Loose Particulate Mixture (i.e., Composition) Containing Metal Particles Patents (Class 75/255)
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Patent number: 7776442Abstract: A nanoparticle powder of silver has an average particle diameter measured by TEM observation (DTEM) of 30 nm or less, an aspect ratio of less than 1.5, an X-ray crystallite size (Dx) of 30 nm or less, a degree of single crystal grain {(DTEM)/(Dx)} of 5.0 or less, and a CV value {100×standard deviation (?)/number average diameter (DTEM)} of less than 40%. The nanoparticle powder of silver has adhered to the particle surface thereof an organic protective agent having a molecular weight of 100 to 400. The nanoparticle powder is obtained by subjecting a silver salt to reduction treatment at a temperature of 85 to 150° C. in an alcohol having a boiling point of 85 to 150° C. and in the co-presence of an organic protective agent.Type: GrantFiled: February 1, 2006Date of Patent: August 17, 2010Assignee: Dowa Electronics Materials Co., Ltd.Inventor: Kimitaka Sato
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Patent number: 7767035Abstract: A metallic magnetic material for magnetic element for magnetic element of a choke coil and an SMD choke power coil for accommodating low voltage and high current in a personal computer, graphic card, high frequency power supply, etc, is prepared by baking a powder of Fe—Si—Al alloy sendust, obtained by an atomization process and having an average particle diameter of 10 to 70 ?m, at 600° C. to 1000° C. in air or in an oxidizing atmosphere and mixing the baked sendust with 3 to 45 wt % of a carbonyl iron powder with an average particle diameter of 1 to 10 ?m. The metallic magnetic material for magnetic element according to the present invention is used in a coil-embedded SMD power choke coil having a square or rectangular shape with a height of 1 mm to 7 mm and with a length of one side being 3 mm to 13 mm.Type: GrantFiled: November 30, 2007Date of Patent: August 3, 2010Assignee: Sekisin Industry Co., Ltd.Inventors: Namio Sato, Yotaro Toyoshima, Katsutoshi Yamamoto
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Publication number: 20100190025Abstract: A most preferred composition for the mixture, prior to sintering into an article (ideally a valve seat insert), is as follows: 35% hard phase, 65% matrix (excepting incidental impurities), the hard phase component being 2.2% C, 29.1% Cr, 4.9% Co, 5.3% Ni, 20.2% W with the balance being Fe and allowing less than 2% for one or more machinability aids and solid lubricants, and the matrix component being one of a high chrome steel powder (e.g. 18% Cr, 1% Ni, 2.5% Mo, balance Fe), a low alloy steel powder (3% Cu, 1% C, balance Fe; 3% Cr, 0.5% Mo, 1% C, balance Fe; 4% Ni, 1.5% Cu, 0.5% Mo, 1% C, balance Fe; 4% Ni, 2% Cu, 1.4% Mo, 1% C, balance Fe), or a tool steel powder (5% Mo, 6% W, 4% Cr, 2% V, 1% C, balance Fe), or a low-alloy steel powder as above but which issued in conjunction with a copper infiltration process during sintering.Type: ApplicationFiled: August 9, 2007Publication date: July 29, 2010Applicant: FEDERAL-MOGUL SINTERED PRODUCTS LIMITEDInventors: Leslie John Farthing, Paritosh Maulik
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Publication number: 20100180948Abstract: Provided are a paste composition which is capable of sufficiently achieving at least a BSF effect equivalent to or greater than a conventionally achieved BSF effect even when the paste composition is used in either case where a thick back surface electrode layer is formed on a thick silicon semiconductor substrate or where a thin back surface electrode layer is formed on a thin silicon semiconductor substrate and which is capable of not only achieving the BSF effect equivalent to or greater than the conventionally achieved BSF effect but also suppressing a deformation of the silicon semiconductor substrate after being fired when the paste composition is used in the case where the thin back surface electrode layer is formed on the thin silicon semiconductor substrate; and a solar cell element comprising an electrode formed by using the above-mentioned paste composition.Type: ApplicationFiled: April 7, 2008Publication date: July 22, 2010Inventors: Gaochao Lai, Yutaka Ochi, Yoshiteru Miyazawa, Takashi Watsuji, Haruzo Katoh
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Patent number: 7754644Abstract: The present invention provides a noble metal particle with an improved methanol-oxidation property. This noble metal particle has a platinum particle and ruthenium particles deposited on only part of the surface of the platinum particle. This noble metal particle suitably can be produced by precipitating the ruthenium particles out of the solution so that the ruthenium particles are deposited on only part of the surface of the platinum particle by further adding a ruthenium salt into the solution and reducing the ruthenium salt after the reduction of the platinum salt in the solution essentially is completed. This noble metal particle is suitable as a catalyst to be supported on an electrode of a polymer electrolyte fuel cell typified by a direct methanol fuel cell.Type: GrantFiled: September 1, 2006Date of Patent: July 13, 2010Assignee: Nippon Sheet Glass Company, LimitedInventor: Ryohei Ogawa
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Publication number: 20100154590Abstract: A process for producing refractory metal alloy powders includes the steps of blending at least one powder with at least one solvent and at least one binder to form a slurry; forming a plurality of agglomerates from the slurry; screening the plurality of agglomerates; sintering the plurality of agglomerates; and melting said plurality of agglomerates to form a plurality of homogenous, densified powder particles.Type: ApplicationFiled: December 23, 2008Publication date: June 24, 2010Applicant: UNITED TECHNOLOGIES CORPORATIONInventors: James F. Myers, Scott Ohm
