Abstract: Surface metallization technology for ceramic substrates is disclosed herein. It makes use of a known phenomenon that many metal—metal oxide alloys in liquid state readily wet an oxide ceramic surface and strongly bond to it upon solidification. To achieve high adhesion strength of a metallization to ceramic, a discrete metallization layer consisting of metal droplets bonded to ceramic surface using metal—metal oxide bonding process is produced first. Next, a continuous metal layer is deposited on top of the discrete layer and bonded to it using a sintering process. As a result a strongly adhering, glass-free metallization layer directly bonded to ceramic surface is produced. In particular, the process can be successfully used to metalize aluminum nitride ceramic with high thermal and electrical conductivity copper metal.

Abstract: A method of quenching a workpiece is provided with one or more spray quench rings that eject a controlled variable volume of spray quench onto a workpiece passing through the quench rings by dynamically adjusting the axially adjustable distance between the inner and outer ring elements of each quench ring while the workpiece passes through the quench rings in response to mass cooling requirements of the workpiece passing through the quench rings. The quench rings can also be axial adjusted relative to each other in response to the mass cooling requirements. Dynamically adjustable reflected spray guards can be provided to prevent quench spray pattern interference between adjacent quench rings.

Abstract: An electrically conductive GaAs crystal has an atomic concentration of Si more than 1×1017 cm?3, wherein density of precipitates having sizes of at least 30 nm contained in the crystal is at most 400 cm?2. In this case, it is preferable that the conductive GaAs crystal has a dislocation density of at most 2×10?2 cm2 or at least 1×10?3 cm2.

Abstract: A spray quench system is provided with one or more spray quench rings that eject a controlled volume of quenchant spray onto a workpiece passing through the quench rings. Supply of the quenchant to the quench rings is coordinated with control of the quench rings to selectively change the pressure, quenchant spray exit velocity from the quench rings, flow rate or pattern of the quenchant spray onto the workpiece depending upon mass cooling requirements as the workpiece passes through the quench rings.

Abstract: A method for producing a sintered R-T-B based magnet according to the present invention includes the steps of: providing at least one sintered R-T-B based magnet material (where R is a rare-earth element and T is Fe or Fe and Co); providing RH diffusion sources, each of which includes a heavy rare-earth element RH (which is Dy and/or Tb) and 30 to 80 mass % of Fe and has a particle size of more than 53 ?m and equal to or smaller than 5600 ?m; performing an arrangement process to arrange the magnet material and the RH diffusion sources in a process vessel so that some of the RH diffusion sources are in contact with the magnet material; performing an RH diffusion process by carrying out a heat treatment in an inert ambient at a pressure of 5000 Pa or less and at a temperature of 800° C. to 1000° C.

Abstract: Methods for modifying a physical characteristic of finished endodontic instruments made from one or more superelastic alloys is described which include heat treating one or more finished endodontic instruments in a salt bath for a specific time (e.g., from about four hours to about six hours), at a specified temperature (e.g., from about 475° C. to about 550° C.), and preferably at a specified pH range.

Abstract: A method for heat treating a serviced turbine part to improve a hold time fatigue cracking resistance of the serviced turbine part is provided. The method includes positioning the serviced turbine part in a vacuum furnace configured to limit surface oxidation. The serviced turbine part is controllably heated to prevent distortion. A surface damage layer is recrystallized into a fine grain structure to prevent fatigue crack initiation. The serviced turbine part is controllably cooled to prevent distortion.

Abstract: Aluminum or aluminum alloy sputter targets and methods of making same are provided. The pure aluminum or aluminum alloy is mechanically worked to produce a circular blank, and then the blank is given a recrystallization anneal to achieve desirable grain size and crystallographic texture. A 10-50% additional strain is provided to the blank step after the annealing to increase the mechanical strength. Further, in a flange area of the target, the strain is greater than in the other target areas with the strain in the flange area being imparted at a rate of about 20-60% strain. The blank is then finished to form a sputtering target with desirable crystallographic texture and adequate mechanical strength.

Abstract: Illustrative embodiments provide systems, methods, apparatuses, and applications related to annealing nuclear fission reactor materials.

