Metal Containing Patents (Class 423/592.1)
  • Publication number: 20100025627
    Abstract: The present invention aims at: providing an accelerated reaction in a liquid-phase reaction; forming, by way of the reaction, a metal oxide nanoparticle and carbon that carries the metal oxide nanoparticle in a highly dispersed state; and providing an electrode containing the carbon and an electrochemical device using the electrode. In order to solve the above-mentioned problem, shear stress and centrifugal force are applied to the reactant in the rotating reactor so that an accelerated chemical reaction is attained in the course of the reaction. Further, the carbon carrying a metal oxide nanoparticle in a highly dispersed state comprises: a metal oxide nanoparticle produced by the accelerated chemical reaction, wherein shear stress and centrifugal force are applied to a reactant in a rotating reactor in the course of the reaction; and carbon dispersed in the rotating reactor by applying shear stress and centrifugal force.
    Type: Application
    Filed: November 30, 2006
    Publication date: February 4, 2010
    Applicants: K & W LIMITED, NIPPON CHEMI-CON CORPORATION
    Inventors: Katsuhiko Naoi, Nobuhiro Ogihara, Shuichi Ishimoto
  • Publication number: 20100028236
    Abstract: There is disclosed a process of making nano-sized or micro-sized precipitate particles. The process comprising the steps of mixing, in a reaction zone, a metal salt solution with a precipitant solution to form a precipitate, said precipitate being at least one of a metal chalcogenide, metal hydroxide and metal oxide; and applying a shear force to said mixing solutions in said reaction zone during said mixing step, wherein said shear force and the conditions within said reaction zone form said nano-sized or micro-sized precipitate particles.
    Type: Application
    Filed: October 2, 2007
    Publication date: February 4, 2010
    Applicant: NANOMATERIALS TECHNOLOGY PTE LTD
    Inventors: Zhigang Shen, Jiyao Zhang, Giawen Sim, Jimmy Sung Lai Yun, Jianfeng Chen
  • Publication number: 20100028674
    Abstract: Nanofibers and methods for making the nanofibers are described. Porous metal oxide nanofibers and porous metal oxide nanofibers comprising metal nanoparticles made via electrospinning methods are also described.
    Type: Application
    Filed: July 31, 2008
    Publication date: February 4, 2010
    Inventor: Fredrick O Ochanda
  • Patent number: 7655214
    Abstract: Valve metal suboxides having a primary suboxide phase and optionally a secondary suboxide phase, a valve metal phase, and/or at least one tertiary suboxide phase can be present in varying amounts. Also disclosed is anodes and capacitors containing the valve metal suboxides of the present invention. Also, a method to prepare a valve metal suboxide is further described which includes granulating one or more of the starting materials individually or together and/or granulating the final product.
    Type: Grant
    Filed: February 25, 2004
    Date of Patent: February 2, 2010
    Assignee: Cabot Corporation
    Inventors: David M. Reed, Sridhar Venigalla, Jeffrey A. Kerchner
  • Patent number: 7654323
    Abstract: An embodiment consistent with the present invention is a high strength proppant comprising an electrofused pellet. In another embodiment, a high strength proppant comprises a substantially solid and substantially spherical pellet produced by electrofusion of at least one metal oxide. A method of making a proppant is also provided, with that method comprising melting at least one metal oxide in an electrical arc furnace, pouring the molten metal oxide to create a pour stream, and separating the pour stream to form at least one electrofused pellet. A method of fracturing subterranean formations is also provided, with that method comprising injecting a fluid containing at least one electrofused pellet.
    Type: Grant
    Filed: August 18, 2006
    Date of Patent: February 2, 2010
    Assignee: Imerys
    Inventors: Jean Andre Alary, Sebastian Sachse, Thomas Parias
  • Publication number: 20090307967
    Abstract: Cerium or other metal oxide is used with bio-derived fuels to reduce coking and to clean up combustion chamber surfaces.
    Type: Application
    Filed: March 26, 2007
    Publication date: December 17, 2009
    Applicant: Oxonica Energy Ltd
    Inventors: Martin Gardener, Gareth Wakefield, Andrew Elphick
  • Patent number: 7625836
    Abstract: To provide a heat-resistant oxide which is excellent in heat resistance and durability at high temperature and has high activity, a heat-resistant oxide which has an oxide crystal structure and in which a rate of a solid solution of a noble metal in the oxide crystal structure is 50% or more is obtained by heat-treating (secondarily baking) a precursor composition comprising zirconia, at least one coordinative element selected from the group consisting of rare earth elements, alkaline earth elements, aluminum and silicon, and at least one noble metal selected from the group consisting of platinum, rhodium and palladium at 650° C. or higher.