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Patent number: 7740683Abstract: The present invention relates to metal powders mixtures which are intended for manufacturing precious metal products which have special designs and complex geometries, also including those which consist of several uninterrupted parts which are indivisibly but flexibly coupled to each other. From the powder mixture jewelry and other objets d'art are manufactured by making use of free form fabrication (FFF) technique. The invention also comprises jewelry and other ornamental products which are manufactured from the powder material in question using the FFF technique.Type: GrantFiled: June 19, 2006Date of Patent: June 22, 2010Assignee: EOS GmbH Electro Optical SystemsInventors: Lena Thorsson, Allan Hede, Björn Eklund
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Publication number: 20100150822Abstract: The present invention relates to pulverulent materials suitable for storing hydrogen, and more particularly to a method of preparing such a material, in which: (A) a composite metallic material having a specific granular structure is prepared by co-melting the following mixtures: a first metallic mixture (m1), which is an alloy (a1) of body-centred cubic crystal structure, based on titanium, vanadium, chromium and/or manganese, or a mixture of these metals in the proportions of the alloy (a1); and a second mixture (m2), which is an alloy (a2), comprising 38 to 42% zirconium, niobium, molybdenum, hafnium, tantalum and/or tungsten and 56 to 60 mol % of nickel and/or copper, or else a mixture of these metals in the proportions of the alloy (a2), with a mass ratio (m2)/(m1+m2) ranging from 0.1 wt % to 20 wt %; and (B) the composite metallic material thus obtained is hydrogenated, whereby the composite material is fragmented (hydrogen decrepitation).Type: ApplicationFiled: February 22, 2007Publication date: June 17, 2010Applicant: Centre National De La Recherche Scientifique (C.N. R.S.)Inventors: Jean Charbonnier, Patricia De Rango, Daniel Fruchart, Salvatore Miraglia, Sophie Rivoirard, Natalia Skryabina
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Patent number: 7727303Abstract: Provided are non-magnetic nickel powders and a method for preparing the same. The nickel powders are non-magnetic and have a HCP crystal structure. An exemplary method includes (a) dispersing nickel powders with a FCC crystal structure in an organic solvent to prepare a starting material dispersion, and (b) heating the starting material dispersion to transform the nickel powders with the FCC crystal structure to the nickel powders with the HCP crystal structure. The nickel powders do not exhibit magnetic agglomeration or aggregation phenomenon. Therefore, exemplary pastes for inner electrode formation in various electronic devices, which contain the nickel powders of the present disclosure, can be provided in a relatively uniform, well-dispersed state because of the reduced aggregation and agglomeration of the nickel powder. Also, inner electrodes made of the nickel powders can have a low impedance value even at high frequency band.Type: GrantFiled: February 26, 2007Date of Patent: June 1, 2010Assignee: Samsung Electronics Co., Ltd.Inventors: Soon-ho Kim, Jae-young Choi, Tae-wan Kim, Eun-bum Cho, Young-kyun Lee
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Patent number: 7718843Abstract: An iron powder for decomposition of organic chlorinated compounds, comprising from 0.03 to 0.5% by weight of Ni and from 0.005 to 5% by weight of carbon, wherein particles having a particle size of less than 53 ?m occupies less than 40% by weight, is used. It is particularly preferable that Ni, carbon and iron are partially alloyed. When the iron powder for decomposition is used by mixing with, for example, an Ni-free iron powder, the total Ni content can be reduced without deterioration of decomposition performance to organic chlorinated compounds. The iron powder has high decomposition performance in the treatment of a solid such as soil.Type: GrantFiled: July 17, 2007Date of Patent: May 18, 2010Assignee: Tosoh CorporationInventors: Yoju Shimizu, Yasuyuki Nagai
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Patent number: 7713328Abstract: There are disclosed metallic colloid particles containing platinum fine particles wherein platinum colloid particles are supported on the surfaces of gold colloid particles, and the platinum fine particles have an average particle diameter of at most 5 nm; a process for producing the metallic colloid particles; a metallic corpuscular carrying body wherein the above metallic colloid particles are supported on a carrier and a process for producing the carrying body. The resultant metallic colloid particles, which have higher sensitivity, are well suited as a label for immunological measurement and protein-staining agent for various proteins.Type: GrantFiled: February 16, 2005Date of Patent: May 11, 2010Assignees: Nippon Sheet Glass Co., Ltd., BL KKInventors: Kiyoshi Miyashita, Ryohei Ogawa, Masamichi Kezuka