Abstract: A process for manufacturing a component with a base of Co—Cr—Mo alloys having values of average ultimate elongation at 800° C. greater than 10% and of average yielding load at 800° C. greater than 400 MPa, comprising: obtaining a sintered component by additive sintering of powders of Co—Cr—Mo alloys containing carbides irregularly dispersed in the molten matrix; Conducting a first heat treatment on the sintered component for solubilization of the carbides at a temperature of between 1100° C. and 1300° C. for at least 2 hours to form a solubilization intermediate; and cooling the solubilization intermediate at a cooling rate at least equal to that of cooling in air to form a cooled intermediate; and conducting a second heat treatment on the cooled intermediate at a temperature of between 700° C. and 1000° C.

Abstract: A method and process for at least partially forming a medical device that is at least partially formed of a metal alloy which improves the physical properties of the medical device.

Abstract: A process for heat treating a component formed of an alloy. The process includes manipulating uniaxial strain test data of the alloy using a triaxiality factor to determine an equivalent multiaxial stress state. Conditions are then applied to the multiaxial stress state to identify a cooling path for the component. The cooling path includes boundaries for heat treatment temperatures and cooling rates that do not exceed predetermined stresses or strains and/or avoid predetermined residual stress patterns in the alloy. The component is then heated to a heat treatment temperature and quenched according to the cooling path identified in the applying step.

Abstract: An apparatus has a first structure, a second structure, and an activated seal. The second structure has a first position adjacent to the first structure such that the first structure is not in contact with the second structure. The activated seal is attached to at least one of the first structure and the second structure. The activated seal has a variable stiffness that may be changed in response to a stimuli such that the activated seal is capable of being deformed when at least one of the first structure and the second structure are moved relative to each other.

Abstract: A hybrid prosthesis for deployment in a body vessel includes a tubular stent body comprising a wire comprising a shape memory alloy, where the tubular stent body has a self-expanding portion comprising a distal portion of the wire and a balloon-expandable portion comprising a proximal portion of the wire. The shape memory alloy comprises an Af of less than 37° C. in the self-expanding portion and an As of greater than 37° C. in the balloon-expandable portion.

Abstract: A shape memory alloy including a Ni—Ti based alloy is superelastic at temperatures of about ?40° C. to about 60° C. after being exposed to temperatures of about ?55° C. to about 85° C. A method of forming a memory shape alloy may include preparing a rod comprising a Ni—Ti alloy, drawing a wire from the rod, and treating the wire at a temperature of about 500° C. to about 550° C. for about less than 1 minute.

Abstract: A method of forming an earth-boring tool includes introducing metal into a die, rotating the die to generate centrifugal forces on the metal, and cooling the metal in the rotating die. A rotary drill bit may include a unitary, centrifugally cast bit body including an integral shank, at least one blade, and at least one cutting element on the blade. A rotary drill bit or a roller cone may include a first centrifugally cast material and a second centrifugally cast material. Another rotary drill bit includes a bit body comprising a maraging steel alloy. A method of forming a rotary drill bit may include disposing cutting elements on a rotary drill bit comprising maraging steel and aging the rotary drill bit to form at least one intermetallic precipitate phase. Methods of repairing a rotary drill bit include annealing and aging at least a portion of a rotary drill bit.

Abstract: Disclosed is a heat treatment method for a cylinder block of an internal combustion engine. More specifically, the method includes heating the cylinder block to a solution heat treatment temperature, processing the cylinder block at the solution heat treatment temperature between 440° C. to 460° C. for one to two hours, quenching the cylinder block and then immediately aging the cylinder block for a predetermined amount of time.

Abstract: The subject invention discloses a process for strengthening and obtaining the desired dimensions for a metal part comprising: (1) heating at least a portion of a preformed metal part to a temperature above about 1300° F. to transform the metal in at least said portion of the part to an austenitic state to produce an austenitized preformed metal part, (2) quenching the austenitized preformed metal part to a temperature of 300° F. to 650° F. to put the metal in the preformed part in a metastable austenitic state, (3) coining, drawing or extruding the preformed metal part while said metal of said preformed metal part is maintained in the metastable austenitic state at a temperature of 300° F. to 650° F., and (4) quenching the coined, drawn, or extruded metal part at a temperature which allows for the rapid transformation from austenite to martensite.

