminated object repeats a depositing step and an irradiating step alternatively. The irriating step comprises the operations of: covering a deposited layer with a mask having a pattern configuration for penetrating the laser beam; and scanning the lader beam on the desposited layer covered with the mask in such a manner that the laser beam depicts an irradiated continous wave trace being wider than the pattern configuration of the mask, by moving the laser beam in the Y-direction with a Y-rotating mirror, while repeating oscillations of the laser beam in the X-direction with a X-rotating nirror, The laminated object may be a casting mold.

Abstract: A diamond wafer including a substrate and a (100) oriented polycrystalline diamond film grown on the substrate for making surface acoustic wave devices, semiconductor devices or abrasion-resistant discs. The (100) oriented film is produced by changing a hydrocarbon ratio in a material gas halfway from a higher value to a lower value. The wafer is monotonously distorted with a distortion height H satisfying 2 .mu.m.ltoreq..vertline.H.vertline..ltoreq.150 .mu.m. The film is polished to a roughness of less than Rmax50 nm and Ra20 nm.

Abstract: The present invention is directed to a method of forming a new material layer or region near an interface region of two dissimilar materials, and an optional third layer, wherein at least one of said dissimilar materials or optional third is capable of being heated by microwave energy. The method of the present invention includes a step of irradiating a structure containing at least two dissimilar materials and an optional third layer under conditions effective to form the new material layer in the structure. An apparatus for conducting the microwave heating as well as the structures formed from the method are also described herein.

Abstract: A method for imprinting woodprints onto the blade of fan generally includes the steps of 1) molding the plastic blade; 2) coloring the blade with woodprints; and 3) deploying a protective coating thereof. Characterized in that when the plastic blade is molded by injected molding, the surface of the plastic blade is formed with a plurality of recesses that stimulate the annular rings. The plastic material can be dyed with white or other colors that stimulates the wood color. Then the surface of the plastic blade is printed with a first UV coating that is darker than the color of plastic blade. Afterward, the UV coating is then flattened by means of a rubber knife such that the UV coating is left only within the recesses on the surface of the plastic blade. Before the UV coating is cured and dried, a brush can be used to brush the UV coating longitudinally to generate a pattern of fibrils. Then the coating is undergone the UV light to cure and dry the UV coating.

Abstract: A method of forming a region of impurity in a semiconductor substrate with minimal damage. The method includes the steps of: forming a reaction-inhibiting impurity region in the semiconductor substrate to a depth below the semiconductor substrate; and applying laser energy to the semiconductor substrate at a sufficient magnitude to liquify the semiconductor substrate in the region.

Abstract: UV-hardenable and thermally hardenable epoxy resins for the underfilling process in electrical and electronic components are provided. A new casting resin component has an increased storage stability at room temperature of at least 6 months and improved characteristics for the underfilling process including faster hardening and lower viscosity. Filler material with a maximum grain size of 20 .mu.m and a siloxane component are provided in addition to the casting resin formulation.

Abstract: The present invention relates to coating and printing methods for the deposition of aqueous compositions. The composition may be adapted to any method without the need to change its chemical content. Viscosity is determined and adjusted by rising and lowering the temperature. High gloss value, increased film integrity and enhanced more resistance result.

Abstract: A sol-gel coating of conductive materials, such as ITO, which is applied to a substrate, for example a display window of a cathode ray tube, is cured by means of a laser. This is preferably carried out in a water-containing atmosphere, for example an aqueous aerosol and/or a hydrogen-containing gas, such as a forming gas. This results in a stable resistance reduction by several hundred times.

Abstract: A film of a coating material is produced on a substrate by a pulsed laser deposition method in which the material that forms the coating material is first combined with a matrix material to form a target. The target is then exposed to a source of laser energy to desorb the matrix material from the target and lift the coating material from the surface of the target. The target and the substrate are oriented with respect to each other so that the lifted coating material is deposited as a film upon said substrate. The matrix material is selected to have the property of being more volatile than the coating material and less likely than the coating material to adhere to the substrate. The matrix material is further selected as having the property such that when the target is exposed to a source of laser energy, the matrix material desorbs from the target and lifts the coating material from the surface of the target.

Abstract: Low gloss appearance in a coating derived from UV curable powder coatings can be achieved by using UV curable powder containing crystalline resins or blends of crystalline and amorphous resins and after heat fusing the powders together, allowing the crystalline resins in the coating to cool and recrystallize to a low gloss finish before curing with UV radiation.

Abstract: Ultraviolet radiation curing of inks on game balls, golf balls and the like is disclosed. Production inks, logo inks and methods for forming production prints and logos on golf balls, game balls and the like are disclosed. To form an ultraviolet radiation curable water-insoluble production ink, at least an adhesion promoting component is added to an ink base.

Abstract: Methods and apparatus for the preparation and use of a substrate having an array of diverse materials in predefined regions thereon. A substrate having an array of diverse materials thereon is generally prepared by delivering components of materials to predefined regions on a substrate, and simultaneously reacting the components to form at least two materials. Materials which can be prepared using the methods and apparatus of the present invention include, for example, covalent network solids, ionic solids and molecular solids. More particularly, materials which can be prepared using the methods and apparatus of the present invention include, for example, inorganic materials, intermetallic materials, metal alloys, ceramic materials, organic materials, organometallic materials, non-biological organic polymers, composite materials (e.g., inorganic composites, organic composites, or combinations thereof), etc.