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Patent number: 7704315Abstract: Aqueous dispersion containing a metal oxide powder with a fine fraction and a coarse fraction, in which—the metal oxide powder is silicon dioxide, aluminum oxide, titanium dioxide, zirconium dioxide, cerium oxide or a mixed oxide of two or more of the aforementioned metal oxides,—the fine fraction is present in aggregated form and has a mean aggregate diameter in the dispersion of less than 200 nm,—the coarse fraction consists of particles with a mean diameter of 1 to 20 ?m, —the ratio of fine fraction to coarse fraction is 2:98 to 30:70, and—the content of metal oxide powder is 50 to 85 wt. %, referred to the total amount of the dispersion. The aqueous dispersion is produced by a process comprising the steps:—production of a fine fraction dispersion by dispersing the pulverulent fine fraction in water by means of an energy input of at least 200 KJ/m3?, and—introducing the coarse fraction in the form of a powder into the fine fraction dispersion under dispersing conditions at a low energy input.Type: GrantFiled: July 19, 2005Date of Patent: April 27, 2010Assignee: Degussa AGInventors: Monika Oswald, Corinna Kissner, Roland Weiss, Andreas Lauer
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Patent number: 7691175Abstract: When fine metal particles of a nanometer size are handled in a state of colloidal particles, it is difficult to handle them and the range of the selection of the solvent to be used is limited. The invention offers a granular metal powder that is produced by the steps of (a) preparing a suspension liquid comprising (a1) water, an organic solvent, or a mixture thereof, (a2) metal particles having an average particle diameter of at least 1 nm and at most 100 nm, and (a3) an organic compound capable of being adsorbed on the surface of the metal particles and (b) removing the water, organic solvent, or mixture thereof by drying the suspension liquid and that has an apparent density of at least 1.0 g/ml and at most 5.0 g/ml. The granular metal powder can be handled as a dry metal powder and is readily redispersed in a solvent.Type: GrantFiled: June 24, 2004Date of Patent: April 6, 2010Assignee: Sumitomo Electric Industries, Ltd.Inventors: Kohei Shimoda, Issei Okada, Masatoshi Majima
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Publication number: 20100077887Abstract: The invention is directed to a formulation containing at least one hard material powder and at least 2 binder metal powders. The formulation is characterized in that the cobalt is completely contained in the first binder metal powder and is prealloyed with one or more elements of groups 3 to 8 of the Periodic Table of the Elements which are elements of the fourth period and at least one further binder metal powder from the group consisting of powders of the elements Fe, Ni, Al, Mn, Cr and alloys of these elements with one another is present and the further binder metal powders do not contain any cobalt in unprealloyed form. The invention further relates to the use of the inventive formulation in a cemented hard material, a porous sintered agglomerate and a thermal spray powder. The invention also relates to a method of controlling the toxic effect of cobalt-containing metal formulation by utilizing the inventive formulation.Type: ApplicationFiled: January 25, 2008Publication date: April 1, 2010Applicant: H.C. Starck GmbHInventors: Frank Schrumpf, Benno Gries, Kai-Uwe Clauswitz, Bernd Mende
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Patent number: 7678175Abstract: High purity refractory metals, valve metals, refractory metal oxides, valve metal oxides, or alloys thereof suitable for a variety of electrical, optical and mill product/fabricated parts usages are produced from their respective oxides by metalothermic reduction of a solid or liquid form of such oxide using a reducing agent that establishes (after ignition) a highly exothermic reaction, the reaction preferably taking place in a continuously or step-wise moving oxide such as gravity fall with metal retrievable at the bottom and an oxide of the reducing agent being removable as a gas or in other convenient form and unreacted reducing agent derivatives being removable by leaching or like process.Type: GrantFiled: November 1, 2006Date of Patent: March 16, 2010Assignee: H.C. Starck Inc.Inventors: Leonid N. Shekhter, Terrance B. Tripp, Leonid L. Lanin, Anastasia M. Conlon, Howard V. Goldberg
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Patent number: 7670581Abstract: A method for the production of a robust, chemically stable, crystalline, passivated nanoparticle and composition containing the same, that emit light with high efficiencies and size-tunable and excitation energy tunable color. The methods include the thermal degradation of a precursor molecule in the presence of a capping agent at high temperature and elevated pressure. A particular composition prepared by the methods is a passivated silicon nanoparticle composition displaying discrete optical transitions.Type: GrantFiled: June 4, 2008Date of Patent: March 2, 2010Inventors: Brian A. Korgel, Keith P. Johnston
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Patent number: 7670588Abstract: Hydrogen is stored by adsorbing the hydrogen to a carbon nanomaterial that includes carbon nanospheres. The carbon nanospheres are multi-walled, hollow carbon nanostructures with a maximum diameter in a range from about 10 nm to about 200 nm. The nanospheres have an irregular outer surface and an aspect ratio of less than 3:1. The carbon nanospheres can store hydrogen in quantities of at least 1.0% by weight.Type: GrantFiled: September 5, 2007Date of Patent: March 2, 2010Assignee: Headwaters Technology Innovation, LLCInventors: Bing Zhou, Cheng Zhang
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Publication number: 20100037951Abstract: Disclosed are methods of making multi-element, finely divided, metal powders containing one or more reactive metals and one or more non-reactive metals. Reactive metals include metals or mixtures thereof from titanium (Ti), zirconium (Zr), hafnium (Hf), tantalum (Ta), niobium (Nb), vanadium (V), nickel (Ni), cobalt (Co), molybdenum (Mo), manganese (Mn), and iron (Fe). Non-reactive metals include metals or mixtures such as silver (Ag), tin (Sn), bismuth (Bi), lead (Pb), antimony (Sb), zinc (Zn), germanium (Ge), phosphorus (P), gold (Au), cadmium (Cd), berrylium (Be), tellurium (Te).Type: ApplicationFiled: August 12, 2009Publication date: February 18, 2010Applicant: E. I. DU PONT DE NEMOURS AND COMPANYInventors: William J. Borland, Howard David Glicksman
