Fusing, Curing, Or Annealing (e.g., Ceramics, Etc.) Patents (Class 427/559)
  • Patent number: 5436034
    Abstract: Electrolessly deposited metal films having improved adhesion can be obtained by coating the surface of the substrates to be metallized with a formulation consisting of UV-curable varnishes which contain noble metal compounds as activators and, in addition, either fillers or solvents or a combination of fillers and solvents, curing these varnishes by means of UV radiation, followed by electroless metallization of the substrates thus treated.
    Type: Grant
    Filed: December 19, 1994
    Date of Patent: July 25, 1995
    Assignee: Bayer Aktiengesellschaft
    Inventors: Henning Giesecke, Gerhard-Dieter Wolf, Wilfried Haese
  • Patent number: 5427825
    Abstract: A surface of a ceramic article, such as a glazed surface on a whiteware article, is treated with radiant energy such as infrared light from a laser to provide a localized remelting of the material at the surface in a fusing step. After the fusing step, the surface is treated with further radiant energy, desirably over a larger surface encompassing the fused zone and also desirably at a lower power density so as to limit the rate of cooling of the fusion zone and the immediately surrounding regions, thereby preventing thermal stress cracking. The fusion zone and surrounding regions desirably are preheated by additional radiant energy immediately prior to the fusing step so as to further limit thermal stresses during the fusing step. The process can be employed, among many other uses, for repair of glaze defects and for decoration.
    Type: Grant
    Filed: February 9, 1993
    Date of Patent: June 27, 1995
    Assignee: Rutgers, The State University
    Inventor: Daniel E. Murnick
  • Patent number: 5422146
    Abstract: A process of powder coating of workpieces in which initially a workpiece is coated with color powder such that the powder adheres to the workpiece and subsequently the powder is baked in an oven, in which subsequent to coating and prior to baking the powder adhering to the workpiece is irradiated with electromagnetic radiation within a particular, defined surface portion so that the powder within the defined surface portion will gelate and stick to the workpiece, and in which the color powder adhering to the workpiece outside of said defined surface portion is removed subsequent to irradiation.
    Type: Grant
    Filed: July 6, 1994
    Date of Patent: June 6, 1995
    Assignee: Wagner International AG
    Inventor: Horst Adams
  • Patent number: 5411806
    Abstract: The performance of phosphor screens can be improved by coating the phosphor dispersion/mixture onto a substrate while the dispersion/mixture contains less than 5% by weight of polymerizable components with a molecular weight less than 300, preferably with less than 5% by weight of polymerizable components having molecular weights less than 500. The polymerizable composition should be photopolymerizable, and other components within the coating to be photohardened which have molecular weights below 300 or 500 should likewise be kept to less than 5% by weight of the composition.
    Type: Grant
    Filed: October 7, 1994
    Date of Patent: May 2, 1995
    Assignee: Minnesota Mining and Manufacturing Company
    Inventor: John C. Dahlquist
  • Patent number: 5409742
    Abstract: Large area decorations of glazings, ceramic paint or the like on glass ceramic, glass, ceramic or similar meltable substrates, in particular on glass ceramic cooking plates, are applied by the new method by means of a laser beam which is widened linearly over the entire width of the area to be decorated, as it were in a zone melting method. The linear energy supply zone is advanced at a speed high enough for essentially only the decorating material to be melted on or burnt in but ensuring that the thermal conduction front does not move appreciably into the substrate material.
    Type: Grant
    Filed: December 27, 1993
    Date of Patent: April 25, 1995
    Assignee: Schott Glaswerke
    Inventors: Nanning Arfsten, Klaus Kristen, Erich Rodek, Herwig Scheidler, Waldemar Weinberg
  • Patent number: 5403616
    Abstract: Printing is conducted at the transparent conducting film unnecessary portion on a substrate 1 with a masking ink having a higher thermal decomposition temperature than that of the transparent conducting film forming composition, and the ink is dried and cured by heat or light to form a masking pattern 2. The portion where a transparent conducting film is to be formed is preferably subjected to ozone cleaning and then coated with a transparent conducting film forming composition comprising an indium compound and/or a tin compound and a solvent to form a transparent conducting film forming composition layer 3. The thus worked substrate is subjected to a heat treatment, causing thermal decomposition of the masking pattern 2 after formation of a transparent conducting film. Then the residues of the masking ink and the transparent conducting film are removed to finally obtain a desired patterned transparent conducting film 4.