Abstract: A silicone release composition having a non-gloss, i.e., matte finished, surface and a linerless label incorporating the silicone release composition. The release composition includes a crosslinked silicone-based polymer having microparticles of a polymeric wax at least partially embedded therein. The polymeric wax may be polytetrafluoroethylene, polypropylene or other polyolefin, or a hydrocarbon-based wax. The microparticles of polymeric wax cause incidental light to scatter upon reflection, giving the release composition surface matte appearance. This makes the release composition particularly useful for linerless labels on which bar coded information will be printed. Also, a method for producing linerless label stock. The method includes mixing an uncured silicone material with microparticles of a polymeric wax. The mixture is coated onto a substrate and exposed to UV radiation to cure or crosslink the silicone around the microparticles of wax.

Abstract: A method of fusing a thermal spray coating to a base material employs infrared heating. The thermal spray coating is applied to the base material in a conventional manner. The infrared heater applies unidirectional heat in a first time-temperature relation to the coating during a fusing phase to melt individual coating platelets into a dense layer and to metallurgically bond the coating to the base material. In a base material that is heat treatable, the base material can be heat treated subsequent to the fusing phase. Initial heat treating of the base material occurs during the fusing phase. Continued heat treating of the base material is achieved after the thermal spray coating fusing phase by a second application of time-temperature from the infrared heater. A cold wall process can be used to aid in the quenching phase of the heat treating process.

Abstract: Compounds which possess a complementary structure to a desired molecule, such as a biomolecule, in particular polymeric or oligomeric compounds, which are useful as in vivo or in vitro diagnostic and therapeutic agents are provided. Also, various methods for producing such compounds are provided. These polymeric or oligomeric compounds are useful in particular as antimicrobial agents, receptor, hormone or enzyme agonists and antagonists.

Abstract: An apparatus and method enables screen printing various articles such as glassware with a radiation curable composition using, for example, UV radiation and the like in pre-existing screen printing decorating equipment having a plurality of screen printing workstations. Particularly suitable compositions are those which are environmentally safe by virtue of being free of toxic heavy metals and volatile organic compounds. The applied inked image is at least partially cured at each screen printing workstation to form a skin on the surface of the transferred image of sufficient strength to support the next layer to be applied. The UV radiation may emanate opposing and underlying each of the screen printing workstations were brought thereto from a remotely positioned laser via a fiber optic bundle or light pipe.

Abstract: An insulated metallic strip suitable for use in the coils of power transformers and method of producing the same. Following the extrusion of a flat metallic strip of conductive material for winding into a magnet coil, the flat strip having a predetermined thickness and first and second sides bounded by a pair of fully rounded edges, the method of insulating the strip of conductive material by supporting the flat strip in a level state at a predetermined temperature in a vacuum chamber and while in the vacuum chamber applying a liquid coating of resin to the entire first side of the strip and the pair of rounded edges and extending onto the second side of the strip from each of the edges a distance at least as great as about 0.25" to prevent turn to turn discharge.

Abstract: Methods and apparatus are provided in which a coating is deposited onto a substrate by a process which includes the following steps: depositing a precursor onto the substrate in a desired pattern; depositing an appropriate ligand onto the substrate; and applying sufficient energy to transfer electrons from the ligand to the precursor, thereby decomposing the precursor to form a precipitate. In one aspect of preferred embodiments, the precursor comprises a metallic salt, and the precipitate comprises a metal. Especially preferred salts are carboxylates, halides, nitrates, and pseudo halides. In another aspect of preferred embodiments, the ligand comprises an amine, an amide, a phosphine, a sulfide, or any other ligand containing nitrogen, phosphorous, sulphur or other donor atoms. In another aspect of preferred embodiments, the energy is supplied at least partially as radiant heat.

Abstract: The present invention is generally directed to a process and a system for transforming a liquid into a solid material using light energy. In particular, a solution containing a parent material in a liquid form is atomized in a reaction vessel and directed towards a substrate. The atomized liquid is exposed to light energy which causes the parent material to form a solid coating on a substrate. The light energy can be provided from one or more lamps and preferably includes ultraviolet light. Although the process of the present invention is well suited for use in many different and various applications, one exemplary application is in depositing a dielectric material on a substrate to be used in the manufacture of integrated circuit chips.

Abstract: A method for forming micron-sized or smaller drops of liquid, and the use of the method in fabricating micro electro mechanical and micro mechanical devices is disclosed. A micropipette is formed having an inside diameter no larger than the size of the drops to be formed. The micropipette is connected to a system capable of developing a positive and optionally negative pressure within the micropipette. The tip of the micropipette is placed in liquid. The liquid is drawn into the micropipette via capillary action or from the negative pressure developed by the system. The micropipette is then positioned to deliver liquid to an intended location on a surface. To deliver the liquid, a positive pressure is developed within the micropipette. The positive pressure forces a micron-sized or smaller drop of liquid out of the micropipette. The method can be used to form micron-sized or smaller drops of adhesive for fixing in place various structural members that form microdevices.