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Publication number: 20100028194Abstract: A method for protecting powder metallurgy alloy elements from oxidation and/or hydrolyzation during sintering. The method includes (1) coating the admixed alloy elements in an inert (e.g., nitrogen) atmosphere with a hydrophobic lubricant that is capable of becoming mobile during pressing, the amount of lubricant being at least 45% of the total volume of all components to be added to the base metal powder; (2) mixing the lubricant-coated admixed alloy elements with the base metal powder to form a mixture; (3) pressing the mixture to form a pre-sintered part having a green density that is from about 95% to about 98% of a calculated pore-free density; and (4) sintering the part.Type: ApplicationFiled: August 4, 2009Publication date: February 4, 2010Applicant: APEX ADVANCED TECHNOLOGIES, LLCInventors: Dennis L. Hammond, Richard Phillips
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Patent number: 7655214Abstract: Valve metal suboxides having a primary suboxide phase and optionally a secondary suboxide phase, a valve metal phase, and/or at least one tertiary suboxide phase can be present in varying amounts. Also disclosed is anodes and capacitors containing the valve metal suboxides of the present invention. Also, a method to prepare a valve metal suboxide is further described which includes granulating one or more of the starting materials individually or together and/or granulating the final product.Type: GrantFiled: February 25, 2004Date of Patent: February 2, 2010Assignee: Cabot CorporationInventors: David M. Reed, Sridhar Venigalla, Jeffrey A. Kerchner
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Patent number: 7651782Abstract: The present invention provides a method for producing metallic nanoparticles, which includes reacting a copper compound with a hydrazine reducing agent in an organic solvent in the presence of a precious metal compound, wherein the precious metal compound is a compound containing at least one precious metal selected from the group consisting of platinum, gold, silver, and palladium, and the total number of precious metal atoms in the precious metal compound is in the range of 1 to 10 at. % of the total copper atoms in the copper compound.Type: GrantFiled: July 9, 2007Date of Patent: January 26, 2010Assignee: FUJIFILM CorporationInventors: Masashi Shirata, Hiroyuki Hirai
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Patent number: 7641985Abstract: A boron-free and silicon-free bonding alloy (16) for joining with a superalloy base material (12, 14). The bonding alloy includes aluminum in a concentration that is higher than the concentration of aluminum in the base material in order to depress the melting temperature for the bonding alloy to facilitate liquid phase diffusion bonding without melting the base material. The concentration of aluminum in the bonding alloy may be at least twice that of the concentration of aluminum in the base material. For joining cobalt-based superalloy materials that do no contain aluminum, the concentration of aluminum in the bonding alloy may be at least 5 wt. %.Type: GrantFiled: June 21, 2004Date of Patent: January 5, 2010Assignee: Siemens Energy, Inc.Inventor: Vasudevan Srinivasan
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Patent number: 7637982Abstract: A group of powders (40) for making a wick structure of a heat pipe includes main powders (50) and supplemental powders (60). The melting point of the supplemental powder is lower than that of the main powder. During a sintering process, the powders are filled in a casing of the heat pipe and have a eutectic reaction between the main powders and the supplemental powders to form the wick structure. The temperature for the eutectic reaction is lower than the melting temperature of the supplemental powders.Type: GrantFiled: June 15, 2006Date of Patent: December 29, 2009Assignee: Foxconn Technology Co., Ltd.Inventors: Chuen-Shu Hou, Tay-Jian Liu, Chao-Nien Tung
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Publication number: 20090293673Abstract: Acid mine drainage is treated to form a wet meal-containing precipitate. Such wet metal containing precipitate is dried and processed to form a powder which contains one or more metals. The powder (alone or in combination with other metal powders or other additives) is then compressed (e.g., pressed in a die, rolled, extruded) and sintered to form a desired sintered metal article. In some embodiments, the sintered metal article may be subjected to one or more secondary processes (e.g., oil impregnation, resin impregnation, metal infiltration, copper infiltration, heat treating, steam oxidizing, plating and secondary machining) to alter the strength, configuration or other property of the pressed metal article.Type: ApplicationFiled: May 4, 2009Publication date: December 3, 2009Applicant: Saint Marys Pressed Metals, Inc.Inventor: James R. Aiello
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Patent number: 7625421Abstract: Novel forms of molybdenum metal. Novel forms of molybdenum metal are characterized by a surface area of substantially about 2.1 m2/g to substantially about 4.1 m2/g. Novel forms of molybdenum metal are also characterized by a relatively uniform size.Type: GrantFiled: November 8, 2006Date of Patent: December 1, 2009Assignee: Cyprus Amax Mineral CompanyInventors: Mohamed H. Kahn, Joel Taube, Loyal M. Johnson, Jr.