    Type: Grant
    Filed: December 13, 2005
    Date of Patent: December 1, 2009
    Assignees: Cataler Corporation, Daihatsu Motor Co., Ltd.
    Inventors: Satoshi Matsueda, Mareo Kimura, Naoto Miyoshi, Yoshinori Ishii, Hirohisa Tanaka, Isao Tan, Mari Uenishi, Masashi Taniguchi
  • Patent number: 7625653
    Abstract: A material which conducts protons or oxide ions with high ionic conductivity and is excellent in moisture resistance and reduction resistance is provided. A perovskite oxide represented by the formula (1): BaZraCebM1cL1dO3-???(1) (wherein M1 is at least one member selected from the group consisting of rare earth elements, In, Mn, Fe, Co, Ni, Al and Ga, L1 is at least one member selected from the group consisting of P, B and N and a, b, c, d and a satisfy 0?a<1.2, 0<b<1.2, 0<c<1.2, 0.9<a+b+c<1.2, 0<d<0.1 and 0<?<3) is used as an ionic conductor.
    Type: Grant
    Filed: March 13, 2006
    Date of Patent: December 1, 2009
    Assignee: Panasonic Corporation
    Inventors: Tomohiro Kuroha, Noboru Taniguchi
  • Patent number: 7622098
    Abstract: Method for producing nano-particles includes vaporizing a precursor material to produce a vapor, directing the vapor into an isolation chamber, combining a quench fluid in a gaseous state with a quench fluid in a liquid state to form a quench fluid stream, contacting the vapor contained in the isolation chamber with the quench fluid stream thereby cooling the vapor to produce the nano-particles in a carrier stream, and removing the nano-particles from the isolation chamber.
    Type: Grant
    Filed: November 21, 2008
    Date of Patent: November 24, 2009
    Assignee: Cyprus Amax Minerals Company
    Inventors: Joel A. Taube, Mohamed H. Khan, James A. Cole
  • Patent number: 7622189
    Abstract: Structures and methods for the fabrication of ceramic nanostructures. Structures include metal particles, preferably comprising copper, disposed on a ceramic substrate. The structures are heated, preferably in the presence of microwaves, to a temperature that softens the metal particles and preferably forms a pool of molten ceramic under the softened metal particle. A nano-generator is created wherein ceramic material diffuses through the molten particle and forms ceramic nanostructures on a polar site of the metal particle. The nanostructures may comprise silica, alumina, titania, or compounds or mixtures thereof.
    Type: Grant
    Filed: June 21, 2006
    Date of Patent: November 24, 2009
    Assignee: Babcock & Wilcox Technical Services Y-12, LLC
    Inventors: Edward B. Ripley, Roland D. Seals, Jonathan S. Morrell
  • Publication number: 20090286678
    Abstract: The present invention is directed to methods for making metal oxide compositions, specifically, metal oxide compositions having high surface area, high metal/metal oxide content, and/or thermal stability with inexpensive and easy to handle materials. In one embodiment, the present invention is directed to methods of making metal and/or metal oxide compositions, such as supported or unsupported catalysts. The method includes combining a metal precursor with an organic acid to form a mixture and calcining the mixture for a period of time sufficient to form a metal oxide material.
    Type: Application
    Filed: May 2, 2006
    Publication date: November 19, 2009
    Applicant: Symyx Technologies, Inc.
    Inventor: Alfred Hagemeyer
  • Patent number: 7615201
    Abstract: By using a halogen-free siloxane and an organometallic compound containing at least one metal other than silicon as feed stocks, and simultaneously atomizing and burning them in a flame, spherical particles of silica-containing compound oxide are prepared which are substantially halogen-free, consist of 0.5-99% by weight of metal oxides and the balance of silica, and have a particle size of 10 nm to 3 ?m. The particles are useful as a filler in epoxy resin base semiconductor sealants, a refractive index modifier or the like.
    Type: Grant
    Filed: July 23, 2002
    Date of Patent: November 10, 2009
    Assignee: Shin-Etsu Chemical Co., Ltd.
    Inventors: Yoshiharu Konya, Koichiro Watanabe, Susumu Ueno
  • Patent number: 7615206
    Abstract: Methods for the production of shaped nanoscale-to-microscale structures, wherein a nanoscale-to-microscale template is provided having an original chemical composition and an original shape, and the nanoscale-to-microscale template subjected to a chemical reaction, so as to partially or completely convert the nanoscale-to-microscale template into the shaped nanoscale-to-microscale structure having a chemical composition different than the original chemical composition and having substantially the same shape as the original shape, being a scaled version of the original shape. The shaped nanoscale-to-microscale structure formed comprises an element (such as silicon), a metallic alloy (such as a silicon alloy), or a non-oxide compound (such as silicon carbide or silicon nitride).