Abstract: Method of reducing the formation of folds on metal strips (1) exposed to rapid heating in continuous heat-treatment lines, in which lines said strips are caused to pass through heating sections (2) comprising successive and separate heating means (5; 5a; 5b; 5c; 5d), wherein the average slope of the increase in temperature of the strip between the inlet and the outlet of a heating means decreases from one heating means to the following heating means.

Abstract: A stent and method for manufacturing a stent that achieves both strength as well as ductility. In the manufacturing process, the material used to form the stent is only partially annealed to lower the grain size across the thickness of the stent. The material is partially annealed either prior to or after the cutting a stent pattern into a tube.

Abstract: Embodiments of methods for fabricating refractory-metal articles (e.g., implantable medical devices), and honing and blasting apparatuses for use in such methods are disclosed. Methods for fabricating refractory-metal-containing articles include laser cutting in a vacuum environment and/or at least one mechanical or chemical finishing step configured to remove at least one region affected by the fabrication process (e.g., the laser cutting process) to provide a substantially defect-free surface finish.

Abstract: A method for the low temperature heat treatment of an age-hardenable magnesium based alloy, including following steps: (a) providing a solution heat-treated and quenched age-hardenable magnesium based alloy; and (b) subjecting said alloy to low temperature ageing below 100°C. for a period of time sufficient to develop an enhanced ageing response.

Abstract: The present invention provides a method for processing a metal body which can turn a metal structure of the metal body into a finer grain structure thus obtaining the high strength and the high ductility. In a method or an apparatus for processing a metal body which turns the metal structure of the metal body into the finer grain structure by forming a low deformation resistance region where the deformation resistance is locally lowered in the metal body and by deforming the low deformation resistance region by shearing, using a non-low deformation resistance region forming means which forms a non-low deformation resistance region by increasing the deformation resistance which is lowered in the low deformation resistance region, the non-low deformation resistance region is formed along the low deformation resistance region.

Abstract: A process for repairing cracks in a workpiece, such as a turbine engine component, comprises the steps of: providing a workpiece having a crack to be repaired; applying a nickel or cobalt base alloy material to a root of the crack in an amount sufficient to fill a portion of the crack; subjecting the workpiece with the nickel or cobalt base alloy material to a first heat treatment at a temperature in the range of from about 1950 to 2300° F. for a time period in the range of from about 5.0 to 30 minutes; applying a weld material to the crack; and subjecting the workpiece with the weld material to a second heat treatment.

Abstract: The invention relates to a twist-axle that includes a cross-beam member and two trailing arms, each trailing arm rigidly secured to the cross-beam member in one of two connection regions of the cross-beam member or formed integrally with and extending from one of the two connection regions. The cross-beam member is formed from a tubular blank and has a torsionally elastic central portion and two torsionally stiff connection regions. The cross-beam member has a wall thickness that varies longitudinally along the length of the cross-beam member from the torsionally elastic central portion to each of the torsionally stiff connection regions.

Abstract: A hot formed part of high-strength steel includes a body having an opening and formed in one piece with at least one tab in the form of a tongue projecting into the opening for holding a connection piece captive on the body. The tab thus is formed in one piece with the hot formed part and is produced jointly with the openings during manufacture of the hot formed part in the hot forming process.

Abstract: An article cut from a metallic sheet, has a first pattern of struts forming a plurality of inner apexes situated substantially within a plane that contains the plurality of the inner apexes. There is a second pattern of struts forming a plurality of outer apexes that are situated substantially within the plane containing the inner apexes. Each outer apex has at least one strut in common with an adjacent inner apex. There is also described a method of forming a non-planar three dimensional structure by patterning a planar sheet of material to form an article having a plurality of inner apexes, a plurality of outer apexes with a common curvilinear strut between an inner apex and an adjacent outer apex. Thereafter, everting the article into a non-planar three dimensional structure with the inner apexes at one end of the structure and the outer apexes at another end of the structure.