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Patent number: 7625420Abstract: Copper metal powders, methods for producing copper metal powders and products incorporating the powders. The copper metal powders have a small particle size, narrow size distribution and a spherical morphology. The method includes forming the metal particles in a continuous manner.Type: GrantFiled: February 24, 1998Date of Patent: December 1, 2009Assignee: Cabot CorporationInventors: Toivo T. Kodas, Mark J. Hampden-Smith, James Caruso, Daniel J. Skamser, Quint H. Powell, Clive D. Chandler
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Patent number: 7622010Abstract: A method of making a rare-earth alloy granulated powder according to the present invention includes the steps of: preparing a rare-earth alloy powder; generating remanent magnetization in the powder; and granulating the powder by utilizing agglomeration force produced by the remanent magnetization of the powder. Since the agglomeration force produced by the remanent magnetization is utilized, the addition of a granulating agent may be omitted.Type: GrantFiled: November 27, 2002Date of Patent: November 24, 2009Assignee: Hitachi Metals, Ltd.Inventors: Futoshi Kuniyoshi, Tomoiku Otani
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Publication number: 20090282948Abstract: Methods for forming nanostructures of various shapes are disclosed. Nanocubes, nanowires, nanopyramids and multiply twinned particles of silver may by formed by combining a solution of silver nitrate in ethylene glycol with a solution of poly(vinyl pyrrolidone) in ethylene glycol. Hollow nanostructures may be formed by reacting a solution of solid nanostructures comprising one of a first metal and a first metal alloy with a metal salt that can be reduced by the first metal or first metal alloy. Nanostructures comprising a core with at least one nanoshell may be formed by plating a nanostructure and reacting the plating with a metal salt.Type: ApplicationFiled: July 27, 2009Publication date: November 19, 2009Applicant: The University of WashingtonInventors: Younan Xia, Yugang Sun
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Publication number: 20090285712Abstract: The present invention relates to a metal powder mixture that is suitable for producing sintered bodies. The powder mixture is suitable as a binder for hard metals and contains: a) at least one prealloyed powder selected from the group of iron/nickel, iron/cobalt, iron/nickel/cobalt and nickel/cobalt; b) at least one element powder selected from the group of iron, nickel and cobalt or a prealloyed powder selected from the group consisting of iron/nickel, iron/cobalt, iron/nickel/cobalt and nickel/cobalt which is different from component a). The invention also relates to a cemented hard material which uses the inventive powder mixture and a hard material powder, wherein the overall composition of the components a) and b) together contains not more than 90% by weight of cobalt and not more than 70% by weight of nickel and the iron content.Type: ApplicationFiled: September 21, 2007Publication date: November 19, 2009Applicant: H.C. Starck GmbHInventors: Benno Gries, Leo Prakash
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Patent number: 7618475Abstract: A metal powder for a conductive paste has an average particle diameter D50 not greater than 5 ?m and an X value defined by equation (1) not greater than 0.5: X value=D50 (?m)/BET specific surface area (m2/g)??(1) The metal powder for a conductive paste is particularly preferable when wart-like projections of a diameter not greater than 150 nm are present on the particle surfaces. Typical types of the metal powder include Cu, Ag, Au, Pd, Pt, Ni, Al and alloys thereof. The metal powder for a conductive paste enables fabrication of a conductor having a low void ratio after the paste is fired.Type: GrantFiled: January 27, 2006Date of Patent: November 17, 2009Assignee: Dowa Electronics Materials Co., Ltd.Inventors: Hiroyuki Yamashina, Hidefumi Fujita, Tatsuya Ibaraki
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Publication number: 20090277301Abstract: The invention relates to mixtures of metal, alloy or composite powders which have a mean particle diameter D50 of not more than 75 ?m, preferably not more than 25 ?m, and are produced in a process in which a starting powder is firstly deformed to give platelet-like particles and these are then comminuted in the presence of milling aids together with further additives and also the use of these powder mixtures and shaped articles produced therefrom.Type: ApplicationFiled: July 9, 2007Publication date: November 12, 2009Applicant: H.C. Starck GmbHInventors: Roland Scholl, Ulf Waag, Aloys Eiling
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Patent number: 7604679Abstract: An efficient process for producing fine nickel powder, capable of metallizing the powder at low temperature to prevent its sintering, and fine nickel powder produced by the process, composed of particles having a flat shape, diameter of limited variations and uniform thickness, and suitable for internal electrodes for laminate ceramic capacitors of high electric capacity. The process comprises a step for forming a nickel compound coated with gelatin by adsorbing gelatin on preformed nickel compound particles with different size and shape (Step (A)), and another step for converting said nickel compound coated with gelatin into fine particles containing metallic nickel and nickel oxide by heating the nickel compound coated with gelatin produced in Step (A) in an inert gas atmosphere (Step (B)). It may include an additional step (Step (C)), subsequent to Step (B), for completely reducing nickel oxide in said fine particles by heating at temperature lower than that for Step (B) in a reducing gas atmosphere.Type: GrantFiled: November 4, 2005Date of Patent: October 20, 2009Assignee: Sumitomo Metal Mining Co., Ltd.Inventors: Yasumasa Hattori, Egon Matijevic