    Type: Grant
    Filed: June 6, 1994
    Date of Patent: April 4, 1995
    Assignee: Matsushita Electric Industrial Co., Ltd.
    Inventors: Akiyoshi Hattori, Yoshihiro Hori, Akihiko Yoshida
  • Patent number: 5391406
    Abstract: This invention is a hot melt pressure sensitive adhesive formed by copolymerizing acrylic, or a combination of acrylic and vinyl, monomers, at least one of which is a photoinitiator, with the functional monomer, 1-(1-isocyanato-1methyl ethyl)-3-(1-methyl ethenyl)benzene (m-TMI), to give a saturated polymer with pendant vinyl groups that are crosslinked by UV radiation.
    Type: Grant
    Filed: March 25, 1994
    Date of Patent: February 21, 1995
    Assignee: National Starch and Chemical Investment Holding Corporation
    Inventors: Roopram Ramharack, Rama Chandran
  • Patent number: 5391408
    Abstract: The method for firing enamel on a metal article (2), subjected to a prior step for depositing, onto part of its surface, an enamel frit slip, followed by a step for obtaining a bisque on said component, comprises a step for exposing the article to infrared radiation of a maximum emission wavelength in a firing chamber (1).
    Type: Grant
    Filed: January 29, 1993
    Date of Patent: February 21, 1995
    Assignee: Seb S.A.
    Inventor: Henri Piera
  • Patent number: 5389408
    Abstract: A method and apparatus is disclosed for curing metal particles into continuous metal conductors on a nonconducting substrate. The apparatus includes a generator for supplying radio frequency energy through an impedance matching circuit to a coil positioned proximate to the substrate. The coil and substrate are placed in a chamber which is evacuated prior to curing and then pressurized with nitrogen gas. The electromagnetic flux lines generate eddy currents in the particles which heat them until at least some melt, thereby converting the metal particles into continuous conductors.
    Type: Grant
    Filed: December 23, 1993
    Date of Patent: February 14, 1995
    Assignee: Printron, Inc.
    Inventor: Burt DeVolk
  • Patent number: 5387442
    Abstract: A method of coating heat sensitive materials with powder paint is described, which is based on repetitive heating cycles of paint coating by radiation example infrared, interspersed with cooling cycles, which there is a temperature difference between the paint coating and substrate such as to allow the filmation and subsequent curing of the paint without damaging the substrate.
    Type: Grant
    Filed: January 15, 1993
    Date of Patent: February 7, 1995
    Assignee: Hoechst Italia S.p.A.
    Inventors: Rolf Kroeger, Konrad Ortlieb, Sergio Gazzea
  • Patent number: 5372858
    Abstract: Methods and apparatus for applying a plastic coating to woven yarn tubing to provide conduit for protecting wiring harnesses and the like. The resulting plastic coating layer is very thin so as to generally follow the contours of the woven yarn tubing, without filling in the valleys, thus minimizing the amount of plastic used. Woven yarn tubing is waterproofed by impregnating with latex sealant, and is continuously pulled by a take-up mechanism along a horizontal axis through a heated die and two treating stations in tandem. Each of the treating stations includes a coating pot containing liquid plastisol material and having a resilient circular exit die through which the tubing exits the coating pot to form a layer of liquid plastisol, and an infrared curing oven which heats the plastisol-coated tubing sufficiently to cure the plastisol layer. The tubing, while coated with uncured plastisol material, is not contacted by any element which would tend to deform the tubing from a circular cross section.
    Type: Grant
    Filed: November 24, 1993
    Date of Patent: December 13, 1994
    Assignee: Loom Products, Inc.