Abstract: A method of forging includes a first forging action that changes the shape of a metallic alloy work piece. A second forging action further changes the shape of the metallic alloy work piece after the first forging action. A heat treatment step is conducted after the first forging action and prior to the second forging action. The heat treatment step includes subjecting the metallic alloy work piece to a heat treatment temperature that alters the microstructure of the metallic alloy work piece without the application of a forging action that changes the shape of the metallic alloy work piece.

Abstract: An apparatus for thermally treating a plurality of curved suture needles. The apparatus includes a conveyer for transferring the plurality of curved suture needles from a source of curved suture needles to a receiver, a housing positioned adjacent the conveyer, the housing having a first end, a second end, and an opening running from the first end to the second end, the opening aligned with the conveyer to enable the plurality of curved suture needles to pass therethrough, and a heat source located within the housing for heating the plurality of curved suture needles as the plurality of curved suture needles are transferred by the conveyer from the first end of the housing to the second end of the housing. Also provided is a process for thermally treating a plurality of curved suture needles to enhance the stiffness and yield moment of the curved suture needles. The curved suture needles so treated have a desirable combination of stiffness, strength and ductility.

Abstract: The heat treatment method of the present invention includes: a first step of mist cooling a treatment object retained at a prescribed temperature by supplying mist-like coolant, to a target temperature near to and higher than a first transformation point at which a structure of the treatment object begins to be transformed into a prescribed structure; a second step, following the first step, of retaining the treatment object for a prescribed time in a state where supply of mist-like coolant is stopped; and a third step, following the second step, of cooling the treatment object to a temperature lower than or equal to the first transformation point. According to the present invention, it is possible to provide a heat treatment method capable of suppressing irregularity and deformation in the structure of the treatment object.

Abstract: A method for the low temperature heat treatment of an age-hardenable magnesium based alloy, including following steps: (a) providing a solution heat-treated and quenched age-hardenable magnesium based alloy; and (b) subjecting said alloy to low temperature ageing below 100°C. for a period of time sufficient to develop an enhanced ageing response.

Abstract: A plant for the heat treatment of metallic elements (E) includes: at least a chamber (3) for containing the metallic elements (E) having at least one access opening (A1); a heater (4) of the chamber (3), operating on the chamber (3) for bringing the same at a predetermined temperature; a conveyor (15), connected with a respective actuator and acting on the metallic elements (E) for transferring these latter at the exiting and/or entering with respect to the chamber (3). The conveyor (15) has been positioned outside the chamber (15) during the functioning of the plant (1).

Abstract: An orientation of crystal axis <001> of the metallic material as a solid solution having a structure of body-centered cubic (BCC) is arranged along a work surface of the metallic material by hot rolling process in a temperature range of structuring the metallic material to be BCC single phase solid solution. For example, Fe-Si alloy as the metallic material is heated in the temperature range for BCC single phase solid solution, and processed so as to arrange the orientation of crystal axis <001> along the work surface by pressing the BCC single phase solid solution in a strain rate to maintain work condition for controlling motion of dislocation by atmosphere of solute atom generated in BCC single solid solution and migrating grain boundary by strain energy stored in a crystal grain as driving force.

Abstract: Processes for fabricating components to have two or more regions with different grain structures, and components produced by such processes. The processes entail performing at least one forging step on a preform to produce a profile having at least a first portion corresponding to the first region of the component. The preform is formed of a precipitation-strengthened alloy having a solvus temperature, and the at least one forging step comprises a nonfinal forging step performed at a first strain rate and at a first subsolvus temperature that is below the solvus temperature of the alloy. A subsequent forging step is performed on the profile to produce a final profile comprising the first portion and a second portion corresponding to the second region of the component.