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Publication number: 20090255981Abstract: The invention relates to a method for repairing components that consist of a superalloy. The method comprises the following steps: a solder material is applied to the repair site; the repair site with the applied solder material is heated until the latter melts; and the melted solder material is left to solidify. A powder blend, whose average composition corresponds to the component alloy constitutes the solder material, the blend comprising at least one elementary powder of the component alloy as one powder type and/or a pre-alloy of the component alloy.Type: ApplicationFiled: November 27, 2006Publication date: October 15, 2009Inventors: Robert Singer, Andreas Volek
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Patent number: 7601229Abstract: A method for making soft magnetic material includes: a first heat treatment step applying a temperature of at least 400 deg C. and less than 900 deg C. to metal magnetic particles; a step for forming a plurality of compound magnetic particles in which said metal magnetic particles are surrounded by insulation film; and a step for forming a shaped body by compacting a plurality of compound magnetic particles. This provides a method for making soft magnetic material that provides desired magnetic properties.Type: GrantFiled: October 1, 2004Date of Patent: October 13, 2009Assignee: Sumitomo Electric Industries Ltd.Inventors: Haruhisa Toyoda, Hirokazu Kugai, Kazuhiro Hirose, Naoto Igarashi, Takao Nishioka
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Publication number: 20090252638Abstract: The invention relates to the cost-effective manufacture of near-net shape titanium articles from sintered powders containing titanium and all required alloying elements. The cost-effective initial powder composition for subsequent room temperature consolidation and sintering contains: (a) 10-50 wt. % of underseparated titanium powder with ?500 ?m in particle size manufactured from underseparated titanium sponge comprising up to 2 wt. % of chlorine and up to 2 wt. % of magnesium. The underseparated titanium powder costs significantly less than that for fully separated powder of completely reduced sponge; (b) 10-90 wt. % of hydrogenated titanium powder, whereby this powder is a mixture of two hydrogenated powders A and B containing different amount of hydrogen: powder A contains amount of hydrogen in the range of 0.2-1 wt. % and powder B contains amount of hydrogen in the range of 2-3.9 wt. %.Type: ApplicationFiled: June 11, 2007Publication date: October 8, 2009Inventors: Volodymyr A. Duz, Orest M. Ivasishin, Vladimir S. Moxson, Dmitro G. Savvakin, Vladislav V. Telin
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Publication number: 20090252634Abstract: The invention relates to mixtures of metal, alloy or composite powders which have a mean particle diameter D50 of not more than 75 ?m, preferably not more than 25 ?m, and are produced in a process in which a starting powder is firstly deformed to give platelet-like particles and these are then comminuted in the presence of milling aids together with further additives and also the use of these powder mixtures and shaped articles produced therefrom.Type: ApplicationFiled: July 9, 2007Publication date: October 8, 2009Inventors: Roland Scholl, Ulf Waag, Aloys Eiling
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Patent number: 7594947Abstract: A niobium powder comprising at least one element selected from the group consisting of chromium, molybdenum, tungsten, boron, aluminum, gallium, indium, thallium, cerium, neodymium, titanium, rhenium, ruthenium, rhodium, palladium, silver, zinc, silicon, germanium, tin, phosphorus, arsenic, bismuth, rubidium, cesium, magnesium, strontium, barium, scandium, yttrium, lanthanum, praseodymium, samarium, europium, gadolinium, terbium, dysprosium, holmium, erbium, thulium, ytterbium, lutetium, hafnium, vanadium, osmium, iridium, platinum, gold, cadmium, mercury, lead, selenium and tellurium; a sintered body of the niobium powder; and a capacitor comprising a sintered body as one electrode, a dielectric material formed on the surface of the sintered body, and counter electrode provided on the dielectric material.Type: GrantFiled: January 13, 2003Date of Patent: September 29, 2009Assignee: Showa Denko K.K.Inventors: Kazuhiro Omori, Kazumi Naito
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Patent number: 7582147Abstract: A liquid coating composition including a coating vehicle and composite powder particles disposed within the coating vehicle. Each composite powder particle may include a magnesium component, a zinc component, and an indium component.Type: GrantFiled: August 18, 2005Date of Patent: September 1, 2009Assignee: The United States of America as represented by the Administrator of the National Aeronautics and Space AdministrationInventors: Donald S. Parker, Louis G. MacDowell