    Type: Grant
    Filed: August 13, 2007
    Date of Patent: November 10, 2009
    Assignee: Georgia Tech Research Corporation
    Inventors: Kenneth Henry Sandhage, Zhihao Bao
  • Patent number: 7611688
    Abstract: The present invention is related to a process of manufacturing rutile high-purity titania nano sols in a pure aqueous medium having no ionic impurities. In more detail, the present invention is related to a process for manufacturing titania nano sols, in which high-purity rutile titania nano particles are dispersed stably, through the hydrolysis of titanium tetraisopropoxide in an aqueous solution containing hydrogen peroxide (H2O2), and simultaneously with the hydrolysis, formation of peroxotitanate precursors, and hydrothermal treatment of them at 50-120° C.
    Type: Grant
    Filed: August 23, 2005
    Date of Patent: November 3, 2009
    Assignee: Korea Research Institute of Chemical Technology
    Inventors: Sang-Il Seok, Bok-Yeop Ahn, Hoon Kim
  • Patent number: 7608237
    Abstract: A process for synthesizing nanostructures is disclosed. The process involves forming a liquid crystalline template by combining a block copolymer, a first reactant in a polar phase, and a nonpolar phase, then contacting the template with a gas phase composed of a second reactant, under conditions effective to form nanostructures.
    Type: Grant
    Filed: March 28, 2006
    Date of Patent: October 27, 2009
    Assignee: The Research Foundation of State University of New York
    Inventors: Paschalis Alexandridis, Georgios N. Karanikolos, Triantafillos J. Mountziaris
  • Patent number: 7601324
    Abstract: The method for synthesizing metal oxide nanopowder produces powders of nanoparticle size from metals having relatively low boiling temperatures, such as zinc, tellurium, bismuth, and strontium by vapor-phase oxidation using a conventional 2.45 GHz microwave oven. The energy that initiates the combustion comes from the microwave through a susceptor tube that absorbs radiant microwave energy and transfers it to the metal, which evaporates to small particles inside the susceptor tube and then combusts in air to form nanosize powder. The susceptor is made of silicon carbide composite material.
    Type: Grant
    Filed: July 11, 2008
    Date of Patent: October 13, 2009
    Assignee: King Fahd University of Petroleum and Minerals
    Inventor: Saleh I. Al-Quraishi
  • Patent number: 7601278
    Abstract: Crystalline, single-phased layers of PbMg0.33 Nb0.6703 with relative dielectric constants of 1500 and more are prepared through the use of a precursor solution that comprises a macrocyclic complexing agent. This agent is added to the lead component in an organic solution. The resulting layer is part of a device which may further include semiconductor elements and resistors.
    Type: Grant
    Filed: July 1, 2004
    Date of Patent: October 13, 2009
    Assignee: NXP B.V.
    Inventors: Joerg Meyer, Mareike Katharine Klee, Rainer Kiewitt
  • Patent number: 7597873
    Abstract: A process for the recovery of metal oxides from a solution containing metallic salts by spray roasting of these solutions. The process is particularly suitable for spray roasting spent pickling acids. The process feeds the solution to a reactor for spray roasting of the droplets in at least two stages, where at least one evaporation stage follows at least one conversion stage to convert the metal salts to metal oxides. The device for implementing the process includes a spray roasting reactor having a first heating zone to evaporate the water and a second heating zone to convert the metal salts to oxides.
    Type: Grant
    Filed: August 16, 2005
    Date of Patent: October 6, 2009
    Assignee: Andritz AG
    Inventor: Albert Lebl
  • Patent number: 7582276
    Abstract: The invention relates to nanoscale rutile or oxide powder that is obtained by producing amorphous TiO2 by mixing an alcoholic solution with a titanium alcoholate and with an aluminum alcohalate and adding water and acid. The amorphous, aluminum-containing TiO2 is isolated by removing the solvent, and is redispersed in water in the presence of a tin salt. Thermal or hydrothermal post-processing yields rutile or oxide that can be redispersed to primary particle size. The n-rutile or the obtained oxide having a primary particle size ranging between 5 and 20 nm can be incorporated into all organic matrices so that they remain transparent. Photocatalytic activity is suppressed by lattice doping with trivalent ions. If the amorphous precursor is redispersed in alcohol, or not isolated, but immediately crystallized, an anatase is obtained that can be redispersed to primary particle size.
    Type: Grant
    Filed: August 30, 2002
    Date of Patent: September 1, 2009
    Assignee: ITN Nanovation AG
    Inventor: Ralph Nonninger
  • Publication number: 20090213591
    Abstract: The present invention relates to a reflective member (7). The reflective member (7) includes a reflective layer 61 (7) formed to be porous using an inorganic material. The reflective layer 61 (7) has a porosity of 15-43%. Such reflective layer 61 (7) is formed by partly combining a plurality of inorganic particles with each other.