Abstract: Disclosed embodiments disclose processes for making shaped metal alloy parts, and deal more particularly with forming features and reducing residual stresses in such parts. Residual stresses introduced into a metal alloy part by heat treatment, which may include solution annealing and quenching, are reduced by processes that plastically deform the part while forming part features. An embodiment comprises: producing a metal alloy blank; subjecting the blank to a process that introduces residual stresses into the blank and plastically deforming the blank to reduce the residual stresses in the blank. Embodiments comprise: subjecting a part to a heat treatment that introduces residual stresses in the part; and age forming the part to shape the part and reduce the residual stresses, incrementally forging at least one feature into the part and reducing the residual stresses in the part, friction welding the part, or gauge rolling the cast part to desired dimensions.

Abstract: A method of making sputter targets using rotary axial forging is described. Other thermomechanical working steps can be used prior to and/or after the forging step. Sputter targets are further described which can have unique grain size and/or crystal structures.

Abstract: Disclosed is a process for the heat treatment of metal strip material providing mechanical properties that differ over the width of the strip, wherein the strip is heated and cooled and optionally over-aged during a continuous annealing process. At least one of the following parameters in the process differs over the width of the strip: heating rate, top temperature, top temperature holding time, cooling trajectory after top temperature; or, when over-aging is performed, at least one of the following parameters in the process differs over the width of the strip: heating rate, top temperature, top temperature holding time, cooling trajectory after top temperature, over-aging temperature, over-aging temperature holding time, lowest cooling temperature before over-aging, re-heating rate to over-aging temperature. Also, at least one of the cooling trajectories follows a non-linear temperature-time path. Also disclosed is strip material thus produced.

Abstract: The present invention relates to new compositions of matter, particularly metals and alloys, and methods of making such compositions. The new compositions of matter exhibit long-range ordering and unique electronic character.

Abstract: A method for manufacturing a nonlinear superelastic file comprising the steps of: providing a superelastic file having a shaft and a file axis; providing a fixture including a file groove being defined by one or more displacement members, the file groove configured for receiving the shaft; inserting at least a portion of the shaft into the fixture along the file groove, the portion of the shaft including a first portion of the shaft; contacting the first portion of the shaft with a first displacement member of the one or more displacement members such that the first portion of the shaft is displaced from the file axis thereby forming a first offset portion of the shaft; heating the portion of the shaft while inserted in the fixture to a temperature of at least about 300° C. for a time period of at least about 1 minute to shape-set the portion of the shaft thereby forming a shape-set nonlinear file.

Abstract: A treatment for prevention of stress corrosion cracking (SCC) and a treated component are disclosed. A surface of a relatively high tensile strength component is heated to a temperature at which at least one of tempering or annealing occurs. The surface is then cooled in a controlled manner so as to maintain a reduced tensile strength at the surface that minimizes SCC while keeping a relatively high tensile strength in the remainder of the component.

Abstract: Methods for producing alloy strips including zirconium alloy strips that demonstrate improved formability are disclosed. The strips of the present disclosure have a purity and crystalline microstructure suitable for improved formability, for example, in the manufacture of certain articles such as panels for plate heat exchangers and high performance tower packing components. Other embodiments disclosed herein relate to formed alloy strip, articles of manufacture produced from the alloy strip, and methods for making the articles of manufacture.

Abstract: The present invention relates to a component {1, 2, 3, 4, 6) within the interior of a vehicle. Specifically, the present invention relates to a part of a seat-structure. The present invention further relates to a process to produce a component { 1, 2, 3, 4, 6) Within the interior of a vehicle.

Abstract: The invention encompasses a method of forming a metallic article. An ingot of metallic material is provided, and such ingot has an initial thickness. The ingot is subjected to hot forging. The product of the hot forging is quenched to fix an average grain size of less than 250 microns within the metallic material. The quenched material can be formed into a three dimensional physical vapor deposition target. The invention also includes a method of forming a cast ingot. In particular aspects, the cast ingot is a high-purity copper material. The invention also includes physical vapor deposition targets, and magnetron plasma sputter reactor assemblies.