    Inventor: Frank D. Saylor, III
  • Patent number: 5372859
    Abstract: Thin film ferroelectric capacitors (10) comprising a ferroelectric film (18) sandwiched between electrodes (16 and 20) for nonvolatile memory operations are rendered more stable by subjecting the capacitors to an anneal following deposition of the top electrode (20). The anneal is done so as to form the interface (22) between the ferroelectric film and the top electrode. Heating in an air oven, laser annealing, or electron bombardment may be used to form the interface. Heating in an air oven is done at a temperature at least equal to the crystallization temperature of the ferroelectric film. Where the ferroelectric film comprises lead zirconate titanate, annealing is done at about 550.degree. to 600.degree. C. for about 10 to 15 minutes. The formation treatment reduces the magnitude of charge associated with the non-switching pulse in the thin film ferroelectric capacitors. Reduction of this charge leads to significantly more stable nonvolatile memory operations in both digital and analog memory devices.
    Type: Grant
    Filed: October 20, 1992
    Date of Patent: December 13, 1994
    Assignee: The United States of America as represented by the Administrator of the National Aeronautics and Space Administration
    Inventor: Sarita Thakoor
  • Patent number: 5368901
    Abstract: A method for producing a bottom resist for a two-layer O.sub.2 /Reactive Ion Etching system which fulfills all the requirements set for such a resist. A varnish layer of a base polymer containing an aromatic, a cross-linking agent and an acid-forming agent is applied to a substrate. The varnish layer is flood-exposed to release a strong acid from the acid-forming agent in the surface region of the layer. This is followed by thermal curing.
    Type: Grant
    Filed: September 16, 1992
    Date of Patent: November 29, 1994
    Assignee: Siemens Aktiengesellschaft
    Inventors: Rainer Leuschner, Recai Sezi, Michael Sebald
  • Patent number: 5348693
    Abstract: A method and system for making a three dimensional product wherein the size and shape of a plurality of cross-sectional segments of the three dimensional object are determined which when assembled together in a particular sequence form the desired three dimensional shape. Thin layers of material in the shape of each of the cross-sectional segments are applied in the particular sequence in which they form the three dimensional object. The application of each of the layers is much like a lithographic printing process in that a resin may be applied by a roller in the shape of the cross-sectional segments.
    Type: Grant
    Filed: November 12, 1991
    Date of Patent: September 20, 1994
    Assignee: Advanced Cardiovascular Systems, Inc.
    Inventors: Charles S. Taylor, William B. Tiffany, Paul Cherkas, John J. Frantzen, Hilary J. Hampton, Leonard Nanis, Bhupendra O. Shah
  • Patent number: 5340619
    Abstract: Color filter arrays containing one or more colors for liquid crystal displays and other optoelectronic devices are made by using a laser to ablate portions of a coating on either a colored or transparent substrate. Color filter materials are placed into the ablated openings and cured. The number of laser ablated openings in the coated substrate varies, depending on the quantity and types of colors desired.
    Type: Grant
    Filed: October 18, 1993
    Date of Patent: August 23, 1994
    Assignee: Brewer Science, Inc.
    Inventors: Yih-Wen Chen, Terry Brewer, Jeffery Hunninghake, Dan Hawley
  • Patent number: 5334422
    Abstract: A method of forming solder stops on a thick film, comprising a conductive metal and an inorganic oxide, including the step of directing a laser beam onto the film to form a surface consisting essentially of fused inorganic oxides which acts as a solder stop.
    Type: Grant
    Filed: February 5, 1993
    Date of Patent: August 2, 1994
    Assignee: Delco Electronics Corp.
    Inventors: Bruce A. Myers, John K. Isenberg, Christine R. Coapman, James A. Blanton
  • Patent number: 5304404
    Abstract: A method for grafting hydrophilic monomers containing double bonds onto polymer surfaces in aqueous solution.The grafting is activated by ultraviolet radiation and by the presence in suspension of a photoactivator of controlled particle size distribution.
    Type: Grant
    Filed: October 1, 1992
    Date of Patent: April 19, 1994
    Assignee: Istituto Guido Donegani S.p.A.