    Type: Application
    Filed: March 25, 2006
    Publication date: August 27, 2009
    Applicant: KYOCERA CORPORATION
    Inventors: Kousuke Katabe, Yuki Mori
  • Publication number: 20090214416
    Abstract: The invention provides a process for preparing a metal hydroxide comprising the steps of: (a) providing particles of a metal silicate; (b) mixing the particles with a mineral acid solution to obtain a slurry which comprises precipitated silica; (c) separating the precipitated silica from the slurry to obtain a remaining solution; (d) increasing the pH of the remaining solution to such an extent that a metal hydroxide is formed; (e) separating the metal hydroxide so obtained from the remaining solution; and (f) adding to the remaining solution obtained in step (e) an acid solution, thereby forming a salt containing solution, or (g) removing at least part of the base added in step (d) from the remaining solution obtained in step (e), thereby forming a salt containing solution.
    Type: Application
    Filed: November 9, 2006
    Publication date: August 27, 2009
    Applicant: Nederlandse Organisatie voor toegepast-natuurweten schappelijk onderzoek TNO
    Inventor: Jan Peter Brouwer
  • Patent number: 7576035
    Abstract: A pillar-shaped honeycomb structure has a plurality of cells longitudinally placed in parallel with one another with a wall portion therebetween, wherein the honeycomb structure mainly includes inorganic fibers which form the honeycomb structure without lamination interfaces.
    Type: Grant
    Filed: April 7, 2008
    Date of Patent: August 18, 2009
    Assignee: Ibiden Co., Ltd.
    Inventors: Kazushige Ohno, Tomokazu Oya
  • Publication number: 20090202427
    Abstract: Process for preparing mixed metal oxide powders Abstract Process for preparing a mixed metal oxide powder, in which oxidizable starting materials are evaporated in an evaporation zone of a reactor and oxidized in the vaporous state in an oxidation zone of this reactor, the reaction mixture is cooled after the reaction and the pulverulent solids are removed from gaseous substances, wherein at least one pulverulent metal, together with one or more combustion gases, is fed to the evaporation zone, the metal is evaporated completely in the evaporation zone under nonoxidizing conditions, an oxygen-containing gas and at least one metal compound are fed, separately or together, in the oxidation zone to the mixture flowing out of the evaporation zone, the oxygen content of the oxygen-containing gas being at least sufficient to oxidize the metal, the metal compound and the combustion gas completely.
    Type: Application
    Filed: May 16, 2007
    Publication date: August 13, 2009
    Applicant: EVONIK DEGUSSA GMBH
    Inventors: Stipan Katusic, Guido Zimmermann, Michael Krämer, Horst Miess, Edwin Staab
  • Patent number: 7572532
    Abstract: The invention relates to an oxide material of general formula (I) A2?x?yA?XA?yM1?z M?Z04+?, wherein A and A? are independently a metal cation of a group formed by lanthanides and/or alkalis and/or alkaline earths, A? is a cationic gap, i.e. a cation vacancy A and/or A?, M and M? are independently a metal of a group formed by transition metals such as 0<y<0.30, preferably 0<y=0.20; 0<?<0.25, preferably 0<?<0.10; 0=x=1; and 0=z=1. An air electrode containing said material and an electric power producing device in the form of a fuel cell provided with at least one electrochemical cell comprising said electrode are also disclosed.
    Type: Grant
    Filed: March 21, 2005
    Date of Patent: August 11, 2009
    Assignees: Electricite de France, Centre National de la Recherche
    Inventors: Philippe Stevens, Emmanuelle Boehm, Jean-Marc Basset, Fabrice Mauvy, Jean-Claude Grenier
  • Patent number: 7572423
    Abstract: The invention provides a process for producing fumed metal oxide particles comprising providing a stream of a liquid feedstock comprising a volatizable, non-halogenated metal oxide precursor, providing a stream of a combustion gas having a linear velocity sufficient to atomize and combust or pyrolyze the liquid feedstock, and injecting the stream of the liquid feedstock into the stream of combustion gas to form a reaction mixture such that the liquid feedstock is atomized and subjected to a sufficient temperature and residence time in the combination gas stream for fumed metal oxide particles to form before the combustion gas temperature is reduced below the solidifying temperature of the metal oxide particle. The invention further provides fumed silica particles having a relatively small aggregate size and/or narrow aggregate size distribution.