Abstract: A low alloy steel ingot contains from 0.15 to 0.30% of C, from 0.03 to 0.2% of Si, from 0.5 to 2.0% of Mn, from 0.1 to 1.3% of Ni, from 1.5 to 3.5% of Cr, from 0.1 to 1.0% of Mo, and more than 0.15 to 0.35% of V, and optionally Ni, with a balance being Fe and unavoidable impurities. Performing quality heat treatment including a quenching step and a tempering step to the low alloy steel ingot to obtain a material, which has a grain size number of from 3 to 7 and is free from pro-eutectoid ferrite in a metallographic structure thereof, and which has a tensile strength of from 760 to 860 MPa and a fracture appearance transition temperature of not higher than 40 ° C.

Abstract: The present disclosure relates to a clip manufactured according to a method which can be used to engage body tissue for the purpose of closing wounds. Such clips are generally annular in shape and have radially inwardly extending tines. The present disclosure first forms a precursor which, in one embodiment, has the tines extending radially outwardly from the annular body and then forms the clip by inverting the precursor such that the tines extend radially inwardly. In an alternate embodiment, the precursor is formed with an over-sized lateral dimension and then compressed inwardly to bring the tines closer together and to reduce the lateral dimension of the precursor. Such clips may be manufactured from a superelastic alloy such as nickel-titanium, in which case the inverted or compressed precursor must be heated and quenched to heat set the clip in its final shape.

Abstract: The homogenization cycle of an alloy is optimized and controlled by defining a target degree of transformation to achieve at least one metallurgical property for an alloy. The desired metallurgical properties include, but are not limited to, dissolving precipitation hardening phases, transforming insoluble phases into preferred phases and precipitating the dispersoid phases to the proper size and distribution. Using regression analysis, a transformation model is obtained to predict the degree of transformation of an alloy by analyzing the degree of transformation of a plurality of sample alloys subjected to heating at predetermine temperatures for predetermined amounts of time.

Abstract: A process for quenching heat treated metal parts using a liquid quenchant and high pressure is disclosed. In general, the process includes the steps of providing a load of heat treated metal parts in a pressure vessel wherein the load is at an elevated temperature after being heat treated. In a subsequent step, a liquid quenchant is injected into the pressure vessel such that a vapor of the liquid quenchant forms rapidly in the pressure vessel and cools the metal parts. The step of injecting the liquid quenchant into the pressure vessel is continued for a time sufficient to establish a desired peak vapor pressure in the pressure vessel. An apparatus for carrying out the disclosed process is also described.

Abstract: The present invention provides a hydrogen absorbing alloy containing a phase of a Pr5Co19 type crystal structure having a composition defined by a general formula A(4?w)B(1+w)C19 (A denotes one or more element(s) selected from rare earth elements including Y (yttrium); B denotes an Mg element; C denotes one or more element(s) selected from a group consisting of Ni, Co, Mn, and Al; and w denotes a numeral in a range from ?0.1 to 0.8) and having a composition as a whole defined by a general formula R1xR2yR3z (15.8?x?17.8, 3.4?y?5.0, 78.8?z?79.6, and x+y+z=100; R1 denotes one or more element(s) selected from rare earth elements including Y (yttrium); R2 denotes an Mg element, R3 denotes one or more element(s) selected from a group consisting of Ni, Co, Mn, and Al; the numeral of Mn+Al in the z is 0.5 or higher; and the numeral of Al in the z is 4.1 or lower).

Abstract: A process for producing a profile component from a semi-finished sheet metal part, which at least in certain sections has a structurally increased strength. The semi-finished sheet metal part is formed in an at least a single-stage bending process. The bending process and also subsequent parting and cutting operations on the semi-finished sheet metal part are combined with a thermal treatment of at least one geometrically delineated region of the semi-finished sheet metal part. The thermal treatment comprises at least one heating step and is combined with a subsequent cooling step, in such a way that the at least one geometrically delineated region has a structurally increased strength after cooling. Bending can be effected by using roller profiling wherein rollers are preferably cooled or swage bending.

Abstract: One example embodiment includes methods for making electron emitters. The electron emitter comprises a conductive member that defines a plurality of filament segments that are integral with each other. Each filament segment includes an intermediate portion and an interconnecting portion attached to an adjacent filament segment. The intermediate portions are substantially coplanar with each other and each intermediate portion includes a substantially planar electron emission surface.