    Inventors: Marco Morra, Ernesto Occhiello, Fabio Garbassi
  • Patent number: 5242715
    Abstract: In a process for coating or bonding electronic components and subassemblies with reaction resin mixtures that are stable in storage at room temperature as a one-component system for several months, reaction resin mixtures are used, which contain the following components:a cationically hardenable, solvent-free epoxy resin;a triarylsulphonium salt with hexafluorophosphate, -arsenate or -antimonate as anion, with a mass concentration of 0.01 to 5% (relative to epoxy resin); anda benzylthiolanium salt with hexafluorophosphate, -arsenate or -antimonate as anion, with a mass concentration of 0.01 to 5% (relative to epoxy resin);as well as possibly customary additives.These reaction resin mixtures are hardened through UV radiation and thermally.
    Type: Grant
    Filed: February 14, 1992
    Date of Patent: September 7, 1993
    Assignee: Siemens Aktiengesellschaft
    Inventors: Lothar Schoen, Bernhard Stapp, Heiner Bayer, Helmut Markert, Volker Muhrer
  • Patent number: 5234484
    Abstract: A method for annealing a deposited material on a substrate structure, where the annealing temperature of the deposited material is greater than the melting temperature of the substrate structure, including the step of inserting the substrate structure into an oven preheated to a temperature above the annealing temperature. The substrate structure is kept in the oven for a time interval wherein the mean temperature of the deposited material is above the annealing temperature and the mean temperature of the substrate structure is below its melting temperature. The substrate structure may be actively cooled while in the oven, thus increasing the time interval the mean temperature of the deposited material can be maintained above the annealing temperature.
    Type: Grant
    Filed: February 24, 1992
    Date of Patent: August 10, 1993
    Assignee: ITT Corporation
    Inventors: Peter L. Toch, Nils I. Thomas, Thomas E. Sisneros, James Kane
  • Patent number: 5219623
    Abstract: In the manufacture of an article such as optical fiber which includes a light energy cured coating material, fiber (21) is drawn from a preform (22) and coating with one or preferably two layers (42,44) of light curable coating materials. Afterwards, the coating materials are cured. Increases in manufacturing line speed may be achieved if the cure speed of the coating materials is increased. This is accomplished by the simultaneous application of a magnetic field during irradiation of the curable coating materials to enhance the crosslinking of the coating materials by a free radical polymerization mechanism. Upon absorption of light, a photoinitiator in each composition cleaves to produce two free radical fragments in the spin paired or singlet state. The magnetic field has the effect of enhancing the production of spin parallel radicals which enhances the polymerization initiation of the coating material, thereby allowing an increase in the manufacturing line speed through drawing and coating apparatus.
    Type: Grant
    Filed: April 30, 1992
    Date of Patent: June 15, 1993
    Assignee: AT&T Bell Laboratories
    Inventor: James R. Petisce
  • Patent number: 5219622
    Abstract: A method of forming a sheet of material with indicia thereon comprises applying indicia to the sheet by an electrostatic copying process in which a toner powder is deposited on the sheet and is heated to cause it to fuse. The sheet of material comprises a flexible support layer that is provided with a porous coating of a latent curable material, preferably in particulate and/or filamentary form and especially one based on an epoxy material.It has been found that the indicia are more indelible than those formed on other surfaces by the same process even though the fused toner is not absorbed by the curable material.
    Type: Grant
    Filed: April 9, 1992
    Date of Patent: June 15, 1993
    Assignee: Raychem GmbH
    Inventor: Waldemar Meier
  • Patent number: 5203929
    Abstract: An amorphous magnetic film is produced by irradiating laser beams onto a magnetic metallic target and depositing an evaporated material on a substrate. During or after the evaporation process, the film formed on the substrate is annealed at a temperature lower than a crystallization temperature. The annealing process enables elimination of stresses from the film, thereby improving soft magnetic properties.
    Type: Grant
    Filed: June 26, 1991
    Date of Patent: April 20, 1993
    Assignee: Toyota Jidosha Kabushiki Kaisha
    Inventors: Noboru Takayanagi, Kazuhiro Akihama