    Type: Grant
    Filed: November 24, 2003
    Date of Patent: August 11, 2009
    Assignee: Cabot Corporation
    Inventor: Yakov E. Kutsovsky
  • Patent number: 7566436
    Abstract: A mixing reactor for mixing efficiently streams of fluids of differing densities. In a preferred embodiment, one of the fluids is supercritical water, and the other is an aqueous salt solution. Thus, the reactor enables the production of metal oxide nanoparticles as a continuous process, without any risk of the reactor blocking due to the inefficient mixing inherent in existing reactor designs.
    Type: Grant
    Filed: February 11, 2005
    Date of Patent: July 28, 2009
    Assignee: The University of Nottingham
    Inventors: Edward Henry Lester, Barry James Azzopardi
  • Patent number: 7553474
    Abstract: It is an object to provide a method for producing stable alkaline metal oxide sols having a uniform particle size distribution. The method comprises the steps of: heating a metal compound at a temperature of 60° C. to 110° C. in an aqueous medium that contains a carbonate of quaternary ammonium; and carrying out hydrothermal processing at a temperature of 110° C. to 250° C. The carbonate of quaternary ammonium is (NR4)2CO3 or NR4HCO3 in which R represents a hydrocarbon group, or a mixture thereof. The metal compound is one, or two or more metal compounds selected from a group of compounds based on a metal having a valence that is bivalent, trivalent, or tetravalent.
    Type: Grant
    Filed: August 8, 2005
    Date of Patent: June 30, 2009
    Assignee: Nissan Chemical Industries, Ltd.
    Inventors: Yutaka Ohmori, Hirokazu Kato, Yoshinari Koyama, Kenji Yamaguchi
  • Patent number: 7547431
    Abstract: A method of producing high purity nanoscale powders in which the purity of powders produced by the method exceeds 99.99%. Fine powders produced are of size preferably less than 1 micron, and more preferably less than 100 nanometers. Methods for producing such powders in high volume, low-cost, and reproducible quality are also outlined. The fine powders are envisioned to be useful in various applications such as biomedical, sensor, electronic, electrical, photonic, thermal, piezo, magnetic, catalytic and electrochemical products.
    Type: Grant
    Filed: December 10, 2002
    Date of Patent: June 16, 2009
    Assignee: PPG Industries Ohio, Inc.
    Inventors: Tapesh Yadav, Karl Pfaffenbach
  • Publication number: 20090148347
    Abstract: A nano-crystalline composite-oxide thin film for an environmental gas sensor, an environmental gas sensor using the thin film, and a method of manufacturing the environmental gas sensor are provided. The nano-crystalline composite-oxide thin film is formed of hetero-oxide nano-crystalline particles having independent crystalline phases from each other, and the environmental gas sensor including the thin film has excellent characteristics including high sensitivity, high selectivity, high stability and low power consumption.
    Type: Application
    Filed: August 13, 2008
    Publication date: June 11, 2009
    Applicant: ELECTRONICS AND TELECOMMUNICATIONS RESEARCH INSTITUTE
    Inventors: Su Jae LEE, Jin Ah Park, Jae Hyun Moon, Tae Hyoung Zyung
  • Patent number: 7538068
    Abstract: A carbon dioxide gas absorbent includes a porous body containing a lithium complex oxide. The porous body includes pores having a pore diameter distribution such that main pores which consist of first pores with a diameter of 10 to 100 ?m and second pores with a diameter larger than 100 ?m and 500 ?m or smaller occupy 80 to 100%, third pores with a diameter smaller than 10 ?m occupy 0 to 10% and fourth pores with a diameter larger than 500 ?m occupy 0 to 10%, the main pores have a pore diameter distribution such that the first pores occupy 15 to 85% and second pores occupy 15 to 85%.
    Type: Grant
    Filed: March 16, 2006
    Date of Patent: May 26, 2009
    Assignee: Kabushiki Kaisha Toshiba
    Inventors: Masahiro Kato, Toshihiro Imada, Kenji Essaki
  • Patent number: 7534414
    Abstract: The present invention comprises new materials, material structures, and processes of fabrication of such that may be used in technologies involving the conversion of light to electricity and/or heat to electricity, and in optoelectronics technologies. The present invention provide for the fabrication of a clathrate compound comprising a type II clathrate lattice with atoms of silicon and germanium as a main framework forming lattice spacings within the framework, wherein the clathrate lattice follows the general formula Si136-yGey, where y indicates the number of Ge atoms present in the main framework and 136-y indicates the number of Si atoms present in the main framework, and wherein y>0.