Abstract: This invention relates to a process for applying a coating material comprising a release coating composition or a pressure sensitive adhesive composition to a substrate, the process comprising: (A) atomizing and electrically charging said coating material; and (B) spraying the atomized and charged coating material from step (A) on to a substrate which overlies a grounded support structure. In one embodiment, the coating material sprayed during step (B) is a release coating composition, said process further comprising the additional steps of: (C) curing said release coating composition; (D) atomizing and electrically charging a pressure sensitive adhesive composition; (E) spraying the pressure sensitive adhesive composition from step (D) on to said substrate over the cured release coating composition from step (C); and (F) placing another substrate over the sprayed pressure sensitive adhesive composition from step (E).

Abstract: Sheet materials according to the present invention comprise a sheet material substrate, such as for example a film or paper sheet, with a polymer release coating overlying and adhered to a surface of the sheet material substrate. Single and multilayer release coatings can be formed on the substrate by vapor deposition of silicone acrylates and/or fluorinated acrylates. These coatings can be applied in thickness of 0.05 micron to 1.0 micron to achieve a range of release properties. These coatings can be applied in a very thin single layer on relatively smooth substrates or in a multilayer form on rough substrates such as paper. The new coating process described here has lower process and materials costs, improved adhesion, low slip, and excellent release characteristics.

Abstract: An optical fiber ribbon is manufactured under a condition where, assuming that the optical fiber ribbon has a thickness of 2d (mm), a guide roller has a diameter of 2R (mm), and a period of time till the optical fiber ribbon comes into contact with the guide roller after leaving an ultraviolet irradiation apparatus is t (ms), a relationship of d/?(R+d).times.t!<0.2 is satisfied. Accordingly, no damages are imparted to the optical fiber ribbon, and no micro-bendings occur in its coated optical fibers, whereby the transmission characteristic can be prevented from deteriorating.

Abstract: The present invention relates to several novel compositions and methods employing infrared radiation, microwave radiation or high voltage polymerization for modifying the surfaces of materials to impart desired characteristics thereto. More particularly, the present invention relates to a method for modifying the surfaces of objects to increase the lubricity, hydrophilicity, hydrophobicity, or biofunctionality of the surface of the object.

Abstract: Methods for preparing viscoelastic compositions (e.g., adhesives such as hot melt adhesives) in which a pre-viscoelastic composition (e.g., a pre-adhesive composition) is combined with a packaging material and then polymerized.

Abstract: A composition comprising at least two resins with widely different molecular weights is disclosed. The composition is particularly suitable as a permanent dielectric which provides an optimum surface for plating upon. The composition is particularly useful in the fabrication of printed circuit boards.

Abstract: The present invention provides for a number of interrelated methods for the production of random and ordered arrays of particles as well as films containing the same. In another aspect, the present invention relates to the random and ordered arrays of particles and films prepared therefrom. The ordered arrays are obtained by the use of ferrofluid compositions which may be curable, solidifiable or non-curing/non-solidifiable. Especially preferred arrays and films contain electrically conductive particles for use in electronic applications for effecting contact between leads or pads.

Abstract: The incorporation of a non-thermosettable phenolic tackifying resin surprisingly provides improved solvent free, hot melt processing of hydrocarbon elastomers with crosslinking promoters to form pressure sensitive adhesive tapes. The tapes advantageously have a desirable balance of the properties of resistance to slow rate peel and fast rate peel adhesion.

Abstract: The present invention aims to form a thin coating film of even thickness within a short processing time under a curtailed consumption of coating liquid; where, a gas is spouted from nozzle 4 disposed facing to protection glass 2 of cathode ray tube, and a liquid containing fluorescent material is made to spout accompanied by the spouting gas, to be applied on protection glass 2 by shifting the positioning of protection glass 2 relative to nozzle 4 while spouting the liquid containing fluorescent material.

Abstract: A process for manufacturing an organic electroluminescent device, including the steps of sequentially forming a hole transport layer, a bipolar transport layer at need, and an electron transport layer on a transparent electrode side of a transparent substrate having a transparent electrode. After a recombination region layer for electrons and holes of the transport layers is formed, three kinds of fluorescent pigment R, G and B are applied to an upper surface of the recombination region layer. Subsequently, the kinds of fluorescent pigment are heated to be diffused in the recombination layer so that the kinds of fluorescent pigment and the recombination layer constitute a luminescent layer. An organic electroluminescent device produced by this process is disclosed.

Abstract: Methods of producing release coatings, adhesives, primers, and other polymeric coatings are described. A method for producing a release coating on a substrate comprises the steps of applying a polymerizable composition comprising a free radically polymerizable ethylenically unsaturated polysiloxane to a surface of a substrate, and exposing the polymerizable composition to a monochromatic light source having a peak intensity at a wavelength of between about 160 nanometers to 240 nanometers to form a release coating. Methods for producing a pressure sensitive adhesive and other polymeric coatings using a monochromatic light source are also described.