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Patent number: 7569115Abstract: Assemblages of particles of a magnetic alloy that are suited to magnetic recording are represented by the formula [TXM1-X] containing T and M in a composition ratio where X in the formula is in the range from 0.3 or greater to 0.7 or less, where T is one or two members of the group consisting of Fe and Co and M is one or two members of the group consisting of Pt and Pd, and metallic elements other than T and M that constitute no more than 30 at. % (including 0 at. %) of (T+M) as a percentage of atoms, and the remainder consists of impurities that are unavoidable from a production standpoint, wherein: the face-centered tetragonal fraction is 10-100%, the average grain size as measured by TEM observation (DTEM) is in the range from 5-30 nm, the x-ray crystal grain size derived by x-ray diffraction (DX) is no less than 4 nm, the particles of are dispersed from each other at a distance, and the dispersion on the composition of the individual particles is kept within a stipulated range.Type: GrantFiled: July 30, 2004Date of Patent: August 4, 2009Assignee: Dowa Electronics Materials Co., Ltd.Inventor: Kimitaka Sato
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Patent number: 7569164Abstract: A solder paste composition used in a solder precoating method of forming solder bumps by forming a dam around electrodes on a substrate, filling a solder paste composition on the electrodes within opening parts surrounded by the dam, and heating the solder paste composition filled, so that solder is adhered to the surfaces of the electrodes. The solder paste composition contains solder powder, which is of a particle size distribution in which particles having a particle size of below 10 ?m are present 16% or more, and a sum of the particles having a particle size of below 10 ?m and particles having a particle size of 10 ?m or more and below 20 ?m is 90% or more. This enables to suppress occurrence of bump defects, and form solder bumps of a uniform height with a high yield by a solder precoating method using the dam.Type: GrantFiled: January 29, 2007Date of Patent: August 4, 2009Assignee: Harima Chemicals, Inc.Inventors: Hitoshi Sakurai, Yoichi Kukimoto
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Publication number: 20090165595Abstract: The invention provides a hard-particle powder for sintered body, which contains, by mass %, 2% to 3.5% of Si, 6% to 10% of Cr, 20% to 35% of Mo, 0.01% to 0.5% of REM, and the remainder being Co and unavoidable impurities. The invention further provides a sintered body obtained through a mixing step of mixing the above-mentioned hard-particle powder for sintered body with a pure iron powder and a graphite powder to obtain a powder mixture, a forming step of compacting the powder mixture to obtain a compact, and a sintering step of sintering the compact. The hard-particle powder according to the invention has the effect of giving a sintered body having improved wear resistance without substantially impairing powder characteristics and sintering characteristics. Additionally, the sintered body according to the invention has the effect of having excellent wear resistance.Type: ApplicationFiled: December 19, 2008Publication date: July 2, 2009Applicant: DAIDO TOKUSHUKO KABUSHIKI KAISHAInventors: Tomomi Yamamoto, Seiji Kurata
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Patent number: 7550513Abstract: It is to provide fine particles of copper, nickel or palladium hydride having an average particle diameter of at most 50 nm, which are hardly oxidized in the atmosphere and are excellent in storage stability and are thereby very suitable for formation of metallic materials, and their production process. Further, it is to provide a dispersion containing fine particles of copper, nickel or palladium hydride, which is excellent in storage stability, and a metallic material obtained by applying the dispersion, followed by baking. The fine particles of copper, nickel or palladium hydride and the dispersion thereof, to be obtained by the present invention, are applicable to various applications, and they can be used for e.g. formation and repair of printed wiring, etc. employing a dispersion, interlayer wiring in semiconductor packages, and joining of printed wiring boards and electronic components.Type: GrantFiled: December 8, 2005Date of Patent: June 23, 2009Assignee: Asahi Glass Company, LimtedInventors: Hideyuki Hirakoso, Keisuke Abe, Yasuhiro Sanada, Kentarou Tsunozaki
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Patent number: 7534490Abstract: In various aspects provided are methods for producing a nanoparticle within a cross-linked, collapsed polymeric material. In various embodiments, the methods comprise (a) providing a polymeric solution comprising a polymeric material; (b) collapsing at least a portion of the polymeric material about one or more precursor moieties; (c) cross-linking the polymeric material; (d) modifying at least a portion of said precursor moieties to form one or more nanoparticles and thereby forming a composite nanoparticle.Type: GrantFiled: September 23, 2008Date of Patent: May 19, 2009Assignee: Northern Nanotechnologies, Inc.Inventors: Cynthia M. Goh, Jose Amado Dinglasan, Jane B. Goh, Richard Loo, Emina Veletanlic