    Type: Grant
    Filed: April 16, 2008
    Date of Patent: May 19, 2009
    Assignee: University of South Florida
    Inventors: George S. Nolas, Sarath Witanachchi, Pritish Mukherjee
  • Publication number: 20090110930
    Abstract: An indium oxide-based particle is provided. The indium oxide-based particle has a mono-dispersive and spherical non-crystalline structure (spherical morphology with amorphous phase). The diameter of particle is ranged between 0.10 ?m and 0.70 ?m, and the content of an indium oxide is ranged between 10.0 percent by mass and 99.9 percent by mass. The indium oxide-based particle is generated by the precursor with indium ion reacting with alpha hydroxyl acid in an aqueous solution with alkali-modifier additive at a constant temperature. The indium-oxide based particle can be further calcinated as a crystalline indium oxide particle.
    Type: Application
    Filed: January 28, 2008
    Publication date: April 30, 2009
    Applicant: NATIONAL TAIWAN UNIVERSITY
    Inventors: Wen-Cheng WEI, Sung-En LIN
  • Patent number: 7517614
    Abstract: The negative active material for a rechargeable lithium battery of the present invention includes a carbonaceous material and a silicon-based compound represented by Formula 1: Si(1-y)MyO1+x(1) where 0?y?1, ?0.5?x?0.5, and M is selected from the group consisting of Mg, Ca, and mixtures thereof.
    Type: Grant
    Filed: September 9, 2008
    Date of Patent: April 14, 2009
    Assignee: Samsung SDI Co., Ltd.
    Inventors: Goo-Jin Jeong, Sang-Min Lee, Sung-Soo Kim, Yoshiaki Nitta
  • Patent number: 7514065
    Abstract: A layered ruthenic acid compound is converted to a protonic layered ruthenic acid hydrate, which is then converted to a layered alkylammonium-ruthenic acid intercalation compound to obtain a colloid containing ruthenic acid nanosheets having a thickness of 1 nm or smaller. Thereby, a ruthenic acid nanosheet is obtained.
    Type: Grant
    Filed: March 26, 2004
    Date of Patent: April 7, 2009
    Inventors: Yoshio Takasu, Yasushi Murakami, Wataru Sugimoto
  • Publication number: 20090087716
    Abstract: One embodiment of the invention includes an assembly of metal oxide comprising valve metal oxide nanotubes.
    Type: Application
    Filed: September 27, 2007
    Publication date: April 2, 2009
    Applicant: GM Global Technology Operations, Inc.
    Inventors: Mahmoud H. Abd Elhamid, Gayatri Vyas Dadheech, Curtis A. Wong, Youssef M. Mikhail, Michael J. Lukitsch
  • Patent number: 7510693
    Abstract: Process for the production of a metal oxide powder having a BET surface area of at least 20 m2/g by reacting an aerosol with oxygen in a reaction space at a reaction temperature of more than 700° C. and then separating the resulting powder from gaseous substances in the reaction space, wherein the aerosol is obtained by atomisation using a multi-component nozzle of at least one starting material, as such in liquid form or in solution, and at least one atomising gas, the volume-related mean drop diameter D30 of the aerosol is from 30 to 100 ?m and the number of aerosol drops larger than 100 ?m is up to 10%, based on the total number of drops, and metal oxide powder obtainable by this process.
    Type: Grant
    Filed: January 30, 2006
    Date of Patent: March 31, 2009
    Assignee: Degussa AG
    Inventors: Stipan Katusic, Michael Kraemer, Michael Kroell, Peter Kress, Edwin Staab
  • Publication number: 20090058264
    Abstract: Disclosed herein are nanocrystal-metal oxide composites. The composites comprise nanocrystals and a metal oxide bound to the nanocrystals wherein the metal oxide has organic groups. The composites are stable to mechanical stress and exhibit improved processability. Also disclosed herein is a method for preparing the composites.
    Type: Application
    Filed: July 22, 2008
    Publication date: March 5, 2009
    Applicant: SAMSUNG ELECTRONICS CO., LTD.
    Inventors: Shin Ae Jun, Eun Joo Jang
  • Publication number: 20090060830
    Abstract: The invention concerns a method for manufacturing nanoporous metal oxide or metal active sites frameworks in which the metal oxide precursor is distributed into the framework in the form of a metal soap surfactant. The invention also covers a nanostructure framework comprising metal oxide active sites which are evenly distributed in the framework.
    Type: Application
    Filed: August 19, 2005
    Publication date: March 5, 2009
    Applicant: Nanologica AB
    Inventor: Alfonso E. Garcia-Bennet
  • Patent number: 7488464
    Abstract: Methods and systems for processing metal oxides from metal containing solutions. Metal containing solutions are mixed with heated aqueous oxidizing solutions and processed in a continuous process reactor or batch processing system. Combinations of temperature, pressure, molarity, Eh value, and pH value of the mixed solution are monitored and adjusted so as to maintain solution conditions within a desired stability area during processing. This results in metal oxides having high or increased pollutant loading capacities and/or oxidation states. These metal oxides may be processed according to the invention to produce co-precipitated oxides of two or more metals, metal oxides incorporating foreign cations, metal oxides precipitated on active and inactive substrates, or combinations of any or all of these forms.