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Patent number: 7534282Abstract: A sintered sputtering target for forming a high purity metal Mo thin film having a remarkably little particle generation is provided. A high purity metal Mo coarse powder as a raw material is provided for making this target. The sintered sputtering target has a theoretical density ratio of 98% or more. The target is obtained by sintering the high purity metal Mo coarse powder. This particle powder has the high purity of 99.99 or more % by mass and an average particle diameter of 5.5 to 7.5 ?m.Type: GrantFiled: September 10, 2004Date of Patent: May 19, 2009Assignee: Japan New Metals Co., Ltd.Inventors: Masayuki Ibaraki, Kenji Iwamoto
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Patent number: 7531022Abstract: A liquid for the preparation of powder mixtures on the basis of hard metals, comprising water and an inhibitor, wherein the inhibitor is in the form of at least one of the following materials: polyvinyllactam or wax emulsion, or the inhibitor is in the form of at least one of the following materials: carboxylic acid, amines or their derivatives.Type: GrantFiled: October 13, 2005Date of Patent: May 12, 2009Assignee: Zschimmer & Schwarz GmbH & Co. KG Chemische FabrikenInventors: Peter Quirmbach, Michael Hölzgen, Alfred Vuin
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Publication number: 20090114061Abstract: A method of producing de-alloyed nanoparticles. In an embodiment, the method comprises admixing metal precursors, freeze-drying, annealing, and de-alloying the nanoparticles in situ. Further, in an embodiment de-alloyed nanoparticle formed by the method, wherein the nanoparticle further comprises a core-shell arrangement. The nanoparticle is suitable for electrocatalytic processes and devices.Type: ApplicationFiled: September 8, 2008Publication date: May 7, 2009Applicant: UNIVERSITY OF HOUSTONInventors: Peter Strasser, Shirlaine Koh, Prasanna Mani, Srivastava Ratndeep
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Patent number: 7527667Abstract: Metallurgical powder compositions of the present invention include an iron based powder combined with a master alloy powder, as a mechanical property enhancing powder. The addition of master alloy powders has been found to enhance the mechanical properties of the final, sintered, compacted parts made from metallurgical powder compositions, especially at low sintering temperatures. Metallurgical powder compositions include at least about 80 weight percent of an iron-based metallurgical powder and from about 0.10 to about 20 weight percent of a master alloy powder. Master alloy powders include iron and from about 1.0 to about 40 weight percent chromium, and from about 1.0 to about 35 weight percent silicon, based on the weight of the master alloy powder.Type: GrantFiled: November 10, 2006Date of Patent: May 5, 2009Assignee: Hoeganaes CorporationInventors: Bruce T. Lindsley, Patrick King, Christopher Schade
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Publication number: 20090107291Abstract: This invention relates to powder metallurgy, more specifically, to methods of fabricating hard alloy items. The invention can be used as an iron, cobalt or nickel base binder for the fabrication of diamond cutting tools for the construction industry and stone cutting, including segmented cutting discs of different designs and wires for reinforced concrete and asphalt cutting used in the renovation of highway pavements, runways in airports, upgrading of metallurgical plants, nuclear power plants, bridges and other structures, monolithic reinforced concrete cutting drills, as well as discs and wires for the quarry production of natural stone and large scale manufacturing of facing construction materials. This invention achieves the objective of providing binders for the fabrication of diamond tools having higher wear resistance without a significant increase in the sintering temperature, as well as higher hardness, strength and impact toughness.Type: ApplicationFiled: September 25, 2006Publication date: April 30, 2009Inventors: Evgeny Aleksandrovich Levashov, Vladimir Alekseevich Andreev, Viktoriya Vladimirovna Kurbatkina
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Patent number: 7524351Abstract: A nano-sized metal particle composition includes a first metal that has a particle size of about 20 nanometer or smaller. The nano-sized metal particle can include a second metal that forms a shell about the first metal. A microelectronic package is also disclosed that uses the nano-sized metal particle composition. A method of assembling a microelectronic package is also disclosed. A computing system is also disclosed that includes the nano-sized metal particle composition.Type: GrantFiled: September 30, 2004Date of Patent: April 28, 2009Assignee: Intel CorporationInventors: Fay Hua, C. Michael Garner
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Patent number: 7524582Abstract: The invention is directed to a zinc powder or zinc alloy powder for alkaline batteries, which powder has a grain size distribution wherein 60 to 100 wt.-% of the particles, relative to the zinc powder or zinc alloy powder, have a diameter of from 40 to 140 ?m. The invention is also directed to an alkaline battery.Type: GrantFiled: June 5, 2006Date of Patent: April 28, 2009Assignee: Grillo-Werke AGInventors: Armin Melzer, Petra Merkel, Jochen Spiestersbach, Rudi Kube, Norbert Schulz