    Type: Grant
    Filed: July 28, 2004
    Date of Patent: February 10, 2009
    Assignee: EnviroScrub Technologies Corporation
    Inventors: Charles F. Hammel, Richard M. Boren
  • Publication number: 20090033200
    Abstract: The invention relates to a barrier layer provided on the electrode assembly of a discharge lamp comprising at least a layer of nanoclusters of a non-oxidizing material. Further, the invention relates to an electrode assembly for a discharge lamp comprising an electrode having a foil attached thereto to create an electrode assembly, the assembly being coated with a multi-layer coating comprising at least a layer of non-oxidizing material in the form of nanoclusters, and at least another layer of non-oxidizing material, such that the total coating thickness is up to 1500 nm.
    Type: Application
    Filed: August 1, 2007
    Publication date: February 5, 2009
    Inventor: Deeder M. Aurongzeb
  • Publication number: 20090031930
    Abstract: The present invention relates to apparatus for incinerating dangerous waste, and in particular, apparatus for incinerating dangerous waste in various forms. It comprises a continuous feeding device, an incineration furnace, a flue gas quenching device, a flue gas treating device, and an online monitoring system. The continuous feeding device includes device for feeding paste, powder, and solid device. The quenching device is connected to a steam boiler and a thermal oil tank, thus achieving comprehensive utilization of the thermal energy generated during incineration of the waste. Apparatus for incinerating dangerous waste according to the present invention enables sufficient combustion of the waste, recycling of the metal oxides or noble metals from the combustion flue gas and/or sinters and/or furnace ashes, effective elimination of the concurrent degradation and re-forming of dioxins.
    Type: Application
    Filed: December 19, 2005
    Publication date: February 5, 2009
    Inventor: Fuchang Shen
  • Patent number: 7485282
    Abstract: A process is described for the synthesis of metal oxides in a nanometric particle form that cannot be easily obtained by conventional bulk synthesis techniques. The method makes use of Colloid Occluded Carbons (COC) and Colloid Imprinted Carbons (CIC) as reagents and as templating agents for the preparation of metal oxides in nanometric particle form. The nanometric particles are suitable useful in the field of chemical catalysis, particularly for petroleum refining when in porous form, and as sensors, optical wave guides, and coatings.
    Type: Grant
    Filed: March 23, 2005
    Date of Patent: February 3, 2009
    Assignee: Board of Trustees of Michigan State University
    Inventors: Thomas J. Pinnavaia, Seong-Su Kim
  • Publication number: 20090029146
    Abstract: A method for synthesising metal oxide particles comprises preparing a pre-sol solution, and hydrolysing and condensing the pre-sol solution under supercritical fluid conditions to form macroscopic mesoporous particles having ordered pore structures. The pre-sol solution may contain a mixture of surfactants such as CTAB and P123. The supercritical fluid may be scCO2. The mesoporous particles may be spheres with a mesopore diameter in the range of 2 to 15 nm and macroscopic diameters of from 1 to 5 microns. The particles are useful in chromatography and other applications.
    Type: Application
    Filed: April 5, 2006
    Publication date: January 29, 2009
    Inventors: Justin Derek Holmes, John Paul Hanrahan, Michael Anthony Morris, Trevor Richard Spalding
  • Publication number: 20090013906
    Abstract: The invention relates to a metallic effect pigment, which metallic effect pigment has a substantially homogeneous chemical composition comprising at least one metal M and having an average content of oxygen of from 25 to 58 atomic percent, based on the total content of M and oxygen. The invention further relates to a method for the production of said metallic effect pigment.
    Type: Application
    Filed: February 14, 2007
    Publication date: January 15, 2009
    Inventors: Martin Fischer, Wolfgang Herzing, Bernhard Geissler, Ralph Schneider
  • Publication number: 20080311031
    Abstract: The invention provides a method for the formation of small-size metal oxide particles, comprising the steps of a) preparing a starting aqueous solution comprising at least one of metallic ions and complexes thereof, at a concentration of at least 0.1 % w/w of the metal component; b) maintaining the solution at a temperature lower than 50° C. for a retention time in which hydrolysis takes place, the extent of the hydrolysis being sufficient to produce O.1 mmol protons per mmol of metal present in solution, wherein the time does not exceed 14 days, to form a system containing a retained solution; and c) adjusting the conditions in the system by at least one of the steps of: i) heating the retained solution to elevate the temperature thereof by at least 1° C.; ii) changing the pH of the retained solution by at least 0.1 units; and iii) diluting the retained solution by at least 20% whereby there are formed particles, wherein the majority of the particles formed are between about 2 nm and about 500 nm in size.
    Type: Application
    Filed: December 21, 2006
    Publication date: December 18, 2008
    Applicant: JOMA INTERNATIONAL AS
    Inventors: Asher Vitner, Aharon Eyal
  • Publication number: 20080305025
    Abstract: The invention provides a method for the formation of small-size metal oxide particles, comprising the steps of: a) preparing a starting aqueous solution comprising at least one of metallic ion and complexes thereof, at a concentration of at least 0.1% w/w of the metal component; b) preparing a modifying aqueous solution having a temperature greater than 50° C.; c) contacting the modifying aqueous solution with the starting aqueous solution in a continuous mode in a mixing chamber to form a-modified system; d) removing the modified system from the mixing chamber in a plug-flow mode; wherein the method is characterized in that: i) the residence time in the mixing chamber is less than about 5 minutes; and iii) there are formed particles or aggregates thereof, wherein the majority of the particles formed are between about 2 nm and about 500 nm in size.
    Type: Application
    Filed: December 21, 2006
    Publication date: December 11, 2008
    Applicant: Joma International AS
    Inventors: Asher Vitner, Aharon Eyal
  • Patent number: 7458384
    Abstract: Nano-sized rare earth metal oxide particles are prepared from aqueous reverse micelles. The engineered nanoparticles have large surface area to volume ratios, and uniformly incorporate a surfactant in each particle, so that when applied to the inner surface of a pipeline or sprayed onto a fluid stream in a pipeline, the particles reduce the roughness of the inside surface of pipe being used to transport fluid. The application of a nanolayer of this novel nanoceria mixture causes a significant reduction in pressure drops, friction, and better recovery and yield of fluid flowing through a pipeline.
    Type: Grant
    Filed: July 14, 2005
    Date of Patent: December 2, 2008
    Assignees: University of Central Florida Research Foundation, Inc., CC Technologies Laboratories, Inc.
    Inventors: Sudipta Seal, William P. Jepson, Sameer Deshpande, Suresh C. Kuiry, Swanand H. Patil
  • Patent number: 7455823
    Abstract: The invention discloses methods for making micron/nano meter sized particles of various inorganic materials such as minerals/oxides/sulphides/metals/ceramics at a steadily expanding liquid-liquid interface populated by suitable surfactant molecules that spontaneously organize themselves into superstructures varying over large length-scales. This experiment is realized in a radial Hele-Shaw cell where the liquid-liquid interfacial growth rate and consequently time scales such as arrival of surfactant molecules to the interface, the hydrodynamic flow effect to modulate the material organization into super structures at the dynamic charged interface.
    Type: Grant
    Filed: February 23, 2006
    Date of Patent: November 25, 2008
    Assignee: Council of Scientific & Industrial Research
    Inventors: Sastry Murali, Rautaray Debabrata
  • Publication number: 20080267852
    Abstract: Process for preparing pulverulent solids, in which one or more oxidizable and/or hydrolysable metal compounds are reacted in a high-temperature zone in the presence of oxygen and/or steam, the reaction mixture is cooled after the reaction, and the pulverulent solid is removed from gaseous substances, wherein at least one metal compound is introduced into the high-temperature zone in solid form and the evaporation temperature of the metal compound is below the temperature of the high-temperature zone.
    Type: Application
    Filed: November 29, 2006
    Publication date: October 30, 2008
    Applicant: EVONIK DEGUSSA GmbH
    Inventors: Kai Schumacher, Stefan Fiedler, Roland Schilling, Ronald Ihmig, Stipan Katusic
  • Publication number: 20080267858
    Abstract: A method of continuously producing reduced compounds, which comprises continuously feeding our oxidised compound into a reaction chamber and contracting the oxidised compound with a reductant gas. The oxidised compound may be titanium dioxide. the reaction chamber may be a rotating kiln.
    Type: Application
    Filed: June 1, 2005
    Publication date: October 30, 2008
    Applicant: ATRAVERDA LIMITED
    Inventors: Andrew Hill, John Hill
  • Patent number: 5136002
    Abstract: Disclosed is a resin composition comprising a copolymer [I] having a number average molecular weight of at least 15,000, which comprises at least 30 mole % of the following recurring units [A]: ##STR1## and a compound [II] having a number average molecular weight of at least 1,000, which is comprised of perfluoroalkylether recurring units [D]. This resin composition is used as a cladding of a core-clad optical fiber.
    Type: Grant
    Filed: April 26, 1991
    Date of Patent: August 4, 1992
    Assignee: Mitsubishi Rayon Company, Ltd.
    Inventors: Teruhiko Sugimori, Takashi Yamamoto, Tsuruyoshi Matsumoto, Katsuhiko Shimada